CN104403794A - Preparation method and application of Pu'er tea extract to cigarettes - Google Patents
Preparation method and application of Pu'er tea extract to cigarettes Download PDFInfo
- Publication number
- CN104403794A CN104403794A CN201410492973.1A CN201410492973A CN104403794A CN 104403794 A CN104403794 A CN 104403794A CN 201410492973 A CN201410492973 A CN 201410492973A CN 104403794 A CN104403794 A CN 104403794A
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- Prior art keywords
- tea
- cigarette
- filter stick
- filter
- cigarettes
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
Abstract
The the invention discloses a preparation method and application of a Pu'er tea extract to cigarettes. The method is as below: crushing Pu'er tea, adding a leaching solvent, soaking with heat preservation and cover, filtering to obtain filter residue and a leaching liquor, conducting secondary immersion filtering on the filter residue with thee leaching liquor, merging the two leaching liquor, and conducting vacuum drying to obtain the Pu'er tea extract. The invention uses the Pu'er tea extract as an additive for functional cigarettes; the Pu'er tea extract is dissolved in glycerol triacetate and added to the mouth bar tow as a plasticizer, or added to tobacco shreds as a surface essence; and the processing production does not need to change the existing process, causes no environmental pollution, and enriches the types of natural plant source essence perfume. The volatile aroma and functional components in the Pu'er tea extracts, or the latent fragrant substances in the extract can participate in fume reaction to endow the cigarettes with fresh and elegant aroma, enhance the sensory qualities of saliva secretion promotion, after taste, moistness and mellowness of the cigarettes, and to enrich the flavor of the cigarettes.
Description
Technical field
The present invention relates to a kind of preparation method of Pu'er tea and the application in cigarette thereof.
Background technology
The several functions compositions such as the tea-polyphenol in Leaf of Assam Tea, alkaloid, total free aminoacids, VITAMIN, soaping agents, tea pigment and tea polysaccharide, not only there is very strong oxidation-resistance, the objectionable impurities in flue gas can be reduced, and Polyphenols, amino acid and polyose composition wherein can also improve flue gas and inhale taste, play promote the production of body fluid, effect of humectation.
Polyphenol content in Pu'er raw tea, 25 ~ 28%, has the ability of promoting the production of body fluid, returning sweet organoleptic features and very strong anti-oxidant activity and scavenging free radicals; Tea polysaccharide is the acidic polysaccharose of tea Ye Zhongyi class together with protein bound or acidic protein sugar.Tea polysaccharide has hypoglycemic, reducing blood-fat, strengthening immunity and the various biological such as radioprotective and anticoagulation function, water-soluble sugar is wherein the main component of millet paste sweet taste, it can alleviate the irritation effect of bitter taste material tea-polyphenol, trimethyl-xanthine in millet paste, this part sugared content is higher, and tealeaves flavour is glycol more; Alkaloid in tealeaves has and impels human central nervous excited, produces refreshing effect to the mind, the pharmacological function such as cardiac stimulant diuresis and removing toxic substances, and appropriate absorption has active influence to human body.Tealeaves alkaloid is added in cigarette and can reach the effect of refreshing oneself equally when smoking, and alleviate nicotine (Nicotine) to the toxic action of human body.The flavour fragrance of the amino acid in tealeaves and millet paste has close contacting, especially the effect of theanine, and be the important component forming tea aroma and quality, the fresh refreshing degree of tealeaves in remarkably influenced.Biochemical components many in tealeaves being combined with cigarette, bringing improvement in fragrance and mouthfeel by adding in filter stick when aspirating, increase that cigarette is sweet, alcohol, profit, fragrant mouthfeel.
Tea leaf extract is a kind of cigaret additive of pure natural, a lot of report adopts different extracting method tealeaves fragrance matter to be made extracting solution exploitation cigaret additive at present, and then make up cigarette perfume (or spice), make the increase of cigarette smoke perfume quantity, aroma quality raising, smoking quality improves.And the several functions composition contained in tealeaves, make tea leaf extract have antibacterial anti-inflammatory, clearing heat and detoxicating, return sweetly to promote the production of body fluid, the anti-moth of preventing decayed tooth, antianaphylaxis matter and dispel the effects such as cigarette poison, be applied in cigarette the effect can played and decompose and alleviate the objectionable impurities such as Nicotine and tar.These developments being tea cigarette provide strong theoretical foundation and DEVELOPMENT PROSPECT.
Summary of the invention
For promoting the suction comfortableness of cigarette, improving the organoleptic quality of cigarette, the preparation method that the object of this invention is to provide a kind of Pu'er tea and the application added in cigarette thereof.
