CN108968145A - A kind of tealeaves baking cigarette is with quick-fried pearl and preparation method thereof - Google Patents
A kind of tealeaves baking cigarette is with quick-fried pearl and preparation method thereof Download PDFInfo
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- CN108968145A CN108968145A CN201811070000.3A CN201811070000A CN108968145A CN 108968145 A CN108968145 A CN 108968145A CN 201811070000 A CN201811070000 A CN 201811070000A CN 108968145 A CN108968145 A CN 108968145A
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- fried pearl
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Engineering & Computer Science (AREA)
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- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention relates to a kind of tealeaves baking cigarette preparation methods of quick-fried pearl, include the following steps: step (1), preparation oil bath reactant；Step (2) extracts tealeaves baking perfumery；Step (3) prepares cigarette with quick-fried pearl.The present invention can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance, obtain pure baking perfume (or spice) note substance.Tealeaves baking Studies of The Aromatic Substances of the present invention is compounded with scutelloside, it can significantly reduce free-radical contents in flue gas, obtained cigarette is with quick-fried pearl while can also improve the baking fragrance of cigarette and aspirate mouthfeel, the baking perfume (or spice) quality of cigarette products can effectively be improved, reduce miscellaneous tolerance, the comfort and harmony for improving cigarette, can greatly improve the flavor and taste of abundant cigarette.
Description
Technical field
The present invention relates to a kind of cigarette preparation methods of quick-fried pearl, and in particular to a kind of preparation of quick-fried pearl of tealeaves baking cigarette
Method further relates to the tealeaves obtained by the preparation method baking cigarette with quick-fried pearl, belongs to cigarette auxiliary material field.
Background technique
Low tar high-quality cigarette has become the emphasis of current tealeaves research.However, necessarily adjoint while low tar
Cigarette flavor loss and comfort level be deteriorated.Country's cigarette product exists in terms of sucking quality and sense organ at present
It is certain insufficient, such as fragrance is faint, dry sensation is strong, sweet degree is inadequate, comfort level is poor.
Quick-fried pearl cigarette is to be pre-filled with one or more flavored capsules, smoker in filter tip to select in sucking process
Capsule is pinched quick-fried, release fragrance by selecting property.Quick-fried pearl is that cigarette assigns fragrant, flavouring humectation technology new way, is in category construction work
Effective support and cigarette brand rejuvenation of " can perceive ", personalized realization rate.
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research
Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing,
The note for enriching red date extract to a certain extent increases the content of flavor component.Utilize the common volume such as malt extract
It is fragrant to increase flue gas baking for cigarette additive.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still contains
There are the macromolecular substances such as a certain amount of protein, pectin, polysaccharide, these substances can crack generation during cigarette is burnt and sucked
Harmful components, increase cigarette smoking irritation and miscellaneous gas.
Tealeaves is disappeared as the important drink in people's daily life with the quality and pleasant sense organ flavor of its health
Expense person likes, is widely used.Therefore, how to apply to tealeaves, which improves cigarette, inhales on taste, is to be worth research.
Summary of the invention
In order to solve the above-mentioned technical problem, we attempt tea extract being used for cigarette in quick-fried pearl, provide a kind of tealeaves
Cigarette is toasted with the preparation method of quick-fried pearl, technical solution of the present invention is specific as follows:
A kind of tealeaves baking cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
Weigh 16-125 parts of tea raw materials, be added in round-bottomed flask, be then added 100-500 parts of polyalcohols and 0.01-1 parts of magnesium from
Sub- complex stirs evenly, and is condensed back 0.5~3h under 150~250 DEG C of oil baths to get oil bath reactant is arrived；
Step (2) extracts tealeaves baking perfumery
The solvent supersonic that 200~2000 parts by weight are added in the oil bath reactant extracts 10~60min, then concussion extraction
10~60min, then it is centrifuged 4~15min, after taking the organic membrane filtration of supernatant liquid, it is evaporated under reduced pressure, solvent is removed,
Obtain tealeaves baking perfumery；
Step (3) prepares cigarette with quick-fried pearl
Above-mentioned tealeaves baking perfumery is dissolved in water or Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 5%~15% is configured to,
0.5~1 times of the scutelloside that tealeaves bakes perfumery quality is added later, 20~30min is stirred at room temperature, is placed in and is protected from light shady place
Refine 24~48h, solution after alcoholization is prepared into dripping pill using pill dripping machine, collects molding dripping pill, is dried to get required tea is arrived
Leaf toasts fragrant cigarette with quick-fried pearl.
