CN1756660A - 可成型热塑性层压材料、成型的层压材料、制品、及其制造方法 - Google Patents
可成型热塑性层压材料、成型的层压材料、制品、及其制造方法 Download PDFInfo
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- CN1756660A CN1756660A CNA2004800060789A CN200480006078A CN1756660A CN 1756660 A CN1756660 A CN 1756660A CN A2004800060789 A CNA2004800060789 A CN A2004800060789A CN 200480006078 A CN200480006078 A CN 200480006078A CN 1756660 A CN1756660 A CN 1756660A
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- Prior art keywords
- polymer
- acrylonitrile
- layer
- tack coat
- copolymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920001169 thermoplastic Polymers 0.000 title claims abstract description 65
- 239000004416 thermosoftening plastic Substances 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 229920000642 polymer Polymers 0.000 claims abstract description 97
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims abstract description 49
- 229920000578 graft copolymer Polymers 0.000 claims abstract description 43
- 239000000758 substrate Substances 0.000 claims abstract description 42
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 claims abstract description 38
- 229920000728 polyester Polymers 0.000 claims abstract description 35
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims abstract description 33
- 229920002877 acrylic styrene acrylonitrile Polymers 0.000 claims abstract description 30
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 claims abstract description 26
- SCUZVMOVTVSBLE-UHFFFAOYSA-N prop-2-enenitrile;styrene Chemical compound C=CC#N.C=CC1=CC=CC=C1 SCUZVMOVTVSBLE-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920001893 acrylonitrile styrene Polymers 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims description 144
- -1 alkyl thioesters Chemical class 0.000 claims description 79
- 238000000034 method Methods 0.000 claims description 50
- 229920001577 copolymer Polymers 0.000 claims description 46
- DRZPXZMMDBMTHL-UHFFFAOYSA-N (3-hydroxyphenyl) prop-2-enoate Chemical compound OC1=CC=CC(OC(=O)C=C)=C1 DRZPXZMMDBMTHL-UHFFFAOYSA-N 0.000 claims description 42
- 150000002148 esters Chemical class 0.000 claims description 36
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims description 33
- 238000000465 moulding Methods 0.000 claims description 32
- IISBACLAFKSPIT-UHFFFAOYSA-N Bisphenol A Natural products C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 30
- 239000000463 material Substances 0.000 claims description 21
- 239000002648 laminated material Substances 0.000 claims description 17
- 239000003381 stabilizer Substances 0.000 claims description 17
- 229940106691 bisphenol a Drugs 0.000 claims description 12
- 229920001909 styrene-acrylic polymer Polymers 0.000 claims description 9
- 229920003023 plastic Polymers 0.000 claims description 7
- 239000004033 plastic Substances 0.000 claims description 7
- 229920001187 thermosetting polymer Polymers 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000003856 thermoforming Methods 0.000 claims description 4
- 238000007906 compression Methods 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims description 3
- 230000002708 enhancing effect Effects 0.000 claims description 2
- 229920002285 poly(styrene-co-acrylonitrile) Polymers 0.000 claims 2
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 abstract description 22
- YAAQEISEHDUIFO-UHFFFAOYSA-N C=CC#N.OC(=O)C=CC=CC1=CC=CC=C1 Chemical compound C=CC#N.OC(=O)C=CC=CC1=CC=CC=C1 YAAQEISEHDUIFO-UHFFFAOYSA-N 0.000 abstract 1
- 239000010410 layer Substances 0.000 description 150
- 239000000178 monomer Substances 0.000 description 61
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 39
- 229920001971 elastomer Polymers 0.000 description 36
- 239000005060 rubber Substances 0.000 description 36
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 28
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 28
- 125000003118 aryl group Chemical group 0.000 description 25
