CN110522795A - A kind of wine desert cistanche prepared slices of Chinese crude drugs and preparation method thereof - Google Patents
A kind of wine desert cistanche prepared slices of Chinese crude drugs and preparation method thereof Download PDFInfo
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- A61K36/88—Liliopsida (monocotyledons)
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Abstract
The present invention relates to Chinese medicine processing technique fields, and in particular to a kind of wine desert cistanche prepared slices of Chinese crude drugs and preparation method thereof, preparation method is the following steps are included: (1) Herba Cistanches fresh medicinal material is screened, cleans, drained；(2) Herba Cistanches are placed in citric acid solution after impregnating and take out, drains；(3) Herba Cistanches are sliced, are placed in semen coicis extracting solution infiltration to saturating, drain, it is dry；(4) Herba Cistanches slice is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；(5) Herba Cistanches are sliced, extremely using micro-wave drying；(6) freezing processing will be carried out by Herba Cistanches slice；(7) the Herba Cistanches particle obtained after Herba Cistanches slice chopping is subjected to extrusion processing, cooling obtains the wine desert cistanche prepared slices of Chinese crude drugs.Wine desert cistanche prepared slices of Chinese crude drugs bioavailability of the invention is high, effective component dissolution rate is fast, and convenient, stable product quality made from preparation method, loss of effective components is few, convenient operation and control, high production efficiency, is conducive to industrialized production.
Description
Technical field
The present invention relates to Chinese medicine processing technique fields, and in particular to a kind of wine desert cistanche prepared slices of Chinese crude drugs and preparation method thereof.
Background technique
(alias cun rue, desert cistanche look into dry announcement Asia (Mongolian) to Herba Cistanches, belong to endangered species.Tall and big draft, it is 40-160 centimetres high, greatly
Partly lower life.The month at florescence 5-6, the fruiting period 6-8 month.Main product is also distributed in Xinjiang, Alashan Area, inner Mongolia Autonomous Region alliance, Gansu, Ningxia.Meat
Desert cistanche is a kind of parasitic plant for colonizing in desert trees sacsaoul root, and nutrient and moisture are drawn from sacsaoul host.It is known as " husky
The good reputation of unconcerned ginseng " has high medical value, is the rare traditional Chinese medicine of Chinese tradition.Herba Cistanches are just western in history
Domain various countries are as one of highest help drug of usage frequency in the treasure and successive dynasties tonifying kidney and strengthening yang class prescription of Shang Gong imperial court.
With the rapid development of separation and Extraction and detection technique, the separated a plurality of types of substances out of Herba Cistanches, be can be divided mainly at present
Benzyl carbinol glycoside, iridoids, lignanoids, polysaccharide, ten several amino acid, a variety of alkaloids etc., it is micro- rich in needed by human body
Secondary element, wherein phenylethanoid glycosides are main actives in Herba Cistanches, have and improve male's sexual, treatment woman's palace cold not
Pregnant, anti-oxidant, anti-aging improves the functions such as immunity, enhancing memory.
Wine desert cistanche is with the Herba Cistanches after wine Preparation process.In the prior art to take raw meat desert cistanche, yellow rice wine is added, it is suitable to set
Container in, it is closed, water proof or stewed thoroughly with steam heating, or stew to yellow rice wine when being sucked completely, cool, take out, dry in the air to sixty percent
It is dry, it is sliced, it is dry.However, each technological parameter controllability is bad during the preparation process, loss of effective components is more, bioavailability
It is low, and product quality is irregular, and few using effective component dissolution when water tanning, preparation method has much room for improvement.
Summary of the invention
The purpose of the present invention is being directed to above-mentioned deficiency in the prior art, a kind of preparation side of wine desert cistanche prepared slices of Chinese crude drugs is provided
Method, the preparation method stable product quality, loss of effective components is few, convenient operation and control, high production efficiency, and it is big to be conducive to industrialization
Production.
Another object of the present invention is to provide a kind of wine desert cistanche prepared slices of Chinese crude drugs, the wine desert cistanche prepared slices of Chinese crude drugs raw material availabilities
Height, convenient for being absorbed and utilized, the wine desert cistanche prepared slices of Chinese crude drugs of long shelf-life.