Further, the tea raw material is by 10~60 parts of green tea powders, 1~5 part of black tea powder and 5~60 parts of dark green tea powder
End composition.
Further, in step (1), the green tea is one of Xihu Longjing Tea, Xinyang Maojian Tea and Pilochun (a green tea) or more
Kind；The black tea is one of Keemun black tea, Yunnan black tea and Yixing black tea or a variety of；The dark green tea is Pu'er tea, Sichuan
One of dark green tea and Hunan dark green tea are a variety of.
Further, in step (2), the polyalcohol is one of ethylene glycol, propylene glycol, glycerol or a variety of.
Further, in step (2), the magnesium ion complex is magnesium tartrate ionic complex or ethylenediamine tetrem
Sour magnesium ion complex.
Further, in step (2), the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, acetic acid
One of ethyl ester and methyl acetate are a variety of.
Further, in step (3), the dripping pill diameter is 2.5~4.5cm.
The tealeaves obtained the invention further relates to above-mentioned preparation method toasts cigarette with quick-fried pearl.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) tealeaves of the invention is in specific modulated process, it will the substance that distinctive tealeaves toasts fragrant note is generated, to it
Product carries out targeting extraction to it using certain solvent, can remove the flue gases such as macromolecular substances irritation or miscellaneous gas substance,
Obtain pure baking perfume (or spice) note substance.
(2) tealeaves baking Studies of The Aromatic Substances of the present invention is compounded with scutelloside, can significantly reduce free-radical contents in flue gas, simultaneously also
The baking fragrance and suction mouthfeel that cigarette can be improved, can effectively improve the baking perfume (or spice) quality of cigarette products, reduce miscellaneous gas
Amount, improves the comfort and harmony of cigarette, can greatly improve the flavor and taste of abundant cigarette, while preparation method operates
Simply, product safety is with a wide range of applications.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.In the examples where no specific technique or condition is specified, described technology or item according to the literature in the art
Part is carried out according to product description.Reagents or instruments used without specified manufacturer is that can be obtained by purchase
Conventional products.The sensory evaluation of all embodiments is all carried out according to GB5606.4-2005.
Embodiment 1
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
By 15 parts of Xihu Longjing Tea, 3 parts of Keemun black tea, 5 parts of Pu'er tea, 120 parts of ethylene glycol, 0.01 part of magnesium tartrate ionic complex
Be added round-bottomed flask stir evenly, flask mouth connects condenser pipe, be put into later oil bath heating to 150 DEG C of condensing reflux 3h to get
To oil bath reactant.
Step (2) extracts tealeaves baking perfumery
300 parts of petroleum ethers are added in above-mentioned oil bath reactant, ultrasonic extraction 55min is carried out then after concussion extraction 50min
Centrifuge separation 15min carries out conventional vacuum distillation after taking the organic membrane filtration of supernatant liquid, solvent is removed to get arriving
Tealeaves toasts Studies of The Aromatic Substances.
Step (3) prepares cigarette with quick-fried pearl
5 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in water, the solution that mass percent is 5% is configured to, 2.5 parts of radix scutellariae is added later
Glycosides, it is uniform to dissolution mixing to be stirred at room temperature 20min, is placed in and is protected from light shady place alcoholization for 24 hours, using pill dripping machine by above-mentioned alcoholization
Solution afterwards is prepared into the dripping pill that diameter is 2.5cm, collects molding dripping pill, dries to get the cigarette fragrant to required tealeaves baking
With quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By be not added with the cigarette identical cigarette of quick-fried pearl
(using 555 cigarette), comparison, which is smoked panel test, to be shown: prepared cigarette toasts note with quick-fried pearl and protrudes, and irritation reduces, and comfort mentions
It is high.Smoking result is as shown in table 7.It is measured by flue gas free-radical contents using electron spin resonance, shows embodiment 1
Gained sample cigarette free-radical contents reduce 45%.
