IL45122A - Process for the recovery of cyanuric chloride - Google Patents

Process for the recovery of cyanuric chloride

Info

Publication number: IL45122A
Authority: IL; Israel
Prior art keywords: chloride; cyanogen; column; cyanuric; fractionation
Prior art date: 1973-06-27

Application number

IL45122A

Other languages

English (en)

Other versions

IL45122A0 (en

Original Assignee

Degussa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-06-27

Filing date

1974-06-26

Publication date

1977-10-31

1973-06-27 Priority claimed from DE19732332636 external-priority patent/DE2332636C3/de

1974-06-26 Application filed by Degussa filed Critical Degussa

1974-09-10 Publication of IL45122A0 publication Critical patent/IL45122A0/xx

1977-10-31 Publication of IL45122A publication Critical patent/IL45122A/en

Links

MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 title claims description 31
238000000034 method Methods 0.000 title claims description 22
238000011084 recovery Methods 0.000 title description 4
QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims description 28
239000007789 gas Substances 0.000 claims description 16
JMANVNJQNLATNU-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 claims description 16
239000002904 solvent Substances 0.000 claims description 15
239000000203 mixture Substances 0.000 claims description 14
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 11
238000005194 fractionation Methods 0.000 claims description 11
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 10
239000000460 chlorine Substances 0.000 claims description 10
229910052801 chlorine Inorganic materials 0.000 claims description 10
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 8
239000001257 hydrogen Substances 0.000 claims description 8
229910052739 hydrogen Inorganic materials 0.000 claims description 8
239000007788 liquid Substances 0.000 claims description 8
239000007864 aqueous solution Substances 0.000 claims description 6
238000009835 boiling Methods 0.000 claims description 5
CKUAXEQHGKSLHN-UHFFFAOYSA-N [C].[N] Chemical compound [C].[N] CKUAXEQHGKSLHN-UHFFFAOYSA-N 0.000 claims description 4
NCSHGROOCJHAFK-UHFFFAOYSA-N [Cl].N#CC#N Chemical compound [Cl].N#CC#N NCSHGROOCJHAFK-UHFFFAOYSA-N 0.000 claims description 3
239000003513 alkali Substances 0.000 claims description 2
150000001491 aromatic compounds Chemical group 0.000 claims description 2
238000012986 modification Methods 0.000 claims description 2
230000004048 modification Effects 0.000 claims description 2
125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 claims description 2
GETTZEONDQJALK-UHFFFAOYSA-N (trifluoromethyl)benzene Chemical group FC(F)(F)C1=CC=CC=C1 GETTZEONDQJALK-UHFFFAOYSA-N 0.000 claims 1
GKXWTRSVUPXQMM-UHFFFAOYSA-N 1,1,1,2,2-pentachloro-3,3,3-trifluoropropane Chemical compound FC(F)(F)C(Cl)(Cl)C(Cl)(Cl)Cl GKXWTRSVUPXQMM-UHFFFAOYSA-N 0.000 claims 1
BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 claims 1
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
YVBBRRALBYAZBM-UHFFFAOYSA-N perfluorooctane Chemical compound FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YVBBRRALBYAZBM-UHFFFAOYSA-N 0.000 claims 1
239000011541 reaction mixture Substances 0.000 claims 1
LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 14
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 10
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
238000005660 chlorination reaction Methods 0.000 description 6
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
229910052799 carbon Inorganic materials 0.000 description 5
229910002092 carbon dioxide Inorganic materials 0.000 description 5
239000001569 carbon dioxide Substances 0.000 description 5
239000011551 heat transfer agent Substances 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
238000005406 washing Methods 0.000 description 4
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
238000010521 absorption reaction Methods 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
230000003197 catalytic effect Effects 0.000 description 2
238000004821 distillation Methods 0.000 description 2
229910000041 hydrogen chloride Inorganic materials 0.000 description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000000746 purification Methods 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000002912 waste gas Substances 0.000 description 2
239000002699 waste material Substances 0.000 description 2
KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 1
MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 description 1
241000725101 Clea Species 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
LTJDCQQWATZCDA-UHFFFAOYSA-N N#CCl.[Cl] Chemical compound N#CCl.[Cl] LTJDCQQWATZCDA-UHFFFAOYSA-N 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
KPAMAAOTLJSEAR-UHFFFAOYSA-N [N].O=C=O Chemical compound [N].O=C=O KPAMAAOTLJSEAR-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
239000002253 acid Substances 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
SURLGNKAQXKNSP-DBLYXWCISA-N chlorin Chemical compound C\1=C/2\N/C(=C\C3=N/C(=C\C=4NC(/C=C\5/C=CC/1=N/5)=CC=4)/C=C3)/CC\2 SURLGNKAQXKNSP-DBLYXWCISA-N 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000011109 contamination Methods 0.000 description 1
-1 cyanogen cyanuric chloride Chemical compound 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000000945 filler Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
CABDFQZZWFMZOD-UHFFFAOYSA-N hydrogen peroxide;hydrochloride Chemical compound Cl.OO CABDFQZZWFMZOD-UHFFFAOYSA-N 0.000 description 1
230000000266 injurious effect Effects 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000011707 mineral Substances 0.000 description 1
JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
ZRWRYPIDQULHRE-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N.N#CC#N ZRWRYPIDQULHRE-UHFFFAOYSA-N 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
230000000149 penetrating effect Effects 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
231100000572 poisoning Toxicity 0.000 description 1
230000000607 poisoning effect Effects 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000005201 scrubbing Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011734 sodium Substances 0.000 description 1
CMXPERZAMAQXSF-UHFFFAOYSA-M sodium;1,4-bis(2-ethylhexoxy)-1,4-dioxobutane-2-sulfonate;1,8-dihydroxyanthracene-9,10-dione Chemical compound [Na+].O=C1C2=CC=CC(O)=C2C(=O)C2=C1C=CC=C2O.CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC CMXPERZAMAQXSF-UHFFFAOYSA-M 0.000 description 1
239000007787 solid Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

