EP2512683B1 - Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux - Google Patents

Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux Download PDF

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Publication number
EP2512683B1
EP2512683B1 EP10790780.0A EP10790780A EP2512683B1 EP 2512683 B1 EP2512683 B1 EP 2512683B1 EP 10790780 A EP10790780 A EP 10790780A EP 2512683 B1 EP2512683 B1 EP 2512683B1
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EP
European Patent Office
Prior art keywords
liquid
gas stream
jacket
droplet separator
hood
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
EP10790780.0A
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German (de)
English (en)
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EP2512683A1 (fr
Inventor
Jörg HALPAP
Andreas Bode
Eberhard Herrmann
Markus LINSENBÜHLER
Bernd Sachweh
Michael Pilz
Michael Mertler
Matthias Wilhelm Meier
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BASF SE
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BASF SE
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04CAPPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
    • B04C5/00Apparatus in which the axial direction of the vortex is reversed
    • B04C5/08Vortex chamber constructions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04CAPPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
    • B04C5/00Apparatus in which the axial direction of the vortex is reversed
    • B04C5/02Construction of inlets by which the vortex flow is generated, e.g. tangential admission, the fluid flow being forced to follow a downward path by spirally wound bulkheads, or with slightly downwardly-directed tangential admission
    • B04C5/04Tangential inlets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B7/00Elements of centrifuges
    • B04B7/08Rotary bowls
    • B04B7/12Inserts, e.g. armouring plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04CAPPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
    • B04C5/00Apparatus in which the axial direction of the vortex is reversed
    • B04C5/02Construction of inlets by which the vortex flow is generated, e.g. tangential admission, the fluid flow being forced to follow a downward path by spirally wound bulkheads, or with slightly downwardly-directed tangential admission
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04CAPPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
    • B04C5/00Apparatus in which the axial direction of the vortex is reversed
    • B04C5/14Construction of the underflow ducting; Apex constructions; Discharge arrangements ; discharge through sidewall provided with a few slits or perforations
    • B04C5/181Bulkheads or central bodies in the discharge opening
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04CAPPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
    • B04C9/00Combinations with other devices, e.g. fans, expansion chambers, diffusors, water locks
    • B04C2009/008Combinations with other devices, e.g. fans, expansion chambers, diffusors, water locks with injection or suction of gas or liquid into the cyclone

