JP2006517099A - 脂溶性物質の粉末調製物の製造方法 - Google Patents
脂溶性物質の粉末調製物の製造方法 Download PDFInfo
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- JP2006517099A JP2006517099A JP2006500518A JP2006500518A JP2006517099A JP 2006517099 A JP2006517099 A JP 2006517099A JP 2006500518 A JP2006500518 A JP 2006500518A JP 2006500518 A JP2006500518 A JP 2006500518A JP 2006517099 A JP2006517099 A JP 2006517099A
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- F26B3/00—Drying solid materials or objects by processes involving the application of heat
- F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
- F26B3/06—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried
- F26B3/08—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B3/00—Drying solid materials or objects by processes involving the application of heat
- F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
- F26B3/10—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it
- F26B3/12—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it in the form of a spray, i.e. sprayed or dispersed emulsions or suspensions
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Abstract
Description
(a)垂直噴霧塔の上寄り部分に、噴霧ノズルを介して前記脂溶性物質及び前記マトリックス成分の水性エマルションを供給し、別個の送込み口を介して粉末状デンプン及び熱気流を供給することと、
(b)前記噴霧塔の下寄り部分に冷気流を供給して、前記マトリックス成分、前記脂溶性物質を含むデンプン被覆ビードレットの流動床を形成することと、
(c)前記ビードレットを流動床から捕集し、それを乾燥機に排出することと
を含む方法に関する。さらなる態様で、本発明は、実質的に図2に示すとおりのノズルの構造に関する。
有効成分、たとえば酢酸dl−α−トコフェロール3重量%、水43重量%、リグニンスルホン酸塩50重量%及び添加物4重量%を含むエマルションを調製し、図1に示す設備で処理した。以下、括弧内の参照番号は図1中の各参照番号を指す。
Claims (9)
- 水溶性又は水分散性の非ゲル化性マトリックス中の脂溶性物質のビードレット調製物を製造する方法であって、
(a)垂直噴霧塔の上寄り部分に、噴霧ノズルを介して前記脂溶性物質及び前記マトリックス成分の水性エマルションを供給し、別個の送込み口を介して粉末状デンプン及び熱気流を供給することと、
(b)前記噴霧塔の下寄り部分に冷気流を供給して、前記マトリックス成分、前記脂溶性物質を含むデンプン被覆ビードレットの流動床を形成することと、
(c)前記ビードレットを流動床から捕集し、それを乾燥機に排出することと
を含む方法。 - 噴霧ゾーンが約40℃〜約200℃、好ましくは約60℃〜約120℃の温度を有し、流動床が約0℃〜約40℃、好ましくは約5〜約20℃の温度を有する、請求項1記載の方法。
- (a)幅広の上端が閉じられ、デンプン/空気分散系のための1個以上の送込み口を保持する第一の中空円錐体と、
(b)第一の中空外側円錐体の中に、前記第一の円錐体中で上を向くような方法で装着されて、端部で、外面と第一の円錐体の内面との間に小さな円形の溝孔を残す第二の内側円錐体と、
(c)下向きに第二の円錐体の上方に突出し、回転噴霧器又は加圧噴霧器で終端する、閉じた端部及び回転噴霧器を有する送込み管と、
(d)外側円錐体を包囲し、両円錐体によって形成される円形溝孔よりもわずかに上方で終端する円形の空気送込み路と
を含む、実質的に図2に示すとおりであるノズル構造を介して水性エマルション、デンプン及び熱気流を噴霧塔に供給する、請求項1又は2記載の方法。 - マトリックス成分がリグニン誘導体である、請求項1〜3のいずれか1項記載の方法。
- リグニン誘導体がリグニンスルホン酸塩である、請求項4記載の方法。
- 脂溶性物質が、ビタミンA、D、E及びK、カロテノイド、多価不飽和脂肪酸、油又は脂肪である、請求項1〜5のいずれか1項記載の方法。
- 脂溶性物質が、β−カロテン、アスタキサンチン、アポカロテナール、カンタキサンチン、アポエステル、シトラナキサンチン又はゼアキサンチンである、請求項1〜5のいずれか1項記載の方法。
- (a)幅広の上端が閉じられ、デンプン/空気分散系のための1個以上の送込み口を保持する第一の中空円錐体と、
(b)第一の中空外側円錐体の中に、前記第一の円錐体中で上を向くような方法で装着されて、端部で、外面と第一の円錐体の内面との間に小さな円形の溝孔を残す第二の内側円錐体と、
(c)下向きに第二の円錐体の上方に突出し、回転噴霧器又は加圧噴霧器で終端する、閉じた端部及び小さな側方開口部を有する回転送込み管と、
(d)外側円錐体を包囲し、両円錐体によって形成される円形溝孔よりもわずかに上方で終端する円形の空気送込み路と
を含む、実質的に図2に示すとおりであるノズル構造。 - 特に実施例及び図面を参照しながら明細書に記載するとおりの発明。
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JP2011529697A (ja) * | 2008-08-04 | 2011-12-15 | ディーエスエム アイピー アセッツ ビー.ブイ. | プロバイオティック混合物を含む小ビーズの製造 |
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JP2011529697A (ja) * | 2008-08-04 | 2011-12-15 | ディーエスエム アイピー アセッツ ビー.ブイ. | プロバイオティック混合物を含む小ビーズの製造 |
JP2011529698A (ja) * | 2008-08-04 | 2011-12-15 | ディーエスエム アイピー アセッツ ビー.ブイ. | 吸湿性植物抽出物を含む小ビーズの製造 |
JP2022532294A (ja) * | 2019-03-28 | 2022-07-14 | リグノピュア ゲーエムべーハー | リグニン超微粒子の生成方法 |
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WO2004062382A1 (en) | 2004-07-29 |
DE602004007480D1 (de) | 2007-08-23 |
KR101088520B1 (ko) | 2011-12-06 |
US7691297B2 (en) | 2010-04-06 |
CN100411549C (zh) | 2008-08-20 |
KR20050092037A (ko) | 2005-09-16 |
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