CN109280580A - A kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof - Google Patents
A kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof Download PDFInfo
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- CN109280580A CN109280580A CN201811069999.XA CN201811069999A CN109280580A CN 109280580 A CN109280580 A CN 109280580A CN 201811069999 A CN201811069999 A CN 201811069999A CN 109280580 A CN109280580 A CN 109280580A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
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Abstract
The present invention relates to a kind of tealeaves baking Studies of The Aromatic Substances and the preparation method and application thereof, which includes the following steps: that step (1), raw material weigh；Step (2) extracts tealeaves baking perfumery.The present invention can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance, obtain pure baking perfume (or spice) note substance.After tealeaves of the invention bakes Studies of The Aromatic Substances wiring solution-forming, a certain amount of isobide is added, for various cigarette materials, so that cigarette is improved with material humid keeping performance, while the baking fragrance and suction mouthfeel of cigarette can be improved, the baking perfume (or spice) quality of tobacco product can effectively be improved, miscellaneous tolerance is reduced, the comfort and harmony of cigarette are improved, preparation method is easy to operate, product safety is with a wide range of applications.
Description
Technical field
The present invention relates to a kind of preparation method for toasting Studies of The Aromatic Substances, especially a kind of preparation side of tealeaves baking Studies of The Aromatic Substances
Method further relates to the tealeaves obtained by the preparation method baking Studies of The Aromatic Substances and its application, belongs to smoking material field.
Background technique
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research
Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing,
The note for enriching red date extract to a certain extent increases the content of flavor component.Utilize the common volume such as malt extract
It is fragrant to increase flue gas baking for cigarette additive.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still contains
There are the macromolecular substances such as a certain amount of protein, pectin, polysaccharide, these substances can crack generation during cigarette is burnt and sucked
Harmful components, increase cigarette smoking irritation and miscellaneous gas.
Tealeaves is one of maximum beverage of world today's consumption figure, it and coffee, cocoa simultaneously claim the world three big non-wine
Smart beverage.Tea from wild into people's artificial cultivation epoch, by the mankind as health care, prevent and cure diseases and apply.And with
The development and people of society constantly improve the raising that the effect of tea recognizes.Tealeaves is as the important drink in people's daily life
Product are liked by consumer with the quality and pleasant sense organ flavor of its health, are widely used.
Currently, after fragrance is used for various smoking materials, although aesthetic quality obtains a degree of promotion, flavoring
Deficiency is still remained in terms of material humectation afterwards, how to guarantee that material also can guarantee material humectation while aesthetic quality is promoted
Property, it is urgent problem.
Summary of the invention
A kind of simple, at low cost, tealeaves baking Studies of The Aromatic Substances is prepared in order to solve the above technical problem, the present invention provides a kind of
And the preparation method and application thereof.Concrete scheme of the invention is as follows:
A kind of preparation method of tealeaves baking Studies of The Aromatic Substances, characterized by the following steps:
Step (1), raw material weigh
Raw material is weighed by following weight point: 10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder；
Step (2) extracts tealeaves baking perfumery
The raw material of step (1) is added to the container, the polyalcohol and 0.01~1 part of weight of 100~500 parts of parts by weight is then added
The magnesium ion complex of part stirs evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths, is then added 200~2000
The solvent supersonic of parts by weight extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4~15min, takes supernatant liquid
It after organic membrane filtration, is evaporated under reduced pressure, solvent is removed and toasts perfumery to get to tealeaves.
Further, in step (1), the green tea is one of Xihu Longjing Tea, Xinyang Maojian Tea and Pilochun (a green tea) or more
Kind；The black tea is one of Keemun black tea, Yunnan black tea and Yixing black tea or a variety of；The dark green tea is Pu'er tea, Sichuan
One of dark green tea and Hunan dark green tea are a variety of.
Further, in step (2), the polyalcohol is one of ethylene glycol, propylene glycol, glycerol or a variety of.
Further, in step (2), the magnesium ion complex is magnesium tartrate ionic complex or ethylenediamine tetrem
Sour magnesium ion complex.
Further, in step (2), the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, acetic acid
One of ethyl ester and methyl acetate are a variety of.
Further, in step (3), the atomized liquid is propylene glycol or glycerol.
The invention further relates to the obtained tealeaves of above-mentioned preparation method toast Studies of The Aromatic Substances.