Definitions

  • the invention relates to a centrifugal droplet separator for separating liquid droplets from a feed gas stream containing them.
  • Centrifugal droplet separators also referred to as cyclones, are known in the art and are used, for example, for separating liquid droplets from gas streams containing them.
  • Centrifugal drop separators are rotationally symmetrical apparatus, usually with a vertical axis of rotation, often predominantly cylindrical apparatuses.
  • By tangentially introducing the biphasic liquid / gas mixture to be separated it is imparted a helical motion along the inner wall of the apparatus, whereby separation of the components of the mixture as a function of their density occurs under the action of the centrifugal force.
  • the heavier liquid droplets are deposited from the gas on the inner walls of the Zentrifugaltropfenabscheiders, accumulate in the lower part of the apparatus and are discharged through a discharge nozzle.
  • droplets with a mean diameter ⁇ 5 ⁇ m with a probability of 50% and droplets with a mean diameter ⁇ 12 ⁇ m with a probability of> 99% are deposited in the centrifugal droplet separator.
  • the problem may arise that deposit the liquid droplets or solid crusts on the inner walls of the apparatus, no longer run through the discharge nozzle, so that it to fowling associated with a worsening deposition and finally flooding the apparatus.
  • a discontinuous or a continuous cleaning of the apparatus described above by spraying a rinsing liquid by means of spray nozzles.
  • the cleaning success is not always guaranteed, since solids are trapped in protected areas, for example in louvers in lamella separators or in a wire mesh, and thus often can not be discharged.
  • the rinsing liquid must be dispersed in the gas stream and also be separated therefrom.
  • the FR 2 147 545 describes a Zentrifugaltropfenabscheider for cleaning a gas with tangential supply thereof in the lower, conically shaped portion of the centrifugal separator, and with supply of an auxiliary gas stream in the region of the outlet of the purified gas through tangentially arranged supply ports, wherein the auxiliary gas flow in countercurrent to the flow direction of the gas to be cleaned is supplied.
  • the centrifugal separator is supplied.
  • the gas stream to be purified and the auxiliary gas stream are guided in opposite directions of rotation, but not in the same direction of rotation as in the method of the present invention.
  • the object is achieved by a Zentrifugaltropfenabscheider for separating liquid droplets from a feed gas stream containing them, with vertical longitudinal axis and circular cross-section, with a jacket and hoods at the top and at the bottom of the shell, with tangential supply of the liquid droplets containing feed gas stream on the jacket and with a discharge nozzle for the liquid separated in the centrifugal droplet separator in the region of the lower hood and with a gas outlet nozzle for the gas stream cleaned in the centrifugal droplet separator in the region of the upper hood, which is characterized in that two, three or more inlet openings arranged symmetrically on the circumference of the upper hood a tangential supply of rinsing liquid, in the same direction as the supply of the liquid droplet-containing feed gas stream, are provided.
  • the liquid preferably runs over an edge so that complete wetting of the wall with rinsing liquid is achieved.
  • the flushing liquid according to the invention is introduced tangentially, and thus to the inner walls of the apparatus, it is directly into the areas where the liquid separates from the mixture to be separated, and does not have to be separated from the mixture. This increases the efficiency and leads to an overall lower energy consumption, since complete wetting of the wall is achieved, dry spots on the wall are avoided and thus crust formation is prevented.
  • liquids are used as the rinsing liquid, which can easily be separated again from the liquid to be separated off from the feed gas stream, and which in particular do not chemically react with it.
  • Solvents for the liquid to be separated from the feed gas stream or the same liquid which can be separated off from the feed gas stream can also be used as the rinsing liquid.
  • the rinsing liquid can be used with or without additives.
  • rinsing liquid can also be a reaction, a chemisorption or a physisorption.
  • water can be used as the rinsing liquid.
  • the inlet openings for the rinsing liquid may have a circular cross-section.
  • the inlet openings for the rinsing liquid are formed with a rectangular cross-section.
  • the lower hood tapers frusto-conically towards the discharge nozzle.
  • the steepness of the truncated cone should be chosen so that the liquid flows freely, i. at higher viscosity of the liquid a greater slope.
  • the cone is very steep.
  • the lower hood may also be flat or designed as a dished bottom.
  • apex cone which may preferably be open at the bottom for reasons of easier manufacture, and at the bottom of the lower hood, perpendicular to the floor and radially Plates arranged, which support a uniform outflow of the liquid and the flow of the réelletParkden mixture in the apparatus do not disturb as possible. In this way non-effluent thrombi are avoided.
  • the diameter of the Apexkegels is advantageously adapted to the inner diameter of the Zentrifugaltropfenabscheiders.
  • the apex cone is formed with a diameter corresponding to 0.6 to 0.8 times the inner diameter of the centrifugal droplet separator.
  • the angle in the tip of the Apexkegels is preferably between 100 and 130 °. However, it is also plate-shaped embodiments - without apex cone - possible.
  • the on the bottom of the lower hood perpendicular to the ground and radially arranged sheets act in particular as a flow breaker.
  • a downwardly open dripping apron is arranged in the region of the upper hood, around the gas outlet nozzle, at which liquid droplets are separated from the gas stream which exits via the gas outlet nozzle and drip back into the apparatus.
  • the drip apron preferably has a length corresponding to 1.2 times the length of the gas outlet nozzle projecting into the apparatus.
  • the upper hood at the periphery of which two, three or more inlet openings are provided for a tangential supply of rinsing liquid, widens frustoconically with respect to the circumference of the jacket, an edge forming at the transition between the jacket and the upper hood the rinse liquid is running.
  • the invention also provides a process for separating liquid droplets from a feed gas stream containing them into a centrifugal droplet separator having a vertical longitudinal axis and a circular cross section, with a jacket and hoods at the top and at the bottom of the jacket, with at least one tangential feed of the liquid droplet containing feed gas stream on the mantle and with a discharge nozzle for the liquid deposited in the centrifugal droplet separator in the region of the lower hood and with a central gas outlet for the gas stream purified in the centrifugal droplet separator in the region of the upper hood, which is characterized in that in the region of the upper hood, over two, three or a plurality of inlet openings arranged symmetrically on the circumference thereof, a flushing liquid being introduced tangentially in the same direction as the feed gas stream containing the liquid droplets.
  • the rinsing liquid can be supplied continuously during the entire duration of the supply of the feed gas stream to be separated.
  • the rinsing liquid is fed discontinuously, at intervals.
  • FIG. 1 shows an embodiment of a centrifugal Tropfenabscheiders invention with sheath 1 and hoods 2 at the top and at the bottom of the shell 1, and with tangential feed 3 for the feed gas stream.
  • Zentrifugaltropfenabscheider liquid is discharged through a discharge nozzle 4 in the region of the lower hood 2 and the purified gas stream via a gas outlet nozzle 7 in the region of the upper hood. 2
  • a bottom open Abtropfschürze 8 is provided in the region of the upper hood 2 in the longitudinal sectional view in FIG. 1 to recognize a tangentially arranged inlet opening 9 for a rinsing liquid.
  • FIG. 2 shows the tangentially arranged in the region of the upper hood 2, for example, three inlet openings 9 for a rinsing liquid.
  • the tangential feed 3 and the central gas outlet nozzle 7 can also be seen.