The purpose of the present invention is achieved through the following technical solutions:
A kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs, includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 18-24wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 12-15wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 7-10 mesh after the Herba Cistanches slice chopping that step (6) is handled squeezes
Expanding treatment is pressed, is cooled to room temperature, the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion are obtained.
The wine desert cistanche prepared slices of Chinese crude drugs of the invention, can solubilized Herba Cistanches benzyl carbinol by citric acid, semen coicis and yellow rice wine processing
The loss of active constituent in Herba Cistanches is effectively reduced in the effective components such as glycoside, improves utilization ratio of drug, enhances the health care of Herba Cistanches
Function, and its oxidation resistance can be improved, keep the shelf-life longer, the effective component in citric acid, semen coicis extracting solution and yellow rice wine
It is permeable to inside Herba Cistanches, plays the role of filling tissue, keep Herba Cistanches particle extruding uniform；Meanwhile wine desert cistanche Chinese medicine is drunk
Piece carries out extruding after the processing of citric acid, semen coicis and yellow rice wine, and wine desert cistanche prepared slices of Chinese crude drugs effective ingredient is lost in puffing process
It is few；Wine desert cistanche prepared slices of Chinese crude drugs bioavailability is high, effective component dissolution rate is fast, rich wine aroma, both can be used as conventional Chinese medicine drink
Piece, and can be used for daily beverage and eat, direct boiled water brews, convenient.
Further, in the step (2), the citric acid solution is aqueous citric acid solution, the quality percentage of citric acid
Specific concentration is 5-8%.The present invention impregnates the inoxidizability that can enhance Herba Cistanches by using above-mentioned concentration addition aqueous citric acid solution
Can, and can play inhibit bacterium, it is fresh-keeping the effects of, improve the stability of Herba Cistanches, the Herba Cistanches after citric acid solution have
Good quality and color, and do not influence the performance of Herba Cistanches itself, and improve its flavor to a certain extent.The step
(2) in, the mass ratio of the Herba Cistanches and citric acid solution is 10:2-3.
Further, in the step (3), the preparation method of semen coicis extracting solution is the following steps are included: by coix seed powder
The mass ratio of broken mistake 100-140 mesh afterwards, addition purified water, the semen coicis and purified water is 1:3-4, is then added using microwave
Thermal extraction, microwave power 800-1000W, extraction time 20-30min.The present invention is by Herba Cistanches piece successively through citric acid water
After solution impregnates, and infiltrated using semen coicis extracting solution to saturating, the semen coicis extracting solution effective component absorbed in Herba Cistanches piece with
Yellow rice wine collective effect, the medium effective component of the solubilized Herba Cistanches of energy, is effectively reduced the loss of active constituent in Herba Cistanches, and lemon
Acid, semen coicis and yellow rice wine match, and make wine desert cistanche obtained rich in wine aroma, and to improvement traditional wine desert cistanche to a certain extent
Flavor.The mass ratio of the Herba Cistanches and semen coicis extracting solution is 10:2.5-3.5.
Further, in the step (3), Herba Cistanches slice with a thickness of 2-4mm.By to Herba Cistanches slice thickness
Addressing, so that Herba Cistanches slice is convenient for microwave drying, the Herba Cistanches particle after making chopping convenient for absorbing effective component in yellow rice wine
Diameter is 1.5-4mm, is suitable for expanding treatment convenient for the Herba Cistanches grain diameter after chopping, keeps the Herba Cistanches prepared slices of Chinese crude drugs normal in effect
When advising Traditional medicine infusion medicine materical crude slice or tea-drinking, effective ingredient can be precipitated in due course.
Further, in the step (4), the ethanol content of yellow rice wine is 15-20wt%.Further, the step (4)
In, the weight ratio of Herba Cistanches and yellow rice wine is 10:(2.5-3.5), the bored profit time is 2-4h.By using above-mentioned steps, make by
Yellow rice wine treated Herba Cistanches particle has wine aroma, and loss of effective components is few.
