CN110192990A - It is a kind of with whitening, the concealing stick of acne-removing and preparation method thereof - Google Patents
It is a kind of with whitening, the concealing stick of acne-removing and preparation method thereof Download PDFInfo
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- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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Abstract
The present invention provides a kind of with whitening, the concealing stick of acne-removing and preparation method thereof.The present invention has whitening, the concealing stick of acne-removing includes rice bran oil, tocotrienols, propylene, two certain herbaceous plants with big flowers acid esters, yeast extract and tioxolone.There is the present invention concealing stick of whitening, acne-removing not add the heavy metals such as mercury, safety, and have good whitening and acne-removing.By addition Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 mixture, can make not having to addition emulsifier in concealing stick, can make during the water-soluble functional component such as water and yeast extract incorporates be formulated well；By using processed colorant, can make concealing stick will not coloured oil float go out, stability is more preferable, and does not allow easy fracture.In addition, the preparation method with whitening, the concealing stick of acne-removing, simple process, condition is controllable, easy to produce.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of with whitening, the concealing stick of acne-removing and its system
Preparation Method.
Background technique
Everybody has a love of beauty, and whitening always is the target that people seeking beauty pursues, but the whitening concealing product having is
Reach quick whitening effect, the mercury and heavy metal component of excessive addition exaggerate its whitening function, and such screening is commonly used
Flaw product can cause irreversible destruction to skin, lead to the outburst of many skin problems.Existing whitening concealing product, function
It imitates single, and brings injury to face skin, it is therefore desirable to develop with adornment or the improper generation that can cause small pox of makeup removing for a long time
The concealing product of the two-in-one safety of a whitening, anti-acne.
In addition, presently commercially available concealing stick is not aqueous, thus water-soluble functional component cannot be added, limit water solubility
Application of the functional component in concealing stick.
Summary of the invention
It is an object of the invention to overcoming drawbacks described above in the prior art, provide a kind of with whitening, acne-removing
Concealing stick and preparation method thereof.
The object of the invention is achieved through the following technical solutions:
A kind of concealing stick with whitening, acne-removing includes functional component 1 and functional component 2；The functional component 1
For rice bran oil, tocotrienols, propylene and two certain herbaceous plants with big flowers acid esters mixture, the 0.5- of Zhan Suoshu concealing stick quality
6%, the rice bran oil, tocotrienols, propylene and two certain herbaceous plants with big flowers acid esters mass ratio be rice bran oil: fertility triolefin
Phenol: propylene and two certain herbaceous plants with big flowers acid esters=50-75:9:25-50；The functional component 2 is yeast extract and thiophene gram rope
The mass ratio of the mixture of ketone, the 0.5-8% of Zhan Suoshu concealing stick quality, the yeast extract and tioxolone mentions for yeast
Take object: tioxolone=20-60:35-70.
There is a kind of compound vitamin B in rice bran oil, facilitates skin irritatin circulation, cell growth and skin and highlight, also contain
There is a large amount of saualane, saualane is natural moisturizer, in the case where skin is in serious dermatitis state, can effectively treat skin
Dry and aging；Tocotrienols can stimulate collage synthesis to prevent skin old by the activity of reduction matrix metalloproteinase
Change and improve skin elasticity, and skin-whitening can be promoted by reducing tyrosinase activity and reducing melanin content, accelerates
Wound healing and scar reparation improve blood miniflow, reduce inflammation and rubefaction；Propylene and two certain herbaceous plants with big flowers acid esters energy
Promote the Transdermal absorption of functional component；Yeast extract contains the biological substances such as the necessary amino acid of a large amount of skins, peptide, nucleic acid,
Also contain the necessary zinc of skin metabolism, zinc and chelating amino acids form in the presence of stimulation of the zinc for skin is reduced, has fine
Anti-acne, inflammation-diminishing function；Tioxolone contains 19% sulphur, has cutin softening, antibacterium, antimycotic and adjusting sebum point
The function of secreting, the present invention is by by rice bran oil, tocotrienols, propylene, two certain herbaceous plants with big flowers acid esters, yeast extract and thiophene
The combination of gram rope ketone, finds there is good synergistic function between this in terms of whitening and anti-acne.
