CN111329930A - Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof - Google Patents
Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
- A61K31/465—Nicotine; Derivatives thereof
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- A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
- A61K31/34—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having five-membered rings with one oxygen as the only ring hetero atom, e.g. isosorbide
- A61K31/345—Nitrofurans
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
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- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/22—Heterocyclic compounds, e.g. ascorbic acid, tocopherol or pyrrolidones
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61K9/00—Medicinal preparations characterised by special physical form
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- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/006—Oral mucosa, e.g. mucoadhesive forms, sublingual droplets; Buccal patches or films; Buccal sprays
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Abstract
The invention discloses a plant tobacco flavor oral cavity atomized liquid and a preparation method thereof, wherein the preparation method comprises the following steps: s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store; s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis; s3: extracting the mint in the S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into menthol extract with the mass concentration of 4-10% by using distilled water and the menthol extract. The invention has low manufacturing cost and convenient use, is added with nicotine salt, honeysuckle, clove, 0.02 percent nitrofural solution, propolis, edible ethanol, borneol, tea, distilled water, mint and preservative, smells the taste of cigarettes, enables smokers to relieve the craving for cigarettes, also can refresh the mind and refresh the brain, and can better meet the use requirements of people.
Description
Technical Field
The invention relates to the technical field of oral cavity spraying, in particular to a plant tobacco flavor oral cavity atomized liquid and a preparation method thereof.
Background
Halitosis, which is an odor emitted from the oral cavity or other air-filled cavities such as the nose, sinuses, and pharynx, seriously affects social interaction and mental health of people, has been reported by WHO as a disease. The survey shows that the prevalence rate of the Chinese halitosis is 27.5%. And 50% in western countries. About 10% to 65% of people worldwide have had halitosis.
The oral cavity atomized liquid in the market can effectively remove breath, but the smoking crowd is more, the oral cavity atomized liquid in the market has unpleasant smell and the manufacturing cost is higher.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a plant tobacco flavor oral cavity atomized liquid and a preparation method thereof.
The plant tobacco flavor oral cavity atomized liquid provided by the invention comprises the following components in percentage by weight: 2 to 4 percent of nicotine salt, 2 to 4 percent of honeysuckle, 4 to 6 percent of clove, 1 to 2 percent of furacilin solution with the concentration of 0.02 percent, 2 to 5 percent of propolis, 6 to 8 percent of edible ethanol, 1 to 2 percent of borneol, 2 to 3 percent of tea, 58 to 75 percent of distilled water, 4 to 6 percent of mint and 1 to 2 percent of preservative.
The plant tobacco flavor oral cavity atomized liquid comprises the following components in percentage by weight: 2% of nicotine salt, 2% of honeysuckle, 4% of clove, 1% of 0.02% nitrofurazone solution, 2% of propolis, 6% of edible ethanol, 1% of borneol, 2% of tea, 75% of distilled water, 4% of mint and 1% of preservative.
The preparation method of the plant tobacco flavor oral cavity atomized liquid comprises the following steps:
s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store;
s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis;
s3: extracting the mint in the S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into menthol extract with the mass concentration of 4-10% by using distilled water and the menthol extract;
s4: cleaning and drying the honeysuckle, the clove, the tea and the mint in the S1, and then putting the honeysuckle, the clove, the tea and the mint into an extractor for extraction to obtain extract liquor of the honeysuckle, the clove, the tea and the mint;
s5: adding the honeysuckle, clove, tea and mint extract in the step S4 into a glass container, adding the propolis alcohol extract in the step S2 and the menthol extract in the step S3 while stirring, and stirring for five minutes to obtain a mixed solution A;
s6: adding nicotine salt, 0.02% nitrofurazone solution, borneol, preservative and the rest of distilled water into the mixed solution in the S5, and stirring in the adding process to obtain a mixed solution B;
s7: and (4) filling the mixed solution B obtained in the step (S6) and filling the mixed solution B into a spray can.
Preferably, in the step S3, after adding the distilled water, stirring and shaking are performed, wherein the stirring time is 5 min.
Preferably, in S4, separate parameter settings are performed as required during extraction, and the extracts of honeysuckle, clove, tea and mint are mixed and placed.
Preferably, in S5, the stirring is performed by using a glass rod, and the stirring is performed for 2 minutes clockwise and 3 minutes counterclockwise.
Preferably, in S6, the stirring time is 30min, and a glass stirring rod is used for stirring during the stirring process.