- 150000001875 compounds Chemical class 0.000 description 24
- 239000000047 product Substances 0.000 description 24
- 150000008065 acid anhydrides Chemical class 0.000 description 21
- 150000001991 dicarboxylic acids Chemical class 0.000 description 21
- 238000001125 extrusion Methods 0.000 description 21
- 239000011145 styrene acrylonitrile resin Substances 0.000 description 21
- 238000006243 chemical reaction Methods 0.000 description 20
- 239000003795 chemical substances by application Substances 0.000 description 20
- 229920000638 styrene acrylonitrile Polymers 0.000 description 20
- 125000000217 alkyl group Chemical group 0.000 description 19
- 239000012071 phase Substances 0.000 description 19
- 229930185605 Bisphenol Natural products 0.000 description 17
- 238000002360 preparation method Methods 0.000 description 15
- 230000008569 process Effects 0.000 description 15
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 14
- 239000004417 polycarbonate Substances 0.000 description 13
- 239000000376 reactant Substances 0.000 description 13
- 239000011159 matrix material Substances 0.000 description 12
- 229960003742 phenol Drugs 0.000 description 12
- 229960001755 resorcinol Drugs 0.000 description 12
- 229920001634 Copolyester Polymers 0.000 description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 11
- 229910052736 halogen Inorganic materials 0.000 description 11
- 150000002367 halogens Chemical class 0.000 description 11
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 10
- 125000004432 carbon atom Chemical group C* 0.000 description 10
- 150000005690 diesters Chemical class 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 10
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000003153 chemical reaction reagent Substances 0.000 description 9
- 238000000576 coating method Methods 0.000 description 9
- 125000001142 dicarboxylic acid group Chemical group 0.000 description 9
- 229920000515 polycarbonate Polymers 0.000 description 9
- 238000006116 polymerization reaction Methods 0.000 description 9
- 150000003512 tertiary amines Chemical class 0.000 description 9
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 8
- 239000002585 base Substances 0.000 description 8
- 229910052799 carbon Inorganic materials 0.000 description 8
- 239000011248 coating agent Substances 0.000 description 8
- 150000001993 dienes Chemical class 0.000 description 8
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 7
- 125000005250 alkyl acrylate group Chemical group 0.000 description 7
- 239000006085 branching agent Substances 0.000 description 7
- 239000003054 catalyst Substances 0.000 description 7
- 238000007334 copolymerization reaction Methods 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 7
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 7
- 238000001746 injection moulding Methods 0.000 description 7
- 150000005677 organic carbonates Chemical class 0.000 description 7
- 239000002245 particle Substances 0.000 description 7
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 7
- 229920001707 polybutylene terephthalate Polymers 0.000 description 7
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 6
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 6
- 229920004142 LEXAN™ Polymers 0.000 description 6
- 239000004418 Lexan Substances 0.000 description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- 239000000654 additive Substances 0.000 description 6
- 230000000996 additive effect Effects 0.000 description 6
- 125000001118 alkylidene group Chemical group 0.000 description 6
- 235000010290 biphenyl Nutrition 0.000 description 6
- 239000004305 biphenyl Substances 0.000 description 6
- 230000031709 bromination Effects 0.000 description 6
- 238000005893 bromination reaction Methods 0.000 description 6
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 6
- 229910052804 chromium Inorganic materials 0.000 description 6
