DE69726440T2 - Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne turm-verfahren - Google Patents
Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne turm-verfahren Download PDFInfo
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- DE69726440T2 DE69726440T2 DE69726440T DE69726440T DE69726440T2 DE 69726440 T2 DE69726440 T2 DE 69726440T2 DE 69726440 T DE69726440 T DE 69726440T DE 69726440 T DE69726440 T DE 69726440T DE 69726440 T2 DE69726440 T2 DE 69726440T2
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- Prior art keywords
- surfactant
- mixer
- agglomerates
- detergent
- mixtures
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- 239000003599 detergent Substances 0.000 title claims description 84
- 238000000034 method Methods 0.000 title claims description 70
- 239000000203 mixture Substances 0.000 title claims description 55
- 238000004519 manufacturing process Methods 0.000 title description 14
- 239000004094 surface-active agent Substances 0.000 claims description 44
- 230000008569 process Effects 0.000 claims description 38
- 239000000843 powder Substances 0.000 claims description 29
- 239000007788 liquid Substances 0.000 claims description 26
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 19
- -1 fatty alcohol sulfates Chemical class 0.000 claims description 19
- 239000012530 fluid Substances 0.000 claims description 15
- 229920000642 polymer Polymers 0.000 claims description 14
- 150000004760 silicates Chemical class 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 14
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 12
- 239000003945 anionic surfactant Substances 0.000 claims description 12
- 239000011248 coating agent Substances 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000005243 fluidization Methods 0.000 claims description 10
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 6
- 235000017550 sodium carbonate Nutrition 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical class [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- 239000002736 nonionic surfactant Substances 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 239000003093 cationic surfactant Substances 0.000 claims description 4
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- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 150000008051 alkyl sulfates Chemical class 0.000 claims description 3
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical class OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims description 3
- 235000021317 phosphate Nutrition 0.000 claims description 3
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- 235000013162 Cocos nucifera Nutrition 0.000 claims description 2
- 244000060011 Cocos nucifera Species 0.000 claims description 2
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- 239000002563 ionic surfactant Substances 0.000 claims description 2
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 2
- 239000002888 zwitterionic surfactant Substances 0.000 claims description 2
- 239000000463 material Substances 0.000 description 21
- 239000002245 particle Substances 0.000 description 19
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- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 13
- 229920005646 polycarboxylate Polymers 0.000 description 13
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- 150000003839 salts Chemical class 0.000 description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 9
- 239000011734 sodium Substances 0.000 description 9
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- 150000007942 carboxylates Chemical group 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
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- 239000002994 raw material Substances 0.000 description 6
- 238000001694 spray drying Methods 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 5
- 229910052783 alkali metal Inorganic materials 0.000 description 5
- 150000001340 alkali metals Chemical class 0.000 description 5
- 125000002947 alkylene group Chemical group 0.000 description 5
- 125000000129 anionic group Chemical group 0.000 description 5