Landscapes

  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Separating Particles In Gases By Inertia (AREA)
  • Cyclones (AREA)
  • Centrifugal Separators (AREA)

Claims (5)

  1. Procédé pour la séparation de gouttes de liquide dans un flux gazeux qui les contient dans un séparateur de gouttes par centrifugation avec un axe longitudinal vertical et une section transversale circulaire comportant une enceinte (1) ainsi que des hottes (2) à l'extrémité supérieure et inférieure de l'enceinte (1), avec introduction tangentielle (3) du flux gazeux contenant des gouttes de liquide dans l'enceinte (1) ainsi qu'un tuyau d'évacuation (4) pour le liquide séparé dans le séparateur de gouttes par centrifugation dans la région de la hotte inférieure (2) et un tuyau d'échappement de gaz (7) pour le flux gazeux épuré dans le séparateur de gouttes par centrifugation dans la région de la hotte supérieure (2), caractérisé l'on introduit un liquide de rinçage dans la même direction que le flux gazeux contenant des gouttes de liquide au moyen de deux, trois ou davantage, ouvertures d'entrée (9) disposées tangentiellement et symétriquement sur le pourtour de la hotte supérieure (2).
  2. Procédé selon la revendication 1, caractérisé en ce que l'on introduit le liquide de rinçage de façon continue.
  3. Procédé selon la revendication 1 ou 2, caractérisé en ce que l'on utilise un séparateur de gouttes par centrifugation, dans lequel il est prévu au-dessus du tuyau d'évacuation (4) un cône formant sommet (5) et des tôles disposées radialement et perpendiculairement au fond sur le fond de la hotte inférieure.
  4. Procédé selon l'une quelconque des revendications 1 à 3, caractérisé en ce que l'on utilise un séparateur de gouttes par centrifugation, dans lequel il est prévu une jupe d'égouttage ouverte vers le bas disposée autour du tuyau d'échappement de gaz (7) dans la région de la hotte supérieure (2), sur laquelle des gouttes de liquide sont séparées du flux gazeux qui s'échappe par le tuyau d'échappement de gaz (7).
  5. Procédé selon l'une quelconque des revendications 1 à 4, caractérisé en ce que l'on utilise un séparateur de gouttes par centrifugation, dans lequel la hotte supérieure, sur le pourtour de laquelle il est prévu deux, trois ou davantage, ouvertures d'entrée pour une introduction tangentielle de liquide de rinçage, s'élargit en forme de tronc de cône par rapport au pourtour de l'enceinte (1), dans lequel il se forme à la transition entre l'enceinte (1) et la hotte supérieure (2) une arête, par-dessus laquelle coule le liquide de rinçage.
EP10790780.0A 2009-12-15 2010-12-13 Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux Active EP2512683B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP10790780.0A EP2512683B1 (fr) 2009-12-15 2010-12-13 Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09179245 2009-12-15
PCT/EP2010/069521 WO2011082975A1 (fr) 2009-12-15 2010-12-13 Séparateur de gouttes centrifuge pour la séparation de gouttelettes de liquide sur un flux de gaz opérationnel contenant ces gouttelettes
EP10790780.0A EP2512683B1 (fr) 2009-12-15 2010-12-13 Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux

