CN108421980A - A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing - Google Patents

A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing Download PDF

Info

Publication number
CN108421980A
CN108421980A CN201810216847.1A CN201810216847A CN108421980A CN 108421980 A CN108421980 A CN 108421980A CN 201810216847 A CN201810216847 A CN 201810216847A CN 108421980 A CN108421980 A CN 108421980A
Authority
CN
China
Prior art keywords
hot isostatic
isostatic pressing
jacket
layer
manufacturing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810216847.1A
Other languages
Chinese (zh)
Other versions
CN108421980B (en
Inventor
史玉升
蔡超
严倩
薛鹏举
魏青松
宋波
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huazhong University of Science and Technology
Original Assignee
Huazhong University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huazhong University of Science and Technology filed Critical Huazhong University of Science and Technology
Priority to CN201810216847.1A priority Critical patent/CN108421980B/en
Publication of CN108421980A publication Critical patent/CN108421980A/en
Application granted granted Critical
Publication of CN108421980B publication Critical patent/CN108421980B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y10/00Processes of additive manufacturing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y30/00Apparatus for additive manufacturing; Details thereof or accessories therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
    • B22F2003/153Hot isostatic pressing apparatus specific to HIP

Abstract

The invention belongs to advanced manufacturing fields, and specifically disclose a kind of hot isostatic pressing manufacturing process based on increasing material manufacturing, thought of this method based on increasing material manufacturing replaces the raw material that dusty material is shaped as hot isostatic pressing using layer structure material, and realizes that the hot isostatic pressing of part to be formed shapes by using backing material and twice hip treatment.This method, which has been abandoned, is used to common dusty material in heat and other static pressuring processes, and it is replaced by stratified material, fundamentally solve that complicated jacket is removed with inside control shape core difficulty difficult processing, the simulation of powder densification process sophisticated computers is difficult to realize precisely to control the problems such as powder particle boundary difficulty dispelling fatigue performance in shape, product is low in hot isostatic pressing, have many advantages, such as that forming is controllable, operation is convenient, is suitable for the quick high accuracy with complex internal constitutional detail part such as casing, gear, turbine and shapes.

Description

A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing
Technical field
The invention belongs to advanced manufacturing fields, more particularly, to a kind of hot isostatic pressing forming side based on increasing material manufacturing Method.
Background technology
Heat and other static pressuring processes be one kind using inert gases such as nitrogen or argon gas as pressure transmission medium, product is positioned over close Among the container closed, under the collective effect of 0-2000 DEG C of temperature and 50-200MPa pressure, apply to product each to same pressure Power.The technology can be used as the powder metallurgical technique for making powder directly heat pressure sintering forming.In recent years, this technology and mould Tool control shape technology and computer simulation are combined so that loose powder realizes that powder is fine and close under the driving of pressure and temperature While complete target part whole near-net-shape.Currently, because of the part even tissue of the process forming, at the same mechanical property with Same material forging is suitable, and is widely used among the forming of high-performance difficulty processing part, especially aerospace key zero The manufacture of part.
Although Powder hot isostatic pressure technology has greater advantage on whole near-net-shape, for complex internal knot Still there are certain technical bottleneck and processing difficulties on the part (casing, turbine class in such as aerospace engine) of structure, It is specific as follows:
1) external complex jacket and internal control shape core difficulty processing, hardly possible remove.For with complex internal structure casing, The parts such as turbine class often make heat etc. using multisteps manufacturing process such as machining, punching press, hot investment casting and integral solder techniques Static pressure outer wrap and internal control shape core, process is cumbersome, can not even be manufactured to labyrinth, become and restrict the big model of the technique Enclose one of the bottleneck of application.Simultaneously, it is difficult to which irregular outer wrap and complicated interior is removed using conventional machine-tooled method Shape core is controlled in portion, can only often be removed by the method for acid corrosion, and acid corrosion removal efficiency is low, and environmental pollution is very big, Exist simultaneously the risk for eroding drip molding.