- 239000011651 chromium Substances 0.000 description 6
- 239000000155 melt Substances 0.000 description 6
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 description 6
- 239000003960 organic solvent Substances 0.000 description 6
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 6
- 229920001485 poly(butyl acrylate) polymer Polymers 0.000 description 6
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 6
- 239000004926 polymethyl methacrylate Substances 0.000 description 6
- 239000004814 polyurethane Substances 0.000 description 6
- 239000011347 resin Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- 229920002554 vinyl polymer Polymers 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 125000004400 (C1-C12) alkyl group Chemical group 0.000 description 5
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 5
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 5
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 5
- 239000005977 Ethylene Substances 0.000 description 5
- 238000005618 Fries rearrangement reaction Methods 0.000 description 5
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 description 5
- 239000004433 Thermoplastic polyurethane Substances 0.000 description 5
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 5
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 5
- 229910052794 bromium Inorganic materials 0.000 description 5
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 5
- 239000000839 emulsion Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000000835 fiber Substances 0.000 description 5
- 229920001519 homopolymer Polymers 0.000 description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 239000001294 propane Substances 0.000 description 5
- JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 5
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical class OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000000725 suspension Substances 0.000 description 5
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 5
- GZHWPYMWTAUJPC-UHFFFAOYSA-N terephthalic acid;dihydrochloride Chemical compound Cl.Cl.OC(=O)C1=CC=C(C(O)=O)C=C1 GZHWPYMWTAUJPC-UHFFFAOYSA-N 0.000 description 5
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 5
- ONIKNECPXCLUHT-UHFFFAOYSA-N 2-chlorobenzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1Cl ONIKNECPXCLUHT-UHFFFAOYSA-N 0.000 description 4
- TVONJMOVBKMLOM-UHFFFAOYSA-N 2-methylidenebutanenitrile Chemical compound CCC(=C)C#N TVONJMOVBKMLOM-UHFFFAOYSA-N 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 4
- 239000005062 Polybutadiene Substances 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 125000002723 alicyclic group Chemical group 0.000 description 4
- SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 4
- 239000003638 chemical reducing agent Substances 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 125000000753 cycloalkyl group Chemical group 0.000 description 4
- 239000003112 inhibitor Substances 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 125000000962 organic group Chemical group 0.000 description 4
- 229920001603 poly (alkyl acrylates) Polymers 0.000 description 4
- 229920000058 polyacrylate Polymers 0.000 description 4
- 229920002857 polybutadiene Polymers 0.000 description 4
- 229920002635 polyurethane Polymers 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 229920001897 terpolymer Polymers 0.000 description 4
- NHGXDBSUJJNIRV-UHFFFAOYSA-M tetrabutylammonium chloride Chemical compound [Cl-].CCCC[N+](CCCC)(CCCC)CCCC NHGXDBSUJJNIRV-UHFFFAOYSA-M 0.000 description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 4
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 3
- SSZOCHFYWWVSAI-UHFFFAOYSA-N 1-bromo-2-ethenylbenzene Chemical compound BrC1=CC=CC=C1C=C SSZOCHFYWWVSAI-UHFFFAOYSA-N 0.000 description 3
- HXDOZKJGKXYMEW-UHFFFAOYSA-N 4-ethylphenol Chemical compound CCC1=CC=C(O)C=C1 HXDOZKJGKXYMEW-UHFFFAOYSA-N 0.000 description 3
