CN109053138A - One kind thin black pottery product modelled after an antique and preparation method thereof - Google Patents
One kind thin black pottery product modelled after an antique and preparation method thereof Download PDFInfo
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- CN109053138A CN109053138A CN201811108912.5A CN201811108912A CN109053138A CN 109053138 A CN109053138 A CN 109053138A CN 201811108912 A CN201811108912 A CN 201811108912A CN 109053138 A CN109053138 A CN 109053138A
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C04B33/32—Burning methods
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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Abstract
The present invention provides a kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 45 ~ 50 parts of clay, 20 ~ 25 parts of feldspar, 10 ~ 15 parts, 10 ~ 15 parts of mica of quartz.The production method of the thin black pottery product modelled after an antique, including choosing soil shine soil, impregnate filtering, precipitating shrinks, controls mud pugging, forms, the base repaired biscuit that dries in the air, press polish texturing, dry body, firing, kiln discharge.The thin black pottery product modelled after an antique being burnt into using raw material provided by the invention and technique, production is exquisite, and the thin such as eggshell of pottery tire, pottery color is pure, and quality is hard, and impermeable, entire body distributes unprecedented pitch-black black bright metallic luster, serious and sedate.
Description
Technical field
The invention belongs to ceramic technology fields, and in particular to one kind thin black pottery product modelled after an antique and preparation method thereof.
Background technique
Basalt appears in the Yunnan-Tibet culture of period of late Neolithic, Dawenkou Culture, the Longshan culture, the ridge Qu Jia text
In the ruins such as change and Liangzhu Culture.The firing temperature of black pottery up to 1000 degree hereinafter, black pottery has thin mud, shale and three kinds of burning into sand,
In with thin mud thin-walled black pottery production technique highest, have the laudatory title of " black as paint, thin as a piece of paper ".The clay of this black pottery, which passes through, to be eluriated,
Wheel system, only 0.5-1 millimeters of tyre sidewall thickness, then polished, it is burnt into pitch-dark light, there is the title of " egg-shell pottery ", shows surprising skill,
It enjoys great prestige at home and abroad.The black pottery of this period is polished most with vegetarian noodles, with the less of decorative pattern, had raised line design, designated pattern, is engraved hole etc. and is several.It is black
Tao Caiyong wheel system, device shape is perfectly round carefully and neatly done, and beautiful design, decoration is exquisite, the artistic characteristic with " black, thin, light, knob ".
Traditional black pottery product, most it is representational be exactly the Longshan culture egg-shell pottery, at this time the type of black pottery, make
Type, manufacture craft etc. are reached ultimate attainment, are in a peak and most brilliant period.The manufacture craft of egg-shell pottery later
Obvious decline, is embodied in wall and thickens, and technique is coarse, and variation in moulding is little, and quantity falls sharply, until the Longshan culture it
The cultural later period of Yue Shi afterwards, the eggshell pottery that can most represent black pottery highest level are vanished from sight.Mainly since black pottery makes
Technique is cumbersome, involves great expense, and does not have generality, and black pottery manufacture craft is gradually lost, while in black pottery manufacturing process, tradition
Water is added from kiln top using the final stage in firing in method, and charcoal extinguishing is made to produce thick smoke, and allows the infiltration charcoal of sootiness green body
Technique, the problem of existing here, meet steam that water generates to the certain security risk of operator with the presence of: high temperature；And there are products
The chance water capacity is easy to crack, green body colours non-uniform deficiency.
Summary of the invention
Based on the above prior art, the purpose of the present invention is to provide thin black pottery product modelled after an antique and preparation method thereof,
Production is exquisite, and the thin such as eggshell of pottery tire, pottery color is pure, and quality is hard, and impermeable, entire body distributes unprecedented pitch-black black bright
Metallic luster, it is serious and sedate.
In order to achieve the goal above, the technical solution adopted by the present invention are as follows: a kind of thin black pottery product modelled after an antique, feature exist
In the blank includes following raw material: 45~50 parts of clay, 20~25 parts of feldspar, 10~15 parts of quartz, mica 10~
15 parts.
