JP2011513171A - ケイ酸塩ガラス用の清澄剤 - Google Patents
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- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
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- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
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- C03C1/004—Refining agents
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- C03C14/00—Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix
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- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
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- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
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- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
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- C03C3/087—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal containing calcium oxide, e.g. common sheet or container glass
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- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
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- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/095—Glass compositions containing silica with 40% to 90% silica, by weight containing rare earths
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/28—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture specially adapted for farming
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31—Surface property or characteristic of web, sheet or block
- Y10T428/315—Surface modified glass [e.g., tempered, strengthened, etc.]
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Abstract
Description
バッチを提供し、前記バッチがケイ酸塩ガラスのための原材料と、少なくとも1種類の清澄剤とを含み、ここで前記少なくとも1種類の清澄剤が、溶融物が形成される温度において水源として作用する、少なくとも1種類の無機化合物を含み、
前記バッチを溶融して前記溶融物を形成し、
前記水を蒸発させて水蒸気を形成し、ここで、前記水蒸気が前記溶融物中に複数の泡を形成し、
前記複数の泡を前記溶融物中のシードと融合させて、前記溶融物中の前記複数のシードの濃度を所定の濃度未満に低減し、
前記融合させた泡とシードを前記溶融物から少なくともある程度除去する、
各工程を有してなる。
バッチを提供し、前記バッチがケイ酸塩ガラスのための原材料と、少なくとも1種類の清澄剤とを含み、ここで前記少なくとも1種類の清澄剤が、溶融物の温度において水源として作用する少なくとも1種類の無機化合物を含み、
前記バッチを溶融して前記溶融物を形成し、
前記水を蒸発させて水蒸気を形成し、ここで、前記水蒸気が前記溶融物中に複数の泡を形成し、
前記複数の泡を前記溶融物中のシードと融合させて、前記溶融物中の前記複数のシードの濃度を所定の濃度未満に低減し、
前記融合させた泡とシードを前記溶融物から少なくともある程度除去し、
前記溶融物を固化させて前記ケイ酸塩ガラスを形成し、ここで前記ケイ酸塩ガラスは約1シード/cm3未満のシード濃度を有する、
各工程を有してなる。
Al(OH)3 → AlO・(OH) + H2O、および
AlO・(OH) → 1/2 Al2O3 + 1/2 H2O
NaOH → 1/2 Na2O + 1/2 H2O
CS=CT ×(t−2DOL)/DOL;
ここで、tはガラスの厚さであり、DOLは交換の深さであり、層の深さとも称される。
実施例1は、本発明の清澄剤の有効性を例証する役割をする。アルミノケイ酸塩のるつぼ溶融物の9つのサンプルを調製した。各サンプルに使用するバッチ材料を表1aに示す。本発明の清澄剤のさまざまな組合せをサンプル11〜18に加えた。サンプル19は本明細書に記載の上記清澄剤を含まず、よって、対照サンプルとしての役割をする。サンプル12、13、14、および18では、バッチにおけるアルミナ(Al2O3)を清澄剤の水酸化アルミニウム(Al(OH)3)に置換した。サンプル15および16ではソーダ灰を水酸化ナトリウム(NaOH)に置換した。サンプル11〜18にはセリアおよび酸化スズ(IV)を加え、サンプル17および18には酸化剤の硝酸ナトリウム(NaNO3)を加えた。
実施例2は、ケイ酸塩ガラス中の泡/シードの濃度を効果的に低減するために必要な清澄剤(または薬剤)の量を例証している。アルミノケイ酸塩のるつぼ溶融物の9つのサンプルを調製した。各サンプルに用いるバッチ材料を表2aに示す。セリアおよび酸化スズ(IV)をサンプル21〜29に加えたが、それらはサンプル29に存在する唯一の清澄剤である。サンプル21および22におけるバッチのアルミナ(Al2O3)を清澄剤水酸化アルミニウム(Al(OH)3)と置換し、サンプル23および24におけるソーダ灰を水酸化ナトリウム(NaOH)と置換した。サンプル21および23はそれぞれ、所定量の水酸化物の清澄剤(サンプル21のAl(OH)3およびサンプル23のNaOH)を含み、3モルのH2Oを生じるのに対し、サンプル22および24はそれぞれ、所定量の水酸化物の清澄剤(サンプル21におけるAl(OH)3およびサンプル23におけるNaOH)を含み、6モルのH2Oを生じる。サンプル27および28に酸化剤として硝酸ナトリウムを加えた。
実施例3では、水酸化物の清澄剤の水素透過に対する有効性を比較する。各サンプルに用いられるバッチ材料を表3aに示す。
Claims (10)
- 1シード/cm3未満のシード濃度を有するケイ酸塩ガラスであって、
前記ケイ酸塩ガラスが少なくとも1種類の清澄剤を含む原材料バッチから形成され、
前記清澄剤が、溶融物が形成される温度において水源として作用する、少なくとも1種類の無機化合物を含み、
前記ケイ酸塩ガラスおよび前記少なくとも1種類の清澄剤がアンチモンおよびヒ素を実質的に含まない、
