JP2013534574A - 表面被覆されたポリエステル系繊維基材 - Google Patents
表面被覆されたポリエステル系繊維基材 Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/002—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from unsaturated compounds
- C08G65/005—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from unsaturated compounds containing halogens
- C08G65/007—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from unsaturated compounds containing halogens containing fluorine
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
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- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/22—Yarns or threads characterised by constructional features, e.g. blending, filament/fibre
- D02G3/36—Cored or coated yarns or threads
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
- D06N3/0015—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
- D06N3/0036—Polyester fibres
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G2650/28—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type
- C08G2650/46—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing halogen
- C08G2650/48—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing halogen containing fluorine, e.g. perfluropolyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/23907—Pile or nap type surface or component
- Y10T428/23986—With coating, impregnation, or bond
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
- Y10T428/2964—Artificial fiber or filament
- Y10T428/2967—Synthetic resin or polymer
- Y10T428/2969—Polyamide, polyimide or polyester
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/20—Coated or impregnated woven, knit, or nonwoven fabric which is not [a] associated with another preformed layer or fiber layer or, [b] with respect to woven and knit, characterized, respectively, by a particular or differential weave or knit, wherein the coating or impregnation is neither a foamed material nor a free metal or alloy layer
- Y10T442/273—Coating or impregnation provides wear or abrasion resistance
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- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Description
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む。
(i)式I:
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む被覆組成物を繊維基材の表面の少なくとも一部に塗布する工程と、
(ii)被覆された繊維基材を乾燥させる工程と、
(iii)工程(ii)からの被覆された繊維基材を水で洗浄し、かつ洗浄された繊維基材を乾燥させる任意(optional)の工程と
を含む方法である。
ポリエステルポリマーは、当業者に良く知られており、エステルそれ自体を含めアルコールおよびジカルボン酸に由来する、エステル化反応またはエステル交換反応による、いずれかの縮重合生成物を挙げることができる。
それらのエンドキャップ誘導体および伸長鎖誘導体を含む、ヘキサフルオロプロピレンオキシドの高分子量ポリマーは、その分子量およびさまざまな物理的特性に基づき、高性能なエラストマー、分散剤、または潤滑剤として、有用である。式Iのパーフルオロポリエーテルを含む被覆組成物によるポリエステル系繊維基材の表面処理が耐消耗性および/または耐摩耗性における驚くべき有利な結果をもたらすとの知見は、予想されていなかった。
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む。
本発明はさらに、下記のように、ポリエステルで構成される繊維基材の耐消耗性および/または耐摩耗性を改善するための方法に関する。
(i)繊維基材の表面の少なくとも一部を式I:
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む被覆組成物に浸漬する工程と、
(ii)表面を被覆された繊維基材を乾燥させる工程と、
(iii)工程(ii)からの繊維基材を水で洗浄し、かつ洗浄された繊維基材を乾燥させる任意の工程と
を含む方法に関する。
(i)繊維基材の表面の少なくとも一部に式I:
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む被覆組成物を吹付けする工程と、
(ii)表面を被覆された繊維基材を乾燥させる工程と、
(iii)工程(ii)からの繊維基材を水で洗浄し、かつ洗浄された繊維基材を乾燥させる任意の工程と
を含む方法を提供する。
本実施例におけるポリエステル系繊維基材は、PTTで構成される織物(平織り)であって、SORONA(登録商標)としても知られており、E.I.du Pont de Nemours and Company(Wilmington,DE,USA)から購入可能であった。
1)被覆溶液A:Krytox(登録商標)GPL104を2H,3H−デカフルオロペンタン(CAS番号138495−42−8)で10wt%溶液に希釈。
2)被覆溶液B:Krytox(登録商標)GPL105を2H,3H−デカフルオロペンタン(CAS番号138495−42−8)で10wt%溶液に希釈。
3)被覆溶液C:Krytox(登録商標)GPL106をメトキシノナフルオロブタンとメトキシノナフルオロイソブタンとの混合溶剤、HFE−7100(3M株式会社のNovec(登録商標))で10wt%溶液に希釈。
実施例1〜6:織物サンプルを幅10cmで長さ10cmの細片に切断し、当初重量(W0)を記録した。この織物サンプルを被覆組成物中に30秒間浸漬し、一定重量となるまで周囲温度で乾燥し、表面処理された織物サンプルの重量(W1)を記録した。乾燥された織物サンプルを1000mLの水に沈漬し、ゆっくり撹拌しながら1時間保った。織物サンプルを取り出し、平らにし、一定重量となるまで真空オーブン内で周囲温度で乾燥し、最終重量(W2)を記録した。
式Iのパーフルオロポリエーテルの非存在下で、織物を、1000mLの水に浸漬する(比較例1〜3について)または水を噴霧する(比較例4〜5について)のいずれかで、比較織物サンプルを試験サンプルと同様に調製した。