Further, in the step (5), micro-wave drying power is 700-850W.Micro-wave drying temperature is
65-80℃.By using micro-wave drying, steamed relative to traditional heating, it is easy to operate easily-controllable, it is time-consuming short, effectively at
Divide loss few, is conducive to industrialized production.
Further, in the step (6), freezing processing temperature is -10~-15 DEG C, and the processing time is 5-7h.The present invention
By using freezing processing, Herba Cistanches internal fiber structure is had cured at low ambient temperatures, is conducive to product shape in puffing process
The holding of shape can prevent Herba Cistanches to be easy to appear volume rebound phenomenon, and increase the brittleness of Herba Cistanches in puffing process.
Further, in the step (7), swelling temperature is 70-80 DEG C, and control pressure is 0.4-0.6MPa, and keeping should
After pressure 20-30min, it is depressurized to 0.008MPa or less rapidly.Preferably, it is depressurized to 0.008MPa or less rapidly in 2s.Into
One step, expanding treatment step 2-3 times in the step (7).The present invention is by using above-mentioned bulking step, so that wine desert cistanche
Uniformly, in the reduction of expansion process pressure moment, the expansion rapidly of Herba Cistanches tissue forms uniform honeycomb structure, wine desert for expansion
Effect of the Rong without explosion, few disintegrating slag；And interval extruding is carried out under the conditions of 70-80 DEG C, it prevents from being easy to appear volume rebound phenomenon,
Product porous structure is caused to collapse, puffed degree decline；Simultaneously in puffing process, steam the partial moisture moment inside Herba Cistanches
Hair releases vacuum so that the water content of the wine desert cistanche prepared slices of Chinese crude drugs is 5-7% when being cooled to room temperature, take out product to get warp is arrived
The wine desert cistanche prepared slices of Chinese crude drugs of extrusion processing.
In wine desert cistanche prepared slices of Chinese crude drugs process of the invention, each processing step and parameter are controlled, the effective of Herba Cistanches is made
Component damages are seldom, and its appearance, color, smell meet demand, convenient operation and control, and stable product quality guarantees meat desert processed
The safety and validity of Rong's prepared slices of Chinese crude drugs, high production efficiency are conducive to industrialized production.
The present invention also provides the wine desert cistanche prepared slices of Chinese crude drugs made from a kind of preparation method as the above-mentioned wine desert cistanche prepared slices of Chinese crude drugs.
Beneficial effects of the present invention: the wine desert cistanche prepared slices of Chinese crude drugs of the invention are by citric acid, semen coicis and yellow rice wine processing, energy
The loss of active constituent in Herba Cistanches is effectively reduced in the effective component of solubilized Herba Cistanches, enhances the healthcare function of Herba Cistanches, and can
Its oxidation resistance is improved, keeps the shelf-life longer；Meanwhile the wine desert cistanche prepared slices of Chinese crude drugs are by citric acid, semen coicis and yellow rice wine processing
After carry out extruding, effective ingredient is lost few in puffing process；Wine desert cistanche prepared slices of Chinese crude drugs bioavailability is high, effective component dissolution is fast
Degree is fast, and rich wine aroma not only can be used as the conventional prepared slices of Chinese crude drugs, but also can be used for daily beverage and eat, and direct boiled water brews, and eats
Convenient, stable product quality made from preparation method, loss of effective components is few, convenient operation and control, and high production efficiency is conducive to
Industrialized production.
Specific embodiment
For the ease of the understanding of those skilled in the art, below with reference to embodiment, the present invention is further illustrated, real
The content that the mode of applying refers to not is limitation of the invention.
Embodiment 1
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 19wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 13wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 9 meshes after the Herba Cistanches slice chopping that step (6) is handled squeeze swollen
Change processing, is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion.
Further, in the step (2), the citric acid solution is aqueous citric acid solution, the quality percentage of citric acid
Specific concentration is 6%.In the step (2), the mass ratio of the Herba Cistanches and citric acid solution is 10:2.5.