IL45122A 1973-06-27 1974-06-26 Process for the recovery of cyanuric chloride IL45122A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19732332636 DE2332636C3 (de)		1973-06-27	Verfahren zur Gewinnung von Cyanurchlorid in flüssiger Form

Publications (2)

Publication Number	Publication Date
IL45122A0 IL45122A0 (en)	1974-09-10
IL45122A true IL45122A (en)	1977-10-31

Family

ID=5885212

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IL45122A IL45122A (en)	1973-06-27	1974-06-26	Process for the recovery of cyanuric chloride

Country Status (15)

Country	Link
US (1)	US3925377A (fr)
JP (1)	JPS5324956B2 (fr)
AT (1)	AT338281B (fr)
BE (1)	BE816936A (fr)
CH (1)	CH603604A5 (fr)
DD (1)	DD111378A5 (fr)
DK (1)	DK150983C (fr)
FR (1)	FR2235123B1 (fr)
GB (1)	GB1412725A (fr)
HU (1)	HU175723B (fr)
IL (1)	IL45122A (fr)
IT (1)	IT1014286B (fr)
NL (1)	NL7406062A (fr)
RO (1)	RO66325A (fr)
SE (1)	SE418965B (fr)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
RO70804A (fr) *	1974-11-20	1980-08-15	Deutsche Gold-Und Silber-Scheideanstalt Vormals Roessler,De	Procede et disposit pour la preparation des solutions ou suspensions de chlorure de cyanurile
DE2537673C2 (de) *	1975-08-23	1977-09-29	Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt	Verfahren zur Herstellung von feinteiligem, festem Cyanurchlorid
JPS5724710Y2 (fr) *	1976-06-14	1982-05-28
JPS5373558U (fr) *	1976-11-22	1978-06-20
DE2843378C3 (de) *	1978-10-05	1982-04-08	Degussa Ag, 6000 Frankfurt	Verfahren zum Gewinnen von festem Cyanurchlorid
DE2843379C3 (de) *	1978-10-05	1985-08-01	Degussa Ag, 6000 Frankfurt	Verfahren zum Gewinnen von festem Cyanurchlorid
DE2843382B2 (de) *	1978-10-05	1980-11-13	Degussa Ag, 6000 Frankfurt	Verfahren zur Gewinnung von Cyanurchlorid in fester oder flüssiger Form
DE2843381B2 (de) *	1978-10-05	1980-07-10	Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt	Verfahren zur Gewinnung von Cyanurchlorid in fester und flüssiger Form
DE2843380B2 (de) *	1978-10-05	1980-07-10	Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt	Verfahren zur Gewinnung von Cyanurchlorid in fester oder flüssiger Form
DE2850331C2 (de) *	1978-11-20	1981-02-26	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von ggf. substituierten 2-Amino-4,6-dichlors-triazinen
DE2850338B2 (de) *	1978-11-20	1981-05-07	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von trisubstituierten s-Trianzinverbindungen
DE2850339C2 (de) *	1978-11-20	1981-02-26	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von 2-Alkoxy-4,6-dichlor-s-triazinen
DE2850242C2 (de) *	1978-11-20	1984-10-04	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von Suspensionen von Cyanurchlorid in Wasser