ASTM基準D3884−07に準拠したテーバー摩耗試験を用いて、織物サンプルの摩耗特性を評価した。試験装置はCS−10摩耗輪付きTaber(登録商標)5131摩耗機で、荷重は1000gであった。回転速度は、60サイクル/分であった。各摩耗試験の後、25サイクル毎に摩耗輪を研磨紙で再研磨した。耐摩耗性は、織り糸が1本破断されるまでの摩耗サイクル数で評価した。
Claims (9)
- ポリエステルを含む繊維基材を含む被覆基材であって、前記繊維基材が式I:
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む被覆組成物で少なくとも部分的に被覆されている、被覆基材。 - nが10〜60の整数である、請求項1の被覆基材。
- 前記ポリエステルが、ポリエチレンテレフタレート、ポリトリメチレンテレフタレート、ポリブチレンテレフタレート、またはそれらのブレンドから選択される、請求項1の被覆基材。
- 前記ポリエステルが、ポリトリメチレンテレフタレートのホモポリマーまたは少なくとも70wt%のポリトリメチレンテレフタレートを含むポリトリメチレンテレフタレートのコポリマーである、請求項1の被覆基材。
- 前記繊維基材が、繊維、織物、織り糸、またはカーペットから選択される、請求項1の被覆基材。
- 前記被覆組成物が、被覆組成物の総重量に基づき、約0.1〜50wt%の式Iのパーフルオロポリエーテルを含む、請求項1の被覆基材。
- 前記被覆基材の総重量に基づき、0.1〜50wt%の式Iのパーフルオロポリエーテルを含む、請求項1の被覆基材。
- ポリエステルを含む繊維基材の耐摩耗性を改善するための方法であって:
(i)前記繊維基材の表面の少なくとも一部に式I:
F−[CF(CF3)−CF2O]n−CF2CF3 (I)
(式中、nは5〜100の整数である)
のパーフルオロポリエーテルを含む被覆組成物を塗布する工程と、
(ii)被覆された繊維基材を乾燥させる工程と、
(iii)工程(ii)からの被覆された繊維基材を水で洗浄し、かつ前記洗浄された繊維基材を乾燥させる任意の工程と
を含む、方法。 - 塗布方法が、はけ塗り、浸漬、噴霧、パディング、ロールコーティング、または発泡から選択される、請求項8の繊維基材の耐摩耗性を改善するための方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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CN201010229883.5 | 2010-07-14 | ||
CN201010229883.5A CN102337677B (zh) | 2010-07-14 | 2010-07-14 | 表面涂覆过的聚酯纤维基质及其制备方法 |
PCT/US2011/043806 WO2012009404A1 (en) | 2010-07-14 | 2011-07-13 | Surface coated polyester-based fibrous substrate |
Publications (3)
Publication Number | Publication Date |
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JP2013534574A true JP2013534574A (ja) | 2013-09-05 |
JP2013534574A5 JP2013534574A5 (ja) | 2014-08-28 |
JP5868970B2 JP5868970B2 (ja) | 2016-02-24 |
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JP2013519786A Expired - Fee Related JP5868970B2 (ja) | 2010-07-14 | 2011-07-13 | 表面被覆されたポリエステル系繊維基材 |
Country Status (7)
Country | Link |
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US (1) | US9708505B2 (ja) |
EP (1) | EP2593522B1 (ja) |
JP (1) | JP5868970B2 (ja) |
KR (1) | KR20130126894A (ja) |
CN (1) | CN102337677B (ja) |
DK (1) | DK2593522T3 (ja) |
WO (1) | WO2012009404A1 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2014514467A (ja) * | 2011-03-18 | 2014-06-19 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 本質的に耐燃性のポリマー糸の耐燃仕上げ剤およびその製造方法 |
WO2018164140A1 (ja) | 2017-03-07 | 2018-09-13 | Agc株式会社 | 撥水撥油性物品、その製造方法及び撥水撥油剤組成物 |
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- 2011-07-13 US US13/807,945 patent/US9708505B2/en active Active
- 2011-07-13 DK DK11746059.2T patent/DK2593522T3/en active
- 2011-07-13 JP JP2013519786A patent/JP5868970B2/ja not_active Expired - Fee Related
- 2011-07-13 WO PCT/US2011/043806 patent/WO2012009404A1/en active Application Filing
- 2011-07-13 KR KR1020137003617A patent/KR20130126894A/ko not_active Application Discontinuation
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2014514467A (ja) * | 2011-03-18 | 2014-06-19 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 本質的に耐燃性のポリマー糸の耐燃仕上げ剤およびその製造方法 |
WO2018164140A1 (ja) | 2017-03-07 | 2018-09-13 | Agc株式会社 | 撥水撥油性物品、その製造方法及び撥水撥油剤組成物 |
KR20190127658A (ko) | 2017-03-07 | 2019-11-13 | 에이지씨 가부시키가이샤 | 발수발유성 물품, 그 제조 방법 및 발수발유제 조성물 |
US11504740B2 (en) | 2017-03-07 | 2022-11-22 | AGC Inc. | Water/oil repellent article, method for its production and water/oil repellent composition |
KR20220163534A (ko) | 2017-03-07 | 2022-12-09 | 에이지씨 가부시키가이샤 | 발수발유성 물품, 그 제조 방법 및 발수발유제 조성물 |
Also Published As
Publication number | Publication date |
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US9708505B2 (en) | 2017-07-18 |
CN102337677B (zh) | 2014-03-19 |
KR20130126894A (ko) | 2013-11-21 |
WO2012009404A1 (en) | 2012-01-19 |
JP5868970B2 (ja) | 2016-02-24 |
CN102337677A (zh) | 2012-02-01 |
DK2593522T3 (en) | 2016-08-15 |
US20130108822A1 (en) | 2013-05-02 |
EP2593522B1 (en) | 2015-09-02 |
EP2593522A1 (en) | 2013-05-22 |
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