CN111297740A

CN111297740A - Nicotinamide VB3 mask composition

Info

Publication number: CN111297740A
Application number: CN202010285574.3A
Authority: CN
Inventors: 周海军
Original assignee: Coris Cosmetics Shanghai Co ltd
Current assignee: Coris Cosmetics Shanghai Co ltd
Priority date: 2020-04-13
Filing date: 2020-04-13
Publication date: 2020-06-19

Abstract

The invention discloses a nicotinamide VB3 facial mask composition, and relates to the technical field of skin care products. The technical key points are as follows: the nicotinamide VB3 facial mask composition consists of essence and facial mask liquid, wherein the essence comprises the following components in parts by weight: deionized water: 80-90 parts of a solvent; methyl propylene glycol: 5-15 parts; white fungus extract: 0.01-0.05 part; carbomer: 0.05-0.2 part; p-hydroxyacetophenone: 0.1-0.5 part; triethanolamine: 0.05-0.2 part; moisturizing and smoothing agent: 1-5 parts; plant allergy-relieving agent: 0.1-1 part; sodium hyaluronate: 0.05-0.2 part; plant preservative: 0.5-1 part; nicotinamide: 0.3-0.8 part; grape seed oil: 0.001 to 0.005 portion; hydrogenated castor oil: 0.001 to 0.005 portion; propylene glycol: 0.005-0.01 portion; nicotinic acid: 1-3 parts of nicotinamide and nicotinic acid are compounded and used, and the dosage ratio is controlled, so that the obtained mask composition has good whitening, anti-aging, water-locking and moisturizing effects.

Description

Nicotinamide VB3 mask composition

Technical Field

The invention relates to the technical field of skin care products, in particular to a nicotinamide VB3 facial mask composition.

Background

The principle of the facial mask is that the facial mask is covered on the face for a short time, so that the external air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, the secretion and metabolism of sweat glands are promoted, the oxygen content of the skin is increased, products of metabolism of epidermal cells and accumulated grease substances are favorably discharged by the skin, and the moisture in the facial mask permeates into the horny layer of the epidermis of the skin to replenish the moisture in the skin.

In the Chinese patent application with publication number CN110897954A, a composition for a hair melanin is disclosed, which comprises ginseng fermentation filtrate and nicotinamide, wherein the content of the ginseng fermentation filtrate is 0.01-96 wt% based on the total weight of the composition, and the content of the nicotinamide is 4-98 wt% based on the total weight of the composition.

According to the invention, through compounding of the ginseng fermentation filtrate and the nicotinamide, the whitening effects of the ginseng fermentation filtrate and the nicotinamide can be increased, the using amount of the nicotinamide can be reduced, the content of nicotinic acid in the product is reduced, the intolerance probability is reduced, and the composition for inhibiting melanin is added into the essence for constantly generating melanin, so that the whitening effect is improved. However, the melanin inhibiting composition has little other effect, especially weak free radical scavenging ability, i.e., weak antioxidant ability.

Therefore, a new solution is needed to solve the above problems.

Disclosure of Invention

Aiming at the defects in the prior art, the invention aims to provide the nicotinamide VB3 mask composition which has the advantages of remarkable whitening effect and good antioxidant effect.

In order to achieve the purpose, the invention provides the following technical scheme:

the nicotinamide VB3 facial mask composition consists of essence and facial mask liquid, wherein the essence comprises the following components in parts by weight:

deionized water: 80-90 parts of a solvent;

methyl propylene glycol: 5-15 parts;

white fungus extract: 0.01-0.05 part;

carbomer: 0.05-0.2 part;

p-hydroxyacetophenone: 0.1-0.5 part;

triethanolamine: 0.05-0.2 part;

moisturizing and smoothing agent: 1-5 parts;

plant allergy-relieving agent: 0.1-1 part;

sodium hyaluronate: 0.05-0.2 part;

plant preservative: 0.5-1 part;

nicotinamide: 0.3-0.8 part;

grape seed oil: 0.001 to 0.005 portion;

hydrogenated castor oil: 0.001 to 0.005 portion;

1, 3-propanediol: 0.005-0.01 portion;

nicotinic acid: 1-3 parts.