Preferably, the functional component 1 accounts for the 3% of the concealing stick quality, and the functional component 2 accounts for the concealing stick matter
The 4% of amount.With this condition, rice bran oil, tocotrienols, propylene, two certain herbaceous plants with big flowers acid esters, yeast extract and thiophene gram
Synergistic function between rope ketone is stronger, and the white-skinned face function of concealing stick and acne-removing can be made stronger.
Preferably, the concealing stick also includes skin sense improver and water, and the skin sense improver is Jojoba esters, Xiang
The mixture of sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3, the Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and poly-
The mass ratio of glycerol -3 is Jojoba esters: sunflower seed wax: Acacia decurrens floral wax and polyglycereol -3=50-75:25-50:1-5:
1-5.Commercially available concealing stick generally passes through emulsifier and disperses water or aqueous substance in oily phase, but the irritation of emulsifier compares
By force, the mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 can make concealing stick not have to addition emulsification
Water or aqueous substance can be incorporated oily Xiangli by agent, to keep concealing stick obtained safer, and stability also compares
Relatively good, furthermore the mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 can also improve concealing stick
Texture.
Preferably, the skin sense improver accounts for the 1-6% of the concealing stick quality, and the water accounts for the concealing stick quality
0.5-8%.With this condition, the stability of concealing stick is more lasting, and texture is more preferable, and price is also relatively low.
Preferably, the skin sense improver accounts for the 3% of the concealing stick quality, and the water accounts for the concealing stick quality
2%.With this condition, concealing stick has extraordinary stability and texture.
Preferably, the concealing stick also includes the coloring for accounting for the colorant 1,0.05-5% of the concealing stick quality 1-25%
The colorant 3 of agent 2 and 0.05-5%, the colorant 1 are titanium dioxide, isononyl isononanoate, isopropyl myristate, department's drawing
Oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid mixture, colorant 2 is
Oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, carbon draw in red iron oxide, isononyl isononanoate, isopropyl myristate, department
The mixture of acid propylene glycol ester and poly- hydroxy stearic acid, colorant 3 are that yellow iron oxide, isononyl isononanoate, myristic acid are different
Propyl ester, department draw the mixture of oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid.
Compare titanium dioxide and iron oxide, the concealer that these three colorants are made will not coloured oil float go out, and concealing effect is relatively good.
Preferably, the concealing stick also includes thickener, adhesive, emollients, colorant dispersant, pH adjusting agent, anti-corrosion
Agent and antioxidant, the thickener include synthetic wax and beeswax, and described adhesive is microwax, and the emollients include different ten
Triol isononoate, glycerol three (thylhexoic acid) ester, neopentyl glycol dicaprate, octyl dodecanol stearoyl-oxy stearic acid
The mixture of ester, thorn A Ganshu benevolence oil and dipentaerythritol hexahydroxystearic acid ester, six stearates and six rosinates,
The colorant dispersant is diisooctadecanol malate, and the pH adjusting agent is citric acid, and the preservative is glycerol octanoic acid
Ester, the antioxidant are tocopherol.