In order to preferably realize the present invention, further, the blank includes following raw material: 50 parts of clay, length
20 parts of stone, 15 parts, 15 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, is used after stirring into mud
Strainer is filtered, and is removed impurity, is collected filtered mud；
(3) precipitating is shunk: mud obtained in step (2) is staticly settled, after muddy water layering, removes upper water,
Lower sediment carries out natural evaporation and shrink, the clod that drying shrinkage is 28~32% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content；
(5) it forms: being fabricated to the pottery mud that step (4) is perfected using one of throwing molding, abrasive tool moulding, hand-pressing method
Greenwave；
(6) dry in the air base repaired biscuit: by greenwave after molding in step (5) in cool place dry and nonventilated closed room dry to
Moisture content 13~17% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, adjusts greenwave not
It is 0.3~1.5cm with part thickness, keeps green body bright and clean, smooth；
(7) press polish texturing: carrying out press polish for the green body fixed, and divides calendering, scratch brushing, three steps of polishing to be operated, press polish knot
Carve corresponding floral designs after beam on greenwave, sun quarter can be used in when engraving, yin is carved, deep, light engraving etc., carve it is good after again into
Row calendering polishing；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 10-15 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
In order to preferably realize the present invention, further, amount of water is the 3~5 of blank when impregnating in the step (2)
Times, the aperture of institute's filter screen is 200 mesh.
In order to preferably realize the present invention, further, calendering operation is specifically in the step (7): calendering uses light
China push type broach or cobblestone polish back and forth in billet surface, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface come
Backwash, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface.
In order to preferably realize the present invention, further, burning process in the step (9) specifically includes the following steps:
1. dried greenwave is put into kiln, use pine branch or cypress as fuel, small fire slowly heats up, and makes temperature
Degree is ramped up 500~600 DEG C in 15~20h；
2. increasing firepower, under oxidizing atmosphere, temperature is made to be ramped up 800~900 DEG C in 4~6h；
3. after keeping the temperature 2~4h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, kilneye, fire box mouth and smoke outlet are closed,
Cigarette cannot be leaked, carries out carburizing under reducing atmosphere；
4. smouldering fire played kiln after 3~5 days.
Beneficial effect
Beneficial effects of the present invention are as follows:
(1) thin black pottery product modelled after an antique provided by the invention, using clay and mica, quartz, feldspar as blank, wherein
Clay is main blank, accounts for blank half, and viscosity is big, plasticity is strong, promotes the plasticity of blank raw material, the base after making sizing
Body consistency is high, viscosity is high, can make that the green body of very thin thickness after being formed is indeformable, do not crack, not arrisdefect after being combined with quartz,
The aluminum oxide contained will have a direct impact on the formation of thin tire；The addition of mica avoids generating fission when heating, also prevents half
Cracking role occurs in drying or firing for finished product, and quartzy addition makes blank raw material be easier to be formed, the green body after also making sizing
Have certain dry tenacity and does not influence and deform vulnerable to external force, cracks；Feldspar can play non-plastic raw material before firing,
The dry contraction and deformation for reducing green body, improve drying property, shorten drying time, can be used as flux reduction firing in firing
Temperature promotes quartz and clay melting, and diffuses into one another the formation for permeating and accelerating mullite in the liquid phase, generates in melting
Feldspar vitreum is filled between the mullite grains of green body, is kept green body fine and close and is reduced gap, to improve its mechanical strength
And dielectric properties, increase its high-intensitive resistance to falling property, furthermore the generation of feldspar glass can also improve the translucency of green body；To increase
Yield rate in black pottery manufacturing process.
(2) thin black pottery product modelled after an antique provided by the invention uses to guarantee that last black pottery finished product has certain brightness
Calendering, scratch brushing, polishing three steps operation, and carry out a calendering again after texturing, it ensure that the light without glaze of black pottery, make
Carcass surface compact is bright and clean after must firing, fine and smooth smooth.
(3) thin black pottery product modelled after an antique provided by the invention is sealed when firing using fresh pine tree leaf or Chinese weeping cypress leaf
Fire guarantees that the dense smoke in kiln generates, and adds flame-out produce thick smoke of water to have the advantage that from kiln top kilneye compared with traditional handicraft
1. kiln seals, high pressure is generated, carburizing time is shortened；2. not having to plus water being avoided without steam generation by steam scald
Risk；3. sealing immediately after producing thick smoke, environmental requirement is reached；4. product does not meet water, avoids chance water quick cooling green body and open
It splits, improves yield rate；5. carburizing time is controllable, carcass uniform coloring.
