CN1092933C - Powdered sweetener composition for animal feed - Google Patents
Powdered sweetener composition for animal feed Download PDFInfo
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- CN1092933C CN1092933C CN96180383A CN96180383A CN1092933C CN 1092933 C CN1092933 C CN 1092933C CN 96180383 A CN96180383 A CN 96180383A CN 96180383 A CN96180383 A CN 96180383A CN 1092933 C CN1092933 C CN 1092933C
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- sweetener
- synergist
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Abstract
The present invention relates to a sweetening agent composition for animal feed, which is composed of an intimate mixture. The present invention has basically uniform non-statistic distribution of a sweetening agent/a synergistic agent, namely that the size of all the particles is basically constant and unchanged. The size of the particles of the sweetening agent composition is particularly from 10 to 100 mum and has Gaussian distribution. The sweetening agent composition is particularly useful for preparing feeds of animal offsprings, such as piglets. Under the condition of the present invention, the sweetening agent is saccharine salt, and the synergistic agent is neohesperidin dihydrochalcone (NHDC), thaumatin or glycyrrhizin.
Description
The invention relates to a kind of Powdered sweetener composition as animal feed, the feed that is used for making letting animals feed young baby such as piggy, calf and lamb is useful especially.Traditionally as the Powdered sweetener class of animal feed, forms by the statistic mixture of two kinds of powder of variable grain size, that is form by the sweet taste powder of relative big particle and than the mixture of the synergist of fine powdered.Sweetener also can provide the material of sweet taste, and normally asccharin, or sodium saccharinate or calcium perhaps are other natural or artificial reinforcement sweetener sometimes.
Synergist has double action.The first, from its title as can be known, it has the effect that prolongs the sweet taste sensation, but when it did not exist, the time of sweet taste sensation was very short.A kind of good sweet taste synergist, for example traditional employed, can increase sweet taste sensation time about 50% to 80%.The another kind effect of synergist is not inessential, is the secondary or parasitic taste of sheltering sweetener, for example bitter taste of asccharin or its sodium salt or calcium salt, metallic taste etc.
Though the present invention also can be applicable to other young animal such as calf, lamb, kid, colt, fawn etc., specification of the present invention is for practical reason with for people understand herein the problem that proposes better, below we will address little swine rearing especially more.
For little pig, between weaning period, raise and consume essential optimization, so that make it easily carry out the transition to solid feed from breast milk.This stage can cause damage to the health of piggy, and is sick in order to prevent, feed need replenish to get rid of the medicine of peculiar smell sometimes.This is in order to stimulate the appetite of piggy, for example to supply with the food that contains sweetener it is eaten food as much as possible.The young animal misses potter confectionery, gets used to its breast milk edible.The porkling that for example grows and weaned in 28 days, 6.5 kilograms to 8 kilograms of body weight can be eaten the food of 200 grams to 300 gram grain shapes usually every day.Each mouth of piggy approximately can absorb 8 grams, promptly about 50 particles, and this is seldom.But piggy is from growing 8 days, just can be raised with pellet, gets used to its following food under the protection of sow gradually.Only eat 30 to 40 gram foods every day, this explanation is only eaten about 10 foods for every mouthful.Having or do not having under the medicine supplementary information, the fragrance food that its appetite can be passed through to be provided stimulates increase, and why this can get used to adding the particle of sweetener just gradually.These particles, weight are about 0.15 gram, and it is 1.5 centimetres with length that average diameter is 0.3 centimetre, be to be about 1/4 sweetener by weight to be dispersed in weight and to be about in 3/4 carrier or the matrix and to make, carrier can be a glucose, silica gel, the cereal of pulverizing or its bond.The ratio of asccharin and synergist is 100: 1-2 joins about 400 gram/tons (per metric ton gram number) of this mixture in the finished product feedstuff.
Obscure for avoiding any, below in the predicate of Shi Yonging, " sweetener " speech is meant a kind of sweetener/synergist mixture, it is purpose of the present invention, and with the traditional corresponding product of the usefulness of making comparisons, when suitable sweetener is dispersed in the carrier, will express with " sweet taste prescription " or " sweet taste pre-composition ".This sweet taste prescription is a kind of flavouring of mode such as human food's salt or capsicum pepper, joins in the last feed of feeding young pigs.
