JP5455656B2 - フルオロカーボンコーティング組成物に使用するための超分散剤 - Google Patents
フルオロカーボンコーティング組成物に使用するための超分散剤 Download PDFInfo
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- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
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- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
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- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/5046—Amines heterocyclic
- C08G59/5053—Amines heterocyclic containing only nitrogen as a heteroatom
- C08G59/506—Amines heterocyclic containing only nitrogen as a heteroatom having one nitrogen atom in the ring
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- C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
- C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
- C09D127/16—Homopolymers or copolymers of vinylidene fluoride
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- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/26—Esters containing oxygen in addition to the carboxy oxygen
- C08F220/32—Esters containing oxygen in addition to the carboxy oxygen containing epoxy radicals
- C08F220/325—Esters containing oxygen in addition to the carboxy oxygen containing epoxy radicals containing glycidyl radical, e.g. glycidyl (meth)acrylate
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- C08L33/04—Homopolymers or copolymers of esters
- C08L33/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
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- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
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Description
本出願は、2006年2月3日に出願された米国特許出願第11/275,916号の一部継続出願である。
発明の属する分野
本発明は一般的に超分散剤に関する。更に詳細には、本発明の超分散剤はフルオロカーボンコーティング組成物に有用である。
フルオロカーボン樹脂、例えば、ポリ弗化ビニリデン(PVDF)は、優れた耐候性を有する製剤用コーティングに有用である。フルオロカーボン樹脂は不良なレオロジー及び顔料湿潤性を有するため、バインダー樹脂、又は超分散剤を、フルオロカーボンコーティング組成物に添加することが一般的である。最適な耐候性及び耐薬品性を達成するために、コーティング組成物において高いフルオロカーボン樹脂含有率が所望されている。多くのコーティング用途は、70質量%以上のフルオロカーボン樹脂を有し、残りはバインダー樹脂であるコーティング組成物を要求している。フルオロカーボン樹脂、特にPVDF、及びバインダー樹脂を含有するコーティング組成物は、比較的高い粘度を有する傾向がある。幾つかのコーティング用途、特にコイルコーティング用途の場合、バインダー樹脂に関してフルオロカーボン樹脂の含有率は高いが、関連技術の組成物で現在可能であるよりも低い粘度であることが望ましい。
本発明はフルオロカーボンコーティング組成物中で使用される超分散剤を提供する。超分散剤はポリグリシジルオリゴマー及び少なくとも1つのアミノ化合物の反応生成物を含む。ポリグリシジルオリゴマーは、少なくとも1つの内部エーテル結合及びエステル結合を有する炭素数1から25までの炭素鎖と複数のエポキシ基とを含む。超分散剤は環状、複素環状、アルキル、又はヘテロアルキル構造を有する少なくとも1つのアミノ化合物を有し、該構造は、少なくとも1つのエポキシ基と反応し且つ該基を開環させるために、少なくとも1つの第1級又は第2級アミン基で置換されている。得られた超分散剤は、フルオロカーボン樹脂の分散を補助するアミノ化合物からのアミン官能性を有し且つ少なくとも1つのエポキシ基の開環によるヒドロキシル官能性を有し、該フルオロカーボンコーティング組成物中で架橋剤による架橋を向上させる。
フルオロカーボンコーティング組成物中で使用される超分散剤が開示される。フルオロカーボンコーティング組成物は一般的にフルオロカーボン樹脂、バインダー樹脂(又は分散剤樹脂)、架橋剤、超分散剤、溶媒、及び添加剤を含む。他のバインダー樹脂、特に非−アミノ樹脂を、フルオロカーボンコーティング組成物中で使用してよいことは当業者には分かるはずである。
Claims (14)
- フルオロカーボン樹脂;
バインダー樹脂;
架橋剤;及び
1)内部エーテル結合及び内部エステル結合のうちの少なくとも1つを有する炭素数1から25までの炭素鎖と複数のエポキシ基とを含むポリグリシジルオリゴマーと2)前記エポキシ基の1つと反応し且つ該基を開環させるために、少なくとも1つの第1級又は第2級アミン基で置換された、環状、複素環状、アルキル、又はヘテロアルキル構造を有する少なくとも1つのアミノ化合物との反応生成物を含む超分散剤であって、
前記フルオロカーボン樹脂の分散を補助する前記アミノ化合物からのアミン官能性と前記架橋剤との架橋を向上させる少なくとも1つの前記エポキシ基の開環からのヒドロキシル官能性とを有する前記超分散剤
を含む、フルオロカーボンコーティング組成物。 - 前記ポリグリシジルオリゴマーが前記超分散剤の全質量を基準として30から90パーセントまでの量で存在する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記アミノ化合物が前記超分散剤の全質量を基準として15から50パーセントまでの量で存在する、請求項2記載のフルオロカーボンコーティング組成物。
- 前記ポリグリシジルオリゴマーが150から1000までの質量平均分子量を有する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記炭素鎖が線状、分枝鎖状、及びそれらの組み合わせから選択される、請求項1記載のフルオロカーボンコーティング組成物。
- 前記炭素鎖が脂肪族、脂環式、芳香族、及びそれらの組み合わせから選択される、請求項1記載のフルオロカーボンコーティング組成物。
- 前記アミノ化合物が、エチレン尿素、ピロリジン、2−ピロリドン、ピペリジン、モルホリン、t−ブチルアミン、イソプロピルアミン、ジイソプロピルアミン、2−アミノ−2−メチル−1−プロパノール、エタノールアミン、ジシクロヘキシルアミン、N,N−ジメチル−1,3−プロパンジアミン、ジメチルアミン、ジエタノールアミン、及びそれらの組み合わせから選択される、請求項1記載のフルオロカーボンコーティング組成物。
- 前記フルオロカーボン樹脂中に分散された顔料を更に含む、請求項1記載のフルオロカーボンコーティング組成物。