Embodiment 2
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
3 parts of Xinyang Maojian Tea and Pilochun (a green tea) is 25 parts each, 3 parts of Yunnan black tea and Yixing black tea, Sichuan dark green tea and Pu'er tea is 25 parts each, second two
Pure and mild propylene glycol is 240 parts each, 1 part of addition round-bottomed flask of ethylenediamine tetra-acetic acid magnesium ion complex stirs evenly, and flask mouth connects
Condenser pipe is put into oil bath heating to 250 DEG C of condensing reflux 0.5h to get to oil bath reactant later.
Step (2) extracts tealeaves baking perfumery
2000 parts of n-hexanes and chloroform are added in the oil bath reactant, wherein 1:1 is mixed by volume for n-hexane and chloroform
It closes, ultrasonic extraction 20min, then after concussion extraction 10min, 4min is centrifuged, takes supernatant liquid with organic filter membrane mistake
It after filter, is evaporated under reduced pressure, solvent is removed and toasts Studies of The Aromatic Substances to get to tealeaves.
Step (3) prepares cigarette with quick-fried pearl
15 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 15% is configured to, is added later
15 parts of scutelloside, be stirred at room temperature 30min to dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 48h.
Using pill dripping machine by solution after alcoholization be prepared into diameter be 4.5cm dripping pill, collect molding dripping pill, drying to get
Fragrant cigarette is toasted with quick-fried pearl to required tealeaves.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By the cigarette fragrant with tealeaves baking is not added with quick-fried pearl
Comparison is smoked panel test and shown: the fragrant cigarette of prepared tealeaves baking is with quick-fried pearl, and baking note is dense, and miscellaneous gas is reduced, harmony increase.It comments
The results are shown in Table 7 for suction.
It is measured by flue gas free-radical contents using electron spin resonance, shows 2 gained sample cigarette of embodiment
Free-radical contents reduce 56%.
Embodiment 3
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
Xihu Longjing Tea and Xinyang Maojian Tea is 30 parts each, 3 parts of Yunnan black tea, 15 parts of Pu'er tea, 200 parts of glycerol, magnesium tartrate ion complex
0.2 part of addition round-bottomed flask of object stirs evenly, and flask mouth connects condenser pipe, is put into oil bath heating later to 200 DEG C of condensing refluxes
1h to get arrive oil bath reactant.
Step (2) extracts tealeaves baking perfumery
1000 parts of ethyl acetate are added in the oil bath reactant, then ultrasonic extraction 30min shakes after extracting 30min, into
Row centrifuge separation 4min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, solvent is removed to get tealeaves is arrived
Toast Studies of The Aromatic Substances.
Step (3) prepares cigarette with quick-fried pearl
10 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 10% is configured to, is added later
8 parts of scutelloside, be stirred at room temperature 25min to dissolution mixing it is uniform, be placed in be protected from light shady place refine 30 h.
Above-mentioned solution is prepared into the dripping pill that diameter is 3cm using pill dripping machine, molding dripping pill is collected, dries to get tea is arrived
Leaf toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By the cigarette fragrant with tealeaves baking is not added with quick-fried pearl
Comparison, which is smoked panel test, to be shown: the fragrant cigarette of prepared tealeaves baking toasts note foot with quick-fried pearl, tealeaves, and in good taste, irritation reduces.It comments
The results are shown in Table 7 for suction.
It is measured by flue gas free-radical contents using electron spin resonance, shows 3 gained sample cigarette of embodiment
Free-radical contents reduce 33%.
Embodiment 4
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
Xinyang Maojian Tea and Pilochun (a green tea) is 10 parts each, 2 parts of Yixing black tea, Pu'er tea and Hunan dark green tea it is 30 parts each, 300 parts of propylene glycol,
0.2 part of addition round-bottomed flask of ethylenediamine tetra-acetic acid magnesium ion complex stirs evenly, and flask mouth connects condenser pipe, is put into oil later
Bath is heated to 210 DEG C of condensing reflux 2h to get oil bath reactant is arrived.
Step (2) extracts tealeaves baking perfumery
400 parts of methylene chloride are added in the oil bath reactant and then 1500 parts of methyl acetates, ultrasonic extraction 20min shake
After swinging extraction 13min, 8min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent
Removal toasts Studies of The Aromatic Substances to get to tealeaves.