The invention further relates to utilization of the above-mentioned tealeaves baking Studies of The Aromatic Substances in tobacco aromaticss, be carried out as follows:
Tealeaves baking Studies of The Aromatic Substances is dissolved in solvent, the solution that mass percent is 0.5%~1% is configured to, is added later
Tealeaves bake 0.5~1 times of Studies of The Aromatic Substances quality isobide, be stirred at room temperature to dissolution mixing it is uniform, be placed in and be protected from light shady place
Refine 24~48h, solution after alcoholization is then sprayed on pipe tobacco, expanded cut tobacco or volume by 1%~3% ratio uniform of its weight
Cigarette obbbin surface.
Further, the tealeaves baking Studies of The Aromatic Substances is dissolved in solvent, and the solvent is in alcohol, propylene glycol or glycerol
One kind.
Further, 20-30min is stirred at room temperature.
Compared with the existing technology, the present invention have with the utility model has the advantages that
(1) tealeaves of the invention is in specific modulated process, it will the substance that distinctive tealeaves toasts fragrant note is generated, to it
Product carries out targeting extraction to it using certain solvent, can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance,
Obtain pure baking perfume (or spice) note substance.
(2) after tealeaves of the invention bakes Studies of The Aromatic Substances wiring solution-forming, a certain amount of isobide is added, for various cigarette objects
On material, so that cigarette is improved with material humid keeping performance, while the baking fragrance and suction mouthfeel of cigarette, Ke Yiyou can be improved
The baking perfume (or spice) quality of the raising tobacco product of effect, reduces miscellaneous tolerance, improves the comfort and harmony of cigarette, preparation method behaviour
Make simply, product safety is with a wide range of applications.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.In the examples where no specific technique or condition is specified, described technology or item according to the literature in the art
Part is carried out according to product description.Reagents or instruments used without specified manufacturer is that can be obtained by purchase
Conventional products.The sensory evaluation of all embodiments is all carried out according to GB5606.4-2005.
Embodiment 1
The preparation method of the tealeaves baking Studies of The Aromatic Substances of the present embodiment, is carried out as follows:
By 10 parts of Xihu Longjing Tea, 1 part of Keemun black tea, 5 parts of Pu'er tea, 100 parts of ethylene glycol, 0.01 part of magnesium tartrate ionic complex
Round-bottomed flask stirring is added, flask mouth connects condenser pipe, is put into oil bath heating later to 150 DEG C of condensing reflux 3h.
200 parts of petroleum ethers are added in above-mentioned reaction product, then ultrasonic extraction 60min shakes after extracting 60min, into
Row centrifuge separation 15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed to get needed for
Tealeaves toast Studies of The Aromatic Substances.
0.5 part of tealeaves baking Studies of The Aromatic Substances is dissolved in alcohol, the solution that mass percent is 0.5% is configured to, is added 0.5 part
Isobide, 20min is stirred at room temperature, ingredient is dissolved to uniform solution, then by it in 1% ratio of pipe tobacco weight
Even application is on pipe tobacco surface to get the pipe tobacco fragrant to tealeaves baking.
By 1 sample of embodiment and blank tobacco sample (reference examples), and in constant-temperature constant-humidity environment (22 ± 1 DEG C of temperature, humidity
60 ± 2%) different time is balanced, surveys its moisture content, the results are shown in Table 1.
By the pipe tobacco that the baking of tealeaves made from embodiment 1 is fragrant, with the conventional humectant glycerol pipe tobacco of addition equal proportion with
And un-added blank pipe tobacco (reference examples), when (22 ± 1 DEG C of temperature, humidity 60 ± 2%) balances are different in constant-temperature constant-humidity environment
Between, its moisture content is surveyed, the results are shown in Table 1.As seen from table, the baking of tealeaves made from embodiment 1 fragrant pipe tobacco and blank pipe tobacco
It is close to originate moisture content, can all be reduced as the time increases moisture content, but embodiment sample moisture content is both greater than blank sample,
Simultaneously also greater than glycerol pipe tobacco, show that 1 sample of embodiment has good humectation effect.
Table 1
Above-mentioned pipe tobacco is prepared into cigarette 1 using the auxiliary material of 555 board cigarette.Shown by smokeing panel test: using prepared tealeaves
After toasting fragrant pipe tobacco, relatively original 555 board cigarette, 1 tealeaves of cigarette toasts note and protrudes, and irritation reduces, and comfort improves.