Publications (2)

Publication Number Publication Date
EP2512683A1 EP2512683A1 (fr) 2012-10-24
EP2512683B1 true EP2512683B1 (fr) 2015-03-18

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EP10790780.0A Active EP2512683B1 (fr) 2009-12-15 2010-12-13 Séparateur cyclonique pour la séparation de gouttes de liquide dans un flux gazeux

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US (1) US20120302420A1 (fr)
EP (1) EP2512683B1 (fr)
JP (1) JP5745536B2 (fr)
KR (1) KR101770362B1 (fr)
CN (1) CN102725069B (fr)
ES (1) ES2539360T3 (fr)
WO (1) WO2011082975A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022228938A1 (fr) 2021-04-26 2022-11-03 Basf Se Dispositif et procédé pour séparer des gouttes de liquide d'un flux de gaz au moyen d'un séparateur de gouttes centrifuge

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KR101770356B1 (ko) 2009-12-15 2017-08-22 바스프 에스이 공급 기체 세제곱 미터 당 액체 10 리터 초과의 액체 하중으로 액체 소적을 포함하는 공급 기체 스트림으로부터 그 액체 소적을 분리하기 위한 장치
CN104280263A (zh) * 2014-10-15 2015-01-14 国网重庆市电力公司电力科学研究院 电气设备中六氟化硫固体分解产物取样装置
CN105879501B (zh) * 2016-06-13 2018-08-10 杭州中能汽轮动力有限公司 汽水分离器
CN106731055A (zh) * 2016-12-29 2017-05-31 宁波沪港食品机械制造有限公司 多出口蜗轮机
ES2807752T3 (es) * 2017-06-22 2021-02-24 Metso Minerals Ind Inc Separador hidrociclón
JP7320759B2 (ja) * 2018-04-24 2023-08-04 パナソニックIpマネジメント株式会社 検出装置及び検出方法
CN109603316B (zh) * 2018-12-05 2021-01-29 东华工程科技股份有限公司 具有迷宫式进气管保温装置的高凝固点介质气液分离器
TWI707716B (zh) * 2019-10-17 2020-10-21 湯秉輝 油氣分離裝置以及旋風分離器
CN111545362B (zh) * 2020-06-19 2022-01-28 安徽天顺环保设备股份有限公司 防止旋风除尘器锥体部位出现二次扬尘的方法
FR3117884B1 (fr) 2020-12-21 2024-02-16 Commissariat Energie Atomique Système de tri par taille de particules expulsées par centrifugation et procédé de configuration d'un tel système

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WO2022228938A1 (fr) 2021-04-26 2022-11-03 Basf Se Dispositif et procédé pour séparer des gouttes de liquide d'un flux de gaz au moyen d'un séparateur de gouttes centrifuge

Also Published As

Publication number Publication date
US20120302420A1 (en) 2012-11-29
CN102725069B (zh) 2015-11-25
JP5745536B2 (ja) 2015-07-08
KR20120101713A (ko) 2012-09-14
JP2013513476A (ja) 2013-04-22
EP2512683A1 (fr) 2012-10-24
KR101770362B1 (ko) 2017-08-22
ES2539360T3 (es) 2015-06-30
WO2011082975A1 (fr) 2011-07-14
CN102725069A (zh) 2012-10-10

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