Some traditional sweeteners are by the statistic mixture of one or more sweeteners and one or more synergist, as noted earlier, have different granular sizes.Though careful making can make it idealized, can only obtain a kind of very big polyphasic mixture that has, and below this mixture is called " rough sweetener ".
This bigger inhomogeneities, only eat with each mouthful of piggy and to have absorbed the pellet of very few number, just the effect that causes brood to be felt, from flatly to another mouthful, may be very inequality (cause food consumption changeable): a bite feed has the sweet taste that is difficult to feel, and down a bite feed may be too sweet, perhaps when it is too dense owing to being difficult to cover the aftertaste of asccharin even can feeling bitter taste and metallic taste, although synergist is arranged.Based on the traditional sweet taste ingredients of rough sweetener,,, only obtained a little satisfaction because of not improving though be widely used in animal feeding.
Generally, with some related problems of use sweetener in the animal feed, be curious uncommon on document, we can utilize for example revealing of German patent DE-2029749, this document and purpose of the present invention are irrelevant, but because of it be about by one deck sweet substance and the formed nutriment of absorption and assimilation iron that contained.
The present invention has solved the problems referred to above, method for making is very simple, composition of the present invention is to have proposed a kind of powder sweetener as animal feed, be a kind of form of mixtures closely uniformly basically, sweetener/synergist with Organization of African Unity metering distributes, and wherein the ratio of sweetener and synergist all substantial constant is constant in all particles.
According to the present invention, best powder sweetener has granular size and is between Gaussian distribution (Gaussiandistribution) 10 μ m and the 100 μ m.And preferably the ratio of sweetener/synergist (class) is to be between 100: 0.2 and 100: 2 with the parts by weight expression.
As mentioned above with as described below, because to be substantial constant constant and a particle and another particle are equal-sized for the ratio of synergist and sweetener, so in the sweetener prescription, all be constant to its size of another particle from a particle, wherein sweetener is to be dispersed in the carrier, and is distributed in nutrition purposes, especially for feeding animals in the feed at last.
Can easily understand, under these conditions, when raising to piggy with its needed invariable sweet taste, with invariable sweetness intensities and distribution, to another mouthful feed taste no change, just can make the appetite of piggy be stimulated increase better from a bite feed.
Purpose of the present invention, yes in order to increase the economic benefit of immature letting animals feed, and specific energy is faster and put on weight more regularly mutually with all animals to allow it.
Be placed on the brood of sweetener of the present invention front, can take food, thereby more or less be effectively, and the weight of animals increase that can be more immature than the rough sweetener feed of edible same component is faster with better appetite.As a result, discarded object is less, from as can be seen following, compares with the rough sweetener of tradition, and this can use less sweetener in feed granules, and the sweet taste powder is generally fine powder form.
Really, this is one of the preferred embodiments of the present invention, and the powder that sweetener can a certain Gaussian distribution according to the present invention occurs, and average particulate diameter is between 10 μ m and the 100 μ m, contain every gram 65,000,000-85,000,000, for example better about 75,000,000 particle, and by contrast, asccharin is the 40-80 sieve mesh, particle size is 100-1000 μ m, and every gram only contains 50,000-700,000 particle, 60,000 particles of average out to.
Do so more economical, promptly to brood use more regular property feed and due to the fact that, promptly can use less sweetener to be used in feed granules and the last feed according to the sweet taste of wanting required for the present invention.
Mention sodium saccharinate or calcium and asccharin above and can be used as sweetener; and other sweetener is just like the aspartyl phenylalanine, and acetoacetate derivative (acesulfam) and cyclamate class (cyclamates) and stevioside (stevioside) are a kind of glucosides of natural source.
As synergist, the protein " thaumatin " that little pig feed can use a kind of plant source (thaumatin) and some glucoside class such as NHDC (neohesperidinedihydrochalcone, NHDC), glycyrrhizin etc., their independent or its mixtures.These materials can guarantee bigger sweet taste holdup time and the bitter taste and the metal aftertaste of sheltering asccharin and its esters.