Synthetic wax has good feel, gloss, and the duration is longer；Beeswax can nourish and soft skin, enhancing
The persistence of concealer；Microwax has good elasticity and viscosity, and relatively safety；Different tridecanol isononoate can make skin
With good soft and moist property；(thylhexoic acid) ester of glycerol three has good hydrolytic stability and oil compatibility, can reduce screening
The greasy feeling of flaw stick makes it have good spreadability and stability；Neopentyl glycol dicaprate plays moist skin in concealer
Skin, the effect for supplementing oil content and moisture-locking, and skin can be made to keep gas permeability；The dry benevolence oil of setting of Ci A is from Morocco nutwood
Fruit extracts, fatty acid, vitamin E, squalene and sterol rich in etc., is commonly used for treatment skin disease, is added
In cosmetics, good alimentary and skin sense can be improved, has preferable oxidation resistance to human body, and repair the lipid of skin
Barrier, fixed maintenance effect another to sensibility skin；Dipentaerythritol hexahydroxystearic acid ester, six stearates and six pines
The mixture of resin acid ester is tasteless hazel body of paste, has highly polar, armful aqueous and moisture feeling, and cosmetics can be made to keep soft
Soft sense of touch；Diisooctadecanol malate has good dispersion effect to colorant, and can moisturize the skin；Citric acid can add
Fast cutin updates, and facilitates melanin in skin and peels off, and pore receives thin, blackhead dissolution, and can play moisturizing, whitening to skin
Effect, facilitate improve skin blackspot, it is coarse situations such as；Glycerol caprylate not only has good preservative efficacy, moreover it is possible to grow
Moisten skin；Tocopherol has good antioxidant effect, is good nutrition moisturizing agent for skin.
Preferably, by mass percentage, the concealing stick includes the synthetic wax of 2-30%, the beeswax of 1-8%, 1-10%
Microwax, the different tridecanol isononoate of 1-15%, glycerol three (thylhexoic acid) ester of 1-15%, the neopentyl glycol of 2-25%
Dicaprate, the octyl dodecanol stearoyl-oxy stearate of 1-15%, the Ci Agan tree benevolence oil of 1-15%, the two of 1-6%
The mixture of polypentaerythritol hexahydroxystearic acid ester, six stearates and six rosinates, the two isooctadecanol apples of 1-15%
Tartaric acid ester, the citric acid of 0.005-0.05%, the glycerol caprylate of 0.1-2% and the tocopherol of 0.1-1%.With this condition,
Concealer has preferably texture, moistness, spreadability and stability.
Preferably, by mass percentage, the concealing stick includes 12% synthetic wax, 2% beeswax, 3% crystallite
Wax, 12% different tridecanol isononoate, 10.39% glycerol three (thylhexoic acid) ester, 9% neopentyl glycol dicaprate,
8% octyl dodecanol stearoyl-oxy stearate, 7% Ci Agan tree benevolence oil, 2.5% dipentaerythritol hexahydroxy
The mixture of stearate, six stearates and six rosinates, 6% diisooctadecanol malate, 0.01% lemon
Acid, 0.3% glycerol caprylate and 0.3% tocopherol.With this condition, concealer has extraordinary moistness, sprawls
Property and stability, and price is also relatively low.
The present invention also provides a kind of preparation methods of concealing stick, comprising the following steps:
(1) thickener, emollients, adhesive, colorant dispersant and functional component 1 are heated to 90-100 DEG C, keep its complete
80-90 DEG C is cooled to after running down, obtains A phase；
(2) it adds a colorant in A phase, is dispersed with stirring uniformly until obtaining B phase entirely without particle；
(3) felt improver is heated to 80-90 DEG C, then solvent, pH adjusting agent and function is added to being completely melt in stirring
Ingredient 2 is imitated, insulated and stirred is continued, it is wrapped up by skin sense improver completely, obtains C phase；
(4) C is added in B phase, is dispersed with stirring uniformly, then cools to 60-70 DEG C, preservative and anti-oxidant is added
Agent is dispersed with stirring uniformly to get the concealing stick.
The advantages of the present invention are as follows:
1, there is the present invention concealing stick of whitening, acne-removing not add the heavy metals such as mercury, safety, and have good beauty
Contour painting effect and acne-removing；By addition Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 mixture,
It can not have to addition emulsifier, the water-soluble functional component such as water and yeast extract can be made to be incorporated in formula well；By adopting
With processed colorant, can make concealing stick will not coloured oil float go out, stability is more preferable, and does not allow easy fracture.