DE2850332C2 (de) *	1978-11-20	1981-02-19	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von substituierten 2-Mercapto-4,6-di-chlor-striazinen
DE2850308C2 (de) *	1978-11-20	1984-09-20	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von Suspensionen oder Lösungen von Cyanurchlorid in wasserhaltigen organischen Lösungsmitteln
DE2850243C2 (de) *	1978-11-20	1984-09-20	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von Suspensionen von Cyanurchlorid in organischen Lösungsmitteln
JPS57194971A (en) *	1981-05-19	1982-11-30	Yoshino Kogyosho Co Ltd	Atomizer
JPS61179A (ja) *	1984-06-12	1986-01-06	東洋エアゾ−ル工業株式会社	エアゾ−ル容器の爆発防止装置
JP2725232B2 (ja) *	1993-11-30	1998-03-11	誠一北林	エアゾール噴出弁の安全弁機構によるエアゾール容器の爆発防止装置
DE19642449A1 (de)	1996-10-15	1998-04-16	Degussa	Cyanurchlorid-Formlinge und Verfahren zu ihrer Herstellung
DE10123072B4 (de) *	2001-05-11	2004-12-30	Degussa Ag	Vorrichtung zur Aufreinigung von Cyanurchlorid
DE102007059863A1 (de) *	2007-12-12	2009-06-18	Evonik Degussa Gmbh	Verfahren zur Reinigung der bei der Cyanurchlorid-Herstellung anfallenden Abgase

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2742977A (en) *		1956-04-24		Vapors of
CH510038A (de) *	1967-02-17	1971-07-15	Agripat Sa	Verfahren zur Herstellung einer Cyanurchloridlösung aus gasförmigem Cyanurchlorid
US3741729A (en) *	1970-03-26	1973-06-26	Ciba Geigy Corp	Apparatus for producing a solution of cyanuric chloride from gaseous cyanuric chloride
US3607671A (en) *	1970-07-02	1971-09-21	Ciba Geigy Corp	Condensing liquid cyanuric chloride from cases including washing the gases with liquid phosphorous oxychloride

1974
- 1974-04-11 DD DD177839A patent/DD111378A5/xx unknown
- 1974-04-19 GB GB1726074A patent/GB1412725A/en not_active Expired
- 1974-05-06 NL NL7406062A patent/NL7406062A/xx unknown
- 1974-06-04 IT IT68754/74A patent/IT1014286B/it active
- 1974-06-20 RO RO7479241A patent/RO66325A/fr unknown
- 1974-06-21 JP JP7124274A patent/JPS5324956B2/ja not_active Expired
- 1974-06-26 FR FR7422286A patent/FR2235123B1/fr not_active Expired
- 1974-06-26 HU HU74DE856A patent/HU175723B/hu unknown
- 1974-06-26 US US483454A patent/US3925377A/en not_active Expired - Lifetime
- 1974-06-26 DK DK344374A patent/DK150983C/da active
- 1974-06-26 IL IL45122A patent/IL45122A/en unknown
- 1974-06-26 BE BE6044660A patent/BE816936A/fr not_active IP Right Cessation
- 1974-06-27 AT AT532774A patent/AT338281B/de active
- 1974-06-27 CH CH885074A patent/CH603604A5/xx not_active IP Right Cessation
- 1974-06-27 SE SE7408530A patent/SE418965B/xx unknown

