HUP9700189A1 - Eljárás 5-amino-2,4,6-trijód-1,3-benzoldikarbonsav előállítására - Google Patents

Eljárás 5-amino-2,4,6-trijód-1,3-benzoldikarbonsav előállítására

Info

Publication number
HUP9700189A1
HUP9700189A1 HU9700189A HUP9700189A HUP9700189A1 HU P9700189 A1 HUP9700189 A1 HU P9700189A1 HU 9700189 A HU9700189 A HU 9700189A HU P9700189 A HUP9700189 A HU P9700189A HU P9700189 A1 HUP9700189 A1 HU P9700189A1
Authority
HU
Hungary
Prior art keywords
benzenedicarboxylic acid
amino
sodium salt
halosubstituted
producing
Prior art date
Application number
HU9700189A
Other languages
English (en)
Inventor
Massimo Gagna
Marina Mauro
Carlo Felice Viscardi
Original Assignee
Fructamine S.P.A.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from ITMI951045A external-priority patent/IT1274547B/it
Priority claimed from IT95RM000549 external-priority patent/IT1277899B1/it
Application filed by Fructamine S.P.A. filed Critical Fructamine S.P.A.
Publication of HUP9700189A1 publication Critical patent/HUP9700189A1/hu
Publication of HUP9700189A3 publication Critical patent/HUP9700189A3/hu
Publication of HU217686B publication Critical patent/HU217686B/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/04—Formation of amino groups in compounds containing carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)

Abstract

A találmány értelmében az 5-aminő-2,4,6-trijód-1,3-benzől-dikarbőnsavat úgy állítják elő, hőgya) 5-nitrő-1,3-benződikarbőnsavat semleges vagy bázikűs közegben,katalitikűs hidrőgénezéssel 5-aminő-1,3-benzőldikarbőnsav-nátriűmsóvizes őldatává alakítják,b) az a) lépésben kapőtt 5-aminő-1,3-benzőldikarbőnsav-nátriűmsóttővábbi tiszítás nálkül ICI HCL-lel készült őldalával közvetlenüljódőzzák, miűtán az 5-aminő-1,3-benzőldikarbőnsav-nátriűmsó-őldatőthidrőgén-klőriddal és kénsavval adalékőlták.ŕ
HU9700189A 1995-05-23 1996-05-17 Eljárás 5-amino-2,4,6-trijód-1,3-benzoldikarbonsav előállítására HU217686B (hu)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ITMI951045A IT1274547B (it) 1995-05-23 1995-05-23 Processo per la preparazione dell'acido 5-ammino-2,4,6- triiodoisoftalico
IT95RM000549 IT1277899B1 (it) 1995-08-04 1995-08-04 Processo per la preparazione dell'acido 5-ammino-2,4,6 -triiodo- isoftalico"
PCT/EP1996/002105 WO1996037458A1 (en) 1995-05-23 1996-05-17 Process for the preparation of a halosubstituted aromatic acid

Publications (3)

Publication Number Publication Date
HUP9700189A1 true HUP9700189A1 (hu) 1998-01-28
HUP9700189A3 HUP9700189A3 (en) 1998-03-02
HU217686B HU217686B (hu) 2000-03-28

Family

ID=26331278

Family Applications (1)

Application Number Title Priority Date Filing Date
HU9700189A HU217686B (hu) 1995-05-23 1996-05-17 Eljárás 5-amino-2,4,6-trijód-1,3-benzoldikarbonsav előállítására

Country Status (23)