2, preparation method simple process of the present invention with whitening, the concealing stick of acne-removing, condition is controllable, is easy to raw
It produces.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
Embodiment 1 is a kind of concealing stick with whitening, acne-removing, and ingredient and its content are shown in Table 1.This has beauty
The preparation method of white, acne-removing concealing stick the following steps are included:
(1) by synthetic wax 1, synthetic wax 2, beeswax, microwax, different tridecanol isononoate, glycerol three (thylhexoic acid) ester,
Neopentyl glycol dicaprate, octyl dodecanol stearoyl-oxy stearate, thorn A Ganshu benevolence oil, dipentaerythritol hexahydroxy
The mixture of stearate, six stearates and six rosinates, two octanoic acid of diisooctadecanol malate and propylene glycol
Ester, two certain herbaceous plants with big flowers acid esters, rice bran oil and tocotrienols mixture be heated to 90 DEG C, 80 DEG C are cooled to after being completely melt it, is obtained
To A phase；
(2) draw oronain hectorite, three isostearic acids different titanium dioxide, isononyl isononanoate, isopropyl myristate, department
The mixture of third oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid, red iron oxide, isononyl isononanoate, myristic acid
Isopropyl ester, department draw the mixture of oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid
With yellow iron oxide, isononyl isononanoate, isopropyl myristate, department draw oronain hectorite, three isostearic acid isopropyl oxygen titanium esters,
The mixture of propylene glycol carbonate and poly- hydroxy stearic acid is added in A phase, is dispersed with stirring uniformly until obtaining B entirely without particle
Phase；
(3) mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 is heated to 80 DEG C, stirred
Mixing is completely melt it, and the mixture of yeast extract and tioxolone, water and citric acid is then added, and continues insulated and stirred,
It is allowed to be wrapped up by the mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 completely, obtains C phase；
(4) C is added in B phase, is dispersed with stirring uniformly, then cool to 60 DEG C, glycerol caprylate and tocopherol is added
It is dispersed with stirring uniformly, it is filling up to the concealing stick.
Embodiment 2
Embodiment 2 is a kind of concealing stick with whitening, acne-removing, and ingredient and its content are shown in Table 1.This has beauty
The preparation method of white, acne-removing concealing stick the following steps are included:
(1) by synthetic wax 1, synthetic wax 2, beeswax, microwax, different tridecanol isononoate, glycerol three (thylhexoic acid) ester,
Neopentyl glycol dicaprate, octyl dodecanol stearoyl-oxy stearate, thorn A Ganshu benevolence oil, dipentaerythritol hexahydroxy
The mixture of stearate, six stearates and six rosinates, two octanoic acid of diisooctadecanol malate and propylene glycol
Ester, two certain herbaceous plants with big flowers acid esters, rice bran oil and tocotrienols mixture be heated to 95 DEG C, 85 DEG C are cooled to after being completely melt it, is obtained
To A phase；
(2) draw oronain hectorite, three isostearic acids different titanium dioxide, isononyl isononanoate, isopropyl myristate, department
The mixture of third oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid, red iron oxide, isononyl isononanoate, myristic acid
Isopropyl ester, department draw the mixture of oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid
With yellow iron oxide, isononyl isononanoate, isopropyl myristate, department draw oronain hectorite, three isostearic acid isopropyl oxygen titanium esters,
The mixture of propylene glycol carbonate and poly- hydroxy stearic acid is added in A phase, is dispersed with stirring uniformly until obtaining B entirely without particle
Phase；
(3) mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 is heated to 85 DEG C, stirred
Mixing is completely melt it, and the mixture of yeast extract and tioxolone, water and citric acid is then added, and continues insulated and stirred,
It is allowed to be wrapped up by the mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 completely, obtains C phase；
(4) C is added in B phase, is dispersed with stirring uniformly, then cool to 65 DEG C, glycerol caprylate and tocopherol is added
It is dispersed with stirring uniformly, it is filling up to the concealing stick.
