EP1456508A1 - Heissgaspfad-baugruppe einer gasturbine - Google Patents
Heissgaspfad-baugruppe einer gasturbineInfo
- Publication number
- EP1456508A1 EP1456508A1 EP02805240A EP02805240A EP1456508A1 EP 1456508 A1 EP1456508 A1 EP 1456508A1 EP 02805240 A EP02805240 A EP 02805240A EP 02805240 A EP02805240 A EP 02805240A EP 1456508 A1 EP1456508 A1 EP 1456508A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- gas
- cooling
- coolant
- hot gas
- permeable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01D—NON-POSITIVE DISPLACEMENT MACHINES OR ENGINES, e.g. STEAM TURBINES
- F01D11/00—Preventing or minimising internal leakage of working-fluid, e.g. between stages
- F01D11/08—Preventing or minimising internal leakage of working-fluid, e.g. between stages for sealing space between rotor blade tips and stator
- F01D11/12—Preventing or minimising internal leakage of working-fluid, e.g. between stages for sealing space between rotor blade tips and stator using a rubstrip, e.g. erodible. deformable or resiliently-biased part
- F01D11/127—Preventing or minimising internal leakage of working-fluid, e.g. between stages for sealing space between rotor blade tips and stator using a rubstrip, e.g. erodible. deformable or resiliently-biased part with a deformable or crushable structure, e.g. honeycomb
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01D—NON-POSITIVE DISPLACEMENT MACHINES OR ENGINES, e.g. STEAM TURBINES
- F01D11/00—Preventing or minimising internal leakage of working-fluid, e.g. between stages
- F01D11/08—Preventing or minimising internal leakage of working-fluid, e.g. between stages for sealing space between rotor blade tips and stator
- F01D11/10—Preventing or minimising internal leakage of working-fluid, e.g. between stages for sealing space between rotor blade tips and stator using sealing fluid, e.g. steam
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01D—NON-POSITIVE DISPLACEMENT MACHINES OR ENGINES, e.g. STEAM TURBINES
- F01D25/00—Component parts, details, or accessories, not provided for in, or of interest apart from, other groups
- F01D25/08—Cooling; Heating; Heat-insulation
- F01D25/12—Cooling
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05D—INDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
- F05D2260/00—Function
- F05D2260/20—Heat transfer, e.g. cooling
- F05D2260/201—Heat transfer, e.g. cooling by impingement of a fluid
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05D—INDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
- F05D2300/00—Materials; Properties thereof
- F05D2300/60—Properties or characteristics given to material by treatment or manufacturing
- F05D2300/612—Foam
Definitions
- the present invention relates to a
- the efficiency of an axially flowing gas turbine is influenced, among other things, by leakage flows of the compressed gas that occur between rotating and non-rotating components of the turbine.
- the gap that occurs between the tips of the rotor blades and the housing wall surrounding the rotor blades plays an important role here. The aim is therefore to keep the column as small as possible. If there are deviations from the design point, it is easy for the moving components to touch the static components. For this reason, components that are tolerant of abrasion and / or abrasion, such as for example Honeycomb seals, or also porous ceramic or metal structures or felts, are used, which serve as mating surfaces for the sealing tips of the rotor blades, and which are partially cut by these during a running-in phase.
- Honeycomb seals or also porous ceramic or metal structures or felts
- sealing-tolerant sealing elements reduces serious machine breakdowns in the event of smaller rubbing events, since the rubbing is absorbed by the soft structure of the mating surface without damaging the blades.
- JP 61149506 shows a similar embodiment, in which the honeycomb seals are carried by a layer of porous metal, which adjoins a supply chamber for cooling air. In this embodiment, too, the cooling air is brought up to the blade tips through the honeycomb seals.