Specific embodiment
Invention is further described in detail combined with specific embodiments below.
Embodiment 1
A kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 45 parts of clay,
25 parts of feldspar, 15 parts, 15 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, amount of water when immersion
It is 3 times of blank, is filtered after stirring into mud with the strainer that aperture is 200 mesh, removes impurity, collect filtered mud；
(3) precipitating is shunk: mud obtained in step (2) is staticly settled, after muddy water layering, removes upper water,
Lower sediment carries out natural evaporation and shrink, the clod that drying shrinkage is 28% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content on chopping board；
(5) it forms: the pottery mud that step (4) is perfected being fabricated to greenwave using abrasive tool moulding；
(6) dry in the air base repaired biscuit: greenwave after molding is dried in the dry nonventilated closed room in cool place to aqueous in step (5)
Rate 13% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, and the different parts for adjusting greenwave are thick
Degree is 0.3~1.5cm, keeps green body bright and clean, smooth；
(7) press polish texturing: the green body fixed carries out press polish, divides calendering, scratch brushing, three steps of polishing to be operated, specifically presses and smooth
Light is polished using the push type broach of brilliance in billet surface back and forth, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface come
Backwash, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface；Corresponding floral designs are carved after press polish on greenwave, when engraving
Positive quarter, yin quarter, deep, light engraving etc. can be divided, carry out calendering polishing again after quarter is good；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 15 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；The specific steps are 1. dried greenwaves to be put into kiln, uses
As fuel, small fire slowly heats up for pine branch or cypress, and temperature is made to be ramped up 500 DEG C in 15h；2. increasing firepower, aoxidizing
Under atmosphere, temperature is made to be ramped up 800 DEG C in 4h；3. after keeping the temperature 4h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, closing
Kilneye, fire box mouth and smoke outlet, cannot leak cigarette, carry out carburizing under reducing atmosphere；4. smouldering fire played kiln after 3 days.
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
Embodiment 2
A kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 46 parts of clay,
24 parts of feldspar, 14 parts, 14 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, amount of water when immersion
It is 3.5 times of blank, is filtered after stirring into mud with the strainer that aperture is 200 mesh, removes impurity, collect filtered mud
Slurry；
(3) precipitating is shunk: mud obtained in step (2) is staticly settled, after muddy water layering, removes upper water,
Lower sediment carries out natural evaporation and shrink, the clod that drying shrinkage is 29% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content on chopping board；
(5) it forms: the pottery mud that step (4) is perfected being fabricated to greenwave using abrasive tool moulding；
(6) dry in the air base repaired biscuit: greenwave after molding is dried in the dry nonventilated closed room in cool place to aqueous in step (5)
Rate 14% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, and the different parts for adjusting greenwave are thick
Degree is 0.3~1.5cm, keeps green body bright and clean, smooth；
(7) press polish texturing: the green body fixed carries out press polish, divides calendering, scratch brushing, three steps of polishing to be operated, specifically presses and smooth
Light is polished using cobblestone in billet surface back and forth, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface back and forth
Brush, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface；Carve corresponding floral designs after press polish on greenwave, when engraving can
Point sun is carved, yin is carved, is deep, light engraving etc., carve it is good after carry out calendering polishing again；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 14 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；The specific steps are 1. dried greenwaves to be put into kiln, uses
As fuel, small fire slowly heats up for pine branch or cypress, and temperature is made to be ramped up 520 DEG C in 16h；2. increasing firepower, aoxidizing
Under atmosphere, temperature is made to be ramped up 830 DEG C in 4.5h；3. after keeping the temperature 3.5h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette,
Kilneye, fire box mouth and smoke outlet are closed, cigarette cannot be leaked, carry out carburizing under reducing atmosphere；4. smouldering fire played kiln after 4 days.