By adopting the technical scheme, the tremella extract contains rich protein, vitamins and the like, has the effects of moisturizing, resisting aging, removing wrinkles and firming skin, can be used for removing freckles and chloasma and the like after being frequently applied, also comprises tremella polysaccharide as a main active component, has elegant and unique smooth skin feeling and high-efficiency moisturizing and skin care functions, and is natural 'plant hyaluronic acid'.

Niacinamide is a derivative of vitamin B3, and it is also a recognized whitening and anti-aging ingredient in the skin care community. The nicotinamide can effectively block the generation of melanin in cells and accelerate the metabolism of the melanin, so the nicotinamide has good whitening and freckle removing effects; in addition, the niacinamide can promote the generation of skin collagen and increase skin moisture, so that the niacinamide can also play an anti-aging role; meanwhile, the niacinamide can regulate the oil secretion of skin, so the niacinamide also has good oil control effect.

The nicotinic acid can inhibit the transfer of melanin from melanocytes to protein cells and reduce hyperpigmentation, and is different from common whitening components which only focus on inhibiting the generation of melanin but act on the generated melanin, so that the skin color and luster can be improved in various links from the generation of the melanin to the shedding of the melanin; accelerating skin metabolism, promoting the exfoliation of melanin horny cells, keeping cell balance level and presenting a young state; promoting the synthesis of epidermal layer protein, enhancing skin moisture content, and improving skin quality.

According to the invention, the nicotinamide and the nicotinic acid are compounded and used, and the dosage ratio is controlled, so that the obtained mask composition has good whitening, anti-aging, water-locking and moisturizing effects. Furthermore, the method is simple. The invention also uses a plurality of components such as a moisturizing smoothing agent, a plant soothing agent and the like in a compounding way, so that the aging phenomena such as skin dryness, looseness, fine lines and the like can be improved, damaged skin cells can be repaired, damaged elastic fibers can be repaired, and each cell of the skin is full of youth activity.

Further preferably, the mask liquid comprises the following components in parts by weight:

deionized water: 80-90 parts of a solvent;

methyl propylene glycol: 5-10 parts;

glycerol: 1-3 parts;

carbomer: 0.05-0.1 part;

glyceryl polyether-26: 1-3 parts;

xanthan gum: 0.05-0.1 part;

sodium polyglutamate: 0.01-0.05 part;

hydroxyethyl cellulose: 0.05-0.1 part;

methyl ester: 0.1-0.2 parts;

triethanolamine: 0.05-0.1 part;

panthenol: 0.5-2 parts;

moisturizing and smoothing agent: 1-3 parts;

plant allergy-relieving agent: 0.5-1 part;

a91 preservative: 0.1-0.5 part;

skin conditioner: 0.01-0.1 part;

grape seed oil: 0.005-0.01 portion;

hydrogenated castor oil: 0.01-0.05 part;

1, 3-propanediol: 0.02-0.03 portion.

More preferably, the dosage ratio of the essence to the facial mask liquid is 1 volume part to 5 volume parts.

Through adopting above-mentioned technical scheme, facial mask liquid and essence independently prepare and pack, mix according to above-mentioned volume ratio during the use, can pack facial mask liquid and facial mask cloth in the wrapping bag, pack the essence in soft capsule, then fix soft capsule on the wrapping bag, adopt the film to separate between soft capsule and the wrapping bag, during the use, extrude soft capsule, wherein the essence flows into in the wrapping bag and mixes with facial mask liquid, high durability and convenient use, and can prolong nicotinamide VB 3's shelf life, keep the activity, secondary pollution that can also avoid causing during the use.

More preferably, the moisturizing and smoothing agent is composed of a mixture of mannitol and trehalose in a weight ratio of 1 (1-2).