Smoking result is as shown in table 9.
Embodiment 2
The preparation method of the tealeaves baking Studies of The Aromatic Substances of the present embodiment, is carried out as follows:
3 parts of Xinyang Maojian Tea and Pilochun (a green tea) is 30 parts each, 2 parts of Yunnan black tea and Yixing black tea, Sichuan dark green tea and Hunan dark green tea is 25 parts each, second
Two pure and mild propylene glycol are 250 parts each, 1 part of addition round-bottomed flask of ethylenediamine tetra-acetic acid magnesium ion complex stirs, and flask mouth connects cold
Solidifying pipe, is put into oil bath heating to 250 DEG C of condensing reflux 0.5h later.
2000 parts of n-hexanes and chloroform are added in above-mentioned reaction product, wherein 1:1 is mixed by volume for n-hexane and chloroform
It closes, ultrasonic extraction 10min, then after concussion extraction 10min, 4min is centrifuged, takes supernatant liquid with organic filter membrane mistake
It after filter, is evaporated under reduced pressure, solvent is removed and toasts Studies of The Aromatic Substances to get to required tealeaves.
1 part of tealeaves baking Studies of The Aromatic Substances is dissolved in propylene glycol, the solution that mass percent is 1% is configured to, 0.5 is added later
Part isobide, be stirred at room temperature 30min to dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 48h.It then will be by swollen
3% ratio uniform of swollen pipe tobacco weight is sprayed on expanded cut tobacco surface to get the expanded cut tobacco fragrant to tealeaves baking.
By 2 sample of embodiment and blank expanded cut stem sample, in constant-temperature constant-humidity environment (22 ± 1 DEG C of temperature, humidity 60 ±
2%) different time is balanced, surveys its moisture content, the results are shown in Table 2.
It is swollen with the conventional humectant glycerol of addition equal proportion by the expanded cut stem that the baking of tealeaves made from embodiment 2 is fragrant
Swollen stem and un-added blank expanded cut stem sample are put down for (22 ± 1 DEG C of temperature, humidity 60 ± 2%) in constant-temperature constant-humidity environment
Weigh different time, surveys its moisture content, the results are shown in Table 2.As seen from table, the fragrant expansion stem of the baking of tealeaves made from embodiment 2
Silk and blank expanded cut stem sample starting moisture content are close, can all reduce as the time increases moisture content, but embodiment sample
Moisture content is both greater than blank sample, while also greater than glycerol expanded cut stem, showing that 2 sample of embodiment is imitated with good humectation
Fruit.
Table 2
Above-mentioned expanded cut stem is prepared into cigarette.
It is smoked panel test and is shown by the expanded cut stem comparison fragrant with tealeaves baking is not added with: the fragrant expansion of prepared tealeaves baking
Stem, baking note is dense, and miscellaneous gas significantly reduces, and harmony increases.Smoking result is as shown in table 9.
Embodiment 3
The preparation method of the tealeaves baking Studies of The Aromatic Substances of the present embodiment, is carried out as follows:
Xihu Longjing Tea and Xinyang Maojian Tea is 30 parts each, 2 parts of Yunnan black tea, 18 parts of Pu'er tea, 200 parts of glycerol, magnesium tartrate ion complex
0.1 part of addition round-bottomed flask stirring of object, flask mouth connect condenser pipe, are put into oil bath heating later to 200 DEG C of condensing reflux 1h.
1000 parts of ethyl acetate are added in above-mentioned reaction product, then ultrasonic extraction 30min shakes after extracting 30min,
4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get tea is arrived
Leaf toasts Studies of The Aromatic Substances.
0.7 part of tealeaves baking Studies of The Aromatic Substances is dissolved in alcohol, the solution that mass percent is 0.7% is configured to, is added 0.6 part
Isobide is stirred at room temperature 25min and is dissolved to uniform solution, stands 20h.
Then above-mentioned solution is sprayed on cigarette bobbin paper surface by 2% ratio uniform of cigarette bobbin paper weight to get tea is arrived
The fragrant cigarette bobbin paper of leaf baking.
By 3 sample of embodiment and un-added blank cigarette bobbin paper sample, in constant-temperature constant-humidity environment (22 ± 1 DEG C of temperature,
Humidity 60 ± 2%) balance different time, its moisture content is surveyed, the results are shown in Table 3.