Embodiment 3
Embodiment 3 is a kind of concealing stick with whitening, acne-removing, and ingredient and its content are shown in Table 1.This has beauty
The preparation method of white, acne-removing concealing stick the following steps are included:
(1) by synthetic wax 1, synthetic wax 2, beeswax, microwax, different tridecanol isononoate, glycerol three (thylhexoic acid) ester,
Neopentyl glycol dicaprate, octyl dodecanol stearoyl-oxy stearate, thorn A Ganshu benevolence oil, dipentaerythritol hexahydroxy
The mixture of stearate, six stearates and six rosinates, two octanoic acid of diisooctadecanol malate and propylene glycol
Ester, two certain herbaceous plants with big flowers acid esters, rice bran oil and tocotrienols mixture be heated to 100 DEG C, 90 DEG C are cooled to after being completely melt it, is obtained
To A phase；
(2) draw oronain hectorite, three isostearic acids different titanium dioxide, isononyl isononanoate, isopropyl myristate, department
The mixture of third oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid, red iron oxide, isononyl isononanoate, myristic acid
Isopropyl ester, department draw the mixture of oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid
With yellow iron oxide, isononyl isononanoate, isopropyl myristate, department draw oronain hectorite, three isostearic acid isopropyl oxygen titanium esters,
The mixture of propylene glycol carbonate and poly- hydroxy stearic acid is added in A phase, is dispersed with stirring uniformly until obtaining B entirely without particle
Phase；
(3) mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 is heated to 90 DEG C, stirred
Mixing is completely melt it, and the mixture of yeast extract and tioxolone, water and citric acid is then added, and continues insulated and stirred,
It is allowed to be wrapped up by the mixture of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 completely, obtains C phase；
(4) C is added in B phase, is dispersed with stirring uniformly, then cool to 70 DEG C, glycerol caprylate and tocopherol is added
It is dispersed with stirring uniformly, it is filling up to the concealing stick.
Embodiment 4-5
Embodiment 4-5 is a kind of concealing stick with whitening, acne-removing, and ingredient and its content are shown in Table 1.Implement
The preparation method of example 4-5 concealing stick is identical as the preparation method in embodiment 2.
Synthetic wax 1 used in embodiment 1-5 is the POLARWACHS30919 purchased from German TROMM company；Synthetic wax 2
For the POLARWACHS 30750 purchased from German TROMM company, rice bran oil, tocotrienols, propylene and two certain herbaceous plants with big flowers
Rice bran oil in the mixture of acid esters, tocotrienols, propylene and two certain herbaceous plants with big flowers acid esters mass ratio be rice bran oil: fertility
Trienol: propylene and two certain herbaceous plants with big flowers acid esters=50-75:9:25-50；In the mixture of yeast extract and tioxolone
The mass ratio of yeast extract and tioxolone is yeast extract: tioxolone=20-60:35-70；Jojoba esters, to
Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and gather sweet in the mixture of day sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3
The mass ratio of oil -3 is Jojoba esters: sunflower seed wax: Acacia decurrens floral wax and polyglycereol -3=50-75:25-50:1-5:1-
5；The raw material of any form of mixtures used in embodiment 1-5 is all the same.
Mass percent/% of each ingredient in 1 embodiment 1-5 concealing stick of table
Comparative example 1-6
Comparative example 1-6 is a kind of concealing stick, and ingredient and its content are shown in Table 2, the preparation methods of these concealing sticks with
And raw material is same as Example 2.
Mass percent/% of each ingredient in 2 comparative example 1-6 concealing stick of table
For illustrate it is described have effects that the concealing stick of whitening, acne-removing, carried out following test:
1, heat resistance detects
Constant incubator is adjusted in advance and arrives (45 ± 1) DEG C, sample is sloughed into cover and is all screwed out, constant temperature is vertically arranged in
It in incubator, takes out, restores to visual observations after room temperature afterwards for 24 hours, and sample wiped a little on the back of the hand, observing its usability
Energy.
Test result: embodiment 1-5 and comparative example 1-6 concealing stick be put into before constant incubator without obvious shape difference
It is different, illustrate that concealing stick of the present invention has good heat resistance.
