JP2015531028A - 亜鉛及びカドミウムの腐食を防止するための腐食保護剤調製物 - Google Patents
亜鉛及びカドミウムの腐食を防止するための腐食保護剤調製物 Download PDFInfo
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- JP2015531028A JP2015531028A JP2015527855A JP2015527855A JP2015531028A JP 2015531028 A JP2015531028 A JP 2015531028A JP 2015527855 A JP2015527855 A JP 2015527855A JP 2015527855 A JP2015527855 A JP 2015527855A JP 2015531028 A JP2015531028 A JP 2015531028A
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- corrosion
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- corrosion inhibitor
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- cadmium
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- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
- 229940055577 oleyl alcohol Drugs 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical class OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920001983 poloxamer Polymers 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 235000010408 potassium alginate Nutrition 0.000 description 1
- 239000000737 potassium alginate Substances 0.000 description 1
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 description 1
- 235000010289 potassium nitrite Nutrition 0.000 description 1
- 239000004304 potassium nitrite Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000010409 propane-1,2-diol alginate Nutrition 0.000 description 1
- 239000000770 propane-1,2-diol alginate Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- BHRZNVHARXXAHW-UHFFFAOYSA-N sec-butylamine Chemical compound CCC(C)N BHRZNVHARXXAHW-UHFFFAOYSA-N 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- YBRBMKDOPFTVDT-UHFFFAOYSA-N tert-butylamine Chemical compound CC(C)(C)N YBRBMKDOPFTVDT-UHFFFAOYSA-N 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- FAGUFWYHJQFNRV-UHFFFAOYSA-N tetraethylenepentamine Chemical compound NCCNCCNCCNCCN FAGUFWYHJQFNRV-UHFFFAOYSA-N 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- ABVVEAHYODGCLZ-UHFFFAOYSA-N tridecan-1-amine Chemical compound CCCCCCCCCCCCCN ABVVEAHYODGCLZ-UHFFFAOYSA-N 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- 150000004072 triols Chemical class 0.000 description 1
- QFKMMXYLAPZKIB-UHFFFAOYSA-N undecan-1-amine Chemical compound CCCCCCCCCCCN QFKMMXYLAPZKIB-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