- 125000004203 4-hydroxyphenyl group Chemical group [H]OC1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- NTKVWOTYTNWGRK-UHFFFAOYSA-N P.Br.Br.Br Chemical compound P.Br.Br.Br NTKVWOTYTNWGRK-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical group [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 125000003545 alkoxy group Chemical group 0.000 description 3
- 229910002056 binary alloy Inorganic materials 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical group OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 3
- AOGYCOYQMAVAFD-UHFFFAOYSA-N chlorocarbonic acid Chemical class OC(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-N 0.000 description 3
- 238000004132 cross linking Methods 0.000 description 3
- 230000002950 deficient Effects 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 239000003365 glass fiber Substances 0.000 description 3
- 125000005843 halogen group Chemical group 0.000 description 3
- 125000005027 hydroxyaryl group Chemical group 0.000 description 3
- 238000010406 interfacial reaction Methods 0.000 description 3
- XKBGEWXEAPTVCK-UHFFFAOYSA-M methyltrioctylammonium chloride Chemical compound [Cl-].CCCCCCCC[N+](C)(CCCCCCCC)CCCCCCCC XKBGEWXEAPTVCK-UHFFFAOYSA-M 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- AHWALFGBDFAJAI-UHFFFAOYSA-N phenyl carbonochloridate Chemical compound ClC(=O)OC1=CC=CC=C1 AHWALFGBDFAJAI-UHFFFAOYSA-N 0.000 description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 3
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 3
- 230000009183 running Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- HJIAMFHSAAEUKR-UHFFFAOYSA-N (2-hydroxyphenyl)-phenylmethanone Chemical compound OC1=CC=CC=C1C(=O)C1=CC=CC=C1 HJIAMFHSAAEUKR-UHFFFAOYSA-N 0.000 description 2
- FYGHSUNMUKGBRK-UHFFFAOYSA-N 1,2,3-trimethylbenzene Chemical compound CC1=CC=CC(C)=C1C FYGHSUNMUKGBRK-UHFFFAOYSA-N 0.000 description 2
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
- SHKKTLSDGJRCTR-UHFFFAOYSA-N 1,2-dibromoethylbenzene Chemical compound BrCC(Br)C1=CC=CC=C1 SHKKTLSDGJRCTR-UHFFFAOYSA-N 0.000 description 2
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 2
- XHAFIUUYXQFJEW-UHFFFAOYSA-N 1-chloroethenylbenzene Chemical compound ClC(=C)C1=CC=CC=C1 XHAFIUUYXQFJEW-UHFFFAOYSA-N 0.000 description 2
- PAMIQIKDUOTOBW-UHFFFAOYSA-N 1-methylpiperidine Chemical compound CN1CCCCC1 PAMIQIKDUOTOBW-UHFFFAOYSA-N 0.000 description 2
- RKMGAJGJIURJSJ-UHFFFAOYSA-N 2,2,6,6-tetramethylpiperidine Chemical compound CC1(C)CCCC(C)(C)N1 RKMGAJGJIURJSJ-UHFFFAOYSA-N 0.000 description 2
- CISIJYCKDJSTMX-UHFFFAOYSA-N 2,2-dichloroethenylbenzene Chemical compound ClC(Cl)=CC1=CC=CC=C1 CISIJYCKDJSTMX-UHFFFAOYSA-N 0.000 description 2
- DVIPICFRLKAAKK-UHFFFAOYSA-N 2,2-diphenyldecanedioic acid Chemical compound C=1C=CC=CC=1C(C(O)=O)(CCCCCCCC(=O)O)C1=CC=CC=C1 DVIPICFRLKAAKK-UHFFFAOYSA-N 0.000 description 2
- SDJHPPZKZZWAKF-UHFFFAOYSA-N 2,3-dimethylbuta-1,3-diene Chemical compound CC(=C)C(C)=C SDJHPPZKZZWAKF-UHFFFAOYSA-N 0.000 description 2
- BJELTSYBAHKXRW-UHFFFAOYSA-N 2,4,6-triallyloxy-1,3,5-triazine Chemical compound C=CCOC1=NC(OCC=C)=NC(OCC=C)=N1 BJELTSYBAHKXRW-UHFFFAOYSA-N 0.000 description 2
- CJWNFAKWHDOUKL-UHFFFAOYSA-N 2-(2-phenylpropan-2-yl)phenol Chemical compound C=1C=CC=C(O)C=1C(C)(C)C1=CC=CC=C1 CJWNFAKWHDOUKL-UHFFFAOYSA-N 0.000 description 2
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- GOXQRTZXKQZDDN-UHFFFAOYSA-N 2-Ethylhexyl acrylate Chemical compound CCCCC(CC)COC(=O)C=C GOXQRTZXKQZDDN-UHFFFAOYSA-N 0.000 description 2
- CMPIGRYBIGUGTH-UHFFFAOYSA-N 2-bromoprop-2-enenitrile Chemical compound BrC(=C)C#N CMPIGRYBIGUGTH-UHFFFAOYSA-N 0.000 description 2
- ZGHFDIIVVIFNPS-UHFFFAOYSA-N 3-Methyl-3-buten-2-one Chemical compound CC(=C)C(C)=O ZGHFDIIVVIFNPS-UHFFFAOYSA-N 0.000 description 2
- JLBJTVDPSNHSKJ-UHFFFAOYSA-N 4-Methylstyrene Chemical compound CC1=CC=C(C=C)C=C1 JLBJTVDPSNHSKJ-UHFFFAOYSA-N 0.000 description 2