Step (3) prepares cigarette with quick-fried pearl
12 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in water, being configured to mass percent is 12% solution, and 10 parts of radix scutellariae is added later
Glycosides, be stirred at room temperature 30min to dissolution mixing it is uniform, be placed in be protected from light shady place refine 40 h.
Above-mentioned solution is prepared into the dripping pill that diameter is 3cm using pill dripping machine, molding dripping pill is collected, dries to get tea is arrived
Leaf toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By the cigarette fragrant with tealeaves baking is not added with quick-fried pearl
Comparison, which is smoked panel test, to be shown: the fragrant cigarette of prepared tealeaves baking is toasted note and is protruded with quick-fried pearl, tealeaves, and irritation reduces, and flue gas is thin
It is greasy.Smoking result is as shown in table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 4 gained sample cigarette of embodiment
Free-radical contents reduce 29%.
Embodiment 5
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
Xihu Longjing Tea and Pilochun (a green tea) is 20 parts each, 2 parts of Keemun black tea, Pu'er tea and Hunan dark green tea it is 30 parts each, 200 parts of glycerol, second
0.2 part of addition round-bottomed flask of ethylenediamine tetraacetic acid (EDTA) magnesium ion complex stirs evenly, and flask mouth connects condenser pipe, is put into oil bath later
200 DEG C of condensing reflux 2h are heated to get oil bath reactant is arrived.
Step (2) extracts tealeaves baking perfumery
400 parts of methylene chloride are added in the oil bath reactant and then 1000 parts of petroleum ethers, ultrasonic extraction 25min shake
After extracting 10min, 10min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, by solvent
Removal toasts Studies of The Aromatic Substances to get to tealeaves.
Step (3) prepares cigarette with quick-fried pearl
10 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in water, being configured to mass percent is 15% solution, and 10 parts of radix scutellariae is added later
Glycosides, be stirred at room temperature 30min to dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 38h.
Above-mentioned solution is prepared into the dripping pill that diameter is 4cm using pill dripping machine, molding dripping pill is collected, dries to get tea is arrived
Leaf toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By the cigarette fragrant with tealeaves baking is not added with quick-fried pearl
Comparison, which is smoked panel test, to be shown: the fragrant cigarette of prepared tealeaves baking is toasted note and is protruded with quick-fried pearl, tealeaves, and irritation reduces, and flue gas is thin
It is greasy.Smoking result is as shown in table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 5 gained sample cigarette of embodiment
Free-radical contents reduce 40%.
Embodiment 6
The tealeaves of the present embodiment toasts the cigarette preparation method of quick-fried pearl, includes the following steps:
Step (1), preparation oil bath reactant
By 20 parts of Xihu Longjing Tea, 5 parts of Yunnan black tea, 50 parts of Hunan dark green tea, 400 parts of ethylene glycol, 0.6 part of magnesium tartrate ionic complex adds
Enter round-bottomed flask to stir evenly, flask mouth connects condenser pipe, is put into oil bath heating later to 150 DEG C of condensing reflux 1h to get arriving
Oil bath reactant.
Step (2) extracts tealeaves baking perfumery
In the oil bath reactant be added 600 parts of chloroforms, ultrasonic extraction 20min, then concussion extraction 15min after, carry out from
Heart separation 12min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed and is toasted to get to tealeaves
Studies of The Aromatic Substances.
Step (3) prepares cigarette with quick-fried pearl
18 parts of tealeaves baking Studies of The Aromatic Substances are dissolved in Glycerin, mixed triester with caprylic acid capric acid, being configured to mass percent is 20% solution, and 15 are added later
Part scutelloside, be stirred at room temperature 30min to dissolution mixing it is uniform, be placed in be protected from light shady place alcoholization 30h.
Above-mentioned solution is prepared into the dripping pill that diameter is 4.5cm using pill dripping machine, molding dripping pill is collected, dries to get arriving
Tealeaves toasts fragrant cigarette with quick-fried pearl.
Above-mentioned cigarette is added in filter tip with quick-fried pearl and is prepared into cigarette.By the cigarette fragrant with tealeaves baking is not added with quick-fried pearl
Comparison, which is smoked panel test, to be shown: the fragrant cigarette of prepared tealeaves baking is toasted note and is protruded with quick-fried pearl, tealeaves, and irritation reduces, and flue gas is thin
It is greasy.Smoking result is as shown in table 7.