- 125000004432 carbon atom Chemical group C* 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 5
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- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- 239000004115 Sodium Silicate Substances 0.000 description 4
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- 150000004665 fatty acids Chemical class 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 4
- 239000011976 maleic acid Substances 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 235000019351 sodium silicates Nutrition 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 3
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 3
- 229930182556 Polyacetal Natural products 0.000 description 3
- 239000002202 Polyethylene glycol Substances 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
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- 229910052700 potassium Inorganic materials 0.000 description 3
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- 159000000001 potassium salts Chemical class 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- 125000001453 quaternary ammonium group Chemical group 0.000 description 3
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- PSZAEHPBBUYICS-UHFFFAOYSA-N 2-methylidenepropanedioic acid Chemical compound OC(=O)C(=C)C(O)=O PSZAEHPBBUYICS-UHFFFAOYSA-N 0.000 description 2
- 229910017090 AlO 2 Inorganic materials 0.000 description 2
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
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- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
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- 125000001183 hydrocarbyl group Chemical group 0.000 description 2
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- YDSWCNNOKPMOTP-UHFFFAOYSA-N mellitic acid Chemical compound OC(=O)C1=C(C(O)=O)C(C(O)=O)=C(C(O)=O)C(C(O)=O)=C1C(O)=O YDSWCNNOKPMOTP-UHFFFAOYSA-N 0.000 description 2
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- 235000011837 pasties Nutrition 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 239000004633 polyglycolic acid Substances 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 239000001205 polyphosphate Chemical class 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 125000002572 propoxy group Chemical group [*]OC([H])([H])C(C([H])([H])[H])([H])[H] 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 235000019830 sodium polyphosphate Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000013042 solid detergent Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 238000005494 tarnishing Methods 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
WOPCT/US96/15881 | 1996-10-04 | ||
PCT/US1996/015881 WO1998014549A1 (fr) | 1996-10-04 | 1996-10-04 | Procede de production d'une composition de detergent de faible densite par un processus sans colonne |
PCT/US1997/009791 WO1998014553A1 (fr) | 1996-10-04 | 1997-06-05 | Procede de production d'une composition detergente sans l'utilisation d'une tour |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69726440D1 DE69726440D1 (de) | 2004-01-08 |
DE69726440T2 true DE69726440T2 (de) | 2004-09-09 |
Family
ID=22255901
Family Applications (5)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69726440T Expired - Fee Related DE69726440T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne turm-verfahren |
DE69721287T Expired - Fee Related DE69721287T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69723986T Expired - Fee Related DE69723986T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69715224T Expired - Fee Related DE69715224T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69726439T Expired - Fee Related DE69726439T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
Family Applications After (4)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69721287T Expired - Fee Related DE69721287T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69723986T Expired - Fee Related DE69723986T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69715224T Expired - Fee Related DE69715224T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