- KLSLBUSXWBJMEC-UHFFFAOYSA-N 4-Propylphenol Chemical compound CCCC1=CC=C(O)C=C1 KLSLBUSXWBJMEC-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 description 2
- RVNKHYPZYFADMR-UHFFFAOYSA-N C=C.C(C)C=1C=CC=C(C1)CC Chemical compound C=C.C(C)C=1C=CC=C(C1)CC RVNKHYPZYFADMR-UHFFFAOYSA-N 0.000 description 2
- 229920000049 Carbon (fiber) Polymers 0.000 description 2
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Abstract
Description
样品 | PC(%) | ASA/SAN(%) | (0:无粘合性/2:粘合性合格) |
1 | 72 | 28 | 1 |
2 | 60 | 40 | 2 |
3 | 60 | 40 | 2 |
4 | 27 | 78 | 0-1 |
样品 | PC(%) | ABS/SAN(%) | 剥离实验平均值/标准偏差 |
1 | 51 | 19/30 | 21.1/5 |
2 | 73 | 14/13 | 14.5/4.3 |
3 | 82 | 8/10 | 4.5/0.4 |
4 | 65 | 19/16 | 13.4/1.2 |
Claims (12)
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US60/440,097 | 2003-01-14 | ||
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US10/748,941 | 2003-12-30 | ||
PCT/US2004/000925 WO2004065122A1 (en) | 2003-01-14 | 2004-01-14 | A formable thermoplastic laminate, a formed laminate, an article, and a method of making an article |
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EP (1) | EP1587681B1 (zh) |
JP (1) | JP2007524523A (zh) |
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CN (1) | CN1756660B (zh) |
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CN102056742A (zh) * | 2008-06-03 | 2011-05-11 | 沙伯基础创新塑料知识产权有限公司 | 具有a类表面抛光的轻质高刚度复合体 |
CN101474906B (zh) * | 2007-12-31 | 2013-06-12 | 第一毛织株式会社 | 包括硬质涂层的塑料薄板 |
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US7270882B2 (en) * | 2003-02-21 | 2007-09-18 | General Electric Company | Weatherable multilayer articles and method for their preparation |
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US7060217B2 (en) | 2003-06-12 | 2006-06-13 | General Electric Company | Composite articles comprising resorcinol arylate polyester and method for making thereof |
US20050266232A1 (en) * | 2004-05-27 | 2005-12-01 | General Electric Company | Weatherable multilayer articles and process for making |
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KR100645065B1 (ko) * | 2005-06-23 | 2006-11-10 | 삼성전자주식회사 | 핀 전계 효과 트랜지스터와 이를 구비하는 비휘발성 메모리장치 및 그 형성 방법 |
KR100771355B1 (ko) * | 2005-08-29 | 2007-10-29 | 주식회사 엘지화학 | 열가소성 수지 조성물 |
US20070092707A1 (en) * | 2005-10-20 | 2007-04-26 | Basf Corporation. | Multi-layered composite article |
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US20090011213A1 (en) * | 2007-07-03 | 2009-01-08 | General Electric Company | Recyclable Multilayer Thermoplastic Films and Methods of Making |
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-
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- 2003-12-30 US US10/748,941 patent/US7514147B2/en not_active Expired - Fee Related
-
2004
- 2004-01-14 KR KR1020057012985A patent/KR101111045B1/ko active IP Right Grant
- 2004-01-14 EP EP04702204.1A patent/EP1587681B1/en not_active Expired - Lifetime
- 2004-01-14 JP JP2006500951A patent/JP2007524523A/ja not_active Withdrawn
- 2004-01-14 CN CN2004800060789A patent/CN1756660B/zh not_active Expired - Fee Related
- 2004-01-14 WO PCT/US2004/000925 patent/WO2004065122A1/en active Application Filing
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101474906B (zh) * | 2007-12-31 | 2013-06-12 | 第一毛织株式会社 | 包括硬质涂层的塑料薄板 |
CN102056742A (zh) * | 2008-06-03 | 2011-05-11 | 沙伯基础创新塑料知识产权有限公司 | 具有a类表面抛光的轻质高刚度复合体 |
CN105500840A (zh) * | 2008-06-03 | 2016-04-20 | 沙特基础全球技术有限公司 | 刚性轻质的复合片材及其制造方法 |
CN107978682A (zh) * | 2016-10-25 | 2018-05-01 | 上海和辉光电有限公司 | 一种柔性amoled衬底及其制备方法 |
CN107978682B (zh) * | 2016-10-25 | 2019-12-27 | 上海和辉光电有限公司 | 一种柔性amoled衬底及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
KR101111045B1 (ko) | 2012-02-17 |
EP1587681B1 (en) | 2016-06-08 |
EP1587681A1 (en) | 2005-10-26 |
KR20050094434A (ko) | 2005-09-27 |
WO2004065122A1 (en) | 2004-08-05 |
US7514147B2 (en) | 2009-04-07 |
CN1756660B (zh) | 2010-10-27 |
JP2007524523A (ja) | 2007-08-30 |
US20040175593A1 (en) | 2004-09-09 |
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