CN109259297A - A kind of coffee toasts fragrant electronics tobacco tar and its preparation method and application - Google Patents
A kind of coffee toasts fragrant electronics tobacco tar and its preparation method and application Download PDFInfo
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- CN109259297A CN109259297A CN201811116200.8A CN201811116200A CN109259297A CN 109259297 A CN109259297 A CN 109259297A CN 201811116200 A CN201811116200 A CN 201811116200A CN 109259297 A CN109259297 A CN 109259297A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to a kind of coffees to toast fragrant electronics tobacco tar and its preparation method and application, and this method comprises the following steps: step (1) extracts coffee baking Studies of The Aromatic Substances;Step (2) prepares electronics tobacco tar.Method of the invention can obtain pure baking perfume (or spice) note substance, be added on electronics tobacco tar, can greatly improve abundant flavor and taste, reduce miscellaneous tolerance, improve comfort and harmony.Coffee baking Studies of The Aromatic Substances of the invention is compounded with polydextrose, can be substantially reduced stimulation of the tobacco tar to respiratory tract, the effective baking perfume (or spice) quality for improving new tobacco products.Electronics tobacco tar of the invention can be not only used for conventional electrical cigarette, can also be applied to heat the cigarette that do not burn, preparation method is easy to operate, and safe without toxic side effect is with a wide range of applications.
Description
Technical field
The present invention relates to a kind of preparation methods of electronics tobacco tar, and in particular to a kind of coffee toasts the preparation of fragrant electronics tobacco tar
Method further relates to coffee made from this method and toasts fragrant electronics tobacco tar and its application, belongs to tobacco product field.
Background technique
Coffee is known existing more than 300 years history, is initially worked as due to it has effects that refresh oneself and recover from fatigue by people
Make a kind of functional beverage, later, with the abundant of process and diversification so that finished coffee have unique fragrance and
Mouthfeel and it is standby welcomed by the people, and developing is one of big beverage in the world three.The index of quality such as fragrance, flavor, the taste of coffee 70%
Depending on coffee processing technology, wherein roasting modulated process is the key link for influencing coffee flavor quality.Green coffee itself
Only more than 40 kinds of fragrance, but through roasting modulation after its fragrance component activation up to more than 300 kinds.
As cigarette consumption person is to the growing interest of own health, and the requirement to cigarette interior quality is higher and higher,
How to obtain low tar high-quality cigarette and has become the emphasis studied at present.However, being necessarily accompanied with volume while low tar
Cigarette fragrance loss and comfort level variation.And in quality, country's cigarette product is in terms of sucking quality and sense organ at present
There is certain deficiency, such as fragrance is faint, dry sensation is strong, sweet degree is inadequate, comfort level is poor.
In order to improve the quality of cigarette, can by perfuming cigarette feeding technique, come set off, added volume cigarette perfume taste, increase
Flue gas concentration, improvement is jealous, removes and cover miscellaneous gas, reduces irritation, assigns the good characteristic chicken flavor of product, and prominent cigarette produces
The personalized style of product, promote cigarette sucks satisfaction and pleasure degree.
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research
Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing,
The note for enriching red date extract to a certain extent increases the content of flavor component.Utilize the common volume such as malt extract
It is fragrant to increase flue gas baking for cigarette additive.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still contains
There are the macromolecular substances such as a certain amount of protein, pectin, polysaccharide, these substances can crack generation during cigarette is burnt and sucked
Harmful components, increase cigarette smoking irritation and miscellaneous gas.Thus, reduced while how protruding baking fragrant note irritation and
Miscellaneous gas is the problem of being badly in need of research.