It is measured by flue gas free-radical contents using electron spin resonance, shows 6 gained sample cigarette of embodiment
Free-radical contents reduce 45%.
Comparative test 1
Comparative sample 1 is prepared according to method in embodiment 1, but magnesium ion complex is added without in preparation process, respectively detection pair
Than targeting the macromoleculars content such as protein, pectin and polysaccharide in extract in sample 1 and embodiment 1.As shown in Table 1, be added magnesium from
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted after sub- complex to be substantially reduced.
Table 1
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Control 1 | 0.2% | 30 | 24 |
| Embodiment 1 | 0 | 0 | 0.2 |
While quick-fried pearl cigarette 1 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 1 has certain tealeaves baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but magnesium ion complex is changed to magnesium chloride in preparation process, examines respectively
It surveys in comparative sample 2 and embodiment 1 and targets the macromoleculars content such as protein, pectin and polysaccharide in extract.As shown in Table 2, it uses
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted after calcium salt complex to be substantially reduced.
Table 2
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 2 | 0.3% | 28 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
While quick-fried pearl cigarette 2 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 2 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 110 DEG C, detects comparative sample 3 and embodiment 1 respectively
The macromoleculars content such as protein, pectin and polysaccharide in middle targeting extract.As shown in Table 3, embodiment 1 targets albumen in extract
The macromoleculars content such as matter, pectin and polysaccharide is substantially reduced.
Table 3
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 3 | 0.3% | 22 | 15 |
| Embodiment 1 | 0 | 0 | 0.2 |
While quick-fried pearl cigarette 3 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 3 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, comfort
Difference.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and embodiment respectively
The macromoleculars content such as protein, pectin and polysaccharide in extract is targeted in 1.As shown in Table 4, embodiment 1 targets egg in extract
The macromoleculars content such as white matter, pectin and polysaccharide is substantially reduced.
Table 4
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 4 | 0.5% | 32 | 20 |
| Embodiment 1 | 0 | 0 | 0.2 |
While quick-fried pearl cigarette 4 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 4 has certain tealeaves baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, comfortably
Property is very poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to use
Separatory funnel carries out conventional extraction, detects target protein, pectin and polysaccharide in extract in comparative sample 5 and embodiment 1 respectively
Etc. macromoleculars content.As shown in Table 5, it is bright to target the macromoleculars content such as protein, pectin and polysaccharide appearance in extract for embodiment 1
It is aobvious to reduce.
Table 5
| Protein content % | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 5 | 0.4% | 10 | 8 |
| Embodiment 1 | 0 | 0 | 0.2 |
While quick-fried pearl cigarette 5 is compareed according to cigarette described in embodiment 1, is prepared into.Shown by smokeing panel test: the opposite quick-fried pearl of embodiment 1
Cigarette, compareing quick-fried pearl cigarette 5 has certain tealeaves baking note but does not protrude, while miscellaneous gas is obvious, and irritation is slightly strong, comfortably
Property is slightly worse.
Simultaneously according to control filter tip 5 is prepared into described in embodiment 1, using 1 middle period of embodiment group and control filter tip 5, preparation
Cigarette 5 is compareed at cigarette.Shown by smokeing panel test: opposite 1 cigarette 1 of embodiment, control cigarette 5 have certain tealeaves baking note but
It does not protrude, while miscellaneous gas is obvious, irritation is strong, and comfort is poor.
Performance detection
Free-radical contents for compareing cigarette 1-6 detect, as a result such as table 6.
Table 6
| Main flume free radical reduces percentage, % | |
| 555 cigarette | - |
| Embodiment 1 | 45 |
| Compare cigarette 1 | 11 |
| Compare cigarette 2 | 8 |
| Compare cigarette 3 | 7 |
| Compare cigarette 4 | 5 |
| Compare cigarette 5 | 9 |
| Compare cigarette 6 | -3 |
As can be seen from Table 6, the main flume free-radical contents of 1 product of embodiment are well below control cigarette 1-6.Meanwhile it is logical
Comparison is crossed it can be seen that each component and parameter have good synergistic effect in preparation method of the present invention.