2) powder densification process is complicated in hot isostatic pressing, and computer simulation is difficult to realize precisely control shape.HIP at During shape, the volume contraction of 30-40% can occur for powder, and jacket, which is pressurized, occurs larger volume and irregular deformation.Currently, still Lack the ripe number for describing powder HIP densification and the interaction between deformation behavior and powder and jacket and core Learn model.Therefore, cause computer that can only simulate jacket deformation tendency, it is difficult to accurately ensure final formability size essence Degree.
3) the powder particle boundary difficulty in product is eliminated, and fatigue behaviour is low.The product shaped using Powder hot isostatic pressure is micro- The starting powder particle side of powder and powder lap-joint can be clearly observed by seeing in tissue, the defect on this metallurgy is to product Normal tensile property influences less, but in fatigue experiment, and often point is germinated in tired source, and has very to product fatigue behaviour Big harm.
As can be seen that dusty material causes these problems from above-mentioned hot isostatic pressing technique bottleneck and processing difficulties Basic reason.Therefore, there is an urgent need for a kind of novel hot isostatic pressing new methods of research and design for this field, fundamentally to overcome heat etc. quiet Existing technical bottleneck problem when pressing formation complex parts.
Invention content
For the disadvantages described above or Improvement requirement of the prior art, the present invention provides a kind of heat based on increasing material manufacturing etc. is quiet Pressing formation method, this method have incorporated the thought of increasing material manufacturing, and proposition uses stratified material for hot isostatic pressing moulding material, passes through By the forming and manufacture of stratified material accumulated layer by layer and realize complex parts using heat and other static pressuring processes, this method not only can be with The form accuracy and dimensional accuracy for ensuring part simplify packet also without complicated jacket and control shape core by the introducing of supporting layer Nested structure, and can realize the quick removal of jacket, it is suitable for preparing the part with complex internal structure.
To achieve the above object, the present invention proposes a kind of hot isostatic pressing manufacturing process based on increasing material manufacturing, this method Thought based on increasing material manufacturing replaces the raw material that dusty material is shaped as hot isostatic pressing using layer structure material, and leads to It crosses and realizes that the hot isostatic pressing of part to be formed shapes using backing material and twice hip treatment.
Although the method for the present invention introduces the thought of increasing material manufacturing, but it remains as hot isostatic pressing manufacturing process, draws The purpose for entering increasing material manufacturing thought is the form of change raw material, and layer is used instead fundamentally to abandon original dusty material Shape material, existing all kinds of defects, increasing material manufacturing thought are only embodied in when using dusty material to carry out hot isostatic pressing to overcome During folding standby three dimensional practicality using stratiform layer of feed stock material layer heap, i.e., increasing material system is used in the pre-processing of raw material The thought made, but subsequent forming technology is hot isostatic pressing forming technology, and powdered material is substituted by using stratified material The hot isostatic pressing new method of material, to overcome the problems, such as the technical bottleneck of hot isostatic pressing flexible extrusion molding technique.
As it is further preferred that described method includes following steps:
S1 obtains the three-dimensional CAD model of part to be formed, and the three-dimensional CAD model for treating formation of parts carries out slicing treatment, Each slicing layer and corresponding two-dimensional silhouette information are obtained, that chooses part to be formed prepares material as sliced materials, and according to Two-dimensional silhouette information is processed sliced materials and obtains all slicing layers;
S2 prepares thickness supporting layer identical with slicing layer, each slice with the metal material less than part fusing point to be formed Layer is correspondingly arranged on a supporting layer, and corresponding slicing layer is cut away according to the two-dimensional silhouette information of corresponding slicing layer in each supporting layer Shape so that each supporting layer is just nested on corresponding slicing layer;
The every layer of slicing layer processed is sequentially placed into the position of corresponding supporting layer cut away by S3, and then basis is waited for into Assembled slice is sequentially overlapped acquisition three dimensional practicality, to complete heat etc. by the priority ordering of shape part between layers The preparation of the raw material of static pressure forming;
S4 processes corresponding jacket according to the three dimensional practicality exterior contour that superposition obtains, and three dimensional practicality is put into jacket Among obtain base at the beginning of the part with jacket, then by base at the beginning of the part with jacket as being heated in heating furnace, and to jacket Inside is vacuumized, and soldering and sealing is carried out after vacuumizing;
S5 carries out first time hip treatment to base at the beginning of the part with jacket, and jacket is removed after first time hot isostatic pressing; By the three dimensional practicality for removing jacket be put into heating furnace of the temperature between backing material fusing point and formation of parts material melting point into Row heating, obtains base among part after backing material is completely melt and is detached from slicing layer;
S6 takes out base among part, and carries out second of hip treatment to obtain required formation of parts.