Summary of the invention
In order to solve the above technical problem, the present invention provides the preparation method that a kind of coffee toasts fragrant electronics tobacco tar, this hairs
Bright technical solution is specific as follows:
A kind of coffee toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
1~5 part of big grain coffee, 10~60 parts of middle grain coffee and 5~50 parts of arabiancoffee are weighed by weight, and 100- is then added
500 parts of polyalcohols and 0.01-1 parts of Nu-Irons, stir evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths,
Then the solvent supersonic that 200~2000 parts by weight are added extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4
~15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed and toasts perfumery to get to coffee
Matter;
Step (2) prepares electronics tobacco tar
Coffee baking Studies of The Aromatic Substances, polydextrose, the atomized liquid 1-5:5-20:75-94 by weight of step (1) are added,
It is uniform that extremely dissolution mixing is stirred at room temperature, is placed in and is protected from light shady place 24~48 h of alcoholization to get the fragrant electronics tobacco tar of coffee baking is arrived.
Further, in step (1), big grain coffee is the big grain coffee of the big grain coffee of Greece and/or Taiwan;Middle grain coffee is
Grain coffee in Vietnam, grain coffee in India, one of grain coffee or a variety of in Hainan;Arabiancoffee be Brazilian arabiancoffee,
One or more of Jamaica's arabiancoffee, Yunnan arabiancoffee.
Further, in step (1), the polyalcohol is one or more of ethylene glycol, propylene glycol, glycerol.
Further, in step (1), the Nu-Iron is that dextrin polysaccharide iron complexes or iron dextran are multiple
Close object.
Further, in step (1), the solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, acetic acid
One or more of ethyl ester, methyl acetate.
Further, in step (2), mixing time is 20~30min.
Further, the atomized liquid is propylene glycol or glycerol.
The invention further relates to the obtained coffee of above-mentioned preparation method toast fragrant electronics tobacco tar.
The invention further relates to above-mentioned coffee toast the application of fragrant electronics tobacco tar, by the electronics tobacco tar according to 0.3-1g
It is added in conventional electrical cigarette.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) coffee passes through modulation of the invention, the substance that distinctive coffee toasts fragrant note can be generated, to its product using certain
Solvent targeting extraction is carried out to it, the flue gases such as macromolecular substances irritation or miscellaneous gas substance can be removed, obtain pure baking
Roasting perfume note substance, is added on electronics tobacco tar, can greatly improve the flavor and taste of abundant electronic cigarette, reduce miscellaneous gas
Amount, improves the comfort and harmony of cigarette.
(2) coffee of the invention baking Studies of The Aromatic Substances is compounded with polydextrose, can be substantially reduced stimulation of the tobacco tar to respiratory tract,
The effective baking perfume (or spice) quality for improving new tobacco products.
(3) electronics tobacco tar of the invention can be not only used for conventional electrical cigarette, can also be applied to heat the cigarette that do not burn, preparation
Method is easy to operate, and safe without toxic side effect is with a wide range of applications.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.In the examples where no specific technique or condition is specified, described technology or item according to the literature in the art
Part is carried out according to product description.Reagents or instruments used without specified manufacturer is that can be obtained by purchase
Conventional products.The sensory evaluation of all embodiments is all carried out according to GB5606.4-2005.
Embodiment 1
The coffee of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
By 10 parts of grain coffee in Vietnam, 1 part of the big grain coffee of Greece, the powder of Brazilian 5 parts of arabiancoffee and 100 parts of ethylene glycol,
Round-bottomed flask, stirring is added in 0.01 part of dextrin polysaccharide iron complexes, and flask mouth connects condenser pipe, is put into oil bath heating later extremely
150 DEG C of condensing reflux 3h.
200 parts of petroleum ethers are added in above-mentioned reaction product, then ultrasonic extraction 60min shakes after extracting 60min, into
Row centrifuge separation 15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed to get needed for
Coffee toast Studies of The Aromatic Substances.
Step (2) prepares electronics tobacco tar
Above-mentioned coffee is toasted 1 part of Studies of The Aromatic Substances, 5 parts of polydextrose, 94 parts of propylene glycol etc. to be added, 20min is stirred at room temperature, at
Point dissolution mixing is uniform, is placed in and is protected from light shady place alcoholization for 24 hours to get the electronics tobacco tar fragrant to required coffee baking.
Above-mentioned 0.5g electronics tobacco tar is prepared into electronic cigarette.