The invention has the beneficial effects that: the invention has low manufacturing cost and convenient use, is added with nicotine salt, honeysuckle, clove, 0.02 percent nitrofural solution, propolis, edible ethanol, borneol, tea, distilled water, mint and preservative, smells the taste of cigarettes, enables smokers to relieve the craving for cigarettes, also can refresh the mind and refresh the brain, and can better meet the use requirements of people.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The embodiment provides a plant tobacco flavor oral cavity atomized liquid, which comprises 4% of nicotine salt, 4% of honeysuckle, 6% of clove, 2% of 0.02% nitrofurazone solution, 5% of propolis, 8% of edible ethanol, 2% of borneol, 3% of tea, 58% of distilled water, 6% of mint and 2% of preservative.
The preparation method of the plant tobacco flavor oral cavity atomized liquid comprises the following steps:
s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store;
s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis;
s3: extracting the mint in the step S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into a menthol extract with the mass concentration of 10% by using distilled water and the menthol extract;
s4: cleaning and drying the honeysuckle, the clove, the tea and the mint in the S1, and then putting the honeysuckle, the clove, the tea and the mint into an extractor for extraction to obtain extract liquor of the honeysuckle, the clove, the tea and the mint;
s5: adding the honeysuckle, clove, tea and mint extract in the step S4 into a glass container, adding the propolis alcohol extract in the step S2 and the menthol extract in the step S3 while stirring, and stirring for five minutes to obtain a mixed solution A;
s6: adding nicotine salt, 0.02% nitrofurazone solution, borneol, preservative and the rest of distilled water into the mixed solution in the S5, and stirring in the adding process to obtain a mixed solution B;
s7: and (4) filling the mixed solution B obtained in the step (S6) and filling the mixed solution B into a spray can.
Preferably, in S3, need stir the vibration after adding distilled water, the churning time is 5min, in S4, carry out solitary parameter setting as required during the extraction, the extract of honeysuckle, clove, tealeaves and peppermint mixes and places, in S5, adopt the stirring of glass stick during the stirring, clockwise stirring 2 minutes, anticlockwise stirring 3 minutes, in S6, the churning time is 30min, adopts the stirring of glass stick in the stirring process.
Example two
The embodiment provides a plant tobacco flavor oral cavity atomized liquid, which comprises 2% of nicotine salt, 2% of honeysuckle, 4% of clove, 1% of nitrofurazone solution of 0.02%, 2% of propolis, 6% of edible ethanol, 1% of borneol, 2% of tea, 75% of distilled water, 4% of mint and 1% of preservative.
The preparation method of the plant tobacco flavor oral cavity atomized liquid comprises the following steps:
s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store;
s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis;
s3: extracting the mint in the step S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into a menthol extract with the mass concentration of 10% by using distilled water and the menthol extract;
s4: cleaning and drying the honeysuckle, the clove, the tea and the mint in the S1, and then putting the honeysuckle, the clove, the tea and the mint into an extractor for extraction to obtain extract liquor of the honeysuckle, the clove, the tea and the mint;
s5: adding the honeysuckle, clove, tea and mint extract in the step S4 into a glass container, adding the propolis alcohol extract in the step S2 and the menthol extract in the step S3 while stirring, and stirring for five minutes to obtain a mixed solution A;
s6: adding nicotine salt, 0.02% nitrofurazone solution, borneol, preservative and the rest of distilled water into the mixed solution in the S5, and stirring in the adding process to obtain a mixed solution B;
s7: and (4) filling the mixed solution B obtained in the step (S6) and filling the mixed solution B into a spray can.
Preferably, in S3, need stir the vibration after adding distilled water, the churning time is 5min, in S4, carry out solitary parameter setting as required during the extraction, the extract of honeysuckle, clove, tealeaves and peppermint mixes and places, in S5, adopt the stirring of glass stick during the stirring, clockwise stirring 2 minutes, anticlockwise stirring 3 minutes, in S6, the churning time is 30min, adopts the stirring of glass stick in the stirring process.
EXAMPLE III
The embodiment provides a plant tobacco flavor oral cavity atomized liquid, which comprises 3% of nicotine salt, 3% of honeysuckle, 5% of clove, 1% of furacilin solution with the concentration of 0.02%, 4% of propolis, 7% of edible ethanol, 1% of borneol, 2% of tea, 68% of distilled water, 5% of mint and 1% of preservative.