ケイ酸塩ガラス。 - 前記清澄剤が、金属水和物、金属水酸化物、およびそれらの組合せのうち少なくとも1つを含むことを特徴とする請求項1記載のケイ酸塩ガラス。
- 前記金属水和物が、粘土、ゼオライト、雲母、およびそれらの組合せのうちの1つであることを特徴とする請求項2記載のケイ酸塩ガラス。
- 前記金属水酸化物が、水酸化アルミニウム、アルカリ金属水酸化物、アルカリ土類金属水酸化物、水酸化ジルコニウム、およびそれらの組合せのうちの1つであることを特徴とする請求項2記載のケイ酸塩ガラス。
- 前記清澄剤が、前記溶融物に対して酸素源として作用する少なくとも1種類の多価金属酸化物と、随意的に少なくとも1種類の酸化剤とを、さらに含むことを特徴とする請求項1または2記載のケイ酸塩ガラス。
- 前記ケイ酸塩ガラスが、ホウケイ酸塩ガラス、アルミノケイ酸塩ガラス、およびそれらの組合せのうちの1つであることを特徴とする請求項1〜5いずれか1項記載のケイ酸塩ガラス。
- 前記ケイ酸塩ガラスが、60〜70mol%のSiO2;6〜14mol%のAl2O3;0〜15mol%のB2O3;0〜15mol%のLi2O;0〜20mol%のNa2O;0〜10mol%のK2O;0〜8mol%のMgO;0〜10mol%のCaO;0〜5mol%のZrO2;0〜1mol%のSnO2;0〜1mol%のCeO2;50ppm未満のAs2O3;および50ppm未満のSb2O3を含み、
ここで、12mol%≦Li2O+Na2O+K2O≦20mol%および0mol%≦MgO+CaO≦10mol%であり、
前記ケイ酸塩ガラスが実質的にリチウムを含まず、ダウンドロー可能かつイオン交換可能であることを特徴とする請求項7記載のケイ酸塩ガラス。 - 前記ケイ酸塩ガラスが、イオン交換する際に、少なくとも200MPaの表面圧縮応力および、少なくとも30μmの深さの表面圧縮層を有することを特徴とする請求項8記載のケイ酸塩ガラス。
- 前記ケイ酸塩ガラスが、モバイル電子機器のためのカバープレートを形成することを特徴とする請求項1〜8いずれか1項記載のケイ酸塩ガラス。
- 1シード/cm3未満のシード濃度を有するケイ酸塩ガラスの製造方法であって、前記方法が、
a.バッチを提供し、ここで前記バッチが、前記ケイ酸塩ガラスのための原材料と、ガラス1キログラム当たり1モルの水蒸気を生成するのに十分な量の少なくとも1種類の清澄剤とを含み、ここで前記少なくとも1種類の清澄剤が、実質的にヒ素およびアンチモンを含まず、溶融物が形成される温度において水源として作用する少なくとも1種類の無機化合物を含み、
b.前記バッチを溶融してケイ酸塩ガラス溶融物を形成し、
c.前記水を蒸発させて水蒸気を形成し、ここで前記水蒸気が前記溶融物中に複数の泡を形成し、
d.前記溶融物中で前記複数の泡をシードと融合させて、前記溶融物中の前記シード濃度を所定の濃度未満に低減し、
e.前記融合させた泡およびシードを少なくともある程度、前記溶融物から除去し、
f.前記溶融物を固化して前記ケイ酸塩ガラスを形成し、ここで前記ガラスが1シード/cm3未満のシード濃度を有する、
各工程を有してなる方法。
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US6713008P | 2008-02-26 | 2008-02-26 | |
US61/067,130 | 2008-02-26 | ||
PCT/US2009/001063 WO2009108285A2 (en) | 2008-02-26 | 2009-02-18 | Fining agents for silicate glasses |
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JP2015237329A Pending JP2016029021A (ja) | 2008-02-26 | 2015-12-04 | ケイ酸塩ガラス用の清澄剤 |
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EP (3) | EP3138822B1 (ja) |
JP (4) | JP5583606B2 (ja) |
KR (1) | KR101606600B1 (ja) |
CN (2) | CN101980983B (ja) |
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Cited By (4)
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JP2012197226A (ja) * | 2008-02-26 | 2012-10-18 | Corning Inc | ケイ酸塩ガラス用の清澄剤 |
WO2014014003A1 (ja) * | 2012-07-18 | 2014-01-23 | 日本電気硝子株式会社 | 医薬品容器用ガラス、及びこれを用いた医薬品容器用ガラス管、医薬品容器の製造方法、及び、医薬品容器 |
JP2016501818A (ja) * | 2012-11-30 | 2016-01-21 | コーニング インコーポレイテッド | IRタッチスクリーン用途のための低Feガラス |
JP2020100538A (ja) * | 2018-12-25 | 2020-07-02 | 日本電気硝子株式会社 | ガラス製造用混合原料及びこれを用いたガラスの製造方法 |
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JP5467490B2 (ja) | 2007-08-03 | 2014-04-09 | 日本電気硝子株式会社 | 強化ガラス基板の製造方法及び強化ガラス基板 |
KR20100091228A (ko) | 2007-11-29 | 2010-08-18 | 코닝 인코포레이티드 | 개선된 인성 및 내스크래치성을 갖는 유리 |
ES2550515T3 (es) | 2008-08-08 | 2015-11-10 | Corning Incorporated | Artículos de vidrio reforzado y métodos para su elaboración |
CN101508524B (zh) * | 2009-03-31 | 2010-06-30 | 成都光明光电股份有限公司 | 适于化学钢化的玻璃及其化学钢化玻璃 |
US8771532B2 (en) | 2009-03-31 | 2014-07-08 | Corning Incorporated | Glass having anti-glare surface and method of making |
US20100279068A1 (en) * | 2009-05-04 | 2010-11-04 | Glen Bennett Cook | Embossed glass articles for anti-fingerprinting applications and methods of making |
US20100285272A1 (en) * | 2009-05-06 | 2010-11-11 | Shari Elizabeth Koval | Multi-length scale textured glass substrates for anti-fingerprinting |
US8647995B2 (en) | 2009-07-24 | 2014-02-11 | Corsam Technologies Llc | Fusion formable silica and sodium containing glasses |
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