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Abstract
Description
(A)界面活性剤成分として1種以上のアルキルアミンエトキシレート0.01〜5質量%、好適には0.1〜3質量%、特に0.5〜1.5質量%、
(B)1種以上の腐食防止剤、0.01〜10質量%、好適には0.5〜7質量%、特に1〜5質量%、
(C)1種以上の粘稠剤、0〜0.3質量%、好適には0.0001〜0.15質量%、特に0.005〜0.05質量%、
(D)アルカノール、グリコール、ポリアルキレングリコール、及びグリセリンから選択される1種以上の凝固点降下性アルコール、5〜75質量%未満、好適には10〜70質量%、特に25〜55質量%、
(E)1種以上の植物性及び/又は脂肪性の油脂、5〜90質量%、好適には15〜80質量%、特に35〜60質量%、
(F)水0〜5質量%、好適には0.1〜4質量%、特に0.5〜3質量%、及び
(G)通常の乳化剤0〜5質量%、好適には0.1〜4質量%、特に0.5〜3質量%、
を含有する腐食保護剤調製物が判明し、ここで前記成分(A)〜(G)の合計は、あらゆる場合で100質量%となる。
AMS 1435Bに従った、溶融亜鉛メッキ鋼板による亜鉛腐食試験
以下で説明する本発明による教示に従った腐食剤調製物は、亜鉛の腐食に関するその腐食保護作用について、溶融亜鉛メッキ鋼板を用い、AMS 1435B(3.2.5.2 Total Immersion Corrosion)の腐食試験と同様に、それぞれ50質量%の酢酸カリウム水溶液、及びギ酸カリウム水溶液に対して試験した。
(A)市販で得られる、エチレンオキシド単位を2個有するオクチルアミンエトキシレート 0.90
(B)市販で得られるヒマシ油エトキシレート(Leunapon(登録商標)ER40) 0.30
(B)イソノナン酸 1.30
(B)ドデカンジ酸 0.50
(B)安息香酸ナトリウム 0.50
(B)無水フタル酸 0.13
(B)トルトリアゾール 0.10
水酸化カリウム溶液(48質量%) 1.64
(C)ポリアクリレート粘稠剤(Lutexal(登録商標)GP ECO) 0.01
(D)モノプロピレングリコール 41.17
(E)アマニ油ラッカー 49.00
(F)水 2.44
(G)市販の乳化剤(Emulan(登録商標)ELH 60) 2.00
市販の消泡剤 0.01
合計100.00
試験1:ギ酸カリウム溶液、保護されていない溶融亜鉛メッキ鋼板で
・金属:溶融亜鉛メッキ鋼板(50×20×2mm)
・容器:Duran(登録商標)ガラス製のガラス瓶(100ml)
・試験媒体:ギ酸カリウム溶液(50質量%、pH値9〜10)中の、表面保護なし(つまりむき出し)の溶融亜鉛メッキ鋼板
・試験:アセトン中の溶融亜鉛メッキ鋼板(試験体)を、洗浄、乾燥、秤量する(三回測定);
ギ酸カリウム溶液100mlに完全に浸す;
乾燥機内で7日間、40℃
評価:試験媒体から試験体を取り出し、水ですすぎ、アセトン中で洗浄し、秤量する(三回測定)
・金属:溶融亜鉛メッキされた鋼板(50×20×2mm)
・容器:Duran(登録商標)ガラス製のガラス瓶(100ml)
・試験媒体:酢酸カリウム溶液(50質量%、pH値9〜10)中の、表面保護なし(つまりむき出し)の溶融亜鉛メッキ鋼板
・試験:アセトン中の溶融亜鉛メッキ鋼板(試験体)を、洗浄、乾燥、秤量する(三回測定);
酢酸カリウム溶液100mlに完全に浸す;
乾燥機内で7日間、40℃
評価:試験媒体から試験体を取り出し、水ですすぎ、アセトン中で洗浄し、秤量する(三回測定)
・金属:溶融亜鉛メッキされた鋼板(50×20×2mm)
・容器:Duran(登録商標)ガラス製のガラス瓶(100ml)
・試験媒体:ギ酸カリウム溶液(50質量%、pH値9〜10)中の、本発明による調製物(EF)の表面保護を有する溶融亜鉛メッキ鋼板
・試験:アセトン中の溶融亜鉛メッキ鋼板(試験体)を、洗浄、乾燥、秤量する(三回測定);
試験体を本発明による調製物(EF)に浸し、滴を取り(1時間)、時計ガラス上で乾燥させる(1時間)
ギ酸カリウム溶液100mlに完全に浸す;
乾燥機内で7日間、40℃
評価:試験媒体から試験体を取り出し、水ですすぎ、アセトン中で洗浄し、秤量する(三回測定)
・金属:溶融亜鉛メッキされた鋼板(50×20×2mm)
・容器:Duran(登録商標)ガラス製のガラス瓶(100ml)
・試験媒体:酢酸カリウム溶液(50質量%、pH値9〜10)中の、本発明による調製物(EF)の表面保護を有する溶融亜鉛メッキ鋼板
・試験:アセトン中の溶融亜鉛メッキ鋼板(試験体)を、洗浄、乾燥、秤量する(三回測定);
試験体を本発明による調製物(EF)に浸し、滴を取り(1時間)、時計ガラス上で乾燥させる(1時間)
酢酸カリウム溶液100mlに完全に浸す;
乾燥機内で7日間、40℃
評価:試験媒体から試験体を取り出し、水ですすぎ、アセトン中で洗浄し、秤量する(三回測定)
Claims (10)
- 以下の成分(A)〜(G):
(A)界面活性剤成分として1種以上のアルキルアミンエトキシレート0.01〜5質量%、
(B)1種以上の腐食防止剤、0.01〜10質量%、
(C)1種以上の粘稠剤、0〜0.3質量%、