Powder sweetener of the present invention also contains a spot of other composition such as flavor potentiator, sodium glutamate, ucleotides (Sodium Inosinate and guanylic acid sodium), blue or green bud phenol and ethyl malt powder etc., and various spices.These compositions are included in " microcomponent ", and microcomponent is to sneak in the middle formulation of feed or pre-composition, wherein also can contain the medical of various vitamins, trace element even preventive administration.The general consumption of these materials is the about 5-10kg of finished product feedstuff per ton.
Powder sweetener of the present invention, can be easy to preparation, can carry out for example " volume microminiaturization " or " pulverization " according to human food's known technology and the known technology in the spices production technology, that is in a proper device, liquid mixture atomizing and drying are become smalls.This device can adopt tower shape, therein liquid mixture is infeeded nozzle or the turbine from the top, and the powder that has atomized is collected in the bottom of tower mill.In some cases, if necessary, tower mill can charge into inert gas in case the oxidation effect takes place.
Powder sweetener of the present invention can two kinds of methods use when raising immature animal.The first, according to classical way, sweetener of the present invention is dispersed on the carriers such as cereal of glucose, silica gel or pulverizing, its consumption for example is the sweetener of 10 to 75 parts by weight and the carrier of 90 to 25 parts by weight.Based on virtual value, make a kind of finished product feedstuff, having mean dose is 200-600 gram/ton, preferred 400 gram/tons, this amount that is equivalent to sweetener is a 100-150 gram/ton, and based on mean dose 400 gram/tons and sweetener is a 1.2-1.8 gram/ton.Should be understood that sweetener of the present invention is a complete and homogeneous, the granular size of sweetener is enough thin, be not difficult to obtain being dispersed in the sweet taste preparaton on the carrier, thereby finished product feedstuff also is a complete and homogeneous.
The another kind of possible usage of the present invention is sweetener to be dissolved in raisings immature animal, particularly its consumption are 2-3 gram/ton in the feed water, and this sweetener powder is water miscible, dissolves without any difficulty.
The present invention can should be understood better by with reference to the following non-limiting embodiment.The back of these embodiment is some comparative example, so that fully disclose advantage of the present invention, its advantage is:
Regular constant sweet taste ability,
May add assistant by the constant amount of rule,
Good storage stability is arranged, be better than the stability of rough sweetener, form powder and have extremely different particle size because of two kinds of rough sweetener, prolong in time and be tending towards separating or precipitation.
Embodiment 1 to 10
In a vat, add 900 premium on currency and prepare solution A, be heated to 60 ℃ then, add the 1000kg sweetener then lentamente, solution is stirred 30 minutes up to dissolving (solution becomes transparent) fully by one or more sweet tastes.
Simultaneously, be filled with 100 premium on currency in a little cylinder, be heated to 70 ℃, synergist is slowly added wherein, its consumption is equivalent to the ratio of the sweetener/synergist of the sweetener that will prepare, and allows product dissolving 30 minutes then.
One or more synergist are joined in the sweet taste solution A lentamente.
When solution becomes when transparent, the drying process of in a king-post, spraying, its operating condition is as follows:
Solution temperature: 660 ℃
190 ℃ of the air themperatures that enters
100 ℃ of the air themperatures of emitting
Atomizing turbine rotating speed: 15,000rpm to 20,000rpm
The form of the sweetener of the present invention that obtains like this is trickle homogeneous powder, and it is 10-100 μ m that its particle grain size has Gaussian distribution, and average out to 58.5 μ m, every gram contain about 75,000,000 particle or particulate.This powder is water miscible.