Further, in the step (3), the preparation method of semen coicis extracting solution is the following steps are included: by coix seed powder
The mass ratio of broken 120 meshes excessively afterwards, addition purified water, the semen coicis and purified water is 1:3.5, is then mentioned using microwave heating
It takes, microwave power 850W, extraction time 25min.The mass ratio of the Herba Cistanches and semen coicis extracting solution is 10:3.
Further, in the step (3), Herba Cistanches slice with a thickness of 2-4mm.
Further, in the step (4), the ethanol content of yellow rice wine is 18wt%.The weight ratio of Herba Cistanches and yellow rice wine is
10:3, bored profit time are 3h.
Further, in the step (5), micro-wave drying power is 800W.Micro-wave drying temperature is 70 DEG C.
Further, in the step (6), freezing processing temperature is -12 DEG C, and the processing time is 6h.
Further, in the step (7), swelling temperature is 76 DEG C, and control pressure is 0.5MPa, keeps the pressure
After 20min, 0.008MPa is depressurized to rapidly hereinafter, above-mentioned expanding treatment step is repeated 3 times in 2s.
Embodiment 2
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 18wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 12wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 7 meshes after the Herba Cistanches slice chopping that step (6) is handled squeeze swollen
Change processing, is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion.
Further, in the step (2), the citric acid solution is aqueous citric acid solution, the quality percentage of citric acid
Specific concentration is 5%.In the step (2), the mass ratio of the Herba Cistanches and citric acid solution is 10:3.
Further, in the step (3), the preparation method of semen coicis extracting solution is the following steps are included: by coix seed powder
It is sieved with 100 mesh sieve after broken, addition purified water, the mass ratio of the semen coicis and purified water is 1:3, is then mentioned using microwave heating
It takes, microwave power 800W, extraction time 30min.The mass ratio of the Herba Cistanches and semen coicis extracting solution is 10:2.5.
Further, in the step (4), the ethanol content of yellow rice wine is 15wt%.In the step (4), Herba Cistanches and Huang
The weight ratio of wine is 10:3.5, and the bored profit time is 2h.
Further, in the step (5), micro-wave drying power is 700W.Micro-wave drying temperature is 65 DEG C.
Further, in the step (6), freezing processing temperature is -10 DEG C, and the processing time is 7h.
Further, in the step (7), swelling temperature is 70 DEG C, and control pressure is 0.6MPa, keeps the pressure
After 30min, 0.008MPa is depressurized to rapidly hereinafter, above-mentioned expanding treatment step is repeated 2 times in 2s.
Remaining content of the present embodiment is with embodiment 1, and which is not described herein again.
Embodiment 3
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 18-24wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 15wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 10 meshes after the Herba Cistanches slice chopping that step (6) is handled squeezes
Expanding treatment is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion.
Further, in the step (2), the citric acid solution is aqueous citric acid solution, the quality percentage of citric acid
Specific concentration is 8%.In the step (2), the mass ratio of the Herba Cistanches and citric acid solution is 10:2.
Further, in the step (3), the preparation method of semen coicis extracting solution is the following steps are included: by coix seed powder
The mass ratio of broken 140 meshes excessively afterwards, addition purified water, the semen coicis and purified water is 1:4, is then mentioned using microwave heating
It takes, microwave power 1000W, extraction time 20min.The mass ratio of the Herba Cistanches and semen coicis extracting solution is 10:3.5.
Further, in the step (4), the ethanol content of yellow rice wine is 20wt%.The weight ratio of Herba Cistanches and yellow rice wine is
10:2.5, bored profit time are 4h.
Further, in the step (5), micro-wave drying power is 850W.Micro-wave drying temperature is 80 DEG C.
Further, in the step (6), freezing processing temperature is -15 DEG C, and the processing time is 5h.
Further, in the step (7), swelling temperature is 80 DEG C, and control pressure is 0.4MPa, keeps the pressure
After 22min, 0.008MPa is depressurized to rapidly hereinafter, above-mentioned expanding treatment step is repeated 3 times in 2s.
Remaining content of the present embodiment is with embodiment 1, and which is not described herein again.
Embodiment 4
In the present embodiment, in the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 20wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 14wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 9 meshes after the Herba Cistanches slice chopping that step (6) is handled squeeze swollen
Change processing, is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion.
