CN105876846A - Ampelopsis grossedentata extract-containing electronic tobacco liquid and preparation method thereof - Google Patents
Ampelopsis grossedentata extract-containing electronic tobacco liquid and preparation method thereof Download PDFInfo
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- CN105876846A CN105876846A CN201610276965.2A CN201610276965A CN105876846A CN 105876846 A CN105876846 A CN 105876846A CN 201610276965 A CN201610276965 A CN 201610276965A CN 105876846 A CN105876846 A CN 105876846A
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- ampelopsis grossedentata
- electronic cigarette
- grossedentata extrat
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
The invention provides ampelopsis grossedentata extract-containing electronic tobacco liquid and a preparation method thereof. The electronic tobacco liquid is prepared by uniformly mixing an ampelopsis grossedentata extract, edible essence, propylene glycol, glycerin, water and the like according to a proportion, wherein the ampelopsis grossedentata extract is obtained through extraction and filtration. The electronic tobacco liquid provided by the invention has pure aroma and good mouthfeel; and the ampelopsis grossedentata extract contained in the tobacco liquid has the functions of diminishing inflammation, relieving pain, expelling phlegm and relieving cough, protecting liver and alleviating hangover, resisting hypertension, reducing blood glucose, eliminating fat, resisting tumor, enhancing immunity, resisting oxidation, inhibiting bacteria and the like, and realizes a body building effect on consumers.
Description
Technical field
The invention belongs to chemical technology field, specifically, there is provided a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat and preparation method thereof.
Background technology
Electronic cigarette has another name called electronic cigarette, has the outward appearance as Medicated cigarette and the taste of medicated cigarette approximation, even a lot of than the taste weight of general Medicated cigarette.Electronic cigarette does not has other harmful components such as the tar in Medicated cigarette, suspended particulates, is nearly free from second hand smoking yet.Electronic cigarette is typically made up of three parts: tobacco rod, nebulizer and cigarette bullet.
The fragrance of electronic cigarette is that tobacco juice atomization produces.Existing tobacco juice for electronic smoke is mainly made up of chemical substances such as water, propylene glycol and glycerol, as disclosed in Chinese patent application " a kind of electronic smoke agent " (201410719012.X), including ester type compound, water, propylene glycol and/or glycerol, these chemical compositions the most also can produce the material being unfavorable for health.Therefore, have been reported that and some effective ingredients in plant are added in tobacco juice, as in " a kind of electronic smoke agent with tea perfume and preparation method thereof " (201410715919.9) disclosed in Chinese patent, Folium Camelliae sinensis quintessence oil is added in tobacco juice, it can effectively reduce the sweet soapy feeling of propylene glycol or glycerol, give the delicate fragrance of electronic cigarette Folium Camelliae sinensis simultaneously, but its health care is limited.
Ampelopsis grossedentata is the leaf of Vitaceae ampelopsis Ampelopsis grossedentata, its main place of production in the Shrubs of Mountainous Areas of the height above sea level such as Hunan, Hubei 400～1300 meters, Lin Zhong, Shi Shang, river bank, Ampelopsis grossedentata is traditional medication among the people, is once widely used in treating the infectious disease such as dermatosis, furuncle and phyma and osteomyelitis, acute lymphoblastic inflammation.Dihydromyricetin contained therein is a kind of important flavones ingredient, and dihydromyricetin is widely used in treating respiratory tract infection, crapulent Chinese patent medicine preparation, such as tablet, capsule, electuary, such as tablet, capsule, electuary.In recent years antitumor pharmacodynamic study finds that one of its active component, ampelopsin micromolecular compound have stronger antitumaous effect.The research of dihydromyricetin is preparing the application of leukemia and medicine for nasopharyngeal, is the most prepared to enter into clinical experimental stage as a kind new medicine.In Ampelopsis grossedentata, its dihydromyricetin mass fraction is up to 20%-28 % (accounting for dry weight), and the content in spire is higher.In electronic cigarette liquid, add Ampelopsis grossedentata extrat, there is the multiple peculiar effects such as removing free radical, antioxidation, antithrombotic, antitumor, antiinflammatory, blood sugar lowering, hepatoprotective, highly beneficial to health.
Summary of the invention
It is an object of the invention to provide a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat, it not only has preferable fragrance, mouthfeel and moderate strength, also has certain health-care effect.It is a further object to provide the preparation method of a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat.
The technical scheme is that a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat, containing Ampelopsis grossedentata extrat, described Ampelopsis grossedentata extrat is water extract or the alcohol extraction thing of Ampelopsis grossedentata.
