CN208920719U - A kind of rutin sodium prepares drying device - Google Patents

A kind of rutin sodium prepares drying device Download PDF

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Publication number
CN208920719U
CN208920719U CN201821671201.4U CN201821671201U CN208920719U CN 208920719 U CN208920719 U CN 208920719U CN 201821671201 U CN201821671201 U CN 201821671201U CN 208920719 U CN208920719 U CN 208920719U
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China
Prior art keywords
rutin
dry pond
sodium
drying device
reaction tank
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CN201821671201.4U
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Chinese (zh)
Inventor
廖亚金
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Nanjing Ang Keli Pharmaceutical Technology Innovation Research Institute Co Ltd
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Nanjing Ang Keli Pharmaceutical Technology Innovation Research Institute Co Ltd
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Priority to CN201821671201.4U priority Critical patent/CN208920719U/en
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Abstract

The utility model discloses a kind of rutin sodium to prepare drying device, including reaction tank, filtering ponds and dry pond, is provided with water tank outside dry pond, the lateral wall of water tank is provided with thermal insulation layer;The bottom in dry pond is provided with heated at constant temperature metal tube;The bottom of filtering ponds is provided with ceramic filtration membrane.The present utility model is good using rutin sodium thermal stability, but light sensitive feature, make rutin and rutin sodium on the decrease between link and illumination effect, while using vacuum pump and nested type water tank heated at constant temperature heating in vacuum drying technology, make rutin sodium rapid draing.It is also equipped with Temperature Humidity Sensor in dry pond, facilitates the degree of drying and adjustment drying power of monitoring material.For the utility model other than charging, remaining program is closed state, and pollution can be effectively prevented;Illumination can be effectively reduced to the degradation of rutin and rutin sodium;The utility model is integrated equipment, can effectively reduce intermediate process with manually, be suitable for batch production.

Description

A kind of rutin sodium prepares drying device
Technical field
The utility model relates to a kind of rutin sodium to prepare drying device.
Background technique
Zoopery proves that rutin sodium has the function for the treatment of a variety of diseases such as Alzheimer's disease, but lacks criticize at present The device for quantifying production, seriously hinders the clinical conversion process of the drug.Existing rutin sodium preparation method is laboratory system It is standby, in vitro complete;Preparation amount is few, and time-consuming and laborious.
Utility model content
The technical problems to be solved in the utility model is to overcome in the prior art that rutin sodium is due to degradable characteristic, preparation When time-consuming and laborious defect, a kind of rutin sodium is provided and prepares drying device.
In order to solve the above-mentioned technical problem, the utility model provides the following technical solution:
A kind of rutin sodium prepares drying device, including reaction tank, filtering ponds and dry pond, the lower section setting of the reaction tank There is magnetic stirring apparatus, reaction tank is communicated by head product delivery pipe with filtering ponds, and filtering ponds pass through filtration product withdraw Guan Yugan Dry pond communicates, and dry pond is communicated by exhaust column with vacuum pump;Water tank, the lateral wall setting of water tank are provided with outside the dry pond There is thermal insulation layer;The bottom in dry pond is provided with heated at constant temperature metal tube;The bottom of filtering ponds is provided with ceramic filtration membrane.
Further, the center of reaction tank is provided with magnetic stirring apparatus rotor by magnetic stirring apparatus shaft.
Further, the top of reaction tank is provided with rutin feed opening and sodium hydroxide feed opening.
Further, it is provided with head product discharge tube valve on the head product delivery pipe, filters product withdraw Guan Shangshe It is equipped with filtration product withdraw tube valve.
Further, Temperature Humidity Sensor, the touch-control outside Temperature Humidity Sensor and dry pond are provided in the dry pond The connection of formula alarm.
Preferably, the internal diameter of the reaction tank is 0.5 meter, 0.8 meter high.The model number devices can once produce 3kg rutin sodium, Period is 12h.
The utility model beneficial effect achieved is: the present utility model is good using rutin sodium thermal stability, still Light sensitive feature, make rutin and rutin sodium on the decrease between link and illumination effect, while utilize vacuum pump and nested type The heating in vacuum drying technology of water tank heated at constant temperature makes rutin sodium rapid draing.It is also equipped with Temperature Humidity Sensor in dry pond, side Just the degree of drying and adjustment drying power of material are monitored.For the utility model other than charging, remaining program is closed Pollution can be effectively prevented in state;Illumination can be effectively reduced to the degradation of rutin and rutin sodium;The utility model is integrated Change equipment, intermediate process can be effectively reduced with manually, be suitable for batch production.
Detailed description of the invention
Attached drawing is used to provide a further understanding of the present invention, and constitutes part of specification, practical with this Novel embodiment is used to explain the utility model together, does not constitute limitations of the present invention.In the accompanying drawings:
Fig. 1 is the structural schematic diagram of the utility model.
Specific embodiment
It is illustrated below in conjunction with preferred embodiment of the attached drawing to the utility model, it should be understood that described herein excellent It selects embodiment to be only used for describing and explaining the present invention, is not used to limit the utility model.
Embodiment 1
As shown in Figure 1, a kind of rutin sodium prepares drying device, including reaction tank 1, filtering ponds 9 and dry pond 15, reaction tank Lower section be provided with magnetic stirring apparatus 7, reaction tank 1 is communicated by head product delivery pipe 25 with filtering ponds 9, and filtering ponds 9 pass through filter It crosses product withdraw pipe 26 to communicate with dry pond 15, dry pond 15 is communicated by exhaust column 12 with vacuum pump 14;It is arranged outside dry pond 1 There is water tank 18, the lateral wall of water tank 18 is provided with thermal insulation layer 22;The bottom in dry pond 1 is provided with heated at constant temperature metal tube 24;It crosses The bottom in filter tank 9 is provided with ceramic filtration membrane 11.The center of reaction tank 1 is provided with magnetic stirring apparatus by magnetic stirring apparatus shaft 2 Rotor 6.The top of reaction tank is provided with rutin feed opening 4 and sodium hydroxide feed opening 5.It is provided on head product delivery pipe 25 just Product withdraw tube valve 8 filters and is provided with filtration product withdraw tube valve 13 on product withdraw pipe 26.It is provided in dry pond 1 Temperature Humidity Sensor 18, Temperature Humidity Sensor 18 are connect with the touch alarm 16 outside dry pond.21- note is provided on water tank The mouth of a river and 23- water outlet.3 be reaction pool wall, 19 is dry pond inner wall, 20 is dry pond outer wall.
In use, being filled to water tank 18 by water filling port 21,0.1M sodium hydroxide first is added from sodium hydroxide feed inlet 5 Then 100L opens magnetic stirring apparatus 7 and dry 15 heating metal pipe 24 of pond, then rutin 3.3kg is added from rutin feed inlet, stir Reaction 5min is mixed, magnetic stirring apparatus is then shut off, stands 30min.Then the head product delivery pipe of head product delivery pipe 25 is opened Valve 8 is emitted into head product in filtering ponds 9, opens simultaneously the filtration product withdraw tube valve 13 of filtration product withdraw pipe 26 With vacuum pump 14, entered in dry pond 15 after filtering head product by ceramic filtration membrane 11.After all head products have filtered, Close filtration product withdraw tube valve 13.Vacuum pump 14 continues to remain operational state, makes to keep medium vacuum shape in dry pond 15 State, to accelerate liquid evaporation.The data that staff can return according to Temperature Humidity Sensor 17, pass through touch alarm 16 The power of heating metal pipe 24 is adjusted, convenient for appropriate adjustment production and drying efficiency.
Finally, it should be noted that the above descriptions are merely preferred embodiments of the present invention, it is not limited to this Utility model, although the utility model is described in detail with reference to the foregoing embodiments, for those skilled in the art For, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic It is equivalently replaced.Within the spirit and principle of the utility model, any modification, equivalent replacement, improvement and so on, It should be included within the scope of protection of this utility model.

