JP2007314869A - 金属ナノ粒子の製造方法およびこれにより製造された金属ナノ粒子 - Google Patents

金属ナノ粒子の製造方法およびこれにより製造された金属ナノ粒子 Download PDF

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Publication number: JP2007314869A
Authority: JP; Japan
Prior art keywords: solution; metal nanoparticles; weight; parts; metal
Prior art date: 2006-05-25
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Pending

Application number

JP2007052309A

Other languages

English (en)

Japanese (ja)

Inventor

Kwi-Jong Lee

リー、クウィ−ジョン

Byung-Ho Jun

ジュン、ビュン−ホウ

Hye-Jin Cho

チョ、ヒエ−ジン

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Samsung Electro Mechanics Co Ltd

Original Assignee

Samsung Electro Mechanics Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2006-05-25

Filing date

2007-03-02

Publication date

2007-12-06

2007-03-02 Application filed by Samsung Electro Mechanics Co Ltd filed Critical Samsung Electro Mechanics Co Ltd

2007-12-06 Publication of JP2007314869A publication Critical patent/JP2007314869A/ja

Status Pending legal-status Critical Current

Links

239000002082 metal nanoparticle Substances 0.000 title claims abstract description 70
238000000034 method Methods 0.000 title claims abstract description 26
239000006185 dispersion Substances 0.000 claims abstract description 39
229910052751 metal Inorganic materials 0.000 claims abstract description 39
239000002184 metal Substances 0.000 claims abstract description 39
239000003381 stabilizer Substances 0.000 claims abstract description 39
239000002243 precursor Substances 0.000 claims abstract description 38
239000002798 polar solvent Substances 0.000 claims abstract description 21
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
239000000243 solution Substances 0.000 claims description 75
238000004519 manufacturing process Methods 0.000 claims description 38
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 33
229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 22
239000001267 polyvinylpyrrolidone Substances 0.000 claims description 22
235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 22
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 21
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 21
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 17
239000002245 particle Substances 0.000 claims description 17
239000003638 chemical reducing agent Substances 0.000 claims description 13
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 12
238000002347 injection Methods 0.000 claims description 11
239000007924 injection Substances 0.000 claims description 11
239000002253 acid Substances 0.000 claims description 10
229910052709 silver Inorganic materials 0.000 claims description 10
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 9
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 9
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 claims description 9
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 9
239000000203 mixture Substances 0.000 claims description 9
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 9
229910052802 copper Inorganic materials 0.000 claims description 7
229920005862 polyol Polymers 0.000 claims description 7
150000003077 polyols Chemical class 0.000 claims description 7
KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims description 6
101710134784 Agnoprotein Proteins 0.000 claims description 6
ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims description 6
ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 6
239000011259 mixed solution Substances 0.000 claims description 6
239000011949 solid catalyst Substances 0.000 claims description 6
238000005406 washing Methods 0.000 claims description 6
239000003960 organic solvent Substances 0.000 claims description 4
VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 claims description 3
241000080590 Niso Species 0.000 claims description 3
239000002202 Polyethylene glycol Substances 0.000 claims description 3
229910021607 Silver chloride Inorganic materials 0.000 claims description 3
229920002125 Sokalan® Polymers 0.000 claims description 3
UWHCKJMYHZGTIT-UHFFFAOYSA-N Tetraethylene glycol, Natural products OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 claims description 3
150000007513 acids Chemical class 0.000 claims description 3
150000003863 ammonium salts Chemical class 0.000 claims description 3
CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 3
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
239000004584 polyacrylic acid Substances 0.000 claims description 3
229920001223 polyethylene glycol Polymers 0.000 claims description 3
229920001444 polymaleic acid Polymers 0.000 claims description 3
229920001451 polypropylene glycol Polymers 0.000 claims description 3
XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 claims description 3
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 claims description 3
159000000000 sodium salts Chemical class 0.000 claims description 3
DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 claims description 3
ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 3
229910021591 Copper(I) chloride Inorganic materials 0.000 claims description 2
OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 claims description 2
230000009467 reduction Effects 0.000 claims description 2
239000003795 chemical substances by application Substances 0.000 claims 1
238000006243 chemical reaction Methods 0.000 abstract description 20
230000015572 biosynthetic process Effects 0.000 abstract description 9
238000003786 synthesis reaction Methods 0.000 abstract description 8
239000002105 nanoparticle Substances 0.000 description 11
239000010949 copper Substances 0.000 description 10
FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 8
238000002156 mixing Methods 0.000 description 7
239000004332 silver Substances 0.000 description 7
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
239000002923 metal particle Substances 0.000 description 6
238000010899 nucleation Methods 0.000 description 6
230000006911 nucleation Effects 0.000 description 6
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 6
230000008859 change Effects 0.000 description 5
230000007423 decrease Effects 0.000 description 4
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
230000008569 process Effects 0.000 description 4
-1 silver ions Chemical class 0.000 description 4
238000003756 stirring Methods 0.000 description 4
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
239000003054 catalyst Substances 0.000 description 3
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
239000012530 fluid Substances 0.000 description 3
239000007789 gas Substances 0.000 description 3
239000007791 liquid phase Substances 0.000 description 3
229910021645 metal ion Inorganic materials 0.000 description 3
229920000642 polymer Polymers 0.000 description 3
150000003839 salts Chemical class 0.000 description 3
229910001961 silver nitrate Inorganic materials 0.000 description 3
KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
239000012071 phase Substances 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
239000002904 solvent Substances 0.000 description 2
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
239000000654 additive Substances 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
125000004429 atom Chemical group 0.000 description 1
238000009835 boiling Methods 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
238000000366 colloid method Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000000470 constituent Substances 0.000 description 1
238000011109 contamination Methods 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
150000002009 diols Chemical class 0.000 description 1
238000001035 drying Methods 0.000 description 1
238000005868 electrolysis reaction Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
229910052737 gold Inorganic materials 0.000 description 1
239000010931 gold Substances 0.000 description 1
125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
150000002736 metal compounds Chemical class 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
230000001603 reducing effect Effects 0.000 description 1
239000012798 spherical particle Substances 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
238000002371 ultraviolet--visible spectrum Methods 0.000 description 1
229920003169 water-soluble polymer Polymers 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
- B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/05—Metallic powder characterised by the size or surface area of the particles
- B22F1/054—Nanosized particles
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
- B82B1/00—Nanostructures formed by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12014—All metal or with adjacent metals having metal particles