Further, in the step (5), micro-wave drying power is 780W.Micro-wave drying temperature is 70 DEG C.
Further, in the step (6), freezing processing temperature is -14 DEG C, and the processing time is 5.5h.
Further, in the step (7), swelling temperature is 72 DEG C, and control pressure is 0.45MPa, keeps the pressure
After 28min, in 2s be depressurized to 0.008MPa rapidly hereinafter, above-mentioned expanding treatment step is repeated 3 times.
Comparative example 1
With reference to the Pharmacopoeia of the People's Republic of China (referred to as lower " pharmacopeia ") 2010 first, wine Herba Cistanches under Herba Cistanches,
Cutability desert cistanche piece is taken, is stewed according to wine or wine steams method (appendix II D) and stewes or steam to wine exhaustion.
Comparative example 2
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 19wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 8wt%, obtains the wine desert cistanche prepared slices of Chinese crude drugs.
Remaining content of this comparative example is with embodiment 1, and which is not described herein again.
Comparative example 3
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(3) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 13wt%；
(4) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(5) the Herba Cistanches particle obtained after crossing 9 meshes after the Herba Cistanches slice chopping that step (6) is handled squeeze swollen
Change processing, is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion.
Comparative example 4
In the present embodiment, a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs includes the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained the water, and dry
To moisture 19wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 13wt%；
(6) the Herba Cistanches slice by micro-wave drying will be warmed to room temperature；
(7) the Herba Cistanches particle obtained after crossing 9 meshes after the Herba Cistanches slice chopping that step (6) is handled squeeze swollen
Change processing, is cooled to room temperature, and obtains the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion, and swelling temperature is 76 DEG C, controls pressure
0.008MPa or less is depressurized to rapidly in 2s after keeping pressure 60min for 0.5MPa.
Use initial temperature for the wine desert cistanche prepared slices of Chinese crude drugs of 95 DEG C of immersion embodiment 1-4 and comparative example 1-4, soaking time
For 1h, the additional amount of the wine desert cistanche prepared slices of Chinese crude drugs is that the 10g/L(meat dishes to go with liquor desert cistanche prepared slices of Chinese crude drugs deduct moisture content meter).To having in distilled water
Effect ingredient is measured, and measuring method is referring to " pharmacopeia version in 2010 ", as a result as shown in the table:
| Acteoside (%) | Echinacoside (%) | |
| Embodiment 1 | 1.57 | 5.4 |
| Embodiment 2 | 1.51 | 5.2 |
| Embodiment 3 | 1.42 | 5.5 |
| Embodiment 4 | 1.49 | 5.8 |
| Comparative example 1 | 0.74 | 2.9 |
| Comparative example 2 | 0.89 | 3.3 |
| Comparative example 3 | 1.01 | 4.6 |
| Comparative example 4 | 1.15 | 4.3 |
As can be seen from the above table, the effective component dissolution rate of 1-4 of the embodiment of the present invention is apparently higher than comparative example 1-3, illustrates this Shen
Please after citric acid, semen coicis extracting solution and expanding treatment, the content of the effective component of chinese medicine dissolved out in water is significantly increased,
The loss of effective component of chinese medicine can and be effectively reduced, bioavailability is improved.
The wine desert cistanche medicine materical crude slice of 1-4 of the embodiment of the present invention is in dark brown, the dotted vascular bundle in section, and matter is sweet rich in wine aroma,
Slight bitter.Puffed degree of the embodiment 1-4 Jing Guo expanding treatment is 190-230%, and the puffed degree of comparative example 4 is 130-150%, illustrates to pass through
Extruding pre-treating technology and expanding treatment are crossed, expansion rate of the invention is higher.
To sum up, stable product quality made from the preparation method of the wine desert cistanche prepared slices of Chinese crude drugs of the invention, loss of effective components
Few, bioavailability is high, convenient operation and control, high production efficiency, is conducive to industrialized production, meets Chinese Pharmacopoeia quality mark
It is quasi-.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than the present invention is protected
The limitation of range is protected, although explaining in detail referring to preferred embodiment to the present invention, those skilled in the art are answered
Work as understanding, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the reality of technical solution of the present invention
Matter and range.