Claims (6)

1. a kind of rutin sodium prepares drying device, which is characterized in that including reaction tank, filtering ponds and dry pond, the reaction tank Lower section be provided with magnetic stirring apparatus, reaction tank is communicated by head product delivery pipe with filtering ponds, filtering ponds by filtration product Delivery pipe is communicated with dry pond, and dry pond is communicated by exhaust column with vacuum pump;It is provided with water tank outside the dry pond, water tank Lateral wall is provided with thermal insulation layer;The bottom in dry pond is provided with heated at constant temperature metal tube;The bottom of filtering ponds is provided with ceramic filtering Film.
2. rutin sodium as described in claim 1 prepares drying device, which is characterized in that the center of reaction tank passes through magnetic agitation Device shaft is provided with magnetic stirring apparatus rotor.
3. rutin sodium as described in claim 1 prepares drying device, which is characterized in that the top of reaction tank be provided with rutin into Expect hole and sodium hydroxide feed opening.
4. rutin sodium as described in claim 1 prepares drying device, which is characterized in that be provided on the head product delivery pipe Head product discharges tube valve, filters and is provided with filtration product withdraw tube valve on product withdraw pipe.
5. rutin sodium as described in claim 1 prepares drying device, which is characterized in that be provided with temperature and humidity in the dry pond Sensor, Temperature Humidity Sensor are connect with the touch alarm outside dry pond.
6. rutin sodium as described in claim 1 prepares drying device, which is characterized in that the internal diameter of the reaction tank is 0.5 meter, It is 0.8 meter high.
CN201821671201.4U 2018-10-16 2018-10-16 A kind of rutin sodium prepares drying device Active CN208920719U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821671201.4U CN208920719U (en) 2018-10-16 2018-10-16 A kind of rutin sodium prepares drying device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821671201.4U CN208920719U (en) 2018-10-16 2018-10-16 A kind of rutin sodium prepares drying device

Publications (1)

Publication Number Publication Date
CN208920719U true CN208920719U (en) 2019-05-31

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821671201.4U Active CN208920719U (en) 2018-10-16 2018-10-16 A kind of rutin sodium prepares drying device

Country Status (1)

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CN (1) CN208920719U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111122564A (en) * 2019-12-31 2020-05-08 深圳市华域环保科技有限公司 A dregs detection device for preparing sintering class regeneration product

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111122564A (en) * 2019-12-31 2020-05-08 深圳市华域环保科技有限公司 A dregs detection device for preparing sintering class regeneration product
CN111122564B (en) * 2019-12-31 2020-10-02 深圳市华域环保科技有限公司 A dregs detection device for preparing sintering class regeneration product

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