Also Published As

Publication number	Publication date
DK344374A (fr)	1975-02-24
DK150983B (da)	1987-10-05
FR2235123B1 (fr)	1977-06-24
FR2235123A1 (fr)	1975-01-24
CH603604A5 (fr)	1978-08-31
US3925377A (en)	1975-12-09
AT338281B (de)	1977-08-10
IT1014286B (it)	1977-04-20
DE2332636A1 (de)	1975-01-16
DD111378A5 (fr)	1975-02-12
RO66325A (fr)	1979-06-15
SE7408530L (fr)	1974-12-30
NL7406062A (fr)	1974-12-31
JPS5324956B2 (fr)	1978-07-24
IL45122A0 (en)	1974-09-10
JPS5036481A (fr)	1975-04-05
BE816936A (fr)	1974-12-27
DK150983C (da)	1988-02-15
SE418965B (sv)	1981-07-06
DE2332636B2 (de)	1976-11-11
GB1412725A (en)	1975-11-05
HU175723B (hu)	1980-10-28
ATA532774A (de)	1976-12-15

Publication	Publication Date	Title
IL45122A (en)	1977-10-31	Process for the recovery of cyanuric chloride
US3709795A (en)	1973-01-09	Purification of carboxylic acids by chemical treatment and distillation
US4209470A (en)	1980-06-24	Process for the separation of hydrogen fluoride from its mixtures with 1-chloro-1,1-difluoroethane
FI96412B (fi)	1996-03-15	Menetelmä ferrikloridin valmistamiseksi laimennetusta kloorivetyhaposta lähtemällä
EP0634390B1 (fr)	1997-10-15	Méthode pour enlever des impuretés acides ou salines d'une courant gazeux sortant d'un réacteur de synthèse du carbonate de diméthyle
US7217849B2 (en)	2007-05-15	Method for the preparation of n-propyl bromide
US5685957A (en)	1997-11-11	Method for removing acidic and salt impurities from an aqueous condensed phase containing dimethylcarbonate
US2134531A (en)	1938-10-25	Purification of maleic anhydride
JPS62221639A (ja)	1987-09-29	１，２−ジクロルエタンの製造法
US3829509A (en)	1974-08-13	Process for the treatment of aqueous solutions of phenol and hydrogen chloride
JP2828775B2 (ja)	1998-11-25	１，１―ジクロロ―１―フルオロエタンの製造法
US3184458A (en)	1965-05-18	Processes for producing trichloroisocyanuric acid
US4759826A (en)	1988-07-26	Process for purifying thionyl chloride
US3221063A (en)	1965-11-30	Distillation in raschig-phenol process
JPH04300842A (ja)	1992-10-23	ハイドロクロロフルオロカーボン及びハイドロフルオロカーボンの精製方法
US4358609A (en)	1982-11-09	Process for the recovery of carboxylic acid from mixtures containing glycol esters derived from these acids
JPH0819015B2 (ja)	1996-02-28	直接塩素化反応器のベント廃ガスからのエチレン、塩素及び塩化水素の回収
US3961023A (en)	1976-06-01	Process for the production of cyanogen chloride and hydrogen chloride
GB2272696A (en)	1994-05-25	Purification of 1,1-dichloro-1-fluoroethane
US4009186A (en)	1977-02-22	Process for the preparation of maleic anhydride from maleic acid in the presence of sulfolane
SU510990A3 (ru)	1976-04-15	Способ очистки 1,2-дихлорэтана от трихлорэтилена
US4743707A (en)	1988-05-10	Process for purifying allyl alcohol
US3100233A (en)	1963-08-06	Purification of acetylene tetrachloride containing chlorine impurity
US3996112A (en)	1976-12-07	Distillation of hexahalocyclopentadiene
CA1227496A (fr)	1987-09-29	Preparation de 1,2-dichloroethane