Country Link
US (1) US5763650A (hu)
EP (1) EP0773923B1 (hu)
JP (1) JP4012568B2 (hu)
KR (1) KR100269079B1 (hu)
CN (1) CN1109670C (hu)
AT (1) ATE192138T1 (hu)
AU (1) AU707177B2 (hu)
BR (1) BR9606487A (hu)
CA (1) CA2195635C (hu)
CZ (1) CZ289771B6 (hu)
DE (2) DE773923T1 (hu)
DK (1) DK0773923T3 (hu)
ES (1) ES2103254T3 (hu)
GR (2) GR970300029T1 (hu)
HU (1) HU217686B (hu)
IL (1) IL118360A (hu)
MX (1) MX9700549A (hu)
NO (1) NO314257B1 (hu)
PL (1) PL318285A1 (hu)
PT (1) PT773923E (hu)
SI (1) SI9620011A (hu)
SK (1) SK8997A3 (hu)
WO (1) WO1996037458A1 (hu)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7968745B2 (en) 2005-12-19 2011-06-28 Ge Healthcare As Purification process of iodixanol
WO2009091758A1 (en) 2008-01-14 2009-07-23 Mallinckrodt Inc. Process for the preparation of iosimenol
EP2093206A1 (en) * 2008-02-20 2009-08-26 BRACCO IMAGING S.p.A. Process for the iodination of aromatic compounds
EP2230227A1 (en) 2009-03-20 2010-09-22 Bracco Imaging S.p.A Process for the preparation of triiodinated carboxylic aromatic derivatives
EP2243767A1 (en) 2009-04-21 2010-10-27 Bracco Imaging S.p.A Process for the iodination of aromatic compounds
DK2451994T3 (da) * 2009-07-07 2014-01-20 Bracco Imaging Spa Fremgangsmåde til fremstilling af et ioderende middel
US7999134B2 (en) 2009-07-21 2011-08-16 Ge Healthcare As Crystallization of iodixanol using milling
US7999135B2 (en) 2009-07-21 2011-08-16 Ge Healthcare As Crystallization of iodixanol using ultrasound
CN102725249B (zh) 2009-11-26 2014-12-10 好利安中国控股有限公司 碘克沙醇的制备和纯化
EP2394984A1 (en) 2010-06-10 2011-12-14 Bracco Imaging S.p.A Process for the iodination of phenolic derivatives
WO2014090650A1 (en) 2012-12-11 2014-06-19 Bracco Imaging Spa Continuous process for the preparation of (s)-2-acetyloxypropionic acid chloride
PL3066071T3 (pl) 2013-11-05 2018-09-28 Bracco Imaging S.P.A Sposób otrzymywania jopamidolu
BR112016027507B1 (pt) 2014-06-10 2020-11-24 Bracco Imaging Spa método para a preparação de ácido (s)-2-acetiloxipropiônico e seus derivados
NZ757793A (en) 2017-06-07 2022-04-29 Bracco Imaging Spa A process for the recovery of iodine from aqueous solutions

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2820814A (en) * 1955-03-21 1958-01-21 Schering Corp Polyiodinated 5-aminoisophthalic acids, salts, and esters
SU502875A1 (ru) * 1973-03-26 1976-02-15 Войсковая Часть 41598 Способ получени метилового эфира 4-диметиламиносалициловой кислоты
SU502874A1 (ru) * 1973-12-07 1976-02-15 Институт Органического Катализа И Электрохимии Способ получени м-аминоизофталевой кислоты
US4102917A (en) * 1977-06-01 1978-07-25 American Cyanamid Company Substituted phenyl naphthalenesulfonic acids
JP2765696B2 (ja) * 1989-12-27 1998-06-18 三井化学株式会社 ５―アミノ―２，４，６―トリヨードイソフタル酸の製造方法

Also Published As

Publication number Publication date
KR100269079B1 (ko) 2000-10-16
JP4012568B2 (ja) 2007-11-21
CN1154688A (zh) 1997-07-16
DE69607921T2 (de) 2000-08-17
CA2195635C (en) 2008-07-22
PL318285A1 (en) 1997-06-09
BR9606487A (pt) 1997-11-25
EP0773923B1 (en) 2000-04-26
CN1109670C (zh) 2003-05-28
AU5818996A (en) 1996-12-11
CA2195635A1 (en) 1996-11-28
CZ18597A3 (en) 1997-07-16
US5763650A (en) 1998-06-09
GR3033957T3 (en) 2000-11-30
SI9620011A (en) 1997-06-30
CZ289771B6 (cs) 2002-04-17
ATE192138T1 (de) 2000-05-15
MX9700549A (es) 1997-05-31
HU217686B (hu) 2000-03-28
DE773923T1 (de) 1997-12-18
JPH10503530A (ja) 1998-03-31
NO314257B1 (no) 2003-02-24
ES2103254T3 (es) 2000-07-01
ES2103254T1 (es) 1997-09-16
AU707177B2 (en) 1999-07-01
IL118360A0 (en) 1996-09-12
IL118360A (en) 1999-12-22
DE69607921D1 (de) 2000-05-31
PT773923E (pt) 2000-08-31
EP0773923A1 (en) 1997-05-21
NO970263D0 (no) 1997-01-21
DK0773923T3 (da) 2000-09-04
HUP9700189A3 (en) 1998-03-02
GR970300029T1 (en) 1997-09-30
NO970263L (no) 1997-03-24
SK8997A3 (en) 1997-08-06
WO1996037458A1 (en) 1996-11-28

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Owner name: BRACCO IMAGING S.P.A., IT