2, cold resistance detects
Refrigerator is adjusted to -8 DEG C in advance, sample is placed in refrigerator, is taken out afterwards for 24 hours, it is after restoring to room temperature that sample is few
Perhaps it wipes on the back of the hand, its service performance of visual observations.
Test result: embodiment 1-5 and comparative example 1-6 concealing stick be put into before refrigerator without obvious shape difference, say
Bright concealing stick of the present invention has good cold resistance.
3, safety evaluatio
Test object: embodiment 1-5 and comparative example 1-6 concealing stick.
Test method: choose 20-45 years old healthy women 110, be randomly divided into 11 groups, every group of 10 people, every group uses respectively
A kind of sample.Select qualified spot tester that tested material about 0.020-0.025mL is placed in spot in enclosed type patch test method
Try device in, external application medical adhesive tape is pasted on subject back, remove tested material after 24 hours, after removing patch 0.5h,
Dermoreaction is observed with 48h for 24 hours.
2 skin adverse reaction grading standard of table
Test result: 0 there is positive reaction in 110 people, this explanation, and concealing stick safety of the present invention will not cause skin
Adverse reaction.
4, white-skinned face function is evaluated
Test object: embodiment 1-5 and comparative example 1-6 concealing stick.
Test method: choose 20-45 years old healthy women 110, be randomly divided into 11 groups, every group of 10 people, every group uses respectively
A kind of sample.Sample is applied to the left arm Medial upper arm of subject, right arm is blank control.It uses
DelfinSkinColorCatch (Finland) test equipment measures variation (Δ L*) and the ITA degree of colour brightness, L* in the present invention
Being worth (brightness) and ITA degree (color individual type angle) is main indicator, and wherein ITA degree represents coloration entire change situation, ITA °
Value is bigger, and the colour of skin is more shallow.(Δ L*) and ITA degree calculation formula are as follows:
Δ L*=[L* (reference examples or embodiment product carry out after testing 1 month)-L* (before carrying out on-test)]-[L*
(after blank product carries out test 1 month)-L* (before carrying out on-test)]；
Every cell mean；
Every cell mean.
Test result: 3 are shown in Table.
3 whitening effect test result of table
5, acne-removing is evaluated
Acne-removing evaluation is carried out using the inhibition test of propionibacterium acnes.
(1) test specimen
Embodiment 1-5 and comparative example 1-6 concealing stick and 3 groups of propionibacterium acnes bacterial strain (separate at patients with acne skin lesion
To).
(2) test method
1. the culture of anaerobic bacteria, separation, identification: THl0 culture will be inoculated in by isolated sample at patients with acne skin lesion
In base, with airbag method, 37 DEG C of culture 72h in anaerobic jar are placed in, indicator are made with methylene blue, palladium grain is catalysis thorn.
2. the separation of anaerobic bacteria
Picking single bacterium colony turns 2 pieces of plates, and one piece is placed in anaerobic jar, the lower 37 DEG C of pure cultures of anaerobic condition；Another piece with
37 DEG C of aerobic cultures；Result is observed after 48h.
3. the identification of anaerobic bacteria
Without bacterial growth under aerobic culture；Occur uniform form, canescence, tiny, diameter on the plate of Anaerobic culturel about
Bacterium colony is made microscopy, visible chromabacterium biolaceum under mirror by the slightly neat bacterium colony in the circle of 1.0mm protrusion, edge.Micro-bend is in rodlike or bar
Shape, can one end blunt circle, one end attenuates, and coloring is not deep, cell be it is single, can arrange or arrange in pairs is the shapes such as " people ", " v ".Again
It is propionibacterium acnes through oxytolerant test, catalase test, indole test, biochemical serial test for identification.
4. anaerobism drug sensitive test
Strain inoculated: 1 colony inoculation in the bacterium colony more than picking cultivated is on LB plating medium, 37 DEG C of aerobic trainings
It supports for 24 hours, by aerobic culture, propionibacterium acnes are rinsed with sterile saline for 24 hours, and flushing liquor is put into sterile test tube；Using wheat
Family name's turbidimetry is than turbid, and opacity tube is with shaking 12 times is before needed, first than turbid to 3 × 108/ mL, then with normal saline dilution to 106/ mL is standby
With.