JP2007052309A 2006-05-25 2007-03-02 金属ナノ粒子の製造方法およびこれにより製造された金属ナノ粒子 Pending JP2007314869A (ja)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
KR1020060047267A KR100790948B1 (ko)	2006-05-25	2006-05-25	금속 나노입자의 제조방법 및 이에 의해 제조되는 금속나노입자

Publications (1)

Publication Number	Publication Date
JP2007314869A true JP2007314869A (ja)	2007-12-06

Family

ID=38749898

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2007052309A Pending JP2007314869A (ja)	2006-05-25	2007-03-02	金属ナノ粒子の製造方法およびこれにより製造された金属ナノ粒子

Country Status (4)

Country	Link
US (1)	US20070275259A1 (ko)
JP (1)	JP2007314869A (ko)
KR (1)	KR100790948B1 (ko)
CN (1)	CN100569418C (ko)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2010077472A (ja) *	2008-09-25	2010-04-08	Japan Science & Technology Agency	金属ナノ粒子の製造方法
CN102009184A (zh) *	2009-09-04	2011-04-13	施乐公司	金属纳米颗粒的制备方法、其组合物及形成金属框架的方法
WO2013035366A1 (ja) *	2011-09-08	2013-03-14	学校法人関西大学	分散安定性の高い銅ナノ粒子の製造方法
JP5310967B1 (ja) *	2011-11-18	2013-10-09	住友金属鉱山株式会社	銀粉の製造方法
JP2014058713A (ja) *	2012-09-14	2014-04-03	Dowa Electronics Materials Co Ltd	板状銅粉とその製造方法および導電性ペースト

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* Cited by examiner, † Cited by third party
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KR100790457B1 (ko) *	2006-07-10	2008-01-02	삼성전기주식회사	금속 나노입자의 제조방법
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US20070275259A1 (en)	2007-11-29
CN100569418C (zh)	2009-12-16
KR20070113692A (ko)	2007-11-29
CN101077530A (zh)	2007-11-28
KR100790948B1 (ko)	2008-01-03

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JP2007314869A - 金属ナノ粒子の製造方法およびこれにより製造された金属ナノ粒子 - Google Patents

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