CN109126358A - 特种气体的提纯工艺及提纯装置 - Google Patents
特种气体的提纯工艺及提纯装置 Download PDFInfo
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- CN109126358A CN109126358A CN201710497154.XA CN201710497154A CN109126358A CN 109126358 A CN109126358 A CN 109126358A CN 201710497154 A CN201710497154 A CN 201710497154A CN 109126358 A CN109126358 A CN 109126358A
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- gas
- molecular sieve
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- stock bottle
- gas cylinder
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- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000007789 gas Substances 0.000 claims abstract description 115
- 239000002808 molecular sieve Substances 0.000 claims abstract description 55
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 55
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 13
- 239000012535 impurity Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000001307 helium Substances 0.000 claims abstract description 4
- 229910052734 helium Inorganic materials 0.000 claims abstract description 4
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims abstract description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 13
- 229910052782 aluminium Inorganic materials 0.000 claims description 13
- 238000005498 polishing Methods 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 4
- 238000000746 purification Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- RBFQJDQYXXHULB-UHFFFAOYSA-N arsane Chemical compound [AsH3] RBFQJDQYXXHULB-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 229910000078 germane Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910000073 phosphorus hydride Inorganic materials 0.000 description 1
- SPVXKVOXSXTJOY-UHFFFAOYSA-N selane Chemical compound [SeH2] SPVXKVOXSXTJOY-UHFFFAOYSA-N 0.000 description 1
- 229910000058 selane Inorganic materials 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
- B01D2253/108—Zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/65—Employing advanced heat integration, e.g. Pinch technology
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Of Gases By Adsorption (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710497154.XA CN109126358B (zh) | 2017-06-27 | 2017-06-27 | 特种气体的提纯工艺及提纯装置 |
Applications Claiming Priority (1)
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CN201710497154.XA CN109126358B (zh) | 2017-06-27 | 2017-06-27 | 特种气体的提纯工艺及提纯装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN109126358A true CN109126358A (zh) | 2019-01-04 |
CN109126358B CN109126358B (zh) | 2024-02-20 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201710497154.XA Active CN109126358B (zh) | 2017-06-27 | 2017-06-27 | 特种气体的提纯工艺及提纯装置 |
Country Status (1)
Country | Link |
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CN (1) | CN109126358B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110040692A (zh) * | 2019-05-15 | 2019-07-23 | 大连科利德光电子材料有限公司 | 制备高纯度二氧化硫气体的方法及装置 |
CN110548364A (zh) * | 2019-10-17 | 2019-12-10 | 清远先导材料有限公司 | 一种回收分子筛吸附的特种气体的方法和装置 |
CN113041641A (zh) * | 2021-03-07 | 2021-06-29 | 无锡恒大电子科技有限公司 | 一种液化气体分级提纯装置 |
CN113816346A (zh) * | 2021-08-30 | 2021-12-21 | 苏州金宏气体股份有限公司 | 一种利用改性金属有机框架提纯硒化氢的工艺 |
Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1146545A (zh) * | 1995-06-15 | 1997-04-02 | 乔治·克劳德方法的研究开发空气股份有限公司 | 带有深冷分离装置的一氧化碳生产设备 |
JPH09264666A (ja) * | 1996-03-29 | 1997-10-07 | Taiyo Toyo Sanso Co Ltd | 窒素・酸素製造システム |
US6134914A (en) * | 1996-08-30 | 2000-10-24 | Messer Griesheim Gmbh | On-line recovery of xenon from anaesthetic gas |