DE69726439T Expired - Fee Related DE69726439T2 (de) | 1996-10-04 | 1997-06-05 | Verfahren zur herstellung von einer waschmittelzusammensetzung nach ohne-turm-verfahren |
Country Status (12)
Country | Link |
---|---|
EP (9) | EP0929645A1 (fr) |
JP (9) | JP3305327B2 (fr) |
CN (8) | CN1239995A (fr) |
AR (6) | AR010729A1 (fr) |
AT (5) | ATE246726T1 (fr) |
AU (9) | AU7388196A (fr) |
BR (7) | BR9612732A (fr) |
CA (9) | CA2267291C (fr) |
DE (5) | DE69726440T2 (fr) |
ES (5) | ES2178778T3 (fr) |
MX (2) | MX219076B (fr) |
WO (9) | WO1998014549A1 (fr) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2150113T3 (es) * | 1995-04-03 | 2000-11-16 | Novartis Ag | Derivados de pirazol y procedimientos para la preparacion de los mismos. |
GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
GB9712580D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
GB9712583D0 (en) | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
EP1002043B1 (fr) | 1997-07-14 | 2007-08-22 | The Procter & Gamble Company | Procede de production d'une composition detergente de faible densite par agglomeration controlee dans un sechoir a lit fluide |
ES2226153T3 (es) | 1997-07-14 | 2005-03-16 | THE PROCTER & GAMBLE COMPANY | Procedimiento para fabricar una composicion detergente de baja densidad controlando la aglomeracion mediante el tamaño de particulas. |
WO1999003965A1 (fr) | 1997-07-15 | 1999-01-28 | The Procter & Gamble Company | Procede de production d'agglomerats detergents fortement actifs par injection d'une pate tensioactive en plusieurs etapes |
US6440342B1 (en) | 1998-07-08 | 2002-08-27 | The Procter & Gamble Company | Process for making a low density detergent composition by controlling nozzle height in a fluid bed dryer |
EP1105455B1 (fr) | 1998-08-20 | 2006-08-16 | The Procter & Gamble Company | Procede de fabrication de detergent haute densite comportant un melangeur/densificateur a vitesse moderee |
US6794354B1 (en) * | 1998-09-18 | 2004-09-21 | The Procter & Gamble Company | Continuous process for making detergent composition |
ES2184523T3 (es) * | 1998-10-26 | 2003-04-01 | Procter & Gamble | Procedimientos para obtener una composicion detergente granular que tiene un aspecto y solubilidad mejoradas. |
GB9825558D0 (en) * | 1998-11-20 | 1999-01-13 | Unilever Plc | Granular detergent components and particulate detergent compositions containing them |
GB9913546D0 (en) | 1999-06-10 | 1999-08-11 | Unilever Plc | Granular detergent component containing zeolite map and laundry detergent compositions containing it |
US6894018B1 (en) | 1999-06-21 | 2005-05-17 | The Procter & Gamble Company | Process for making granular detergent in a fluidized bed granulator having recycling of improperly sized particles |
WO2000078913A1 (fr) * | 1999-06-21 | 2000-12-28 | The Procter & Gamble Company | Procede de fabrication d'une composition granulaire detergente |
GB0009877D0 (en) † | 2000-04-20 | 2000-06-07 | Unilever Plc | Granular detergent component and process for its preparation |
EP2123742A1 (fr) | 2008-05-14 | 2009-11-25 | The Procter and Gamble Company | Compositions de détergent solide pour lessive comprenant du sel de silicate à faible densité |
WO2011061045A1 (fr) | 2009-11-20 | 2011-05-26 | Unilever Nv | Granulé de détergent et son procédé de fabrication |
MX2016013263A (es) | 2014-04-10 | 2017-01-16 | Procter & Gamble | Granulos detergentes compuestos y composiciones para lavanderia que comprenden estos. |
US11214763B2 (en) | 2018-01-26 | 2022-01-04 | Ecolab Usa Inc. | Solidifying liquid amine oxide, betaine, and/or sultaine surfactants with a carrier |
CA3089624A1 (fr) | 2018-01-26 | 2019-08-01 | Ecolab Usa Inc. | Solidification de tensioactifs d'oxyde d'amine, de betaine et/ou de sultaine liquide a l'aide d'un liant et d'un eventuel un vecteur |
US11377628B2 (en) | 2018-01-26 | 2022-07-05 | Ecolab Usa Inc. | Solidifying liquid anionic surfactants |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3625902A (en) * | 1968-10-11 | 1971-12-07 | Stauffer Chemical Co | Method of preparing agglomerated detergent composition |