The present invention is achieved through the following technical solutions: a kind of preparation method of Pu'er tea, it is characterized in that through following each step:
(1) Pu ' er tea powder is broken to 80 ~ 100 orders, then adds the extracting solvent of 3 ~ 10 times of volumes, at 70 ~ 90 DEG C, add a cover heat-insulation soaking 1 ~ 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 30min ~ 1h with the extraction solvent of 3 ~ 5 times of volumes at 70 ~ 90 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, at 50 ~ 60 DEG C, carry out vacuum concentration drying, namely obtain solid Pu'er tea.
The Leaf of Assam Tea of described step (1) is Pu'er raw tea or Folium camelliae assamicae (processed).
Described extraction solvent is distilled water.
The vacuum concentration drying of described step (3) carries out under vacuum tightness is 0.02 ~ 0.05 Mpa.
The extract outward appearance of Pu'er raw tea is blackish green pulverulent solids, has the pure fragrance of Yunnan distinctive large leaf solar dried green tea.Its main chemical compositions comprises: tea-polyphenol, amino acid, alkaloid, VITAMIN, soaping agents, aromatoising substance and soluble sugar isoreactivity composition.
The extract outward appearance of Folium camelliae assamicae (processed) is chocolate powder solid, without bitter taste, flavour glycol, has the distinctive aged aroma of Leaf of Assam Tea.Primary bioactive components: protein, VITAMIN, tea polysaccharide and tea pigment.
Another object of the present invention is to the application providing Pu'er tea in production of cigarettes, be included in application in filter stick or/and application in pipe tobacco.
Realize especially by following technical proposal:
The application of described Pu'er tea in filter stick, is characterized in that:
After first being mixed by following mass ratio with glycerine triacetate by Pu'er tea, obtain mixture:
Pu'er tea 3 ~ 5%,
Glycerine triacetate 95 ~ 97%;
Press 8 ~ 10% of acetate fibres beam quality again, directly said mixture is sprayed onto on acetate silk when producing filter stick, make the filter stick containing Pu'er tea, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in filter stick.
The application of described Pu'er tea in pipe tobacco, is characterized in that:
First Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 5 ~ 10%
Volumetric concentration is the ethanol 90 ~ 95% of 75%;
Press 0.05 ~ 0.1% of tobacco quality again, above-mentioned solute is evenly sprayed onto in pipe tobacco, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in pipe tobacco.
The application of described Pu'er tea in filter stick and pipe tobacco, is characterized in that:
1), after being mixed by following mass ratio with glycerine triacetate by Pu'er tea, mixture is obtained:
Pu'er tea 3 ~ 5%,
Glycerine triacetate 95 ~ 97%;
Press 8 ~ 10% of acetate fibres beam quality again, directly said mixture being sprayed onto on acetate silk when producing filter stick, making the filter stick containing Pu'er tea;
2) Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 5 ~ 10%
Volumetric concentration is the ethanol 90 ~ 95% of 75%.
Press 0.05 ~ 0.1% of tobacco quality again, above-mentioned solute is added in pipe tobacco, the obtained cigarette shreds containing Pu'er tea;
3) by step 1) containing the filter stick of Pu'er tea and step 2) the pipe tobacco containing Pu'er tea, the cigarette seaming operation through routine makes the cigarette all containing Pu'er tea in pipe tobacco and filter stick.
The invention has the advantages that: adopt the Pu'er tea that obtains of such scheme, extract from the elite of Leaf of Assam Tea to human body beneficial that there is dense refreshing, the organoleptic features that fragrance is fresh clearly of flavour.The present invention using Pu'er tea as functional cigarette additive, Pu'er tea is added in glycerine triacetate and be used as cigarette filter rod softening agent, make the function filter stick containing Pu'er tea, this function filter stick formation physical index is all up to state standards requirement, promotes contribution degree higher to cigarette quality; And Pu'er tea is applied in pipe tobacco as table essence, processing, without the need to changing existing technique and there is not environmental pollution, has enriched the kind of natural plant essence and flavoring agent.Using Pu'er tea as functional cigarette additive, in conjunction with the Volatile infochemicals in Pu'er tea and functional ingredient, or utilize the latent Studies of The Aromatic Substances in extract to participate in smoke reaction, the fragrance of the pure and fresh elegance of cigarette can be given, strengthen the promoting the production of body fluid of cigarette, return sweet, clear and rich, alcohol and organoleptic quality, enrich cigarette perfume (or spice), reduce flue gas pungency and improve suction comfortableness.Smoke panel test through expert and think that the cigarette adding this Pu'er tea obtains larger improvement on suction taste, aroma substance in extract and functional ingredient and smoke perfume, clear and rich, the Oranoleptic indicator such as to promote the production of body fluid are combined, and make flue gas pungency and assorted gas all have reduction in various degree.Building cigarette feature note, improving in suction comfortableness and embody unique advantage and significant effect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Embodiment 1
Pu'er raw tea extract adds in the softening agent of mouth rod tow
(1) Pu'er raw tea is crushed to 80 orders, then adds the distilled water of 8 times of volumes, at 90 DEG C, add a cover heat-insulation soaking 1h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 1h with the distilled water of 4 times of volumes at 70 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 50 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains solid Pu'er tea.