By the cigarette bobbin paper that the baking of tealeaves made from embodiment 3 is fragrant, rolled up with the conventional humectant glycerol of addition equal proportion
Cigarette obbbin and un-added blank cigarette bobbin paper sample are put down for (22 ± 1 DEG C of temperature, humidity 60 ± 2%) in constant-temperature constant-humidity environment
Weigh different time, surveys its moisture content, the results are shown in Table 3.As seen from table, the fragrant cigarette disk of the baking of tealeaves made from embodiment 3
Paper and blank cigarette bobbin paper sample starting moisture content are close, can all reduce as the time increases moisture content, but embodiment sample
Moisture content is both greater than blank sample, while also greater than glycerol cigarette bobbin paper, showing that 3 sample of embodiment is imitated with good humectation
Fruit.
Table 3
Above-mentioned cigarette bobbin paper is prepared into cigarette 3 using the tobacco leaf formulation and auxiliary material of Camel cigarette.Shown by smokeing panel test: being adopted
After the fragrant cigarette bobbin paper of prepared tealeaves baking, relatively original Camel cigarette, 3 tealeaves of cigarette toasts note foot, mouthfeel
Good, irritation reduces.Smoking result is as shown in table 9.
Comparative test 1
Comparative sample 1 prepares tealeaves baking Studies of The Aromatic Substances according to method in embodiment 1, but magnesium ion cooperation is added without in preparation process
Object detects tealeaves in comparative sample 1 and embodiment 1 respectively and toasts the macromoleculars content such as protein, pectin and polysaccharide in Studies of The Aromatic Substances.By
Table 4 is it is found that the macromoleculars content appearance such as protein, pectin and polysaccharide is bright in tealeaves baking Studies of The Aromatic Substances after addition magnesium ion complex
It is aobvious to reduce.
Table 4
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 1 | 0.2% | 30 | 24 |
| Embodiment 1 | 0 | 0 | 0.2 |
Simultaneously according to 1 middle period of embodiment group and accessory formula, it is prepared into cigarette control cigarette 1.Shown by smokeing panel test: opposite to implement
1 cigarette 1 of example, control cigarette 1 has certain tealeaves baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is poor.
Comparative test 2
Comparative sample 2 prepares tealeaves baking Studies of The Aromatic Substances according to method in embodiment 1, but magnesium ion complex is changed in preparation process
Magnesium chloride, detects in comparative sample 2 and embodiment 1 that the macromoleculars such as protein, pectin and polysaccharide contain in tealeaves baking Studies of The Aromatic Substances respectively
Amount.As shown in Table 5, the macromoleculars content such as protein, pectin and polysaccharide in Studies of The Aromatic Substances is toasted using tealeaves after magnesium ion complex
It is substantially reduced.
Table 5
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 2 | 0.3% | 28 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
Simultaneously according to 1 middle period of embodiment group and accessory formula, it is prepared into cigarette control cigarette 2.Shown by smokeing panel test: opposite to implement
1 cigarette 1 of example, control cigarette 2 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Comparative test 3
Comparative sample 3 prepares tealeaves baking Studies of The Aromatic Substances according to method in embodiment 1, but reaction temperature is 120 DEG C, detection pair respectively
The macromoleculars content such as protein, pectin and polysaccharide in Studies of The Aromatic Substances is toasted than tealeaves in sample 3 and embodiment 1.As shown in Table 6, implement
The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in 1 tealeaves of example baking Studies of The Aromatic Substances.
Table 6
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 3 | 0.3% | 22 | 15 |
| Embodiment 1 | 0 | 0 | 0.2 |
Simultaneously according to 1 middle period of embodiment group and accessory formula, it is prepared into cigarette control cigarette 3.Shown by smokeing panel test: opposite to implement
1 cigarette 1 of example, control cigarette 3 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is poor.
Comparative test 4
Comparative sample 4 prepares tealeaves baking Studies of The Aromatic Substances according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects respectively
The macromoleculars content such as protein, pectin and polysaccharide in tealeaves baking Studies of The Aromatic Substances in comparative sample 4 and embodiment 1.As shown in Table 7, real
The macromoleculars content such as protein, pectin and polysaccharide in 1 tealeaves of example baking Studies of The Aromatic Substances is applied to be substantially reduced.