US4169806A (en) * | 1978-08-09 | 1979-10-02 | The Procter & Gamble Company | Agglomeration process for making granular detergents |
US4992079A (en) * | 1986-11-07 | 1991-02-12 | Fmc Corporation | Process for preparing a nonphosphate laundry detergent |
GB2209172A (en) * | 1987-08-28 | 1989-05-04 | Unilever Plc | Preparation of solid particulate components for detergents |
KR0170424B1 (ko) * | 1990-07-05 | 1999-01-15 | 호르스트 헤를레,요한 글라슬 | 세제 및 청정제용 표면 활성제 과립의 제조방법 |
HUT64391A (en) * | 1990-11-14 | 1993-12-28 | Procter & Gamble | Nonphosphated dishwashing compositions with oxygen belach systems and method for producing them |
DE69332270T3 (de) * | 1992-06-15 | 2006-08-17 | The Procter & Gamble Company, Cincinnati | Verfahren zum herstellen von kompakten waschmittelzusammensetzungen |
CN1136824A (zh) * | 1993-10-15 | 1996-11-27 | 普罗格特-甘布尔公司 | 制造高密度洗涤剂颗粒的连续方法 |
GB9322530D0 (en) * | 1993-11-02 | 1993-12-22 | Unilever Plc | Process for the production of a detergent composition |
PT663439E (pt) * | 1994-01-17 | 2000-12-29 | Procter & Gamble | Processo para a preparacao de granulos de detergente |
US5516448A (en) * | 1994-09-20 | 1996-05-14 | The Procter & Gamble Company | Process for making a high density detergent composition which includes selected recycle streams for improved agglomerate |
US5489392A (en) * | 1994-09-20 | 1996-02-06 | The Procter & Gamble Company | Process for making a high density detergent composition in a single mixer/densifier with selected recycle streams for improved agglomerate properties |
US5554587A (en) * | 1995-08-15 | 1996-09-10 | The Procter & Gamble Company | Process for making high density detergent composition using conditioned air |
-
1996
- 1996-10-04 CA CA002267291A patent/CA2267291C/fr not_active Expired - Fee Related
- 1996-10-04 MX MX9903193A patent/MX219076B/es not_active IP Right Cessation
- 1996-10-04 EP EP96936168A patent/EP0929645A1/fr not_active Withdrawn
- 1996-10-04 JP JP53523397A patent/JP3305327B2/ja not_active Expired - Fee Related
- 1996-10-04 BR BR9612732A patent/BR9612732A/pt not_active IP Right Cessation
- 1996-10-04 AU AU73881/96A patent/AU7388196A/en not_active Abandoned
- 1996-10-04 MX MX9903195A patent/MX219077B/es not_active IP Right Cessation
- 1996-10-04 WO PCT/US1996/015881 patent/WO1998014549A1/fr not_active Application Discontinuation
-
1997
- 1997-06-05 JP JP51649098A patent/JP3299982B2/ja not_active Expired - Fee Related
- 1997-06-05 DE DE69726440T patent/DE69726440T2/de not_active Expired - Fee Related
- 1997-06-05 CN CN97180298.XA patent/CN1239995A/zh active Pending
- 1997-06-05 CA CA002268062A patent/CA2268062C/fr not_active Expired - Fee Related
- 1997-06-05 EP EP97931059A patent/EP0929654A1/fr not_active Withdrawn
- 1997-06-05 WO PCT/US1997/009796 patent/WO1998014558A1/fr active Application Filing
- 1997-06-05 CA CA002268055A patent/CA2268055C/fr not_active Expired - Fee Related
- 1997-06-05 BR BR9711865A patent/BR9711865A/pt not_active IP Right Cessation
- 1997-06-05 CN CNB971802971A patent/CN1156563C/zh not_active Expired - Fee Related
- 1997-06-05 AT AT97929815T patent/ATE246726T1/de not_active IP Right Cessation
- 1997-06-05 BR BR9711861A patent/BR9711861A/pt not_active Application Discontinuation
- 1997-06-05 BR BR9713249-7A patent/BR9713249A/pt not_active Application Discontinuation
- 1997-06-05 AU AU34783/97A patent/AU3478397A/en not_active Abandoned
- 1997-06-05 JP JP51648998A patent/JP3299981B2/ja not_active Expired - Fee Related
- 1997-06-05 BR BR9712490-7A patent/BR9712490A/pt not_active IP Right Cessation
- 1997-06-05 CA CA002268052A patent/CA2268052C/fr not_active Expired - Fee Related
- 1997-06-05 JP JP51649298A patent/JP3345022B2/ja not_active Expired - Fee Related
- 1997-06-05 JP JP51649198A patent/JP3299983B2/ja not_active Expired - Fee Related
- 1997-06-05 WO PCT/US1997/009795 patent/WO1998014557A1/fr active IP Right Grant
- 1997-06-05 DE DE69721287T patent/DE69721287T2/de not_active Expired - Fee Related
- 1997-06-05 EP EP97931058A patent/EP0929653B1/fr not_active Expired - Lifetime
- 1997-06-05 CN CNB971802793A patent/CN1156560C/zh not_active Expired - Fee Related