It is smoked panel test and is shown by the electronics tobacco tar comparison fragrant with coffee baking is not added with: prepared coffee is added and toasts perfumery
After matter, electronic cigarette toasts note and protrudes, and irritation reduces, and respiratory tract irritation is substantially reduced.The results are shown in Table 6.
Embodiment 2
The coffee of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
Grain coffee in grain coffee in Hainan and Vietnam is 30 parts each, 3 parts of the big grain coffee of 2 parts of the big grain coffee of Greece and Taiwan, tooth are bought
Add arabiancoffee and each 25 parts of powder of Yunnan arabiancoffee and 250 parts of propylene glycol, 1 part of addition round bottom of dextran iron complexes
Flask, stirring, flask mouth connect condenser pipe, are put into oil bath heating later to 250 DEG C of condensing reflux 0.5h.
2000 parts of n-hexanes and chloroform are added in above-mentioned reaction product, wherein n-hexane and chloroform volume ratio are 1:1,
Ultrasonic extraction 10min is centrifuged 4min, takes supernatant liquid with organic membrane filtration then after concussion extraction 10min
Afterwards, it is evaporated under reduced pressure, solvent is removed and toasts Studies of The Aromatic Substances to get to required coffee.
Step (2) prepares electronics tobacco tar
Above-mentioned coffee is toasted 5 parts of Studies of The Aromatic Substances, 20 parts of polydextrose, 75 parts of glycerol etc. to be added, 30min is stirred at room temperature, at
Divide dissolution mixing uniform, is placed in and is protected from light shady place alcoholization 48h to get fragrant electronics tobacco tar is toasted to required coffee.
Above-mentioned 1g electronics tobacco tar is prepared into electronic cigarette.
It is smoked panel test and is shown by the electronics tobacco tar comparison fragrant with coffee baking is not added with: prepared coffee is added and toasts perfumery
After matter, electronic cigarette baking note is dense, and miscellaneous gas is reduced, and harmony increases, and respiratory tract irritation is substantially reduced.As a result such as 6 institute of table
Show.
Embodiment 3
The coffee of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
Grain coffee in grain coffee in India and Hainan is 30 parts each, 2 parts of the big grain coffee in Taiwan, 18 parts of Yunnan arabiancoffee of powder
With 200 parts of glycerol, 0.1 part of addition round-bottomed flask of dextran iron complexes, stirring, flask mouth connects condenser pipe, is put into later
200 DEG C of condensing reflux 1h of oil bath heating.
In above-mentioned reaction product, 1000 parts of ethyl acetate are added, then ultrasonic extraction 30min shakes after extracting 30min,
4min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, solvent is removed to get institute is arrived
The coffee needed toasts Studies of The Aromatic Substances.
Step (2) prepares electronics tobacco tar
Above-mentioned coffee is toasted 3 parts of Studies of The Aromatic Substances, 10 parts of polydextrose, 87 parts of propylene glycol etc. to be added, 25min is stirred at room temperature,
Ingredient dissolution mixing is uniform, is placed in and is protected from light shady place alcoholization 30h to get the electronics tobacco tar fragrant to required coffee baking.
Above-mentioned 0.7g electronics tobacco tar is prepared into electronic cigarette.
It is smoked panel test and is shown by the electronics tobacco tar comparison fragrant with coffee baking is not added with: prepared coffee is added and toasts perfumery
After matter, electronic cigarette coffee toasts note foot, and in good taste, respiratory tract irritation is substantially reduced.The results are shown in Table 6.
Embodiment 4
The coffee of the present embodiment toasts the preparation method of fragrant electronics tobacco tar, includes the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
Grain coffee in grain coffee in Vietnam and India is 10 parts each, 2 parts of the big grain coffee of Greece, Jamaica's arabiancoffee and Brazil are small
Each 30 parts of powder of grain coffee and 300 parts of propylene glycol, 0.2 part of addition round-bottomed flask of dextrin polysaccharide iron complexes, stirring, flask mouth
Condenser pipe is connected, is put into oil bath heating later to 210 DEG C of condensing reflux 2h.