The preparation method of the plant tobacco flavor oral cavity atomized liquid comprises the following steps:
s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store;
s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis;
s3: extracting the mint in the step S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into a menthol extract with the mass concentration of 2% by using distilled water and the menthol extract;
s4: cleaning and drying the honeysuckle, the clove, the tea and the mint in the S1, and then putting the honeysuckle, the clove, the tea and the mint into an extractor for extraction to obtain extract liquor of the honeysuckle, the clove, the tea and the mint;
s5: adding the honeysuckle, clove, tea and mint extract in the step S4 into a glass container, adding the propolis alcohol extract in the step S2 and the menthol extract in the step S3 while stirring, and stirring for five minutes to obtain a mixed solution A;
s6: adding nicotine salt, 0.02% nitrofurazone solution, borneol, preservative and the rest of distilled water into the mixed solution in the S5, and stirring in the adding process to obtain a mixed solution B;
s7: and (4) filling the mixed solution B obtained in the step (S6) and filling the mixed solution B into a spray can.
Preferably, in S3, need stir the vibration after adding distilled water, the churning time is 5min, in S4, carry out solitary parameter setting as required during the extraction, the extract of honeysuckle, clove, tealeaves and peppermint mixes and places, in S5, adopt the stirring of glass stick during the stirring, clockwise stirring 2 minutes, anticlockwise stirring 3 minutes, in S6, the churning time is 30min, adopts the stirring of glass stick in the stirring process.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. A plant tobacco flavor oral cavity atomized liquid is characterized by comprising the following components in percentage by weight: 2 to 4 percent of nicotine salt, 2 to 4 percent of honeysuckle, 4 to 6 percent of clove, 1 to 2 percent of furacilin solution with the concentration of 0.02 percent, 2 to 5 percent of propolis, 6 to 8 percent of edible ethanol, 1 to 2 percent of borneol, 2 to 3 percent of tea, 58 to 75 percent of distilled water, 4 to 6 percent of mint and 1 to 2 percent of preservative.
2. The plant tobacco flavor oral cavity atomized liquid as claimed in claim 1, which comprises the following components in percentage by weight: 2% of nicotine salt, 2% of honeysuckle, 4% of clove, 1% of 0.02% nitrofurazone solution, 2% of propolis, 6% of edible ethanol, 1% of borneol, 2% of tea, 75% of distilled water, 4% of mint and 1% of preservative.
3. A preparation method of plant tobacco flavor oral cavity atomized liquid is characterized by comprising the following steps:
s1: purchasing nicotine salt, flos Lonicerae, flos Caryophylli, 0.02% furacilin solution, propolis, edible ethanol, Borneolum Syntheticum, folium Camelliae sinensis, distilled water, herba Menthae and antiseptic from regular store;
s2: preparing propolis alcoholic extract from edible ethanol in S1 and propolis;
s3: extracting the mint in the S1 with edible ethanol to obtain a menthol extract, and preparing the menthol extract into menthol extract with the mass concentration of 4-10% by using distilled water and the menthol extract;
s4: cleaning and drying the honeysuckle, the clove, the tea and the mint in the S1, and then putting the honeysuckle, the clove, the tea and the mint into an extractor for extraction to obtain extract liquor of the honeysuckle, the clove, the tea and the mint;
s5: adding the honeysuckle, clove, tea and mint extract in the step S4 into a glass container, adding the propolis alcohol extract in the step S2 and the menthol extract in the step S3 while stirring, and stirring for five minutes to obtain a mixed solution A;
s6: adding nicotine salt, 0.02% nitrofurazone solution, borneol, preservative and the rest of distilled water into the mixed solution in the S5, and stirring in the adding process to obtain a mixed solution B;
s7: and (4) filling the mixed solution B obtained in the step (S6) and filling the mixed solution B into a spray can.
4. The method for preparing the plant tobacco flavor oral cavity atomizing liquid as claimed in claim 3, wherein the step of stirring and shaking is carried out after adding distilled water in the step of S3, and the stirring time is 5 min.
5. The method for preparing the plant tobacco flavor oral cavity atomized liquid as claimed in claim 3, wherein in the step S4, separate parameter setting is performed according to requirements during extraction, and the extracts of honeysuckle, clove, tea and mint are mixed and placed.
6. The method of claim 3, wherein in step S5, the plant tobacco flavor oral cavity atomized liquid is stirred by a glass rod, clockwise stirring is carried out for 2 minutes, and counterclockwise stirring is carried out for 3 minutes.
7. The method for preparing the plant tobacco flavor oral cavity atomizing liquid as claimed in claim 3, wherein in the step S6, the stirring time is 30min, and a glass stirring rod is adopted for stirring in the stirring process.
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CN114128778A (en) * | 2021-11-03 | 2022-03-04 | 上海应用技术大学 | Mint oolong flavored tea beverage and preparation method thereof |
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