The powder sweetener of Sheng Chaning has sweetener and synergist like this, proportionally can be expressed as follows by parts by weight:
Embodiment sweetener class synergy dose ratio
1 sodium saccharinate thaumatin 25/0.05
2 saccharinic acid calcium NHDC 25/0.3
3 sodium saccharinate glycyrrhizins 25/0.1
4 acetoacetate derivative NHDC 25/0.33
(Acesulfam)
5 sodium saccharinate/acetoacetate derivative NHDC 16/8/0.33
6 sodium saccharinate glycyrrhizins
NHDC 25/0.1/0.1
7 sodium saccharinate glycyrrhizins
Stevioside 25/0.1/2
8 sodium saccharinate NHDC
Thaumatin 25/0.2/0.02
9 sodium saccharinate NHDC/ maltol 25/0.33/0.2
10 sodium saccharinate NHDC/ ethyl maltol 25/0.33/0.1
Employed thaumatin is supplied with by Hays compounding ingredient company in embodiment 1 to 8, and its trade mark is Talin.
Comparative example 1 to 4
1. measure the rough sweetener of 40/80 sieve mesh (reference) sample, and with sweetener of the present invention, the sweetener of promptly using above-mentioned " microminiaturized pulverization " process to make is contrasted.
With substantially the same density, that is be 1.5692 gram/cubic centimetres and according to the sample of the present invention 1.5270 gram/cubic centimetres of embodiment 1 to the reference sample, we observe, the every gram of sample of the present invention contains 75,563,288 particulates, and the every gram of reference sample only contains 58,760 particulates.
2. with the rough sweetener of 40/80 sieve mesh of above-mentioned comparative example, make comparisons with the fine sweetener of the first preparation method embodiment 1 with other, these two kinds of sweeteners are same particulate charge.From each batch, arbitrarily take out the particle of same number then.Use high-performance liquid chromatography analysis then separately, use water as 0.1 dilution that restrains, after centrifugal extraction, seek the spectrum peak of sodium saccharinate at per 500 microlitres.
The result is shown in the following table, is their concentration of respectively composing the area at peak and representative about the asccharin hydrochlorate.The spectrum honeybee has clearly been pointed out the very big greatly different inconsistency that has of in comparative sample asccharin hydrochlorate, some sample even do not contain the asccharin hydrochlorate fully.
And sample spectra honeybee of the present invention also indicates, and the saccharinic acid salt distribution has good homogeneity in the sweetener of embodiment 1.
| Asccharin sample of the present invention | Has 40-80 sieve mesh asccharin sample | |
| Observation # area | Observation # area | |
| 1 7870 2 6525 3 7355 4 7082 5 7071 6 8286 7 7174 8 8695 9 6783 10 7792 11 7109 12 7387 | 1 12547 2 33570 3 7215 4 43265 5 4694 6 32594 7 13146 8 34395 9 7254 10 44125 11 4761 12 33147 |
In distributing, asccharin have 33% of 78% observation not contain asccharin
22% of homogeneity observation has average area 33000
11% of observation has average area 43000
11% of observation has average area 12000
11% of observation has average area 7000
11% of observation has average area 5000
Conclusion: the great changes on area are said
Bright shortage definition, i.e. asccharin
Skewness one.
3. the sweetener of the rough sweetener of reference and the embodiment of the invention 1 being contrasted, is to observe in sow wean process by means of two batches of piggys, is to observe in the 19th day to the 23rd day 5 days of being born.The reference piggy is feeds utilized to be the feed of the Palatone trade mark sold by Pancosma company.The other piggy is also supplied with identical Palatone board feed, but contains sweetener of the present invention, rather than uses rough sweetener.The appended Fig. 1 in back is that the mean consumption that is illustrated in these piggys in 5 days changes, and restrains number 5 days every day.Curve below among the figure is the rough reference sweetener of representative, and top curve is a representative sweetener of the present invention.
Can find out immediately, raise to some piggys of the feed that contains sweetener of the present invention are edible and absorbed more food, absorb less feed and raise to some piggys of the feed that contains rough sweetener are edible.Thereby the forward part piggy has increased more body weight.
4. be used to prepare again from the commodity Palatone feed of front comparative example (rough sweetener) with Palatone and sweetener of the present invention, the latter and rough sweetener are made comparisons, some piggys according to freely selecting test, are promptly observed in sow wean process in 4 days situations of 19 days to the 22nd day of piggy growth regulation.The accompanying drawing 2 of back is the differentiation situation that is illustrated in these piggys preferences in 4 days processes.Curve below among the figure is represented the rough sweetener of reference, and top curve is represented sweetener of the present invention.