According to the technical scheme, mannitol is hexahydric alcohol and belongs to polyhydric alcohols, more hydroxyl groups can be combined with water in a hydrogen bond mode, a certain water locking and moisturizing effect is achieved, trehalose is small in molecular weight and easy to absorb by skin, enters cells to play a unique water replacement stress factor effect and a cell membrane protection function, the anti-drying and anti-freezing capacity of the cells is improved, and therefore the skin environment adaptation capacity can be improved.

More preferably, the plant soothing agent is composed of a mixture of radix sophorae flavescentis extract, radix glycyrrhizae inflatae extract and scutellaria baicalensis extract in a weight ratio of 1 (1-2) to (2-3).

By adopting the technical scheme, the plant allergy relieving agent can prevent abnormal conditions such as redness and swelling, itching, molting, allergic dermatitis and the like of skin caused by various stimulation.

More preferably, the plant preservative adopts zanthoxylum bungeanum maxim extract.

By adopting the technical scheme, the zanthoxylum bungeanum maxim fruit extract is a broad-spectrum efficient bactericide, can resist various bacteria, fungi, viruses, parasites and other microorganisms, is a zero-additive preservative which has excellent capability of really inhibiting the microorganisms, and greatly prolongs the shelf life of the mask composition under the condition of ensuring the safety.

Further preferably, the essence is obtained by the following preparation steps: mixing deionized water, methyl propylene glycol, Tremella fuciformis extract, carbomer and p-hydroxyacetophenone, heating to 80-90 ℃, preserving heat and defoaming for 20-30min, cooling to 45-55 ℃, adding triethanolamine and stirring uniformly, cooling to 40-45 ℃, adding moisturizing and smoothing agent, plant soothing agent, sodium hyaluronate, plant preservative, nicotinamide, grape seed oil, hydrogenated castor oil and 1, 3-propylene glycol, stirring uniformly, finally adding nicotinic acid and stirring uniformly, cooling to 25-40 ℃, and discharging to obtain the product.

By adopting the technical scheme, the essence is independently prepared and packaged, and is separately packaged with the mask liquid, so that the essence is disposable during use, the product is prevented from being secondarily polluted in use, the quality guarantee period of the product is greatly prolonged, and the activity of components such as nicotinamide, nicotinic acid and the like in the essence is guaranteed.

Further preferably, the facial mask liquid is obtained by the following preparation steps: mixing deionized water, methyl propylene glycol, glycerol, carbomer, glyceryl polyether-26, xanthan gum, sodium polyglutamate, hydroxyethyl cellulose and methyl ester, heating to 85-90 deg.C, keeping the temperature for defoaming for 20-30min, cooling to 45-50 deg.C, adding triethanolamine, panthenol, moisturizing and smoothing agent, plant soothing agent, A91 antiseptic, skin conditioner, grape seed oil, hydrogenated castor oil and 1, 3-propylene glycol, stirring, cooling to 35-40 deg.C, and discharging.

By adopting the technical scheme, the preparation method of the mask liquid does not involve high-temperature heating reaction, only needs to fully dissolve and mix the raw materials of each component, is simple to operate and is suitable for large-scale production.

In summary, compared with the prior art, the invention has the following beneficial effects:

(1) the essence disclosed by the invention is prepared by compounding nicotinamide and nicotinic acid and controlling the dosage ratio, so that the obtained mask composition has good whitening, anti-aging, water-locking and moisturizing effects. Furthermore, the method is simple. The invention also uses a plurality of components such as a moisturizing smoothing agent, a plant soothing agent and the like in a compounding way, so that the aging phenomena such as skin dryness, looseness, fine lines and the like can be improved, damaged skin cells can be repaired, damaged elastic fibers can be repaired, and each cell of the skin is full of youth activity;

(2) the mask liquid and the essence are separately and independently packaged, and are mixed according to the volume ratio of 5:1 when in use, so that the mask liquid is convenient to use, secondary pollution caused by use can be avoided, the quality guarantee period of nicotinamide and nicotinic acid can be prolonged, and the activity is kept;

(3) the mask liquid provided by the invention mainly takes a moisturizing smoothing agent and a plant allergy relieving agent as main active ingredients, wherein the moisturizing smoothing agent is prepared by compounding mannitol and trehalose and has the effects of locking water and moisturizing, and the plant allergy relieving agent is prepared by combining three natural plant extracts and can play good roles of protecting, repairing and moistening skin.