- a problem with a variety of configurations is that if the gas permeable elements are damaged by rubbing or even an area is torn out completely, the coolant pressure collapses and the entire sealing arrangement overheats and eventually fails. Likewise, if the porosity in a region becomes blocked by deformation due to the abrasion or also by dirt, the coolant flows around this region of the sealing element. Its cooling is no longer guaranteed and local overheating occurs. Overheating can burn out the affected area. The cooling air now flows through the large hole formed in this way, and the areas not previously affected are no longer cooled. As a result, the construction part as a whole, the entire circumference, fails.
- the object of the present invention is now to provide a hot gas path assembly of the type mentioned at the outset which avoids the disadvantages of the prior art.
- a hot gas path assembly should be designed in such a way that the cooling air is used as efficiently as possible, and that in the event of damage to an area, that of the
- the essence of the invention is, on the one hand, to connect two cooling points in series in a cooling air path in such a way that the flowing cooling air is used in succession to perform two cooling tasks.
- the stator of a gas turbine is cooled once in the area of a guide blade row and in the area of a rotor blade row with the same cooling air flow, and at the same time the same cooling air is applied to the blade tips or the blade cover band. In this way, the maximum permissible cooling air heating is achieved and the cooling potential of the cooling air is exploited to the maximum.
- the partition wall is like this explained that the cooling air flow paths of individual segments arranged next to one another in the circumferential direction of the machine are hermetically separated from one another downstream of an impact cooling element.
- An impact cooling element is provided with a large number of comparatively small openings, via which a cooling air flow is directed at high speed onto the cooling side of the component to be cooled.
- Baffle cooling plates are often used. Because of this function, the impingement cooling elements cause a comparatively high pressure loss and are the essential throttle point in the respective coolant path, which also essentially causes the metering of the coolant flowing through.
- the pressure loss coefficient of the impingement cooling element being greater, preferably at least by a factor of 2, than the pressure loss coefficient of the flow cross sections arranged downstream thereof, the entire flow is determined in a first approximation only by the impingement cooling element.
- a plurality of gas-permeable elements are arranged next to one another in the circumferential direction. Due to the multi-piece, lateral, especially in the circumferential direction, Segmented execution of the sealing ring is further guaranteed that a local damage event remains mechanically limited to the segment directly affected. This is all the more fulfilled if the individual sealing ring segments are arranged and fastened in such a way that the greatest possible mutual mechanical decoupling is achieved. At least one individual gas-permeable element is preferably arranged in each segment.
- the assembly according to the invention is particularly useful when the gas-permeable element is a component of a contactless seal of a turbomachine, in particular between a guide vane and the rotor and very particularly between a rotor blade and the stator.
- the gas-impermeable element is arranged upstream of the gas-permeable element in the direction of the hot gas flow. It is advantageous if the gas-impermeable element has a further, redundant, coolant opening, which opens on the hot gas side of the assembly.
- the coolant opening preferably opens upstream of the gas-permeable element, as close as possible to the gas-permeable element
- the coolant opening is designed such that coolant escaping there flows as parallel as possible to the hot gas-side surface of the gas-permeable element, in such a way that a cooling film is formed there.
- the air flowing out of the coolant opening lies as a cooling film over the gas-permeable element, and thus ensures a minimum cooling of this element, although due to the reduced flow, the perspiration cooling effect of the air flowing through the element is reduced or has completely failed. It is advantageous if the flow cross sections of the gas-permeable element and the coolant openings are dimensioned such that the pressure loss of the
- the coolant opening is larger than that of the gas-permeable element, such that, by design, preferably less than 50%, and in particular less than 30%, of the total coolant flow through the coolant opening, and the rest is conducted as a perspiration coolant through the gas-permeable element. If its pressure loss increases due to the effects described above, the coolant shifts into the coolant opening and the proportion of film cooling increases. As stated above, the whole remains
- Coolant mass flow is constant in the first approximation if the pressure loss through the impingement cooling holes predominates.