As it is further preferred that the first time hot isostatic pressing temperature in supporting layer fusing point hereinafter, pressure be 40MPa ~200Mpa, time are 2h~10h.
As it is further preferred that the temperature of second of hot isostatic pressing is 0.5-0.8 times of part fusing point to be formed, Pressure is 40MPa~200MPa, and the time is 2h~10h.
As it is further preferred that the thickness of the slicing layer is preferably 50 microns to 100 millimeters.
As it is further preferred that the fusing point of the supporting layer is no more than 0.8 times of part material fusing point to be formed.
As it is further preferred that base at the beginning of the part with jacket is molten less than backing material in the heating temperature of heating furnace in S4 Point.
As it is further preferred that the vacuum degree inside jacket is 10-3Pa~10-4Pa。
In general, through the invention it is contemplated above technical scheme is compared with the prior art, mainly have below Technological merit:
1. the hot isostatic pressing manufacturing process of the present invention is different from existing conventional hot isostatic pressing method, increasing material manufacturing is managed Thought is introduced into hot isostatic pressing manufacturing process, and to realize the manufacture of complex parts, by the introducing of the theory, it is quiet to have abandoned heat etc. Press technique in be used to common dusty material, and by stratiform (sheet, plate) material replace, with fundamentally solve complicated jacket and The simulation of powder densification process sophisticated computers is difficult in the problem of inside control shape core difficulty difficult processing removes, hot isostatic pressing Difficulty dispelling fatigue performance low problem in powder particle boundary in the problem of realizing precisely control shape and product, controllable with forming, The advantages that operation is convenient.
2. the present invention not only proposes a kind of new hot isostatic pressing manufacturing process, also the concrete technology of the manufacturing process is walked Suddenly studied, by the research and design to each specific process step in this method, obtain it is a set of it is feasible, can have behaviour The property made and process step that flow is relatively simple, it can be achieved that having complex internal constitutional detail such as casing, gear, whirlpool The quick high accuracy forming of the parts such as wheel.
3. the invention also provides the concept of supporting layer, by designing the supporting layer adapted to slicing layer shape, and utilize Slicing layer is effectively assembled in jacket by supporting layer, and effective support and the holding of shape of slicing layer on the one hand can be achieved, and It is polluted by jacket in hot isostatic pressing since the presence of supporting layer can avoid slicing layer, on the other hand drawing due to supporting layer Enter so that the in-profile of jacket determines by supporting layer, therefore when supporting layer is designed as regular geometric shapes, inside jacket For regular geometric shapes the making labyrinth jacket as described in background technology and inside are not necessarily to without carrying out complicated processing Control shape core.
4. the present invention also studies specific heat and other static pressuring processes, research obtains a kind of secondary hot isostatic pressing work Skill, wherein control the temperature of first time hot isostatic pressing in supporting layer fusing point hereinafter, and the control of the pressure of hot isostatic pressing exists 40MPa~200Mpa, the time is 2h~10h, to ensure to ensure under the premise of supporting layer is unfused each stratiform independent of each other Effective sintering between moulding material (i.e. slicing layer), so that after removing backing material, moulding material still can keep target Parts profile;And by the control of the temperature of second of hot isostatic pressing at 0.5-0.8 times of part fusing point to be formed, pressure control exists 40MPa~200Mpa, the time is 2h~10h, so that moulding material is fully sintered, it is ensured that formation of parts has higher mechanics Performance, and finally obtain required product.
5. base at the beginning of the part with jacket is first heated and is vacuumized as in heating furnace by the present invention, in hot conditions The gas absorption object on lower removal sheet layer material surface, realizes the purpose of pumping removal of impurities, convenient for lamella during follow-up hot isostatic pressing Then the sintering of storeroom carries out soldering and sealing to the jacket after vacuumizing and carries out secondary hip treatment again, to ensure lamella material Effective sintering between material.