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
Embodiment 3
A kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 47 parts of clay,
35 parts of feldspar, 13 parts, 13 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, amount of water when immersion
It is 4.5 times of blank, is filtered after stirring into mud with the strainer that aperture is 200 mesh, removes impurity, collect filtered mud
Slurry；
(3) precipitating is shunk: mud obtained in step (2) is staticly settled, after muddy water layering, removes upper water,
Lower sediment carries out natural evaporation and shrink, the clod that drying shrinkage is 31% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content on chopping board；
(5) it forms: the pottery mud that step (4) is perfected being fabricated to greenwave using hand-pressing method；
(6) dry in the air base repaired biscuit: greenwave after molding is dried in the dry nonventilated closed room in cool place to aqueous in step (5)
Rate 16% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, and the different parts for adjusting greenwave are thick
Degree is 0.3~1.5cm, keeps green body bright and clean, smooth；
(7) press polish texturing: the green body fixed carries out press polish, divides calendering, scratch brushing, three steps of polishing to be operated, specifically presses and smooth
Light is polished using the push type broach of brilliance in billet surface back and forth, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface come
Backwash, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface；Corresponding floral designs are carved after press polish on greenwave, when engraving
Positive quarter, yin quarter, deep, light engraving etc. can be divided, carry out calendering polishing again after quarter is good；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 13 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；The specific steps are 1. dried greenwaves to be put into kiln, uses
As fuel, small fire slowly heats up for pine branch or cypress, and temperature is made to be ramped up 550 DEG C in 18h；2. increasing firepower, aoxidizing
Under atmosphere, temperature is made to be ramped up 880 DEG C in 5.5h；3. after keeping the temperature 3h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, envelope
Kilneye, fire box mouth and smoke outlet are closed, cigarette cannot be leaked, carries out carburizing under reducing atmosphere；4. smouldering fire played kiln after 4 days.
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
Embodiment 4
A kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 48 parts of clay,
22 parts of feldspar, 11 parts, 11 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, amount of water when immersion
It is 5 times of blank, is filtered after stirring into mud with the strainer that aperture is 200 mesh, removes impurity, collect filtered mud；
(3) precipitating is shunk: mud obtained in step (2) is staticly settled, after muddy water layering, removes upper water,
Lower sediment carries out natural evaporation and shrink, the clod that drying shrinkage is 32% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content on chopping board；
(5) it forms: being fabricated to the pottery mud that step (4) is perfected using one of throwing molding, abrasive tool moulding, hand-pressing method
Greenwave；
(6) dry in the air base repaired biscuit: greenwave after molding is dried in the dry nonventilated closed room in cool place to aqueous in step (5)
Rate 17% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, and the different parts for adjusting greenwave are thick
Degree is 0.3~1.5cm, keeps green body bright and clean, smooth；
(7) press polish texturing: the green body fixed carries out press polish, divides calendering, scratch brushing, three steps of polishing to be operated, specifically presses and smooth
Light is polished using the push type broach of brilliance in billet surface back and forth, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface come
Backwash, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface；Corresponding floral designs are carved after press polish on greenwave, when engraving
Positive quarter, yin quarter, deep, light engraving etc. can be divided, carry out calendering polishing again after quarter is good；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 10 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；The specific steps are 1. dried greenwaves to be put into kiln, uses
As fuel, small fire slowly heats up for pine branch or cypress, and temperature is made to be ramped up 580 DEG C in 19h；2. increasing firepower, aoxidizing
Under atmosphere, temperature is made to be ramped up 900 DEG C in 6h；3. after keeping the temperature 2.5h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, envelope
Kilneye, fire box mouth and smoke outlet are closed, cigarette cannot be leaked, carries out carburizing under reducing atmosphere；4. smouldering fire played kiln after 5 days.
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
Embodiment 5
A kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 50 parts of clay,
20 parts of feldspar, 15 parts, 15 parts of mica of quartz.