Kinds of cigarettes sensory evaluating smoking's evaluation result in 7 embodiment 1-6 of table
| Sample | Fragrance | Harmony | Miscellaneous gas | Irritation | Pleasant impression |
| Reference examples | 25 | 5 | 7 | 14 | 19 |
| Scutelloside is not used in embodiment 1 | 27 | 4.5 | 8.5 | 16.5 | 21 |
| Embodiment 1 | 28 | 5.5 | 10 | 17 | 22 |
| Embodiment 2 | 28.5 | 6 | 10 | 16.5 | 22 |
| Embodiment 3 | 27 | 5.5 | 9.5 | 16.5 | 23 |
| Embodiment 4 | 27.5 | 6 | 10 | 18.5 | 22 |
| Embodiment 5 | 29 | 5.5 | 11 | 17 | 23 |
| Embodiment 6 | 29 | 5.5 | 9.5 | 19 | 24 |
The cigarette identical cigarette of quick-fried pearl (using 555 cigarette) is not added with as reference examples, without using scutelloside in preparation process,
According to the method for embodiment 1, it is prepared into cigarette.
As can be seen from Table 7, the cigarette tealeaves baking note of opposite 1 cigarette of embodiment, control is prominent without cigarette, comfort
Difference, respiratory tract irritation decrease, but obvious without the reduction of embodiment 1.
It is compounded in embodiment 1 without using scutelloside, cigarette obtained in the case that other techniques are all the same, sensory evaluating smoking's
Coordinate, is undesirable in terms of miscellaneous gas, effect is also less than reference examples, it is seen then that scutelloside compounding effect is significant.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of tealeaves baking cigarette preparation method of quick-fried pearl, characterized by the following steps:
Step (1), preparation oil bath reactant
Weigh 16-125 parts of tea raw materials, be added in round-bottomed flask, be then added 100-500 parts of polyalcohols and 0.01-1 parts of magnesium from
Sub- complex stirs evenly, and is condensed back 0.5~3h under 150~250 DEG C of oil baths to get oil bath reactant is arrived；
Step (2) extracts tealeaves baking perfumery
The solvent supersonic that 200~2000 parts by weight are added in the oil bath reactant extracts 10~60min, then concussion extraction
10~60min, then it is centrifuged 4~15min, after taking the organic membrane filtration of supernatant liquid, it is evaporated under reduced pressure, solvent is removed,
Obtain tealeaves baking perfumery；
Step (3) prepares cigarette with quick-fried pearl
Above-mentioned tealeaves baking perfumery is dissolved in water or Glycerin, mixed triester with caprylic acid capric acid, the solution that mass percent is 5%~15% is configured to,
0.5~1 times of the scutelloside that tealeaves bakes perfumery quality is added later, 20~30min is stirred at room temperature, is placed in and is protected from light shady place
Refine 24~48h, solution after alcoholization is prepared into dripping pill using pill dripping machine, collects molding dripping pill, is dried to get required tea is arrived
Leaf toasts fragrant cigarette with quick-fried pearl.
2. preparation method according to claim 1, it is characterised in that: the tea raw material is by 10~60 parts of green tea powders, 1
~5 parts of black tea powder and 5~60 parts of dark green tea powder constituents.
3. preparation method according to claim 2, it is characterised in that: in step (1), the green tea be Xihu Longjing Tea,
One of Xinyang Maojian Tea and Pilochun (a green tea) are a variety of；The black tea be one of Keemun black tea, Yunnan black tea and Yixing black tea or
It is a variety of；The dark green tea is one of Pu'er tea, Sichuan dark green tea and Hunan dark green tea or a variety of.
4. preparation method according to claim 1, it is characterised in that: in step (2), the polyalcohol be ethylene glycol,
One of propylene glycol, glycerol are a variety of.
5. preparation method according to claim 1, it is characterised in that: in step (2), the magnesium ion complex is wine
Stone acid magnesium ion complex or ethylenediamine tetra-acetic acid magnesium ion complex.
6. preparation method according to claim 1, it is characterised in that: in step (2), the solvent is petroleum ether, just
One of hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate are a variety of.
7. preparation method according to claim 1, it is characterised in that: in step (3), the dripping pill diameter be 2.5~
4.5cm。
8. the tealeaves that preparation method described in one of claim 1-7 obtains toasts cigarette with quick-fried pearl.
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