- 30から70パーセントまでの固体含有率を有する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記フルオロカーボン樹脂が前記フルオロカーボンコーティング組成物の全質量を基準として30から99パーセントまでの量で存在する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記超分散剤が前記フルオロカーボンコーティング組成物の全質量を基準として1から40パーセントまでの量で存在する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記架橋剤が前記フルオロカーボンコーティング組成物の全質量を基準として0.2から10パーセントまでの量で存在する、請求項1記載のフルオロカーボンコーティング組成物。
- 前記フルオロカーボン樹脂がフルオロカーボン粉末である、請求項1記載のフルオロカーボンコーティング組成物。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US11/684,823 | 2007-03-12 | ||
US11/684,823 US7838582B2 (en) | 2006-02-03 | 2007-03-12 | Hyperdispersant for use in fluorocarbon coating compositions |
PCT/US2007/083587 WO2008112026A1 (en) | 2007-03-12 | 2007-11-05 | Hyperdispersant for use in fluorocarbon coating compositions |
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Publication Number | Publication Date |
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JP2010521551A JP2010521551A (ja) | 2010-06-24 |
JP2010521551A5 JP2010521551A5 (ja) | 2010-12-24 |
JP5455656B2 true JP5455656B2 (ja) | 2014-03-26 |
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JP2009553568A Expired - Fee Related JP5455656B2 (ja) | 2007-03-12 | 2007-11-05 | フルオロカーボンコーティング組成物に使用するための超分散剤 |
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Country | Link |
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US (1) | US7838582B2 (ja) |
EP (1) | EP2121854B1 (ja) |
JP (1) | JP5455656B2 (ja) |
CN (1) | CN101636456B (ja) |
AT (1) | ATE550397T1 (ja) |
CA (1) | CA2637767C (ja) |
MX (1) | MX2008010784A (ja) |
RU (1) | RU2460749C2 (ja) |
WO (1) | WO2008112026A1 (ja) |
ZA (1) | ZA200906151B (ja) |
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US20090012235A1 (en) * | 2006-02-03 | 2009-01-08 | Basf Corporation | Dispersant for use in a fluorocarbon coating composition |
CN101891991B (zh) * | 2010-07-08 | 2012-10-03 | 中国科学院宁波材料技术与工程研究所 | 一种高硬度耐指纹涂料及其制备方法 |
CN101942057A (zh) * | 2010-08-20 | 2011-01-12 | 中国海洋石油总公司 | 一种用于金属基材的烘烤型自交联含氟丙烯酸酯树脂 |
EP2698399B1 (en) | 2011-04-13 | 2017-11-15 | LG Chem, Ltd. | Resin composition, multilayer film and photovoltaic module including same |
CN104650666A (zh) * | 2015-02-06 | 2015-05-27 | 天津普罗米化工有限公司 | 一种防污闪氟碳涂料 |
CN111234202B (zh) * | 2020-02-27 | 2022-10-04 | 中科院广州化学有限公司 | 一种无溶剂高含氮多羧基型超分散剂及其制备方法与应用 |
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US6699933B2 (en) * | 2001-08-07 | 2004-03-02 | Ppg Industries Ohio, Inc. | Method of coating coils using a high solids fluorocarbon coating composition |
US6679943B1 (en) * | 2002-05-01 | 2004-01-20 | Basf Corporation | Coating containing adhesion promoting additive |
JP4440590B2 (ja) * | 2003-09-29 | 2010-03-24 | 関西ペイント株式会社 | カチオン性塗料組成物及び塗膜形成方法 |
US7956144B2 (en) | 2006-02-03 | 2011-06-07 | Ppg Industries Ohio, Inc. | Acrylic resin for use in fluorocarbon coating compositions and method of forming the same |
-
2007
- 2007-03-12 US US11/684,823 patent/US7838582B2/en active Active
- 2007-11-05 RU RU2009137616/05A patent/RU2460749C2/ru not_active IP Right Cessation
- 2007-11-05 AT AT07863874T patent/ATE550397T1/de active
- 2007-11-05 CN CN2007800521365A patent/CN101636456B/zh not_active Expired - Fee Related
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CA2637767C (en) | 2012-04-10 |
ZA200906151B (en) | 2010-05-26 |
MX2008010784A (es) | 2009-03-02 |
WO2008112026A1 (en) | 2008-09-18 |
CN101636456A (zh) | 2010-01-27 |
RU2009137616A (ru) | 2011-04-20 |
US20070185249A1 (en) | 2007-08-09 |
JP2010521551A (ja) | 2010-06-24 |
EP2121854A1 (en) | 2009-11-25 |
US7838582B2 (en) | 2010-11-23 |
RU2460749C2 (ru) | 2012-09-10 |
CA2637767A1 (en) | 2008-09-12 |
EP2121854B1 (en) | 2012-03-21 |
ATE550397T1 (de) | 2012-04-15 |
CN101636456B (zh) | 2012-10-10 |
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