The present invention also provides a kind of methods for making thin black pottery product modelled after an antique, which comprises the following steps:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select nothing
Color is transparent or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) it impregnates filtering: the blank that step (1) is dried being placed in pond or large cylinder and is soaked in water, amount of water when immersion
It is 4 times of blank, is filtered after stirring into mud with the strainer that aperture is 200 mesh, removes impurity, collect filtered mud；
(3) precipitating is shunk: mud obtained in step (2) being staticly settled, after mud moisture content layer, removes upper layer
Water, lower sediment carry out natural evaporation and shrink, the clod that drying shrinkage is 30% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, sealed with hermetic bag, be placed in the cellar of sealing and stand 1 year or more by pottery mud,
It takes out the mud stood and rubs, flexible appropriateness uniform to shale moisture content on chopping board；
(5) it forms: the pottery mud that step (4) is perfected being fabricated to greenwave using abrasive tool moulding；
(6) dry in the air base repaired biscuit: greenwave after molding is dried in the dry nonventilated closed room in cool place to aqueous in step (5)
Rate 15% carries out repaired biscuit, successively repairs complete green body from outside to inside, from top to bottom with Fettling knife, and the different parts for adjusting greenwave are thick
Degree is 0.3~1.5cm, keeps green body bright and clean, smooth；
(7) press polish texturing: the green body fixed carries out press polish, divides calendering, scratch brushing, three steps of polishing to be operated, specifically presses and smooth
Light is polished using the push type broach of brilliance in billet surface back and forth, scratch brushing be with the shallow tool of texture appearance such as sponge moulded pottery not yet put in a kiln to bake surface come
Backwash, polishing are to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface；Corresponding floral designs are carved after press polish on greenwave, when engraving
Positive quarter, yin quarter, deep, light engraving etc. can be divided, carry out calendering polishing again after quarter is good；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and closed room is put when drying, avoids leading to
Wind is placed 12 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, after initial oxidation also
It is carried out in former atmosphere, the use of pine branch or cypress is fuel；The specific steps are 1. dried greenwaves to be put into kiln, uses
As fuel, small fire slowly heats up for pine branch or cypress, and temperature is made to be ramped up 600 DEG C in 20h；2. increasing firepower, aoxidizing
Under atmosphere, temperature is made to be ramped up 860 DEG C in 5h；3. after keeping the temperature 2h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, closing
Kilneye, fire box mouth and smoke outlet, cannot leak cigarette, carry out carburizing under reducing atmosphere；4. smouldering fire played kiln after 3 days.
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln in surface and embossed gap
Ash.
Raw material used by the thin black pottery product modelled after an antique provided in above-described embodiment 1 to 5 is as shown in table 1 below:
1 raw material of table and parts by weight
| Blank raw material | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Clay | 45 parts | 46 parts | 47 parts | 48 parts | 50 parts |
| Feldspar | 25 parts | 24 parts | 23 parts | 22 parts | 20 parts |
| Quartz | 15 parts | 14 parts | 13 parts | 11 parts | 15 parts |
| Mica | 15 parts | 14 parts | 13 parts | 11 parts | 15 parts |
Translucency, water-resistance test, test side are carried out to thin black pottery product modelled after an antique obtained in above-described embodiment 1 to 5
Method is as follows:
Light transmittance test: taking each 15 × 15mm of test sample, tri- fritter, be milled to respectively thickness close to 0.300,0.500,
0.800, thickness measure is accurate to 0.01mm, and after the completion of being milled to, top and bottom are polished with magnesia powder, is surveyed with light transmittance instrument
Fixed, instrument indicating value is sample with respect to penetrating light intensity.Numerical value is bigger, and translucency is better.
Water absorption rate test: taking 5 thin black pottery product fragments modelled after an antique as sample, dry after cleaning, claim its weight respectively,
Sample separation is placed in distilled water later, is boiled 3 hours, during which the water surface is kept above sample 10mm or more, later will examination
Sample is pulled out, is wiped the water that specimen surface adheres to water saturated cloth has been inhaled, is weighed its weight respectively rapidly, pass through formula meter later
The water absorption rate for calculating each sample calculates the mean water absorption rate of 5 samples up to the water absorption rate of thin black pottery product modelled after an antique, water suction
Rate is lower, and the water-resistance of sample is better.
To thin black pottery product modelled after an antique obtained in above-described embodiment 1 to 5 with as reference examples common black pottery product into
Row translucency, water-resistance test, test result is as follows shown in table 2:
2 test result of table
| Test result | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Reference examples |
| Translucency % | 85 | 86 | 89 | 88 | 92 | 78 |
| Water-resistance tests % | 0.25 | 0.24 | 0.22 | 0.20 | 0.16 | 0.33 |
The height thin black pottery product modelled after an antique being burnt into above-described embodiment 1 to 5, translucency, water-resistance are better than common black pottery
Product, wherein it is best with the properties for the thin black pottery product modelled after an antique being burnt into embodiment 5, it is most preferred embodiment.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features.
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
1. a kind of thin black pottery product modelled after an antique, which is characterized in that the blank includes following raw material: 45 ~ 50 parts of clay,
20 ~ 25 parts of feldspar, 10 ~ 15 parts, 10 ~ 15 parts of mica of quartz.