The inoculation of LB plating medium: dipping bacterium solution for the swab stick of sterilizing, goes extra bacterium solution in squeezing on tube wall, trains in LB plate
Even spread on base is supported, and sweeps a circle along plate edge ring, covers plate, dry 2min.Sterile steel bowl (diameter 6mm) is light
It is put on plating medium, fills it up with concealer, be put into 37 DEG C of aerobic cultures for 24 hours, without bacterial growth in discovery plate, continue 37 DEG C
Aerobic culture is shown in have inhibition zone to be formed for 24 hours afterwards.Antibacterial circle diameter is surveyed, 3 groups of antibacterial circle diameter values are averaged.
Antibacterial susceptibility grade classification: inhibition zone diameter>20mm be Gao Min, 10-20mm be in it is quick,<10mm is drug resistance.
(3) test result
The results are shown in Table 4 for specific observation.
The antibacterial test result of 4 propionibacterium acnes of table
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of concealing stick with whitening, acne-removing, it is characterised in that: the concealing stick includes functional component 1 and effect
Ingredient 2；The functional component 1 is the mixture of rice bran oil, tocotrienols, propylene and two certain herbaceous plants with big flowers acid esters, accounts for institute
State the 0.5-6% of concealing stick quality, the rice bran oil, tocotrienols, propylene and two certain herbaceous plants with big flowers acid esters mass ratio
For rice bran oil: tocotrienols: propylene and two certain herbaceous plants with big flowers acid esters=50-75:9:25-50；The functional component 2 is ferment
The mixture of female extract and tioxolone, the 0.5-8% of Zhan Suoshu concealing stick quality, the yeast extract and tioxolone
Mass ratio be yeast extract: tioxolone=20-60:35-70.
2. concealing stick according to claim 1, it is characterised in that: the functional component 1 accounts for the concealing stick quality
3%, the functional component 2 accounts for the 4% of the concealing stick quality.
3. concealing stick according to claim 1 or 2, it is characterised in that: the concealing stick also includes skin sense improver and water,
The skin sense improver be Jojoba esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 mixture, the Jojoba
Esters, sunflower seed wax, Acacia decurrens floral wax and polyglycereol -3 mass ratio be Jojoba esters: sunflower seed wax: Acacia decurrens flower
Wax and polyglycereol -3=50-75:25-50:1-5:1-5.
4. concealing stick according to claim 3, it is characterised in that: the skin sense improver accounts for the 1- of the concealing stick quality
6%, the water accounts for the 0.5-8% of the concealing stick quality.
5. concealing stick according to claim 4, it is characterised in that: the skin sense improver accounts for the concealing stick quality
3%, the water accounts for the 2% of the concealing stick quality.
6. concealing stick according to claim 5, it is characterised in that: the concealing stick also includes to account for the concealing stick quality 1-
The colorant 3 of 25% colorant 1, the colorant 2 of 0.05-5% and 0.05-5%, the colorant 1 are titanium dioxide, different nonyl
The different nonyl ester of acid, isopropyl myristate, department draw oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and gather
The mixture of hydroxy stearic acid, colorant 2 are red iron oxide, isononyl isononanoate, isopropyl myristate, department's drawing oronain water
Pyroxene, three isostearic acid isopropyl oxygen titanium esters, propylene glycol carbonate and poly- hydroxy stearic acid mixture, colorant 3 be yellow oxygen
Change iron, oronain hectorite, three isostearic acid isopropyl oxygen titanium esters, carbonic acid the third two draw in isononyl isononanoate, isopropyl myristate, department
The mixture of alcohol ester and poly- hydroxy stearic acid.