Detailed Description

The present invention will be described in detail with reference to examples.

Example 1: a nicotinamide VB3 facial mask composition comprises essence and facial mask liquid which are independently packaged, wherein the components in the essence and the facial mask liquid and the corresponding weight parts of the components are shown in table 1, when the nicotinamide VB3 facial mask composition is used, 5mL of the essence is squeezed into a facial mask containing 25mL of the facial mask liquid, and the mixture is uniformly mixed for use.

The essence in the embodiment is prepared by the following preparation steps: mixing deionized water, methyl propylene glycol, a tremella extract, carbomer and p-hydroxyacetophenone, heating to 80 ℃, preserving heat and defoaming for 20min, cooling to 45 ℃, adding triethanolamine, stirring uniformly at 800rpm, cooling to 40 ℃, adding a moisturizing smoothing agent, a plant soothing agent, sodium hyaluronate, a plant preservative, nicotinamide, grape seed oil, hydrogenated castor oil and propylene glycol, stirring uniformly at 1200rpm, finally adding nicotinic acid, stirring uniformly, cooling to 25 ℃ and discharging.

The mask liquid in this example is prepared by the following steps: mixing deionized water, propylene glycol, glycerol, carbomer, glyceryl polyether-26, xanthan gum, sodium polyglutamate, hydroxyethyl cellulose and methyl ester, heating to 85 ℃, preserving heat and defoaming for 20min, cooling to 45 ℃, adding triethanolamine, panthenol, a moisturizing and smoothing agent, a plant soothing agent, an A91 preservative, a skin conditioner, grape seed oil, hydrogenated castor oil and propylene glycol, uniformly stirring at 800rpm, cooling to 35 ℃, and discharging to obtain the product.

Wherein the moisturizing and smoothing agent consists of mannitol and trehalose in a weight ratio of 1: 1.

The plant allergy relieving agent is a mixture of radix Sophorae Flavescentis extract, radix Glycyrrhizae Inflatae extract and radix Scutellariae extract at a weight ratio of 1:1: 2.

The plant antiseptic is fructus Zanthoxyli extract.

The skin conditioner is prepared from Glycyrrhrizae radix extract.

Examples 2 to 6: the difference between the nicotinamide VB3 facial mask composition and the embodiment 1 is that the components and the corresponding parts by weight of the essence and the facial mask liquid are shown in Table 1.

TABLE 1 Components and parts by weight of examples 1-6

Example 7: a nicotinamide VB3 mask composition is the same as example 1, and is different from example 1 in that:

the essence in the embodiment is prepared by the following preparation steps: mixing deionized water, methyl propylene glycol, a tremella extract, carbomer and p-hydroxyacetophenone, heating to 90 ℃, preserving heat and defoaming for 30min, cooling to 55 ℃, adding triethanolamine, stirring uniformly at 800rpm, cooling to 45 ℃, adding a moisturizing smoothing agent, a plant soothing agent, sodium hyaluronate, a plant preservative, nicotinamide, grape seed oil, hydrogenated castor oil and propylene glycol, stirring uniformly at 1200rpm, finally adding nicotinic acid, stirring uniformly, cooling to 25 ℃ and discharging to obtain the product.

The mask liquid in this example is prepared by the following steps: mixing deionized water, propylene glycol, glycerol, carbomer, glyceryl polyether-26, xanthan gum, sodium polyglutamate, hydroxyethyl cellulose and methyl ester, heating to 90 ℃, preserving heat and defoaming for 30min, cooling to 50 ℃, adding triethanolamine, panthenol, a moisturizing and smoothing agent, a plant soothing agent, an A91 preservative, a skin conditioner, grape seed oil, hydrogenated castor oil and propylene glycol, uniformly stirring at 800rpm, cooling to 40 ℃, and discharging to obtain the product.