- 1997-06-05 JP JP51649698A patent/JP3299987B2/ja not_active Expired - Fee Related
- 1997-06-05 CA CA002267424A patent/CA2267424C/fr not_active Expired - Fee Related
- 1997-06-05 EP EP97932153A patent/EP0929655A1/fr not_active Ceased
- 1997-06-05 WO PCT/US1997/009789 patent/WO1998014551A1/fr active IP Right Grant
- 1997-06-05 CA CA002268063A patent/CA2268063C/fr not_active Expired - Fee Related
- 1997-06-05 BR BR9712492-3A patent/BR9712492A/pt not_active IP Right Cessation
- 1997-06-05 AU AU35683/97A patent/AU3568397A/en not_active Abandoned
- 1997-06-05 ES ES97928871T patent/ES2178778T3/es not_active Expired - Lifetime
- 1997-06-05 AU AU34785/97A patent/AU3478597A/en not_active Abandoned
- 1997-06-05 CA CA002268060A patent/CA2268060C/fr not_active Expired - Fee Related
- 1997-06-05 AU AU33031/97A patent/AU3303197A/en not_active Abandoned
- 1997-06-05 JP JP51649498A patent/JP3299985B2/ja not_active Expired - Fee Related
- 1997-06-05 DE DE69723986T patent/DE69723986T2/de not_active Expired - Fee Related
- 1997-06-05 EP EP97931057A patent/EP0929652A1/fr not_active Ceased
- 1997-06-05 ES ES97931056T patent/ES2210544T3/es not_active Expired - Lifetime
- 1997-06-05 AT AT97931056T patent/ATE255160T1/de not_active IP Right Cessation
- 1997-06-05 JP JP51649598A patent/JP3299986B2/ja not_active Expired - Fee Related
- 1997-06-05 JP JP51649398A patent/JP3299984B2/ja not_active Expired - Fee Related
- 1997-06-05 CN CNB971802939A patent/CN1133739C/zh not_active Expired - Fee Related
- 1997-06-05 WO PCT/US1997/009791 patent/WO1998014553A1/fr active IP Right Grant
- 1997-06-05 EP EP97928872A patent/EP0929649B1/fr not_active Expired - Lifetime
- 1997-06-05 DE DE69715224T patent/DE69715224T2/de not_active Expired - Fee Related
- 1997-06-05 ES ES97931058T patent/ES2193386T3/es not_active Expired - Lifetime
- 1997-06-05 BR BR9713246-2A patent/BR9713246A/pt not_active IP Right Cessation
- 1997-06-05 AT AT97928871T patent/ATE223476T1/de not_active IP Right Cessation
- 1997-06-05 WO PCT/US1997/009792 patent/WO1998014554A1/fr not_active Application Discontinuation
- 1997-06-05 AU AU33030/97A patent/AU3303097A/en not_active Abandoned
- 1997-06-05 ES ES97929815T patent/ES2201305T3/es not_active Expired - Lifetime
- 1997-06-05 CA CA002268068A patent/CA2268068C/fr not_active Expired - Fee Related
- 1997-06-05 WO PCT/US1997/009793 patent/WO1998014555A1/fr not_active Application Discontinuation
- 1997-06-05 CA CA002268067A patent/CA2268067C/fr not_active Expired - Fee Related
- 1997-06-05 EP EP97929815A patent/EP0929650B1/fr not_active Expired - Lifetime
- 1997-06-05 AT AT97931058T patent/ATE238409T1/de not_active IP Right Cessation
- 1997-06-05 EP EP97928871A patent/EP0929648B1/fr not_active Expired - Lifetime
- 1997-06-05 AT AT97928872T patent/ATE255159T1/de not_active IP Right Cessation
- 1997-06-05 CN CNB971802807A patent/CN1156561C/zh not_active Expired - Fee Related
- 1997-06-05 WO PCT/US1997/009790 patent/WO1998014552A1/fr active IP Right Grant
- 1997-06-05 AU AU34784/97A patent/AU3478497A/en not_active Abandoned
- 1997-06-05 ES ES97928872T patent/ES2212109T3/es not_active Expired - Lifetime
- 1997-06-05 CN CNB971802963A patent/CN1156562C/zh not_active Expired - Fee Related
- 1997-06-05 WO PCT/US1997/009794 patent/WO1998014556A1/fr active IP Right Grant
- 1997-06-05 CN CNB971802785A patent/CN1133738C/zh not_active Expired - Fee Related
- 1997-06-05 CN CN97180294.7A patent/CN1239992A/zh active Pending
- 1997-06-05 EP EP97931056A patent/EP0929651B1/fr not_active Expired - Lifetime
- 1997-06-05 DE DE69726439T patent/DE69726439T2/de not_active Expired - Fee Related
- 1997-06-05 AU AU34782/97A patent/AU3478297A/en not_active Abandoned
- 1997-06-05 AU AU33785/97A patent/AU3378597A/en not_active Abandoned
- 1997-10-03 AR ARP970104577A patent/AR010729A1/es unknown
- 1997-10-03 AR ARP970104574A patent/AR010507A1/es unknown
- 1997-10-03 AR ARP970104575A patent/AR010508A1/es unknown
- 1997-10-03 AR ARP970104578A patent/AR010510A1/es unknown
- 1997-10-03 AR ARP970104576A patent/AR010509A1/es unknown
- 1997-10-03 AR ARP970104579A patent/AR010511A1/es unknown
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