(D)アルカノール、グリコール、ポリアルキレングリコール、及びグリセリンから選択される1種以上の凝固点降下性アルコール、5〜75質量%未満、
(E)1種以上の植物性及び/又は脂肪性の油脂、5〜90質量%、
(F)水0〜5質量%、及び
(G)通常の乳化剤0〜5質量%、
を含有する腐食防止剤調製物。 - 前記成分(A)として、少なくとも1種のアルキルアミンエトキシレートを含有し、当該アルキルアミンエトキシレートは、C3〜C20アルキル基を少なくとも1個有するものである、請求項1に記載の腐食防止剤調製物。
- 前記成分(A)として、少なくとも1種のアルキルアミンエトキシレートを含有し、当該アルキルアミンエトキシレートは、エチレンオキシド単位を1〜35個有するものである、請求項1又は2に記載の腐食防止剤調製物。
- 前記成分(A)として、少なくとも1種のアルキルアミンエトキシレートを含有し、当該アルキルアミンエトキシレートは、直鎖状C7〜C12アルキル基を少なくとも1個、及びエチレンオキシド単位を1.8〜9個有するものである、請求項1から3までのいずれか1項に記載の腐食防止剤調製物。
- 前記成分(B)として、
・少なくとも1種のヒマシ油エトキシレート、又は
・少なくとも1種のヒマシ油エトキシレートと、有機カルボン酸及び/又は複素環化合物をベースとする少なくとも1種のさらなる腐食防止剤との混合物
を含有する、請求項1から4までのいずれか1項に記載の腐食防止剤調製物。 - 前記成分(C)として、少なくとも1種のポリアクリレートを含有する、請求項1から5までのいずれか1項に記載の腐食防止剤調製物。
- 前記成分(D)として、
・モノプロピレングリコール、又は
・モノプロピレングリコールと、アルカノール、グリコール、ポリアルキレングリコール、及びグリセリンから選択される1種以上の他の凝固点降下性アルコールとの混合物
を含有する、請求項1から6までのいずれか1項に記載の腐食防止剤調製物。 - 前記成分(E)として、アマニ油を含有する、請求項1から7までのいずれか1項に記載の腐食防止剤調製物。
- 亜鉛、又は亜鉛メッキされた部材若しくは表面、又はカドミウム、又はカドミウムメッキされた金属表面を腐食から保護するための方法において、これらの基材を請求項1から8までのいずれか1項に記載の腐食防止剤調製物で処理することを特徴とする、前記方法。
- 亜鉛、又は亜鉛メッキされた部材若しくは表面、又はカドミウム、又はカドミウムメッキされた金属表面を、空港で使用される滑走路用除氷剤に起因する腐食から保護するための、請求項9に記載の方法。
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PCT/EP2013/066823 WO2014029654A1 (de) | 2012-08-22 | 2013-08-12 | Korrosionsschutzmittel-formulierung zum schutz vor zink- und cadmiumkorrosion |
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WO2018095759A1 (de) * | 2016-11-23 | 2018-05-31 | Basf Se | Kühlmittel für kühlsysteme in elektrofahrzeugen mit brennstoffzellen und/oder batterien enthaltend azolderivate und zusätzliche korrosionsschutzmittel |
CN109929598A (zh) * | 2017-12-19 | 2019-06-25 | 天津工业大学 | 一种工业丁醇副产物改性为燃油的工艺 |
KR102045640B1 (ko) * | 2017-12-22 | 2019-11-15 | 주식회사 포스코 | 방청 조성물, 금속 기재의 방청처리 방법 및 방청 코팅층을 포함하는 금속재 |
CN113801633A (zh) * | 2020-06-15 | 2021-12-17 | 中国石油化工股份有限公司 | 一种防冰液及其制备方法和应用 |
CN115537274B (zh) * | 2022-10-14 | 2024-06-28 | 安徽富德环保设备有限公司 | 一种渣选陶瓷过滤板专用清洗剂及其制备方法与应用 |
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CA2880265A1 (en) | 2014-02-27 |
EP2888386A1 (de) | 2015-07-01 |
KR20150046229A (ko) | 2015-04-29 |
CN104583456B (zh) | 2017-04-26 |
BR112015003102A2 (pt) | 2017-07-04 |
CN104583456A (zh) | 2015-04-29 |
KR102136060B1 (ko) | 2020-07-21 |
JP6316293B2 (ja) | 2018-04-25 |
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