CN1099616C - 静电像显影用调色剂 - Google Patents
静电像显影用调色剂 Download PDFInfo
- Publication number
- CN1099616C CN1099616C CN96104500A CN96104500A CN1099616C CN 1099616 C CN1099616 C CN 1099616C CN 96104500 A CN96104500 A CN 96104500A CN 96104500 A CN96104500 A CN 96104500A CN 1099616 C CN1099616 C CN 1099616C
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- CN
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- Prior art keywords
- toner
- hydroxycarboxylic acids
- aromatic hydroxycarboxylic
- compound
- weight portion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/097—Plasticisers; Charge controlling agents
- G03G9/09783—Organo-metallic compounds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/097—Plasticisers; Charge controlling agents
- G03G9/09733—Organic compounds
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Developing Agents For Electrophotography (AREA)
Abstract
Description
电荷控制剂组合物 | 金属化合物(I)(重量份) | 金属化合物(II)(重量份) | 芳族羟基羧酸*(重量份) |
1 | 铝化合物1(45) | 铝化合物2(50) | DTBSA(5) |
2 | 铝化合物1(42) | 铝化合物2(50) | DTBSA(8) |
3 | 铝化合物1(48) | 铝化合物2(50) | DTBSA(2) |
4(对比) | 铝化合物1(30) | 铝化合物2(50) | DTBSA(20) |
5(对比) | 铝化合物1(49.5) | 铝化合物2(50) | DTBSA(0.5) |
6(对比) | 铝化合物1(95) | - | 3HN2CA(5) |
7(对比) | - | 铝化合物2(95) | 3HN2CA(5) |
8 | 铝化合物1(1) | 铝化合物2(94) | DTBSA(5) |
9 | 铝化合物1(94) | 铝化合物2(1) | DTBSA(5) |
10 | 铝化合物1(95) | - | DTBSA(5) |
11 | 铝化合物2(95) | DTBSA(5) | |
12 | 铝化合物3(95) | - | 3HN2CA(5) |
13 | 铝化合物4(95) | - | 5TOSA(5) |
14 | 铬化合物(95) | - | DTBSA(5) |
15 | 锌化合物(95) | - | DTBSA(5) |
兰绿色调色剂 | 常温/常温(23℃/60%) | ||||||||||
编号 | 凝聚性(%) | 开始阶段 | 10000张后 | ||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | |||
实施1例 2345678910111213 | 12310111213141516171819 | 7.78.18.310.111.311.410.710.912.110.310.211.011.0 | -25.0-25.5-23.8-25.4-24.9-24.5-23.0-30.2-27.8-30.3-25.9-24.9-29.0 | 1.721.711.741.681.651.661.701.521.681.581.711.671.66 | 0.80.70.80.80.91.01.01.21.11.01.02.01.0 | AAABBBBBBBBBB | -25.5-25.8-23.4-24.9-20.4-20.3-22.8-31.2-28.6-28.2-22.0-21.0-33.2 | 1.731.701.761.671.821.811.681.521.611.621.731.681.52 | 1.00.80.80.91.51.50.91.01.11.21.51.21.3 | AAABCCBBBBBCC | AAAAAAAAAAABA |
对比例123456 | 456789 | 11.511.711.912.222.423.8 | -26.8-25.5-26.4-26.4-25.4-24.9 | 1.701.691.651.681.691.70 | 0.90.90.91.01.21.4 | BBBBCC | -22.0-21.3-40.9-18.2-16.5-15.5 | 1.751.761.301.791.801.82 | 1.51.71.11.52.02.3 | CCCCCC | BBBBCC |
兰绿色调色剂编号 | 高温/高湿(30℃/80%) | |||||||||
开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施1例 2345678910111213 | 12310111213141516171819 | -24.1-24.5-22.3-24.6-23.0-22.0-22.3-26.2-23.2-24.1-19.2-22.0-26.0 | 1.741.721.781.681.661.631.681.621.701.651.781.751.73 | 0.90.80.90.90.81.01.01.21.01.11.11.31.2 | AAABBBBBBBBCC | -23.8-24.9-21.4-23.6-19.5-18.0-21.9-22.2-23.1-22.2-18.2-16.4-29.0 | 1.751.681.801.671.831.861.651.721.751.721.881.891.58 | 1.10.91.01.11.51.01.01.41.51.51.51.81.6 | AAABCCBBBBCCC | AAAABBAAAABBB |
对比例123456 | 456789 | -22.1-20.5-24.0-23.9-22.8-22.4 | 1.781.791.721.731.761.80 | 1.51.40.91.01.41.5 | CCABCC | -15.0-14.3-29.5-14.1-13.2-12.9 | 1.861.801.501.851.821.88 | 2.93.21.22.22.83.0 | DDCDDD | CCBCCC |
兰绿色调色剂 | 常温/低湿(23℃/10%) | |||||||||
开始阶段 | After 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施1例 2345678910111213 | 12310111213141516171819 | -26.1-26.5-25.5-26.2-25.2-24.9-25.4-31.2-28.8-31.2-24.0-25.0-29.2 | 1.701.661.701.651.701.721.671.511.681.561.701.681.68 | 0.70.80.60.80.91.01.11.10.60.91.00.80.9 | AAABBBBBBBBBB | -26.0-26.4-25.4-28.0-26.0-26.0-31.0-32.0-29.8-31.0-24.2-23.8-33.4 | 1.711.681.721.521.681.651.501.501.601.601.701.711.46 | 0.80.90.70.91.01.11.21.11.11.01.00.91.0 | AAACBBCBBBBBC | AAAAAAAAAAAAA |