- the assembly according to the invention is particularly suitable for use in turbomachines, the gas-permeable elements having a circumferential ring for contactless sealing form with an opposite blade ring, the gas-impermeable elements preferably also form a circumferential ring; this ring is preferably arranged upstream of the ring of the gas-permeable elements in the direction of the hot gas flow through the turbomachine.
- the gas-impermeable elements are impact-cooled heat accumulation segments, in a further preferred embodiment, the impact-cooled gas-impermeable elements
- Turbine blades in particular guide blades.
- the assembly according to the invention is arranged in the stator of the turbomachine.
- the dividers or partition walls for dividing the segments run parallel to the chords of blades arranged in the flow channel, and in particular on the gas-impermeable elements.
- the assembly consists of a number of subassemblies arranged side by side, in particular in the circumferential direction, which are constructed such that each subassembly comprises a gas-impermeable element and a gas-permeable element.
- a baffle cooling element is then essentially spaced apart on the hot gas side of the subassembly, opposite the gas-impermeable element, and a cover element is arranged opposite the gas-permeable element.
- an annular segment-shaped space or a substantially annular segment-shaped gap for the coolant is formed.
- such a subassembly comprises at least one
- Partitioning wall for fluid-dividing and / or delimiting the annular gap in the lateral direction, in particular in the circumferential direction.
- the subassembly carries at least one turbine blade; the partition wall then preferably runs parallel to the chord of this blade.
- An annular assembly should preferably be subdivided in the circumferential direction into at least four segments which can be acted upon independently by cooling medium. By forming a larger number of segments, the reliability of the cooling is increased if individual sections of the gas-permeable elements are damaged.
- honeycombs In addition to honeycomb structures, “honeycombs”, among other things, porous ones, for example produced by foaming, come as gas-permeable and in particular abrasion-tolerant elements
- means are also provided for applying coolant to at least some of the segments independently of one another.
- This can be realized by a device which controls the supply of cooling medium to the individual segments via the respective supply channels independently of one another. In this way, an inhomogeneous temperature distribution during operation of the
- Fluid machine over the circumference of the flow channel can be compensated by supplying individual segments with appropriately adapted amounts of cooling medium. This is still suitable for realizing a gap width control.
- Figure 1 shows an example of the implementation of the invention in a gas turbine
- FIG. 2 shows an example of the implementation of the invention with an impact-cooled guide vane root
- FIG. 3 shows a simplified partial cross section of an assembly according to the invention
- FIG. 4 shows a subassembly for constructing an assembly according to the invention in a turbomachine, in particular a gas turbine assembly;
- Figure 5 is a simplified top view of the subassembly.
- Figure 1 shows a section of a flow channel of a turbomachine, for example a turbine of a gas turbine group.
- a hot gas flow 12 flows through the flow channel from right to left.
- a guide vane root 16 In the stator 13 is a guide vane root 16 with a not shown and not relevant to the invention, but familiar to the expert
- the opposite element 2 is normally a comparatively soft, touch-tolerant element. In the present case, this is designed as a perspiration-cooled, gas-permeable honeycomb element. The outflow of a coolant flowing through into the leakage gap in a cross-flow to the leakage flow is quite suitable for further reducing the leakage flow.
- the element 2 is held in a carrier 1.
- the assembly according to the invention which is fastened in the stator, further comprises a gas-impermeable, impact-cooled element 8 arranged upstream of the gas-permeable element 2, here a heat accumulation segment.
- Coolant in particular cooling air or steam, is supplied via a feed 14 in the housing 13.
- the coolant 4 is first at a high speed through openings or nozzles
- FIG. Essential elements are self-explanatory in the light of the explanations for Figure 1.
- the gas-impermeable, impact-cooled element 8 also serves as a blade root 16 of the guide vane 10.
- the impingement cooling element 17 Analogously to FIG. 1, between the gas-permeable element 2, the gas-impermeable element 8, the impingement cooling element 17, a cover element 21, and an upstream wall 22 and a downstream wall 23, a space 9 is formed, which is subdivided in the circumferential direction which cannot be seen here. Coolant passes through it
- the coolant 4 at least predominantly flows through the gas-permeable element 2.