Table 7
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 4 | 0.5% | 32 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
Simultaneously according to 1 middle period of embodiment group and accessory formula, it is prepared into cigarette control cigarette 4.Shown by smokeing panel test: opposite to implement
1 cigarette 1 of example, control cigarette 4 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is poor.
Comparative test 5
Comparative sample 5 prepares tealeaves baking Studies of The Aromatic Substances according to method in embodiment 1, but ultrasonic extraction, concussion extraction and centrifugation divide
It is changed to carry out conventional extraction using separatory funnel from step, be detected in comparative sample 5 and embodiment 1 respectively in tealeaves baking Studies of The Aromatic Substances
The macromoleculars content such as protein, pectin and polysaccharide.As shown in Table 8,1 tealeaves of embodiment baking Studies of The Aromatic Substances in protein, pectin and
The macromoleculars content such as polysaccharide is substantially reduced.
Table 8
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 5 | 0.4% | 10 | 8 |
| Embodiment 1 | 0 | 0 | 0.2 |
Simultaneously according to 1 middle period of embodiment group and accessory formula, it is prepared into cigarette control cigarette 5.Shown by smokeing panel test: opposite to implement
1 cigarette 1 of example, control cigarette 5 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Sensory evaluating smoking's evaluation result in 9 embodiment 1-3 of table
| Sample | Fragrance | Harmony | Miscellaneous gas | Irritation | Pleasant impression |
| Reference examples | 25 | 5 | 9 | 16 | 21 |
| Isobide is not used in embodiment 1 | 28 | 4.5 | 8.5 | 16.5 | 21 |
| Embodiment 1 | 28.5 | 5.5 | 10 | 17 | 22 |
| Embodiment 2 | 28.5 | 6 | 10 | 16.5 | 22 |
| Embodiment 3 | 28 | 5.5 | 9.5 | 17 | 24 |
Using cigarette made from un-added blank tobacco sample as reference examples.Meanwhile isobide is not used in preparation process
Compounding, according to the method for embodiment 1, is prepared into cigarette.
As can be seen from Table 9, opposite 1 cigarette of embodiment, control cigarette tealeaves baking note is prominent without cigarette 1, comfort
Slightly poor, respiratory tract irritation does not have the reduction of embodiment 1 obvious.It compares tealeaves baking note to protrude, comfort is slightly good, respiratory tract
Irritation decreases, but obvious without the reduction of embodiment 1.
It is compounded in embodiment 1 without using isobide, cigarette obtained, sensory evaluating smoking in the case that other techniques are all the same
Coordination, undesirable in terms of miscellaneous gas, effect is also less than reference examples, it is seen then that isobide compounding effect is significant.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.
Claims (10)
1. a kind of preparation method of tealeaves baking Studies of The Aromatic Substances, characterized by the following steps:
Step (1), raw material weigh
Raw material is weighed by following weight point: 10~60 parts of green tea powder, 1~5 part of black tea powder and 5~60 parts of dark green tea powder；
Step (2) extracts tealeaves baking perfumery
The raw material of step (1) is added to the container, the polyalcohol and 0.01~1 part of weight of 100~500 parts of parts by weight is then added
The magnesium ion complex of part stirs evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths, is then added 200~2000
The solvent supersonic of parts by weight extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4~15min, takes supernatant liquid
It after organic membrane filtration, is evaporated under reduced pressure, solvent is removed and toasts perfumery to get to tealeaves.
2. preparation method according to claim 1, it is characterised in that: in step (1), the green tea be Xihu Longjing Tea,
One of Xinyang Maojian Tea and Pilochun (a green tea) are a variety of；The black tea be one of Keemun black tea, Yunnan black tea and Yixing black tea or
It is a variety of；The dark green tea is one of Pu'er tea, Sichuan dark green tea and Hunan dark green tea or a variety of.
3. preparation method according to claim 1, it is characterised in that: in step (2), the polyalcohol be ethylene glycol,
One of propylene glycol, glycerol are a variety of.
4. preparation method according to claim 1, it is characterised in that: in step (2), the magnesium ion complex is wine
Stone acid magnesium ion complex or ethylenediamine tetra-acetic acid magnesium ion complex.
5. preparation method according to claim 1, it is characterised in that: in step (2), the solvent is petroleum ether, just
One of hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate are a variety of.
6. preparation method according to claim 1, it is characterised in that: in step (3), the atomized liquid be propylene glycol or
Glycerol.