JP2001269531A (ja) * | 2000-03-27 | 2001-10-02 | Nippon Sanso Corp | 窒素ガス分離方法及び装置 |
CN202212088U (zh) * | 2011-08-20 | 2012-05-09 | 广东科艺普实验室设备研制有限公司 | 一种有机废气的净化回收装置 |
CN103101914A (zh) * | 2013-02-26 | 2013-05-15 | 天津大学 | 从氯硅烷残液中回收和提纯六氯乙硅烷的间歇操作方法及装置 |
CN103269979A (zh) * | 2011-03-31 | 2013-08-28 | 住友精化株式会社 | 氨的精制方法及氨精制*** |
CN203319893U (zh) * | 2012-12-31 | 2013-12-04 | 天津市泰源工业气体有限公司 | 一种采用吸附-精馏联合提纯正丁烷的装置 |
CN103951543A (zh) * | 2014-04-18 | 2014-07-30 | 佛山市华特气体有限公司 | 一种三氟甲烷纯化装置及纯化方法 |
CN204816133U (zh) * | 2015-07-22 | 2015-12-02 | 同济大学 | 一种提高吸附床热气体循环脱附再生效率的装置 |
CN207119236U (zh) * | 2017-06-27 | 2018-03-20 | 清远先导材料有限公司 | 特种气体的提纯装置 |
-
2017
- 2017-06-27 CN CN201710497154.XA patent/CN109126358B/zh active Active
Patent Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1146545A (zh) * | 1995-06-15 | 1997-04-02 | 乔治·克劳德方法的研究开发空气股份有限公司 | 带有深冷分离装置的一氧化碳生产设备 |
JPH09264666A (ja) * | 1996-03-29 | 1997-10-07 | Taiyo Toyo Sanso Co Ltd | 窒素・酸素製造システム |
US6134914A (en) * | 1996-08-30 | 2000-10-24 | Messer Griesheim Gmbh | On-line recovery of xenon from anaesthetic gas |
JP2001269531A (ja) * | 2000-03-27 | 2001-10-02 | Nippon Sanso Corp | 窒素ガス分離方法及び装置 |
CN103269979A (zh) * | 2011-03-31 | 2013-08-28 | 住友精化株式会社 | 氨的精制方法及氨精制*** |
CN202212088U (zh) * | 2011-08-20 | 2012-05-09 | 广东科艺普实验室设备研制有限公司 | 一种有机废气的净化回收装置 |
CN203319893U (zh) * | 2012-12-31 | 2013-12-04 | 天津市泰源工业气体有限公司 | 一种采用吸附-精馏联合提纯正丁烷的装置 |
CN103101914A (zh) * | 2013-02-26 | 2013-05-15 | 天津大学 | 从氯硅烷残液中回收和提纯六氯乙硅烷的间歇操作方法及装置 |
CN103951543A (zh) * | 2014-04-18 | 2014-07-30 | 佛山市华特气体有限公司 | 一种三氟甲烷纯化装置及纯化方法 |
CN204816133U (zh) * | 2015-07-22 | 2015-12-02 | 同济大学 | 一种提高吸附床热气体循环脱附再生效率的装置 |
CN207119236U (zh) * | 2017-06-27 | 2018-03-20 | 清远先导材料有限公司 | 特种气体的提纯装置 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110040692A (zh) * | 2019-05-15 | 2019-07-23 | 大连科利德光电子材料有限公司 | 制备高纯度二氧化硫气体的方法及装置 |
CN110040692B (zh) * | 2019-05-15 | 2024-02-09 | 大连科利德光电子材料有限公司 | 制备高纯度二氧化硫气体的方法及装置 |
CN110548364A (zh) * | 2019-10-17 | 2019-12-10 | 清远先导材料有限公司 | 一种回收分子筛吸附的特种气体的方法和装置 |
CN113041641A (zh) * | 2021-03-07 | 2021-06-29 | 无锡恒大电子科技有限公司 | 一种液化气体分级提纯装置 |
CN113041641B (zh) * | 2021-03-07 | 2022-02-22 | 无锡恒大电子科技有限公司 | 一种液化气体分级提纯装置 |
CN113816346A (zh) * | 2021-08-30 | 2021-12-21 | 苏州金宏气体股份有限公司 | 一种利用改性金属有机框架提纯硒化氢的工艺 |
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Publication number | Publication date |
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CN109126358B (zh) | 2024-02-20 |
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PB01 | Publication | ||
PB01 | Publication | ||
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TA01 | Transfer of patent application right |
Effective date of registration: 20210901 Address after: 511500 Heyun Town Industrial Zone, Qingxin District, Qingyuan City, Guangdong Province (beside Yuba highway) Applicant after: FIRST RARE MATERIALS Co.,Ltd. Address before: 511517 27-9B, Guangdong Qingyuan hi tech Industrial Park Applicant before: FIRST RARE MATERIALS Co.,Ltd. |
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TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20220530 Address after: No. 1116-1, building 1, Dianzhong Business Plaza, Dianzhong new area, Kunming, Yunnan 650212 Applicant after: Kunming forerunner New Material Technology Co.,Ltd. Address before: 511500 Heyun Town Industrial Zone, Qingxin District, Qingyuan City, Guangdong Province (beside Yuba highway) Applicant before: FIRST RARE MATERIALS Co.,Ltd. |
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