500 parts of methylene chloride of addition and 1500 parts of methyl acetates in above-mentioned reaction product, ultrasonic extraction 20min, then
After concussion extraction 15min, 8min is centrifuged, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure, it will be molten
Agent removal toasts Studies of The Aromatic Substances to get to required coffee.
Step (2) prepares electronics tobacco tar
Above-mentioned coffee is toasted 5 parts of Studies of The Aromatic Substances, 15 parts of polydextrose, 80 parts of propylene glycol etc. to be added, 24min is stirred at room temperature,
Ingredient dissolution mixing is uniform, is placed in and is protected from light shady place alcoholization 40h to get the electronics tobacco tar fragrant to required coffee baking.
Above-mentioned 0.6g electronics tobacco tar is prepared into electronic cigarette.
It is smoked panel test and is shown by the electronics tobacco tar comparison fragrant with coffee baking is not added with: prepared coffee is added and toasts perfumery
After matter, electronic cigarette coffee toasts note and protrudes, and flue gas is fine and smooth, and respiratory tract irritation is substantially reduced.The results are shown in Table 6.
Comparative test 1
Comparative sample 1 is prepared according to method in embodiment 1, but Nu-Iron is added without in preparation process, respectively detection pair
The macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance is toasted than coffee in sample 1 and embodiment 1.As shown in Table 1, it is added
Coffee toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance and is substantially reduced after Nu-Iron.
Table 1
Protein content % | Pectin mg/g | Polysaccharide mg/g | |
Control 1 | 0.3% | 31 | 22 |
Embodiment 1 | 0 | 0.1 | 0.1 |
While electronic cigarette 1 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control
Electronic cigarette 1 has certain coffee baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but Nu-Iron is changed to iron chloride in preparation process, examines respectively
It surveys coffee in comparative sample 2 and embodiment 1 and toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 2,
The macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance is toasted using coffee after calcium salt complex to be substantially reduced.
Table 2
Protein content % | Pectin mg/g | Polysaccharide mg/g | |
Comparative sample 2 | 0.2% | 28 | 20 |
Embodiment 1 | 0 | 0.1 | 0.1 |
While electronic cigarette 2 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control
Electronic cigarette 2 has certain coffee baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 120 DEG C, detects comparative sample 3 and embodiment 1 respectively
Middle coffee toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 3, the baking of 1 coffee of embodiment is fragrant
The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in material.
Table 3
Protein content % | Pectin mg/g | Polysaccharide mg/g | |
Comparative sample 3 | 0.3% | 22 | 15 |
Embodiment 1 | 0 | 0.1 | 0.1 |
While electronic cigarette 3 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control
Electronic cigarette 3 has certain coffee baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and embodiment respectively
Coffee toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance in 1.As shown in Table 4, the baking of 1 coffee of embodiment is fragrant
The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in fragrance.
Table 4
Protein content % | Pectin mg/g | Polysaccharide mg/g | |
Comparative sample 4 | 0.5% | 32 | 20 |
Embodiment 1 | 0 | 0.4 | 0.1 |
While electronic cigarette 4 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control
Electronic cigarette 4 has certain coffee baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to use
Separatory funnel carries out conventional extraction, detect respectively coffee in comparative sample 5 and embodiment 1 toast protein in fragrant fragrance, pectin and
The macromoleculars content such as polysaccharide.As shown in Table 5,1 coffee of embodiment toasts the macromoleculars such as protein, pectin and polysaccharide in fragrant fragrance and contains
Amount is substantially reduced.
Table 5
Protein content % | Pectin mg/g | Polysaccharide mg/g | |
Comparative sample 5 | 0.4% | 10 | 8 |
Embodiment 1 | 0 | 0.1 | 0.1 |
While electronic cigarette 5 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test: opposite 1 electronic cigarette of embodiment, control
Electronic cigarette 5 has certain coffee baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Different electronic cigarette sensory evaluating smoking's evaluation results in 6 embodiment 1-4 of table
As a comparison, it is prepared according to method in embodiment 1, but is added without polydextrose in preparation process, extracts without using solvent
It takes.Simultaneously according to described in embodiment 1, it is prepared into control electronic cigarette.