7. the tealeaves that the preparation method of one of claim 1-7 obtains toasts Studies of The Aromatic Substances.
8. utilization of the tealeaves baking Studies of The Aromatic Substances of claim 7 in tobacco aromaticss, it is characterised in that: be carried out as follows:
Tealeaves baking Studies of The Aromatic Substances is dissolved in solvent, the solution that mass percent is 0.5%~1% is configured to, is added later
Tealeaves bake 0.5~1 times of Studies of The Aromatic Substances quality isobide, be stirred at room temperature to dissolution mixing it is uniform, be placed in and be protected from light shady place
Refine 24~48h, then sprays solution after alcoholization by 1%~3% ratio uniform of pipe tobacco, expanded cut tobacco or cigarette bobbin paper weight
It is coated in pipe tobacco, expanded cut tobacco or cigarette bobbin paper surface.
9. application according to claim 8, it is characterised in that: the tealeaves baking Studies of The Aromatic Substances is dissolved in solvent, described
Solvent is one of alcohol, propylene glycol or glycerol.
10. application according to claim 8, it is characterised in that: 20-30min is stirred at room temperature.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109762706A (en) * | 2019-02-01 | 2019-05-17 | 福建绿色黄金生物科技有限公司 | A kind of tea wine composition, preparation method and applications |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR910006520B1 (en) * | 1989-03-07 | 1991-08-27 | 한국전매공사 | Falvorings for tobacco and preparing method thereof |
| CN1451323A (en) * | 2002-04-12 | 2003-10-29 | 中国农业大学 | Biologic enzyme treatment method for promoting natural alcoholization of re-flue-cured tobacco |
| CN101323817A (en) * | 2008-07-29 | 2008-12-17 | 红云烟草(集团)有限责任公司 | Cooked puerh tea essential oil, preparation and use thereof |
| CN102726829A (en) * | 2012-07-04 | 2012-10-17 | 上海烟草集团有限责任公司 | Method for assisting in reducing pectin content of tobacco stalks by using microwaves |
| CN102793265A (en) * | 2012-09-13 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette |
| CN105199848A (en) * | 2015-09-07 | 2015-12-30 | 郑小柏 | Method for preparing flavor substance |
| CN105266190A (en) * | 2014-07-09 | 2016-01-27 | 江西中烟工业有限责任公司 | A humectant capable of improving the physical moisture retention performance of expanded cut tobacco and a preparing method thereof |
| CN106880077A (en) * | 2017-04-10 | 2017-06-23 | 山东烟草研究院有限公司 | A kind of tobacco stalk processing method for lifting papermaking-method reconstituted tobaccos quality |
-
2018
- 2018-09-13 CN CN201811069999.XA patent/CN109280580A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR910006520B1 (en) * | 1989-03-07 | 1991-08-27 | 한국전매공사 | Falvorings for tobacco and preparing method thereof |
| CN1451323A (en) * | 2002-04-12 | 2003-10-29 | 中国农业大学 | Biologic enzyme treatment method for promoting natural alcoholization of re-flue-cured tobacco |
| CN101323817A (en) * | 2008-07-29 | 2008-12-17 | 红云烟草(集团)有限责任公司 | Cooked puerh tea essential oil, preparation and use thereof |
| CN102726829A (en) * | 2012-07-04 | 2012-10-17 | 上海烟草集团有限责任公司 | Method for assisting in reducing pectin content of tobacco stalks by using microwaves |
| CN102793265A (en) * | 2012-09-13 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette |
| CN105266190A (en) * | 2014-07-09 | 2016-01-27 | 江西中烟工业有限责任公司 | A humectant capable of improving the physical moisture retention performance of expanded cut tobacco and a preparing method thereof |
| CN105199848A (en) * | 2015-09-07 | 2015-12-30 | 郑小柏 | Method for preparing flavor substance |
| CN106880077A (en) * | 2017-04-10 | 2017-06-23 | 山东烟草研究院有限公司 | A kind of tobacco stalk processing method for lifting papermaking-method reconstituted tobaccos quality |
Non-Patent Citations (1)
| Title |
|---|
| 肖协忠等: "《烟草化学》", 30 April 1997, 中国农业科技出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109762706A (en) * | 2019-02-01 | 2019-05-17 | 福建绿色黄金生物科技有限公司 | A kind of tea wine composition, preparation method and applications |
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