Can find out have 80% piggy preference to contain the feed of sweetener of the present invention immediately, this preference is by descending to some extent these days, but keeps obviously and be stabilized in 60%, and only accounts for 40% for rough sweetener feed.
Claims (9)
1. the Powdered sweetener that is used for animal feeding, it is characterized in that it is a kind of immixture, have and be essentially homogeneous, non-statistical, sweetener/synergist distribution, wherein the ratio of sweetener and synergist is invariable basically, and this ratio equates in a powder and another powder, feature is that also it has the powder size for 10-100 μ m, has Gaussian distribution.
2. sweetener as claimed in claim 1 is characterized in that the ratio of sweetener/synergist represents it is to be in 100 with parts by weight: 0.2-100: in 2 the scope.
3. sweetener as claimed in claim 1 or 2 is characterized in that this sweetener is to be selected from as next group: sodium saccharinate or calcium, asccharin; the aspartyl phenylalanine, acetoacetate derivative, cyclamate class; and stevioside, and their mixture.
4. sweetener as claimed in claim 1 or 2 is characterized in that synergist is to be selected from as next group: comprise thaumatin, NHDC (NHDC), glycyrrhizin, and their mixture.
5. sweetener as claimed in claim 1 or 2 is characterized in that it also includes the additive composition, is selected from flavor potentiator class and perfumery.
6. the preparation method of any one described sweetener preparation as in above-mentioned each claim is characterized in that preparing the mixture of the solution of a kind of sweetener and a kind of synergist, this mixture is pulverized by spray-drying obtained a kind of powder then.
7. particle sweet taste feed formulation, it is characterized in that it contains any one described sweetener of claim 1 to 5, sweetener is to be scattered on the carrier of cereal of glucose, silica gel or pulverizing, and its consumption is the carrier that the sweetener of 10 to 75 weight portions is used for 90 to 25 weight portions.
As sweet taste feed formulation as described in the claim 7 in the application aspect the letting animals feed young baby feed.
As any one described Powdered sweetener of claim 1 to 5 in the application aspect the letting animals feed young baby, be that it is dissolved in the drinking water, its consumption is every liter of drinking water 2 to 3 gram.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96180383A CN1092933C (en) | 1996-07-19 | 1996-07-19 | Powdered sweetener composition for animal feed |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96180383A CN1092933C (en) | 1996-07-19 | 1996-07-19 | Powdered sweetener composition for animal feed |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1224336A CN1224336A (en) | 1999-07-28 |
| CN1092933C true CN1092933C (en) | 2002-10-23 |
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ID=5127843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN96180383A Expired - Fee Related CN1092933C (en) | 1996-07-19 | 1996-07-19 | Powdered sweetener composition for animal feed |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1092933C (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2935084B1 (en) * | 2008-08-19 | 2011-05-06 | Pancosma Sa Pour L Ind Des Produits Biochimiques | ADDITIVE FOR ANIMAL FEED AND METHOD FOR PREPARING THE SAME |
| FR2935870B1 (en) * | 2008-09-16 | 2010-10-29 | Pancosma Sa Pour L Ind Des Pro | BI-AROMATISE ADDITIVE FOR ANIMAL FEEDING AND METHOD FOR PREPARING THE SAME |
| CN101558827B (en) * | 2009-02-18 | 2012-05-02 | 麦仑（厦门）生物科技有限公司 | Compound sweetening agent for producing feed by being combined with spray drying technology and preparation method thereof |
| CN102987331A (en) * | 2011-09-15 | 2013-03-27 | 上海美农生物科技股份有限公司 | Composite feed sweetening agent capable of rapidly producing sweet taste feeling, and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2185674A (en) * | 1986-01-23 | 1987-07-29 | Tate & Lyle Plc | Sweetening composition for farm animal rearing |
-
1996
- 1996-07-19 CN CN96180383A patent/CN1092933C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2185674A (en) * | 1986-01-23 | 1987-07-29 | Tate & Lyle Plc | Sweetening composition for farm animal rearing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1224336A (en) | 1999-07-28 |
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