Description of the drawings
Fig. 1 is a kind of flow chart of the hot isostatic pressing manufacturing process based on increasing material manufacturing provided in an embodiment of the present invention;
Fig. 2 is the schematic diagram that Ti-6Al-4V titanium alloy gears are manufactured with the method for the present invention, wherein (a) is Ti-6Al- 4V titanium alloy gear schematic diagrames are (b) that Ti-6Al-4V titanium alloy gears are sliced schematic diagram, are (c) Ti-6Al-4V that will be assembled Titanium alloy is put into the schematic diagram of cylindrical jacket with fine aluminium;
Fig. 3 is the schematic diagram that 718 nickel base superalloy turbine components of Inconel are manufactured with the method for the present invention, wherein (a) it is 718 nickel base superalloy turbine schematic three dimensional views of Inconel, is (b) Inconel718 nickel base superalloys turbine two Schematic diagram is tieed up, is (c) that 718 nickel base superalloy turbines of Inconel are sliced schematic diagram, is (d) Inconel 718 that will be assembled Nickel base superalloy turbine is put into the schematic diagram of cylindrical jacket with fine copper.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to the accompanying drawings and embodiments, right The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and It is not used in the restriction present invention.As long as in addition, technical characteristic involved in the various embodiments of the present invention described below It does not constitute a conflict with each other and can be combined with each other.
The present invention provides a kind of hot isostatic pressing manufacturing process based on increasing material manufacturing, this method were shaped in hot isostatic pressing Increasing material manufacturing thought has been incorporated in journey, replaces existing dusty material as heat using stratiform (sheet or plate) structural material The raw material of hydrostatic pressing, and realize by the use of backing material and twice hip treatment the heat of part to be formed Hydrostatic pressing.The method of the present invention changes conventional use of raw material in heat and other static pressuring processes, that is, does not use powdered material Expect (it is the basic reason that various problems and defect occur in existing heat and other static pressuring processes), but replaced with layer structure, with this It can fundamentally overcome the problems, such as that there are various technical bottlenecks and defects in hot isostatic pressing forming process.Wherein, increasing material manufacturing work It is that three-dimensional solid geometry object is split into several planes, utilize different shape according to limited certain thickness as principle Material be successively processed, final accumulation forms required three-dimensional model.
Specifically comprise the following steps as shown in Figure 1, being somebody's turn to do the hot isostatic pressing manufacturing process based on increasing material manufacturing:
One, raw material quasi- stage, including step S1-S3:
S1 obtains the three-dimensional CAD model of part to be formed, using Slice Software treat the three-dimensional CAD model of formation of parts into Row slicing treatment obtains each slicing layer and corresponding two-dimensional silhouette information (i.e. pattern), and that chooses part to be formed prepares material Acquisition is for example processed to sliced materials using laser cutting or machining as sliced materials, and according to two-dimensional silhouette information The thickness of all slicing layers, each slicing layer can be identical or different, and specific thickness is determined according to part type and material, preferably 50 microns~100 millis;
S2 prepares thickness supporting layer identical with slicing layer, each slice with the metal material less than part fusing point to be formed Layer is correspondingly arranged on a supporting layer, i.e. the sum of supporting layer is identical as the slice layer number of part to be formed, and the two thickness phase Deng the geometry that, each supporting layer is rule, cut according to the two-dimensional silhouette information of corresponding slicing layer in each supporting layer Fall the shape of corresponding slicing layer so that each supporting layer is just nested on corresponding slicing layer, so that each slicing layer obtains effectively Support, i.e., dig out shape corresponding with slicing layer, such as cut away in the second supporting layer and cut with second in each supporting layer The corresponding shape of lamella so that the second slicing layer can be nested in the second supporting layer, and the entirety constituted after the two is nested is For the original-shape of the second supporting layer;