The most concrete technical scheme is: a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat, the component of two parts in following be mixed: Ampelopsis grossedentata extrat 5-10 part, edible essence 0.1-1 part, propylene glycol 1-80 part, glycerol 1-70 part, water 5-30 part.
In technique scheme, described for edible Mint Essence, edible cacao essence or table grapes essence.
The present invention provides the preparation method of a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat, including:
(1) weighing clean Ampelopsis grossedentata, add extractant ethanol, ultrasonic extraction three times, filter, united extraction liquid, decompression rotary evaporation is condensed into paste, obtains Ampelopsis grossedentata extrat；
(2) take the component of following weight portion: Ampelopsis grossedentata extrat 5-10 part, edible essence 0.1-1 part, propylene glycol 1-80 part, glycerol 1-70 part, water 5-30 part, mix homogeneously, obtain the electronic cigarette liquid containing Ampelopsis grossedentata extrat.
As optimization, the concentration of described extractant ethanol is 60wt%-90wt%, feed liquid w/v 1:8-20.
As optimization, described ultrasonic extraction condition is: ultrasonic frequency is 50-400kHz, and ultrasonic power is 50-600W, extraction time 20-30min/ time.
As optimization, the temperature that described decompression rotary evaporation concentrates is 50 ° of C, and vacuum is 0.095Mpa.
Electronic cigarette liquid containing Ampelopsis grossedentata extrat provided by the present invention is light yellow, has preferable fragrance, mouthfeel and moderate strength, and itself and do not contain nicotine, there is no the hazardness of Nicotiana tabacum L., but there is the health-care effect such as antitumor, enhancing immunity.Its preparation method is easy, and constant product quality can be widely applied in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1:
(1) a certain amount of dry Ampelopsis grossedentata is weighed, the ethanol of 60% is added according to solid-liquid ratio 1:8, it is 50KHZ in ultrasonic frequency, power is supersound extraction three times under conditions of 50W, 30min every time, united extraction liquid after filtration, is 50 ° of C in temperature, vacuum is that under 0.095Mpa, decompression rotary evaporation is condensed into paste, standby.
(2) by Ampelopsis grossedentata extrat 9 parts, edible Mint Essence 0.5 part, propylene glycol 20 parts, glycerol 45 parts and 30 parts of mix homogeneously of water, the electronic cigarette liquid containing Ampelopsis grossedentata extrat is obtained.
Embodiment 2:
(1) a certain amount of Ampelopsis grossedentata extrat is weighed, the ethanol of 60% is added according to solid-liquid ratio 1:8, it is 50KHZ in ultrasonic frequency, power is supersound extraction three times under conditions of 50W, 30min every time, united extraction liquid after filtration, is 50 ° of C in temperature, vacuum is that under 0.095Mpa, decompression rotary evaporation is condensed into paste, standby.
(2) by Ampelopsis grossedentata extrat 10 parts, edible Mint Essence 0.1 part, propylene glycol 1 part, glycerol 70 parts and 15 parts of mix homogeneously of water, the electronic cigarette liquid containing Ampelopsis grossedentata extrat is obtained.
Embodiment 3:
(1): weigh a certain amount of Ampelopsis grossedentata extrat, the ethanol of 60% is added according to solid-liquid ratio 1:8, it is 50KHZ in ultrasonic frequency, power is supersound extraction three times under conditions of 50W, 30min every time, united extraction liquid after filtration, is 50 ° of C in temperature, vacuum is that under 0.095Mpa, decompression rotary evaporation is condensed into paste, standby.
(2) by Ampelopsis grossedentata extrat 7 parts, edible Mint Essence 7.5 parts, propylene glycol 40 parts, glycerol 45 parts and 5 parts of mix homogeneously of water, the electronic cigarette liquid containing Ampelopsis grossedentata extrat is obtained.
The electronic cigarette liquid containing Ampelopsis grossedentata extrat obtained in the embodiment 1 prepared, embodiment 2, embodiment 3 takes 0.5ML add to electronic cigarette, carry out integrated sensory's quality evaluation.Result shows:
Embodiment one, embodiment two, embodiment three all show that flue gas is full, give off a strong fragrance, mouthfeel is moderate, and pleasant impression is preferable.