Example 8: a nicotinamide VB3 mask composition is different from that in example 1 in that in the example, a moisturizing and smoothing agent is composed of mannitol and trehalose according to a weight ratio of 1: 2.

Example 9: a mask composition of nicotinamide VB3 is different from that in example 1 in that in the example, the plant soothing agent is composed of a radix sophorae flavescentis extract, a radix glycyrrhizae inflatae extract and a scutellaria baicalensis extract according to a weight ratio of 1:2: 2.

Example 10: a nicotinamide VB3 facial mask composition is different from that in example 1 in that a plant soothing agent is composed of a radix sophorae flavescentis extract, a radix glycyrrhizae inflatae extract and a scutellaria baicalensis extract according to a weight ratio of 1:2: 3.

Comparative example 1: the difference from example 1 is that no niacinamide is added to the serum.

Comparative example 2: the difference from example 1 is that no niacin was added to the serum.

Comparative example 3: the difference from example 1 is that nicotinamide was used in an amount of 1 part by weight and nicotinic acid was used in an amount of 0.3 part by weight.

Comparative example 4: the difference from the example 1 is that the plant soothing agent consists of lightyellow sophora root extract and swollen fruit root and liquorice root extract according to the weight ratio of 1: 1.

Comparative example 5: the difference from example 1 is that the plant soothing agent is sophora flavescens extract.

Comparative example 6: the difference from example 1 is that no plant soothing agent was added.

Comparative example 7: the difference from example 1 is that no licorice extract was added.

Performance testing

The facial mask compositions prepared in examples 1 to 10 and comparative examples 1 to 7 were uniformly mixed with 25mL of facial mask solution and 5mL of essence solution to obtain a usable facial mask.

And (3) testing the antioxidant effect: DPPH radical scavenging ability was measured by DPPH oxidation method, hydroxyl radical scavenging ability was measured by salicylic acid method, and the test results are shown in Table 2.

TABLE 2 Oxidation resistance test results

Group of	DPPH radical scavenging Rate (IC)₅₀,mg/mL)	Hydroxyl radical scavenging rate (IC)₅₀,mg/mL)
			Example 1	0.07	0.21
Example 2	0.08	0.21
			Example 3	0.08	0.22
Example 4	0.07	0.24
			Example 5	0.07	0.22
Example 6	0.08	0.23
			Example 7	0.08	0.21
Example 8	0.07	0.23
			Example 9	0.07	0.21
Example 10	0.09	0.25
			Comparative example 1	0.51	1.10
Comparative example 2	0.53	1.11
			Comparative example 3	0.48	1.09
Comparative example 4	0.11	0.86
			Comparative example 5	0.12	0.88
Comparative example 6	0.13	0.90
			Comparative example 7	0.26	0.96

As shown in Table 2, the essence obtained by compounding nicotinamide and nicotinic acid and controlling the dosage ratio has obvious antioxidation.

And (3) testing the whitening effect: the user was tested using a skin color measurement scale, and the amount of change in skin color was recorded in table 3.

Table 3 whitening performance test results

As can be seen from table 3, the essence provided by the invention has a good whitening effect by using nicotinamide and nicotinic acid in a compounding manner and using plant extracts in the essence and the mask liquid in a compounding manner.

And (4) testing the moisturizing effect: 34 volunteers in the same area were selected and divided into 17 groups of 20 persons each, and the use effect was evaluated after 30 days by using the masks obtained in examples 1 to 10 and comparative examples 1 to 7. The results are shown in Table 4.

Skin moisturization: a: the skin moisturizing effect is good; b: the skin moisturizing effect is good; c: the skin has a normal moisturizing effect, and the skin is slightly dry; wherein the group A and the group B are both effective groups.

Table 4 results of moisture retention test

As can be seen from Table 4, the facial mask prepared by the invention has a moisturizing effect obviously superior to that of the comparative examples, has an effective rate of more than 85 percent, and has a remarkable water-locking moisturizing effect.