7. concealing stick according to claim 6, it is characterised in that: the concealing stick also includes thickener, adhesive, soft and moist
Agent, colorant dispersant, pH adjusting agent, preservative and antioxidant, the thickener include synthetic wax and beeswax, described adhesive
For microwax, the emollients include different tridecanol isononoate, glycerol three (thylhexoic acid) ester, neopentyl glycol dicaprate,
Octyl dodecanol stearoyl-oxy stearate, thorn A Ganshu benevolence oil and dipentaerythritol hexahydroxystearic acid ester, six are firmly
The mixture of resin acid ester and six rosinates, the colorant dispersant are diisooctadecanol malate, and the pH adjusting agent is
Citric acid, the preservative are glycerol caprylate, and the antioxidant is tocopherol.
8. concealing stick according to claim 7, it is characterised in that: by mass percentage, the concealing stick includes 2-
30% synthetic wax, the beeswax of 1-8%, the microwax of 1-10%, the different tridecanol isononoate of 1-15%, the glycerol of 1-15%
Three (thylhexoic acid) esters, the neopentyl glycol dicaprate of 2-25%, the octyl dodecanol stearoyl-oxy stearate of 1-15%,
The Ci Agan tree benevolence oil of 1-15%, dipentaerythritol hexahydroxystearic acid ester, six stearates and six rosinates of 1-6%
Mixture, the diisooctadecanol malate of 1-15%, the citric acid of 0.005-0.05%, the glycerol caprylate of 0.1-2%
With the tocopherol of 0.1-1%.
9. concealing stick according to claim 8, it is characterised in that: by mass percentage, the concealing stick includes 12%
Synthetic wax, 2% beeswax, 3% microwax, 12% different tridecanol isononoate, 10.39% three (ethyl hexyl of glycerol
Acid) ester, 9% neopentyl glycol dicaprate, 8% octyl dodecanol stearoyl-oxy stearate, 7% Ci Agan tree benevolence
Oil, the mixture of 2.5% dipentaerythritol hexahydroxystearic acid ester, six stearates and six rosinates, the two of 6% are different
Stearyl alcohol malate, 0.01% citric acid, 0.3% glycerol caprylate and 0.3% tocopherol.
10. the preparation method of the described in any item concealing sticks of claim 1-9, it is characterised in that: the preparation method include with
Lower step:
(1) thickener, emollients, adhesive, colorant dispersant and functional component 1 are heated to 90-100 DEG C, keep it completely molten
80-90 DEG C is cooled to after change, obtains A phase；
(2) it adds a colorant in A phase, is dispersed with stirring uniformly until obtaining B phase entirely without particle；
(3) felt improver is heated to 80-90 DEG C, stirring to being completely melt, be then added solvent, pH adjusting agent and effect at
Divide 2, continue insulated and stirred, wraps up it by skin sense improver completely, obtain C phase；
(4) C is added in B phase, is dispersed with stirring uniformly, then cool to 60-70 DEG C, preservative and antioxidant is added, stirs
It mixes and is uniformly dispersed to get the concealing stick.
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Cited By (3)
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| CN113662870A (en) * | 2021-06-21 | 2021-11-19 | 广州华淼生物科技研究院有限公司 | Cream water composition and preparation method thereof |
| CN114053160A (en) * | 2021-12-06 | 2022-02-18 | 上海大喂科技发展有限公司 | Concealer and preparation method thereof |
| CN114668690A (en) * | 2021-12-31 | 2022-06-28 | 浙江百姿化妆品股份有限公司 | Soft light concealer and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023036813A1 (en) * | 2021-09-10 | 2023-03-16 | Sabo S.P.A. | Blend of tocotrienols, natural oils and esters as additive for topical application |
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| CN113662870A (en) * | 2021-06-21 | 2021-11-19 | 广州华淼生物科技研究院有限公司 | Cream water composition and preparation method thereof |
| CN114053160A (en) * | 2021-12-06 | 2022-02-18 | 上海大喂科技发展有限公司 | Concealer and preparation method thereof |
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| CN114668690A (en) * | 2021-12-31 | 2022-06-28 | 浙江百姿化妆品股份有限公司 | Soft light concealer and preparation method thereof |
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| CN110192990B (en) | 2021-08-03 |
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