The every layer of slicing layer processed is sequentially placed into the position of corresponding supporting layer cut away by S3, i.e., by slicing layer with Its corresponding supporting layer fits together, and both makes concordant, such as third slicing layer is assembled together with third supporting layer makes The two is concordant, then the priority ordering according to part to be formed between layers, and assembled slice is sequentially overlapped and is obtained Slicing layer is only superimposed by three dimensional practicality, this step, to complete the preparation of raw material and the fixation of position, each layer it Between independently of each other, be not connected each other, i.e., only assemble part model, but part and unshaped;
Two, hot isostatic pressing shaping stage, including step S4-S6:
S4 processes corresponding jacket according to the three dimensional practicality exterior contour that superposition obtains, and three dimensional practicality is put into jacket Among obtain the part with jacket at the beginning of base, since slicing layer is inlaid in supporting layer, supporting layer is sleeved in jacket, therefore jacket In-profile determined by the integrally-built outer shape that all supporting layers are constituted, then by base at the beginning of the part with jacket as It is heated in heating furnace, under the high temperature conditions, it is quiet to be conducive to subsequent thermal etc. for the gas absorption object on removal sheet layer material surface Then sintering during pressure between sheet layer material vacuumizes jacket inside, soldering and sealing is carried out after vacuumizing, specific using true Null device carries out vacuumize process by vacuum-pumping tube to jacket inside, and vacuum-pumping tube is arranged in jacket upper and lower side, has vacuumized By exhaust tube soldering and sealing after, to realize the sealing of jacket;
S5 carries out first time hip treatment to base at the beginning of the part with jacket, and jacket is removed after first time hot isostatic pressing, It is stratified material inside jacket, jacket still keeps its original geometry after first time hot isostatic pressing, is added using conventional machine Work method can remove;The three dimensional practicality for removing jacket is put into temperature between backing material fusing point and moulding material fusing point It is heated in the heating furnace of (i.e. temperature is less than moulding material fusing point higher than backing material fusing point), when backing material is completely melt And base among part is obtained after being detached from slicing layer, since part fusing point to be formed is far above backing material, so in backing material Heating temperature at fusing point will not lead to the variation of part generation in shape, just only be left to be formed zero after backing material melts Part;
S6 takes out base among part, and carries out second of hip treatment to obtain required formation of parts.
Specifically, first time hot isostatic pressing purpose is effectively sintered between being to ensure that stratiform moulding material, just can go in this way After backing material, moulding material still can keep target part profile, therefore it is carried out under the conditions of relatively lower temp, For temperature in backing material fusing point hereinafter, pressure is 40MPa~200Mpa, the time is 2h~10h, under above-mentioned process conditions, with It is metallurgy sintered to ensure that part material to be formed occurs so that moulding material is effectively sintered, it is ensured that subsequent high temperature removes backing material Target part profile can be kept afterwards.And the purpose of second of hot isostatic pressing is to promote moulding material fully sintered, it is ensured that Formation of parts has higher mechanical property, therefore it is carried out in the higher condition of relative temperature, and temperature is part to be formed 0.5-0.8 times of material melting point, pressure are 40MPa~200Mpa, and the time is 2h~10h to be made so under above-mentioned process conditions Moulding material it is fully sintered, formation of parts has higher mechanical property.
Further, the fusing point of support layer material is no more than 0.8 times of part material fusing point to be formed, due to being more than 0.8 times, 0.8 times of moulding material can be higher than by melting the temperature of backing material, and the tissue for easily causing drip molding is coarse, is unfavorable for it Mechanical property, the present invention by the way that the fusing point of support layer material is designed to 0.8 times no more than part material fusing point to be formed, with Conducive to ensuring the mechanical property of drip molding, the geometry of backing material is regular circular or rectangular etc., concrete shape root It is determined according to the geometrical morphology of part to be formed, jacket selects material identical with backing material.
More specifically, base at the beginning of the part with jacket is molten less than backing material in the heating temperature of heating furnace in step S4 Point, specially 200 DEG C -600 DEG C.In addition, the vacuum degree inside jacket is 10-3Pa~10-4Pa, can under the vacuum degree condition Ensure that the gas absorption object on sheet layer material surface all removes, and is realized in hot isostatic pressing between certifiable sheet layer material Effectively sintering.