2. thin black pottery product modelled after an antique according to claim 1, which is characterized in that the blank includes that following parts by weight are former
Material: 50 parts of clay, 20 parts of feldspar, 15 parts, 15 parts of mica of quartz.
3. a kind of method for making thin black pottery product modelled after an antique of any of claims 1 or 2, which is characterized in that including following step
It is rapid:
(1) choosing soil shines soil: clay selects 1 meter of argillic horizon below of riverbed topsoil, and feldspar, quartz and mica select colourless
Bright or translucent mineral, by crushing, it is fine ground after ted and dry；
(2) impregnate filtering: the blank that step (1) is dried is placed in pond or large cylinder and is soaked in water, after blend into mud after use
Strainer is filtered, and is removed impurity, is collected filtered mud；
(3) precipitating is shunk: mud obtained in step (2) being staticly settled, after muddy water layering, removes upper water, lower layer
Precipitating carries out natural evaporation and shrink, the clod that drying shrinkage is 28 ~ 32% at moisture content；
(4) control mud pugging: the clod after step (3) are shunk, which is put into vacuum and stirs, rub in mud machine stirring, and obtains helical form pottery mud,
Pottery mud is rubbed and falls into cylindric rear taking-up stripping and slicing, is sealed with hermetic bag, is placed in the cellar of sealing and stands 1 year or more, taken out quiet
The mud set rubs uniform to shale moisture content；
(5) it forms: the pottery mud that step (4) is perfected being fabricated to pottery using one of throwing molding, abrasive tool moulding, hand-pressing method
Base；
(6) dry in the air base repaired biscuit: greenwave after molding in step (5) being dried in dry and nonventilated confined space in cool place to containing
Water rate 13 ~ 17% carries out repaired biscuit, keeps green body bright and clean, smooth；
(7) press polish texturing: carrying out press polish for the green body fixed, and divides calendering, scratch brushing, three steps of polishing to be operated, after press polish
Corresponding floral designs are carved on greenwave, carry out calendering polishing again after carving well；
(8) dry body: the greenwave that step (7) obtains puts naturally dry at shady and cool drying, and confined space is put when drying, avoids divulging information,
It places 10-15 days, is completely dried to moulded pottery not yet put in a kiln to bake；
(9) fire: dried greenwave kiln-firing uses high-temperature carburizing coloring process when firing, restores after initial oxidation
It is carried out in atmosphere；
(10) kiln discharge: the Tao Pin baked in step (9) is taken out from kiln, removes the kiln ash in surface and embossed gap.
4. the method for production thin black pottery product modelled after an antique according to claim 3, which is characterized in that in the step (2)
Amount of water is 3 ~ 5 times of blank when immersion, and the aperture of institute's filter screen is 200 mesh.
5. the method for production thin black pottery product modelled after an antique according to claim 3, which is characterized in that in the step (7)
Calendering operation is specifically: calendering is polished using the push type broach or cobblestone of brilliance in billet surface back and forth, and scratch brushing is to use texture appearance
Shallow tool carrys out backwash on moulded pottery not yet put in a kiln to bake surface, and polishing is to be polished with crocus cloth on moulded pottery not yet put in a kiln to bake surface.
6. the method for production thin black pottery product modelled after an antique according to claim 3, which is characterized in that in the step (9)
Burning process specifically includes the following steps:
1. dried greenwave is put into kiln, small fire slowly heats up, and temperature is made to be ramped up 500 ~ 600 DEG C in 15 ~ 20h；
2. increasing firepower, under oxidizing atmosphere, temperature is made to be ramped up 800 ~ 900 DEG C in 4 ~ 6h；
3. after keeping the temperature 2 ~ 4h, adding fresh needles leaf or Chinese weeping cypress leaf makes it give birth to cigarette, and closing kilneye, fire box mouth and smoke outlet cannot
Cigarette is leaked, carries out carburizing under reducing atmosphere；
4. smouldering fire played kiln after 3 ~ 5 days.
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| CN110845218A (en) * | 2019-12-03 | 2020-02-28 | 王少红 | Argil firing container with built-in rare earth material and preparation process |
| CN111995356A (en) * | 2020-07-17 | 2020-11-27 | 刘小伟 | Ceramic firing method |
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