The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims

1. The nicotinamide VB3 facial mask composition is composed of essence and facial mask liquid, and is characterized in that the essence comprises the following components in parts by weight:

deionized water: 80-90 parts of a solvent;

methyl propylene glycol: 5-15 parts;

white fungus extract: 0.01-0.05 part;

carbomer: 0.05-0.2 part;

p-hydroxyacetophenone: 0.1-0.5 part;

triethanolamine: 0.05-0.2 part;

moisturizing and smoothing agent: 1-5 parts;

plant allergy-relieving agent: 0.1-1 part;

sodium hyaluronate: 0.05-0.2 part;

plant preservative: 0.5-1 part;

nicotinamide: 0.3-0.8 part;

grape seed oil: 0.001 to 0.005 portion;

hydrogenated castor oil: 0.001 to 0.005 portion;

1, 3-propanediol: 0.005-0.01 portion;

nicotinic acid: 1-3 parts.

2. The nicotinamide VB3 facial mask composition of claim 1, wherein the facial mask solution comprises the following components in parts by weight:

deionized water: 80-90 parts of a solvent;

methyl propylene glycol: 5-10 parts;

glycerol: 1-3 parts;

carbomer: 0.05-0.1 part;

glyceryl polyether-26: 1-3 parts;

xanthan gum: 0.05-0.1 part;

sodium polyglutamate: 0.01-0.05 part;

hydroxyethyl cellulose: 0.05-0.1 part;

methyl ester: 0.1-0.2 parts;

triethanolamine: 0.05-0.1 part;

panthenol: 0.5-2 parts;

moisturizing and smoothing agent: 1-3 parts;

plant allergy-relieving agent: 0.5-1 part;

a91 preservative: 0.1-0.5 part;

skin conditioner: 0.01-0.1 part;

grape seed oil: 0.005-0.01 portion;

hydrogenated castor oil: 0.01-0.05 part;

1, 3-propanediol: 0.02-0.03 portion.

3. The nicotinamide VB3 mask composition of claim 2, wherein the essence and the mask solution are used in a ratio of 1 part by volume to 5 parts by volume.

4. The nicotinamide VB3 mask composition of claim 1, wherein the moisturizing and smoothing agent is composed of a mixture of mannitol and trehalose in a weight ratio of 1 (1-2).

5. The nicotinamide VB3 mask composition of claim 1, wherein the plant soothing agent is composed of a mixture of a radix sophorae flavescentis extract, a radix glycyrrhizae inflatae extract and a scutellaria baicalensis extract in a weight ratio of 1 (1-2) to (2-3).

6. The niacinamide VB3 facial mask composition of claim 1, wherein the plant preservative is zanthoxylum bungeanum maxim extract.

7. The niacinamide VB3 mask composition of claim 1, wherein the essence is obtained by the preparation steps of: mixing deionized water, methyl propylene glycol, Tremella fuciformis extract, carbomer and p-hydroxyacetophenone, heating to 80-90 ℃, preserving heat and defoaming for 20-30min, cooling to 45-55 ℃, adding triethanolamine and stirring uniformly, cooling to 40-45 ℃, adding moisturizing and smoothing agent, plant soothing agent, sodium hyaluronate, plant preservative, nicotinamide, grape seed oil, hydrogenated castor oil and 1, 3-propylene glycol, stirring uniformly, finally adding nicotinic acid and stirring uniformly, cooling to 25-40 ℃, and discharging to obtain the product.

8. The niacinamide VB3 mask composition according to claim 2, wherein the mask solution is obtained by the following preparation steps: mixing deionized water, methyl propylene glycol, glycerol, carbomer, glyceryl polyether-26, xanthan gum, sodium polyglutamate, hydroxyethyl cellulose and methyl ester, heating to 85-90 deg.C, keeping the temperature for defoaming for 20-30min, cooling to 45-50 deg.C, adding triethanolamine, panthenol, moisturizing and smoothing agent, plant soothing agent, A91 antiseptic, skin conditioner, grape seed oil, hydrogenated castor oil and 1, 3-propylene glycol, stirring, cooling to 35-40 deg.C, and discharging.