As can be seen from Table 1, the control electronic cigarette in opposite embodiment 1, control electronic cigarette coffee baking note do not protrude,
Comfort is slightly good, and respiratory tract irritation decreases, but reduces obviously without 1 electronic cigarette of embodiment.
In embodiment 1 without using glucose sugar compound other techniques it is all the same in the case where electronics tobacco tar obtained electronics is added
After cigarette, the coordination of electronic cigarette sensory evaluating smoking, miscellaneous gas, irritation aspect are undesirable, especially in terms of coordinating with miscellaneous gas, effect
Fruit is also less than reference examples, it is seen then that glucose sugar compounding effect is significant.
If not using solvent extraction in embodiment 1, after electronic cigarette is added in obtained electronics tobacco tar, effect is worse, it is seen that molten
Agent extraction is also to improve an important factor for inhaling taste.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (9)
1. the preparation method that a kind of coffee toasts fragrant electronics tobacco tar, characterized by the following steps:
Step (1) extracts coffee baking Studies of The Aromatic Substances
1~5 part of big grain coffee, 10~60 parts of middle grain coffee and 5~50 parts of arabiancoffee are weighed by weight, and 100- is then added
500 parts of polyalcohols and 0.01-1 parts of Nu-Irons, stir evenly, and 0.5~3h is condensed back under 150~250 DEG C of oil baths,
Then the solvent supersonic that 200~2000 parts by weight are added extracts 10~60min, then 10~60min of concussion extraction, then is centrifuged 4
~15min is evaporated under reduced pressure after taking the organic membrane filtration of supernatant liquid, and solvent is removed and toasts perfumery to get to coffee
Matter;
Step (2) prepares electronics tobacco tar
Coffee baking Studies of The Aromatic Substances, polydextrose, the atomized liquid 1-5:5-20:75-94 by weight of step (1) are added,
It is uniform that extremely dissolution mixing is stirred at room temperature, is placed in and is protected from light shady place 24~48 h of alcoholization to get the fragrant electronics tobacco tar of coffee baking is arrived.
2. preparation method according to claim 1, it is characterised in that: in step (1), big grain coffee is the big grain coffee of Greece
And/or the big grain coffee in Taiwan;Middle grain coffee be grain coffee in Vietnam, grain coffee in India, in Hainan one of grain coffee or
It is a variety of;Arabiancoffee is one or more of Brazilian arabiancoffee, Jamaica's arabiancoffee, Yunnan arabiancoffee.
3. preparation method according to claim 1, it is characterised in that: in step (1), the polyalcohol be ethylene glycol,
One or more of propylene glycol and glycerol.
4. preparation method according to claim 1, it is characterised in that: in step (1), the Nu-Iron is paste
Smart Nu-Iron or dextran iron complexes.
5. preparation method according to claim 1, it is characterised in that: in step (1), the solvent is petroleum ether, just
One or more of hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate.
6. preparation method according to claim 1, it is characterised in that: in step (2), mixing time is 20~30min.
7. preparation method according to claim 1, it is characterised in that: the atomized liquid is propylene glycol or glycerol.
8. the coffee that preparation method described in one of claim 1-7 obtains toasts fragrant electronics tobacco tar.
9. the application that coffee according to any one of claims 8 toasts fragrant electronics tobacco tar, it is characterised in that: by the electronics tobacco tar according to
0.3-1g is added to conventional electrical cigarette or electric heating and does not burn in cigarette.
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CN113693265A (en) * | 2021-08-31 | 2021-11-26 | 深圳市真味生物科技有限公司 | Nut coffee electronic atomized liquid and preparation method thereof |
CN115381130A (en) * | 2022-08-19 | 2022-11-25 | 深圳萨特瓦生物科技有限公司 | Coffee refined product, preparation method and application thereof, and electronic cigarette tobacco tar |
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