- the gas-impermeable element 8 has a further, redundant coolant opening 18, through which the coolant 4 can flow out of the space 9.
- This coolant opening opens out on the hot gas side of the assembly in such a way that coolant emerging there flows as a cooling film over the hot gas side of the gas-permeable element.
- the redundant coolant opening 18 opens essentially tangentially to the hot gas-side surface of the gas-permeable element 2.
- the redundant coolant opening is preferably dimensioned such that under undisturbed nominal conditions less than half, in particular less than 30%, of the coolant mass flow 4 flow through the redundant coolant openings 18.
- FIG. 3 shows a schematic view of an assembly according to the invention in a cross-sectional view.
- Essentially radially and axially extending webs or partition walls 24 divide the space 9 in the circumferential direction into segments 26.
- a separate redundant coolant opening 18 is also arranged for each segment 26; at least their mouth is elongated, in order to achieve the largest possible distribution of film coolant if necessary.
- the entire coolant path is thus subdivided into segments that are completely independent of one another, at least downstream of the impingement cooling elements 17, by the partition walls 24.
- a single gas-permeable element 2 is still arranged for each segment 26. If a blade tip 7a (not shown here), see in this regard FIG.
- the assembly according to the invention is advantageously constructed from a plurality of sub-assemblies arranged next to one another in the circumferential direction, which considerably simplifies the handling of the invention.
- a subassembly is shown by way of example in FIG. 4 in a perspective view. It is a subassembly of the assembly from FIG. 2, and comprises a peripheral segment with a guide vane 10, together with its impingement-cooled blade root 16.
- the subassembly further comprises a gas-permeable one
- the subassembly comprises a partition wall 24, which en can be arranged on a peripheral side of the subassembly or at another peripheral position.
- the partition wall is designed such that, as explained in connection with FIG. 3, it creates a fluid separation between the two circumferential sides.
- FIG. 5 finally shows a schematic plan view of the subassembly from the outside radially, with “separated” walls 22, 23, 24. It can be seen that in this preferred embodiment the one that is not explicitly identified in FIG. 5 but in the light for the person skilled in the art of the preceding explanations, clearly recognizable, space 9 is divided in the circumferential direction by a dividing wall 14 in the circumferential direction, which runs parallel to the dash-dotted chord of the blade 10.
- the partition wall 24 is arranged directly on a peripheral side of the sub-assembly; but it could easily be arranged at another circumferential position.
- Circumferential segments are arranged side by side.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Turbine Rotor Nozzle Sealing (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH22792001 | 2001-12-13 | ||
CH227901 | 2001-12-13 | ||
PCT/CH2002/000686 WO2003054360A1 (de) | 2001-12-13 | 2002-12-12 | Heissgaspfad-baugruppe einer gasturbine |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1456508A1 true EP1456508A1 (de) | 2004-09-15 |