Claims (10)
1. a kind of preparation method of the wine desert cistanche prepared slices of Chinese crude drugs, characterized by the following steps:
(1) the Herba Cistanches fresh medicinal material after harvesting is screened, cleaned, drained；
(2) it will take out, drain after the Herba Cistanches drained are placed in citric acid solution and impregnate；
(3) by the Herba Cistanches slice by step (2) processing, infiltration is placed in semen coicis extracting solution to saturating, is drained, it is dry to water
It is divided into 18-24wt%；
(4) the Herba Cistanches slice by step (3) processing is placed in bored profit in yellow rice wine, until yellow rice wine is fully absorbed by Herba Cistanches；
(5) Herba Cistanches after bored profit are sliced, use micro-wave drying to moisture for 12-15wt%；
(6) the Herba Cistanches slice by micro-wave drying is subjected to freezing processing；
(7) the Herba Cistanches particle obtained after crossing 7-10 mesh after the Herba Cistanches slice chopping that step (6) is handled squeezes
Expanding treatment is pressed, is cooled to room temperature, the wine desert cistanche prepared slices of Chinese crude drugs handled through extrusion are obtained.
2. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs described in claim 1, it is characterised in that: in the step (2), institute
Stating citric acid solution is aqueous citric acid solution, and the mass percent concentration of citric acid is 5-8%.
3. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (3)
In, purified water is added the following steps are included: semen coicis is smashed it through 100-140 mesh in the preparation method of semen coicis extracting solution,
The semen coicis and the mass ratio of purified water are 1:3-4, then use extracting through microwave heating, and microwave power 800-1000W is mentioned
Taking the time is 20-30min.
4. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (4)
In, the ethanol content of yellow rice wine is 15-20wt%.
5. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (4)
In, the weight ratio of Herba Cistanches and yellow rice wine is 10:(2.5-3.5), the bored profit time is 2-4h.
6. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (5)
In, micro-wave drying power is 700-850W.
7. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (6)
In, freezing processing temperature is -10~-15 DEG C, and the processing time is 5-7h.
8. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 1, it is characterised in that: the step (7)
In, swelling temperature is 70-80 DEG C, and control pressure is that 0.4-0.6MPa is depressurized to rapidly after keeping pressure 20-30min
0.008MPa or less.
9. a kind of preparation method of wine desert cistanche prepared slices of Chinese crude drugs according to claim 6, it is characterised in that: the step (7)
In expanding treatment step repeat 2-3 times.
10. a kind of wine desert cistanche prepared slices of Chinese crude drugs, it is characterised in that: drunk by wine desert cistanche Chinese medicine described in any one of claim 1-9
The preparation method of piece is prepared.
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Citations (4)
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| CN101223985A (en) * | 2007-12-28 | 2008-07-23 | 中山大学 | Producing process of improving desertliving cistanche sheet quality |
| CN103893274A (en) * | 2012-12-28 | 2014-07-02 | 中国医学科学院药用植物研究所 | Processing method of wine-fried cistanche |
| CN105125642A (en) * | 2015-10-10 | 2015-12-09 | 四川中庸药业有限公司 | Method for preparing life cultivation and health preservation cistanches herba |
| CN107693583A (en) * | 2017-09-06 | 2018-02-16 | 张可池 | A kind of concocting method of saline cistanche |
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2019
- 2019-08-28 CN CN201910799946.1A patent/CN110522795A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101223985A (en) * | 2007-12-28 | 2008-07-23 | 中山大学 | Producing process of improving desertliving cistanche sheet quality |
| CN103893274A (en) * | 2012-12-28 | 2014-07-02 | 中国医学科学院药用植物研究所 | Processing method of wine-fried cistanche |
| CN105125642A (en) * | 2015-10-10 | 2015-12-09 | 四川中庸药业有限公司 | Method for preparing life cultivation and health preservation cistanches herba |
| CN107693583A (en) * | 2017-09-06 | 2018-02-16 | 张可池 | A kind of concocting method of saline cistanche |
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Application publication date: 20191203 |