The application of gained Pu'er tea in filter stick, specifically through the following step:
After first being mixed by following mass ratio with glycerine triacetate by Pu'er tea, obtain mixture:
Pu'er tea 3%,
Glycerine triacetate 97%;
Press 8% of acetate fibres beam quality again, directly said mixture is sprayed onto on acetate silk when producing filter stick, make the filter stick containing Pu'er tea, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in filter stick.
Embodiment 2
Pu-Er ripe tea extract is added in the softening agent of mouth rod tow
(1) Folium camelliae assamicae (processed) is crushed to 90 orders, then adds the distilled water of 10 times of volumes, at 70 DEG C, add a cover heat-insulation soaking 2h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 50min with the distilled water of 5 times of volumes at 70 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 55 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains Pu'er tea.
The application of gained Pu'er tea in filter stick, specifically through the following step:
After first being mixed by following mass ratio with glycerine triacetate by Pu'er tea, obtain mixture:
Pu'er tea 5%,
Glycerine triacetate 95%;
Press 10% of acetate fibres beam quality again, directly said mixture is sprayed onto on acetate silk when producing filter stick, make the filter stick containing Pu'er tea, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in filter stick.
Embodiment 3
Pu'er raw tea extract adds in pipe tobacco as table spice liquid
(1) Pu'er raw tea is crushed to 100 orders, then adds the distilled water of 3 times of volumes, at 80 DEG C, add a cover heat-insulation soaking 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 30min with the distilled water of 3 times of volumes at 90 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 60 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains Pu'er tea.
Gained Pu'er tea is applied to as table essence in pipe tobacco, specifically through the following step:
First Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 5%
Volumetric concentration is the alcohol 95 % of 75%.
Press 0.1% of tobacco quality again, above-mentioned solute is evenly sprayed onto in pipe tobacco, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in pipe tobacco.
Embodiment 4
Pu-Er ripe tea extract is added in pipe tobacco as table spice liquid
(1) Folium camelliae assamicae (processed) is crushed to 90 orders, then adds the distilled water of 7 times of volumes, at 70 DEG C, add a cover heat-insulation soaking 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 1h with the distilled water of 5 times of volumes at 80 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 60 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains Pu'er tea.
First Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 10%
Volumetric concentration is the ethanol 90% of 75%.
Press 0.05% of tobacco quality again, above-mentioned solute is evenly sprayed onto in pipe tobacco, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in pipe tobacco.
Embodiment 5
Pu'er raw tea extract adds in mouth rod softening agent simultaneously and is sprayed onto in pipe tobacco
(1) Pu'er raw tea is crushed to 100 orders, then adds the distilled water of 3 times of volumes, at 70 DEG C, add a cover heat-insulation soaking 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 30min with the distilled water of 3 times of volumes at 90 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 58 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains Pu'er tea.
Gained Pu'er tea is applied in filter stick and pipe tobacco, specifically through the following step:
1), after being mixed by following mass ratio with glycerine triacetate by Pu'er tea, mixture is obtained:
Pu'er tea 4%,
Glycerine triacetate 96%;
Press 9% of acetate fibres beam quality again, directly said mixture being sprayed onto on acetate silk when producing filter stick, making the filter stick containing Pu'er tea;
2) Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 6%
Volumetric concentration is the ethanol 94% of 75%.
Press 0.09% of tobacco quality again, above-mentioned solute is added in pipe tobacco, the obtained cigarette shreds containing Pu'er tea;
3) by step 1) containing the filter stick of Pu'er tea and step 2) the pipe tobacco containing Pu'er tea, the cigarette seaming operation through routine makes the cigarette all containing Pu'er tea in pipe tobacco and filter stick.
Embodiment 6
Pu-Er ripe tea extract is added in mouth rod softening agent simultaneously and is sprayed onto in pipe tobacco
(1) Pu'er raw tea is crushed to 100 orders, then adds the distilled water of 3 times of volumes, at 80 DEG C, add a cover heat-insulation soaking 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 30min with the distilled water of 3 times of volumes at 80 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, 52 DEG C, vacuum tightness carries out vacuum concentration drying under being 0.02 ~ 0.05 Mpa, namely obtains Pu'er tea.
Gained Pu'er tea is applied in filter stick and pipe tobacco, specifically through the following step:
1), after being mixed by following mass ratio with glycerine triacetate by Pu'er tea, mixture is obtained:
Pu'er tea 3%,
Glycerine triacetate 97%;
Press 8% of acetate fibres beam quality again, directly said mixture being sprayed onto on acetate silk when producing filter stick, making the filter stick containing Pu'er tea;
2) Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 10%
Volumetric concentration is the ethanol 90% of 75%.