EP1456508B1 EP1456508B1 (de) | 2005-08-31 |
Family
ID=4568373
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02805240A Expired - Fee Related EP1456508B1 (de) | 2001-12-13 | 2002-12-12 | Heissgaspfad-baugruppe einer gasturbine |
Country Status (6)
Country | Link |
---|---|
US (1) | US7104751B2 (de) |
EP (1) | EP1456508B1 (de) |
JP (1) | JP2005513330A (de) |
AU (1) | AU2002366846A1 (de) |
DE (1) | DE50204128D1 (de) |
WO (1) | WO2003054360A1 (de) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU2002366847A1 (en) * | 2001-12-13 | 2003-07-09 | Alstom Technology Ltd | Sealing module for components of a turbo-engine |
US7871716B2 (en) * | 2003-04-25 | 2011-01-18 | Siemens Energy, Inc. | Damage tolerant gas turbine component |
DE10360164A1 (de) * | 2003-12-20 | 2005-07-21 | Mtu Aero Engines Gmbh | Gasturbinenbauteil |
EP1591626A1 (de) * | 2004-04-30 | 2005-11-02 | Alstom Technology Ltd | Schaufel für Gasturbine |
US7147429B2 (en) * | 2004-09-16 | 2006-12-12 | General Electric Company | Turbine assembly and turbine shroud therefor |
US7770375B2 (en) * | 2006-02-09 | 2010-08-10 | United Technologies Corporation | Particle collector for gas turbine engine |
GB2447892A (en) * | 2007-03-24 | 2008-10-01 | Rolls Royce Plc | Sealing assembly |
US8128343B2 (en) * | 2007-09-21 | 2012-03-06 | Siemens Energy, Inc. | Ring segment coolant seal configuration |
JP4668976B2 (ja) | 2007-12-04 | 2011-04-13 | 株式会社日立製作所 | 蒸気タービンのシール構造 |
EP2083149A1 (de) * | 2008-01-28 | 2009-07-29 | ABB Turbo Systems AG | Abgasturbine |
US8292573B2 (en) * | 2009-04-21 | 2012-10-23 | General Electric Company | Flange cooled turbine nozzle |
US20110110790A1 (en) * | 2009-11-10 | 2011-05-12 | General Electric Company | Heat shield |
FR2955891B1 (fr) * | 2010-02-02 | 2012-11-16 | Snecma | Secteur d'anneau de turbine de turbomachine |
RU2543101C2 (ru) * | 2010-11-29 | 2015-02-27 | Альстом Текнолоджи Лтд | Осевая газовая турбина |
RU2547541C2 (ru) * | 2010-11-29 | 2015-04-10 | Альстом Текнолоджи Лтд | Осевая газовая турбина |
RU2547351C2 (ru) * | 2010-11-29 | 2015-04-10 | Альстом Текнолоджи Лтд | Осевая газовая турбина |
RU2547542C2 (ru) * | 2010-11-29 | 2015-04-10 | Альстом Текнолоджи Лтд | Осевая газовая турбина |
US8444372B2 (en) | 2011-02-07 | 2013-05-21 | General Electric Company | Passive cooling system for a turbomachine |
US9039350B2 (en) * | 2012-01-09 | 2015-05-26 | General Electric Company | Impingement cooling system for use with contoured surfaces |
US20130318996A1 (en) * | 2012-06-01 | 2013-12-05 | General Electric Company | Cooling assembly for a bucket of a turbine system and method of cooling |
US9422824B2 (en) | 2012-10-18 | 2016-08-23 | General Electric Company | Gas turbine thermal control and related method |
US9238971B2 (en) | 2012-10-18 | 2016-01-19 | General Electric Company | Gas turbine casing thermal control device |
WO2015147930A2 (en) * | 2013-12-19 | 2015-10-01 | United Technologies Corporation | Turbine airfoil cooling |
DE102014217832A1 (de) * | 2014-09-05 | 2016-03-10 | Rolls-Royce Deutschland Ltd & Co Kg | Kühlvorrichtung und Flugzeugtriebwerk mit Kühlvorrichtung |
FR3082872B1 (fr) * | 2018-06-25 | 2021-06-04 | Safran Aircraft Engines | Dispositif de refroidissement d'un carter de turbomachine |
CN110469370B (zh) * | 2019-09-10 | 2024-04-09 | 浙江工业大学 | 一种密封间隙可调的柔顺箔蜂窝密封结构 |