对比例123456 | 456789 | -27.0-26.0-26.5-27.0-26.5-26.2 | 1.681.701.701.621.711.65 | 0.80.80.80.90.80.9 | BBBABB | -26.0-24.3-41.8-22.8-21.5-20.4 | 1.661.671.251.701.791.77 | 1.11.10.91.21.81.6 | BBCBCC | BBBBBB |
兰绿色调色剂 | 低温/低湿(15℃/10%) | |||||||||
开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施1例 2345678910111213 | 12310111213141516171819 | -28.0-28.6-27.8-26.5-26.4-27.2-26.4-32.0-29.0-32.0-25.0-25.0-30.0 | 1.681.671.671.671.651.661.681.501.681.551.701.701.65 | 0.50.60.50.80.91.00.90.80.90.60.70.70.8 | AAABBBBBBBBBB | -27.5-28.3-27.9-29.0-27.2-28.2-32.0-33.0-30.0-31.2-24.8-24.0-34.0 | 1.691.681.681.501.601.601.481.481.611.581.701.701.45 | 0.60.70.60.81.01.11.21.01.10.80.90.90.9 | AAACBBCCBBBBC | AAAAAAAAAAAAA |
对比例123456 | 456789 | -28.0-26.5-28.0-27.5-27.0-26.8 | 1.681.701.701.651.681.65 | 0.80.70.70.60.90.8 | BBBABB | -26.5-24.5-42.0-24.0-23.0-22.9 | 1.651.681.201.701.651.66 | 1.11.00.81.21.21.5 | BBCBBB | AAABBB |
聚合的兰绿色调剂编号 | 粒径分布** | 常温/常湿(23℃/60%) | |||||||||||
D4(μm) | ≤3.17μm(N%) | ≥10.08μm(V%) | 开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | |||||
实施18例 1920 | 123 | 6.26.36.3 | 13.813.713.9 | 3.63.73.6 | -24.5-25.0-23.2 | 1.731.721.75 | 0.80.70.8 | AAA | -25.0-25.2-23.0 | 1.731.701.76 | 1.00.80.8 | AAA | AAA |
对比例78910 | 4567 | 5.78.78.38.2 | 33.319.221.422.5 | 5.512.39.48.9 | -25.9-25.8-24.8-24.3 | 1.661.691.701.70 | 0.91.01.21.4 | BBBC | -40.1-17.7-16.0-15.0 | 1.301.781.811.82 | 1.11.52.02.3 | CCCC | BBCC |
聚合的兰绿色调色剂编号 | 高温/常温 | |||||||||
开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施18例 1920 | 123 | -23.6-24.0-21.8 | 1.741.731.77 | 0.90.80.9 | AAA | -23.5-24.4-21.0 | 1.741.671.79 | 1.10.91.0 | AAA | AAA |
对比例78910 | 4567 | -23.5-23.4-22.3-22.0 | 1.721.731.761.79 | 0.91.01.41.4 | ABCC | -29.0-13.6-12.7-12.4 | 1.511.841.811.87 | 1.22.22.73.1 | CDDD | BCCC |
聚合的兰绿色调色剂编号 | 常温/低湿 | |||||||||
开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施18例 1920 | 123 | -25.6-26.0-25.0 | 1.701.671.69 | 0.70.80.6 | AAA | -25.5-26.0-25.0 | 1.711.671.71 | 0.80.90.7 | AAA | AAA |
对比例78910 | 4567 | -26.0-26.5-26.0-25.7 | 1.691.621.701.64 | 0.80.90.80.9 | BABB | -41.2-22.2-21.0-19.9 | 1.241.701.781.78 | 0.91.21.81.6 | CBCC | ABBB |
聚合的兰绿色调剂编号 | 低温/低湿 | |||||||||
开始阶段 | 10000张后 | |||||||||
TC(mC/kg) | I.D. | 灰雾 | 强光 | TC(mC/kg) | I.D. | 灰雾 | 强光 | 散射 | ||
实施例181920 | 123 | -27.5-28.1-27.3 | 1.681.671.67 | 0.50.60.5 | AAA | -27.0-27.7-27.1 | 1.691.681.67 | 0.60.70.6 | AAA | AAA |
对比例78910 | 4567 | -27.5-27.0-26.3-26.3 | 1.701.641.681.65 | 0.70.60.90.8 | BABB | -41.5-23.5-22.5-22.4 | 1.211.701.651.66 | 0.81.21.21.5 | CBBB | ABBB |
Claims (19)
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP131189/1995 | 1995-05-02 | ||
JP131189/95 | 1995-05-02 | ||
JP13118995 | 1995-05-02 | ||
JP123921/1995 | 1996-04-23 | ||
JP123921/95 | 1996-04-23 | ||
JP12392196A JP3154088B2 (ja) | 1995-05-02 | 1996-04-23 | 静電荷像現像用トナー |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1138709A CN1138709A (zh) | 1996-12-25 |
CN1099616C true CN1099616C (zh) | 2003-01-22 |
Family
ID=26460712
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN96104500A Expired - Fee Related CN1099616C (zh) | 1995-05-02 | 1996-05-02 | 静电像显影用调色剂 |