Press 0.1% of tobacco quality again, above-mentioned solute is added in pipe tobacco, the obtained cigarette shreds containing Pu'er tea;
3) by step 1) containing the filter stick of Pu'er tea and step 2) the pipe tobacco containing Pu'er tea, the cigarette seaming operation through routine makes the cigarette all containing Pu'er tea in pipe tobacco and filter stick.
Filter stick in above-described embodiment or pipe tobacco are used for cloud and mist trade mark cigarette, then transfer to the member of smoking of specialty to carry out sense organ contrast with common vinegar fine mouth rod cigarette for control sample to smoke panel test, smoking result is given a mark according to the requirement of GB5606.4-2005, and result is as following table:
The invention discloses a kind of cigarette additive containing Pu'er tea and be applied in production of cigarettes.The main functional component of this Pu'er tea comprises tea-polyphenol, amino acid, VITAMIN, alkaloid, aromatoising substance, tea pigment, soaping agents and tea polysaccharide class.Described Pu'er tea comprises Pu'er raw tea extract and Pu-Er ripe tea extract.Pu'er tea is dissolved in glycerine triacetate as softening agent add to mouth rod tow in or as table spice liquid join in cigarette shreds.The prepared new cigarette containing Pu'er tea is of value to the increase of the improvement of cigarette flavor matter and perfume quantity, promotes cigarette smoke and promotes the production of body fluid, returns sweet, clear and rich aesthetic quality, and then improve the interior quality of cigarette.
Claims (7)
1. a preparation method for Pu'er tea, is characterized in that through following each step:
(1) Pu ' er tea powder is broken to 80 ~ 100 orders, then adds the extracting solvent of 3 ~ 10 times of volumes, at 70 ~ 90 DEG C, add a cover heat-insulation soaking 1 ~ 3h, then filter and obtain filter residue and vat liquor;
(2) filter after the filter residue of step (1) being soaked 30min ~ 1h with the extraction solvent of 3 ~ 5 times of volumes at 70 ~ 90 DEG C and obtain vat liquor;
(3) by step (1) and the mixing of step (2) gained vat liquor, at 50 ~ 60 DEG C, carry out vacuum concentration drying, namely obtain Pu'er tea.
2. preparation method according to claim 1, is characterized in that: the Leaf of Assam Tea of described step (1) is Pu'er raw tea or Folium camelliae assamicae (processed).
3. preparation method according to claim 1, is characterized in that: described extraction solvent is distilled water.
4. preparation method according to claim 1, is characterized in that: the vacuum concentration drying of described step (3) carries out under vacuum tightness is 0.02 ~ 0.05 Mpa.
5. an application for Pu'er tea as claimed in claim 1, is characterized in that:
After first being mixed by following mass ratio with glycerine triacetate by Pu'er tea, obtain mixture:
Pu'er tea 3 ~ 5%,
Glycerine triacetate 95 ~ 97%;
Press 8 ~ 10% of acetate fibres beam quality again, directly said mixture is sprayed onto on acetate silk when producing filter stick, make the filter stick containing Pu'er tea, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in filter stick.
6. an application for Pu'er tea as claimed in claim 1, is characterized in that:
First Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 5 ~ 10%
Volumetric concentration is the ethanol 90 ~ 95% of 75%
Press 0.05 ~ 0.1% of tobacco quality again, above-mentioned solute is evenly sprayed onto in pipe tobacco, then by conventional cigarette seaming operation, make the cigarette containing Pu'er tea in pipe tobacco.
7. an application for Pu'er tea as claimed in claim 1, is characterized in that:
1), after being mixed by following mass ratio with glycerine triacetate by Pu'er tea, mixture is obtained:
Pu'er tea 3 ~ 5%,
Glycerine triacetate 95 ~ 97%;
Press 8 ~ 10% of acetate fibres beam quality again, directly said mixture being sprayed onto on acetate silk when producing filter stick, making the filter stick containing Pu'er tea;
2) Pu'er tea and ethanol are pressed following quality than after mixed dissolution, obtain solute:
Pu'er tea 5 ~ 10%
Volumetric concentration is the ethanol 90 ~ 95% of 75%
Press 0.05 ~ 0.1% of tobacco quality again, above-mentioned solute is added in pipe tobacco, the obtained cigarette shreds containing Pu'er tea;
3) by step 1) containing the filter stick of Pu'er tea and step 2) the pipe tobacco containing Pu'er tea, the cigarette seaming operation through routine makes the cigarette all containing Pu'er tea in pipe tobacco and filter stick.
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