DE112022000400T5 (de) * | 2021-03-23 | 2023-10-05 | Mitsubishi Heavy Industries, Ltd. | Statorschaufelanordnung einer gasturbine, stationäres elementsegment und verfahren zur herstellung einer statorschaufelanordnung einer gasturbine |
US11834956B2 (en) * | 2021-12-20 | 2023-12-05 | Rolls-Royce Plc | Gas turbine engine components with metallic and ceramic foam for improved cooling |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3728039A (en) | 1966-11-02 | 1973-04-17 | Gen Electric | Fluid cooled porous stator structure |
US3365172A (en) | 1966-11-02 | 1968-01-23 | Gen Electric | Air cooled shroud seal |
US3825364A (en) * | 1972-06-09 | 1974-07-23 | Gen Electric | Porous abradable turbine shroud |
US3970319A (en) | 1972-11-17 | 1976-07-20 | General Motors Corporation | Seal structure |
FR2280791A1 (fr) * | 1974-07-31 | 1976-02-27 | Snecma | Perfectionnements au reglage du jeu entre les aubes et le stator d'une turbine |
US4013376A (en) | 1975-06-02 | 1977-03-22 | United Technologies Corporation | Coolable blade tip shroud |
US4311431A (en) * | 1978-11-08 | 1982-01-19 | Teledyne Industries, Inc. | Turbine engine with shroud cooling means |
FR2519374B1 (fr) * | 1982-01-07 | 1986-01-24 | Snecma | Dispositif de refroidissement des talons d'aubes mobiles d'une turbine |
GB2125111B (en) | 1982-03-23 | 1985-06-05 | Rolls Royce | Shroud assembly for a gas turbine engine |
JPS61149506A (ja) | 1984-12-21 | 1986-07-08 | Kawasaki Heavy Ind Ltd | タ−ビン翼端のシ−ル装置 |
GB2245316B (en) * | 1990-06-21 | 1993-12-15 | Rolls Royce Plc | Improvements in shroud assemblies for turbine rotors |
DE19756734A1 (de) * | 1997-12-19 | 1999-06-24 | Bmw Rolls Royce Gmbh | Passives Spalthaltungssystem einer Gasturbine |
US5993150A (en) * | 1998-01-16 | 1999-11-30 | General Electric Company | Dual cooled shroud |
DE19821365C2 (de) | 1998-05-13 | 2001-09-13 | Man Turbomasch Ag Ghh Borsig | Kühlung einer Wabendichtung im mit Heißgas beaufschlagten Teil einer Gasturbine |
WO2000060219A1 (de) * | 1999-03-30 | 2000-10-12 | Siemens Aktiengesellschaft | Strömungsmaschine mit einer kühlbaren anordnung von wandelementen und verfahren zur kühlung einer anordnung von wandelementen |
EP1124039A1 (de) * | 2000-02-09 | 2001-08-16 | General Electric Company | Vorrichtung zur Prallkühlung des Deckbandes in einer Gasturbine |
US6340285B1 (en) * | 2000-06-08 | 2002-01-22 | General Electric Company | End rail cooling for combined high and low pressure turbine shroud |
-
2002
- 2002-12-12 AU AU2002366846A patent/AU2002366846A1/en not_active Abandoned
- 2002-12-12 WO PCT/CH2002/000686 patent/WO2003054360A1/de active IP Right Grant
- 2002-12-12 DE DE50204128T patent/DE50204128D1/de not_active Expired - Lifetime
- 2002-12-12 EP EP02805240A patent/EP1456508B1/de not_active Expired - Fee Related
- 2002-12-12 JP JP2003555048A patent/JP2005513330A/ja not_active Withdrawn
-
2004
- 2004-06-14 US US10/865,749 patent/US7104751B2/en not_active Expired - Fee Related
Non-Patent Citations (1)
Title |
---|
See references of WO03054360A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO2003054360A1 (de) | 2003-07-03 |
EP1456508B1 (de) | 2005-08-31 |
JP2005513330A (ja) | 2005-05-12 |
AU2002366846A1 (en) | 2003-07-09 |
US20040258517A1 (en) | 2004-12-23 |
DE50204128D1 (de) | 2005-10-06 |
US7104751B2 (en) | 2006-09-12 |
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