It is the embodiment of the present invention below:
Embodiment 1
Referring to Fig. 2 (a)~(c), the present embodiment is with the method manufacture height 100mm of the present invention, the Ti- of diameter 250mm 6Al-4V titanium alloy gear parts, 1 represents Ti-6Al-4V titanium alloys slice for solid line in figure, and 2 represent fine aluminium fid for dotted line Material, 3 be cylindrical jacket, is specifically comprised the following steps:
1) it is that 0.5mm is sliced and cuts that thickness is obtained after being handled by Slice Software according to the three-dimensional CAD model of titanium alloy gear The two-dimensional signal of piece, according to every layer of titanium alloy gear slice pattern, using laser cutting method 0.5mm Ti-6Al-4V All two dimension slicings are processed on titanium alloy plate;
2) it is backing material to choose fine aluminium, in thickness is 0.5mm, a diameter of according to every layer of target part slice information Corresponding chip formation is cut away in the fine aluminium sheet backing material of 280mm, wherein backing material diameter is slightly larger than target part Diameter can be that follow-up machining leaves surplus, while preventing target part from being polluted by jacket on hot isostatic pressing surface;
3) the every layer of Ti-6Al-4V titanium alloy processed slice is put into corresponding fine aluminium slice vacancy position, according to tooth The slice information for taking turns each layer, by the Ti-6Al-4V titanium alloys spliced slice with fine aluminium slice according to the sequence of each slicing layer It is sequentially overlapped into three dimensional practicality;
4) process internal diameter be 280mm, thickness 3mm, be highly 120mm fine aluminium jacket, and by assembled three-dimensional Material object is put among fine aluminium jacket;
5) jacket for being placed with three dimensional practicality is true by taking out as vacuum equipment in heating furnace, is then utilized at 500 DEG C Blank pipe carries out vacuumize process to jacket inside, when vacuum degree reaches 10-3By exhaust tube soldering and sealing after Pa;
6) it is quiet that the jacket equipped with three dimensional practicality after vacuumizing is put into progress first time heat etc. in hot isostatic pressing working chamber Pressure, while increasing temperature and pressure is to 600 DEG C, 120MPa, heat-insulation pressure keeping 3 hours;
7) after first time hot isostatic pressing, machining is taken to remove jacket;
8) it will remove among the three dimensional practicality after jacket is put into 700 DEG C of heating furnace, wait for that fine aluminium is completely melt and is detached from Ti- It is taken out after 6Al-4V titanium alloys in kind;
9) Ti-6Al-4V material objects are put into hot isostatic pressing working chamber and carry out second of hot isostatic pressing, while increasing temperature and pressure To 930 DEG C, 120MPa, heat-insulation pressure keeping 3 hours;
10) material object is taken out after second of hot isostatic pressing, just can directly obtain Ti-6Al-4V titanium alloy gears.
Embodiment 2
The product and process of preparation are same as Example 1, and only the vacuum degree in step 5) is 10-4Pa, it is same in step 6) When increasing temperature and pressure to 600 DEG C, 200MPa, heat-insulation pressure keeping 2 hours, increasing temperature and pressure is protected to 930 DEG C, 100MPa simultaneously in step 9) Ti-6Al-4V titanium alloy gears can be equally prepared in warm pressurize 5 hours.
Embodiment 3
The product and process of preparation are same as Example 1, and only the vacuum degree in step 5) is 10-4Pa, it is same in step 6) When increasing temperature and pressure to 600 DEG C, 80MPa, heat-insulation pressure keeping 7 hours, in step 9) simultaneously increasing temperature and pressure to 930 DEG C, 200MPa, heat preservation Ti-6Al-4V titanium alloy gears can be equally prepared in pressurize 2 hours.