Country Status (7)
Country | Link |
---|---|
US (1) | US5747209A (zh) |
EP (1) | EP0741337B1 (zh) |
JP (1) | JP3154088B2 (zh) |
KR (1) | KR0184326B1 (zh) |
CN (1) | CN1099616C (zh) |
DE (1) | DE69605476T2 (zh) |
HK (1) | HK1012064A1 (zh) |
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AU8897391A (en) * | 1990-12-12 | 1992-06-18 | Mitsubishi Kasei Corporation | Electrostatic image-developing toner |
JPH04347863A (ja) * | 1991-05-24 | 1992-12-03 | Mitsubishi Kasei Corp | 静電荷像現像用トナー |
SG49314A1 (en) * | 1991-11-08 | 1998-05-18 | Canon Kk | Monocomponent-type developer for developing electrostatic image and image forming method |
US5403690A (en) * | 1993-03-31 | 1995-04-04 | Ricoh Company, Ltd. | Developer for developing latent electrostatic images |
US5346795A (en) * | 1993-05-27 | 1994-09-13 | Xerox Corporation | Toner and developer compositions |
JP3028276B2 (ja) * | 1993-10-29 | 2000-04-04 | キヤノン株式会社 | 静電荷像現像用カラートナー,その製造方法及びカラー画像形成方法 |
US5397667A (en) * | 1994-04-28 | 1995-03-14 | Xerox Corporation | Toner with metallized silica particles |
US5547800A (en) * | 1994-06-06 | 1996-08-20 | Konica Corporation | Toner and electrophotographic image forming method using the same |
-
1996
- 1996-04-23 JP JP12392196A patent/JP3154088B2/ja not_active Expired - Fee Related
- 1996-04-30 DE DE69605476T patent/DE69605476T2/de not_active Expired - Lifetime
- 1996-04-30 EP EP96106821A patent/EP0741337B1/en not_active Expired - Lifetime
- 1996-04-30 US US08/640,077 patent/US5747209A/en not_active Expired - Lifetime
- 1996-05-02 CN CN96104500A patent/CN1099616C/zh not_active Expired - Fee Related
- 1996-05-02 KR KR1019960014190A patent/KR0184326B1/ko not_active IP Right Cessation
-
1998
- 1998-12-14 HK HK98113307A patent/HK1012064A1/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
HK1012064A1 (en) | 1999-07-23 |
EP0741337B1 (en) | 1999-12-08 |
US5747209A (en) | 1998-05-05 |
CN1138709A (zh) | 1996-12-25 |
KR960042243A (ko) | 1996-12-21 |
KR0184326B1 (ko) | 1999-04-15 |
JPH0922149A (ja) | 1997-01-21 |
EP0741337A1 (en) | 1996-11-06 |
DE69605476D1 (de) | 2000-01-13 |
JP3154088B2 (ja) | 2001-04-09 |
DE69605476T2 (de) | 2000-09-07 |
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Correction item: Second priority nianhao Correct: 123921/96 False: 123921/95 Number: 4 Page: 322 Volume: 19 Correction item: Inventor Correct: Just|takiguchi okado Kenji|Tian Ming Guzhen|rattan Tian Liang|God Lin Cheng|rice two|rice fields were|Katoo Ida Tetsuya|a constitutional|Valley letter False: Long Kougang|Kenji Okado|Masaaki Taya Number: 4 Page: 322 Volume: 19 |
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CI03 | Correction of invention patent |
Correction item: Second priority nianhao Correct: 123921/96 False: 123921/95 Number: 4 Page: The title page Volume: 19 Correction item: Inventor Correct: Just|takiguchi okado Kenji|Tian Ming Guzhen|rattan Tian Liang|God Lin Cheng|rice two|rice fields were|Katoo Ida Tetsuya|a constitutional|Valley letter False: Long Kougang|Kenji Okado|Masaaki Taya Number: 4 Page: The title page Volume: 19 |
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Free format text: CORRECT: INVENTOR; FROM: TAKIGUCHI OKATO MODESTY AKIRA MAKOTO TAYA TO: TAKIGUCHI OKATO MODESTY AKIRA MAKOTO TAYA HUZITA RIYOUITI CHENG HARUKO REACTIVE INABA IIDA YU KATO YIXIAN TETSUYA MINE LETTER VALLEY 123921/96 |
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