Can be seen that from result, the electronic cigarette liquid containing Ampelopsis grossedentata extrat prepared by the preparation method of the present invention has preferable fragrance, mouthfeel and good pleasant impression, three embodiment tastes are more or less the same, and electronic cigarette liquid in the present invention do not contain nicotine, effective ensure mouthfeel in the case of also reduce the Nicotiana tabacum L. impact on health.Ampelopsis grossedentata extrat has good result at the aspect such as antitumor, enhancing immunity, meets the health demand of smoker, and the preparation method of above-mentioned electronic cigarette liquid is easy, and constant product quality can be widely applied in electronic cigarette product.
Claims (7)
1. electronic cigarette liquid containing Ampelopsis grossedentata extrat and preparation method thereof, it is characterised in that containing Ampelopsis grossedentata extrat, described Ampelopsis grossedentata extrat is water extract or the alcohol extraction thing of Ampelopsis grossedentata.
2. according to a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat described in claim 1, it is characterised in that be mixed by the component of following weight portion: Ampelopsis grossedentata extrat 5-10 part, edible essence 0.1-1 part, propylene glycol 1-80 part, glycerol 1-70 part, water 5-30 part.
3. according to a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat described in claim 1 or 2, it is characterised in that
Described for edible Mint Essence, edible cacao essence or table grapes essence.
4. according to a kind of electronic cigarette liquid containing Ampelopsis grossedentata extrat described in claim 1, it is characterised in that including:
(1) weighing clean Ampelopsis grossedentata, add extractant ethanol, ultrasonic extraction three times, filter, united extraction liquid, decompression rotary evaporation is condensed into paste, obtains Ampelopsis grossedentata extrat；
(2) take the component of following weight portion: Ampelopsis grossedentata extrat 5-10 part, edible essence 0.1-1 part, propylene glycol 1-80 part, glycerol 1-70 part, water 5-30 part, mix homogeneously, obtain the electronic cigarette liquid containing Ampelopsis grossedentata extrat.
The preparation method of the electronic cigarette liquid containing Ampelopsis grossedentata extrat the most according to claim 4, it is characterised in that the concentration of described extractant ethanol is 60wt%-90wt%, feed liquid w/v 1:8-20.
The preparation method of the electronic cigarette liquid containing Ampelopsis grossedentata extrat the most according to claim 4, it is characterised in that described ultrasonic extraction condition is: ultrasonic frequency is 50-400kHz, and ultrasonic power is 50-600W, extraction time 20-30min/ time.
The preparation method of the electronic cigarette liquid containing Ampelopsis grossedentata extrat the most according to claim 4, it is characterised in that the temperature that described decompression rotary evaporation concentrates is 50 ° of C, and vacuum is 0.095Mpa.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610276965.2A CN105876846A (en) | 2016-04-29 | 2016-04-29 | Ampelopsis grossedentata extract-containing electronic tobacco liquid and preparation method thereof |
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| CN201610276965.2A CN105876846A (en) | 2016-04-29 | 2016-04-29 | Ampelopsis grossedentata extract-containing electronic tobacco liquid and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN107510098A (en) * | 2017-10-18 | 2017-12-26 | 厦门诺康得生物科技有限公司 | A kind of tobacco juice for electronic smoke containing stem cell excretion body and preparation method and application |
| CN108315385A (en) * | 2018-02-06 | 2018-07-24 | 云南中烟工业有限责任公司 | A method of electronic cigarette liquid is quickly screened based on escherichia coli |
| CN109619656A (en) * | 2019-01-18 | 2019-04-16 | 薪火高科(深圳)有限公司 | It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial |
| CN115067534A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Preparation method of vine tea extract for cigarettes |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107361398A (en) * | 2017-06-26 | 2017-11-21 | 河南中烟工业有限责任公司 | A kind of tea extraction in May and preparation method thereof and the application in cigarette |
| CN107510098A (en) * | 2017-10-18 | 2017-12-26 | 厦门诺康得生物科技有限公司 | A kind of tobacco juice for electronic smoke containing stem cell excretion body and preparation method and application |
| CN108315385A (en) * | 2018-02-06 | 2018-07-24 | 云南中烟工业有限责任公司 | A method of electronic cigarette liquid is quickly screened based on escherichia coli |
| CN108315385B (en) * | 2018-02-06 | 2021-10-26 | 云南中烟工业有限责任公司 | Method for rapidly screening electronic cigarette liquid based on Escherichia coli |
| CN109619656A (en) * | 2019-01-18 | 2019-04-16 | 薪火高科(深圳)有限公司 | It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial |
| CN115067534A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Preparation method of vine tea extract for cigarettes |
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Application publication date: 20160824 |
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