Embodiment 4
Referring to Fig. 3 (a)~(d), the present embodiment is with the method manufacture height 200mm of the present invention, diameter 600mm 718 nickel base superalloy turbine components of Inconel, 1 represents 718 nickel base superalloys of Inconel slice for solid line in figure, and 2 Fine copper backing material is represented for dotted line, 3 be cylindrical jacket, is specifically comprised the following steps:
1) it is 1.0mm's that thickness is obtained after being handled by Slice Software according to the three-dimensional CAD model of nickel base superalloy turbine Slice and the two-dimensional signal being respectively sliced are existed according to every layer of nickel base superalloy turbine slice pattern using laser cutting method All two dimension slicings are processed on 718 nickel-based high-temperature alloy sheet materials of Inconel of 1.0mm;
2) it is backing material to choose fine copper, in thickness is 1.0mm, a diameter of according to every layer of target part slice information Corresponding chip formation is cut away in the fine copper sheet backing material of 620mm, backing material diameter is slightly larger than target part diameter Can be that follow-up machining leaves surplus, while preventing target part from being polluted by jacket on hot isostatic pressing surface;
3) 718 nickel base superalloys of every layer of Inconel processed slice is put into corresponding fine copper slice vacancy portion 718 nickel base superalloys of Inconel spliced slice and fine copper slice are pressed according to each layer of slice information of turbine position It is sequentially overlapped into three dimensional practicality according to the sequence of each slicing layer;
4) process internal diameter be 620mm, thickness 3mm, be highly 420mm fine copper jacket, and it is the three-dimensional of assembling is real Object is put among fine copper jacket;
5) then the above-mentioned jacket for being placed with three dimensional practicality is passed through at 600 DEG C using vacuum equipment as in heating furnace Vacuum-pumping tube carries out vacuumize process to jacket inside, when vacuum degree reaches 10-3By exhaust tube soldering and sealing after Pa;
6) it is quiet that the jacket equipped with three dimensional practicality after vacuumizing is put into progress first time heat etc. in hot isostatic pressing working chamber Pressure, while increasing temperature and pressure is to 900 DEG C, 120MPa, and heat-insulation pressure keeping 3 hours;
7) after first time hot isostatic pressing, machining is taken to remove jacket;
8) will remove after jacket it is in kind be put into 1100 DEG C of heating furnace among, wait for that fine copper is completely melt and is detached from Inconel It is taken out after 718 nickel base superalloys in kind;
9) 718 nickel base superalloy material objects of Inconel are put into hot isostatic pressing working chamber to carry out second of heat etc. quiet Pressure, while increasing temperature and pressure is to 1200 DEG C, 120MPa, and heat-insulation pressure keeping 3 hours;
10) material object is taken out after second of hot isostatic pressing, just can directly obtain 718 nickel base superalloy turbines of Inconel.
Embodiment 5
The product and process of preparation are same as Example 4, and only the vacuum degree in step 5) is 10-4Pa, it is same in step 6) When increasing temperature and pressure to 600 DEG C, 40MPa, heat-insulation pressure keeping 10 hours, in step 9) simultaneously increasing temperature and pressure to 930 DEG C, 60MPa, heat preservation Inconel718 nickel base superalloy turbines can be equally prepared in pressurize 9 hours.
Embodiment 6
The product and process of preparation are same as Example 4, only in step 6) simultaneously increasing temperature and pressure to 600 DEG C, 180MPa, Heat-insulation pressure keeping 2.8 hours, to 930 DEG C, 40MPa, heat-insulation pressure keeping 10 hours can be equally prepared into increasing temperature and pressure simultaneously in step 9) To 718 nickel base superalloy turbines of Inconel.
The essence of the present invention is that the thought of increasing material manufacturing has been incorporated in hot isostatic pressing forming process, using lamellar structure material Material replaces dusty material, the backing material by low melting point and secondary heat and other static pressuring processes, realizes the hot isostatic pressing of complex parts Forming solves complicated jacket and the processing of core difficulty, the difficult technical barrier removed.
It is emphasized that the present invention is a kind of hot isostatic pressing manufacturing process, substantially work is shaped using hot isostatic pressing Skill is formed with the parts such as the part of complex internal structure, such as casing, gear, turbine, which is used for As the forming technology of complex parts, rather than subsequent treatment process, be different from it is in the prior art using hot isostatic pressing as The defects of subsequent treatment process is to eliminate part void improves part consistency and performance;The method of the present invention utilizes stratiform Material is different from dusty material usual in existing hot isostatic pressing forming technology as raw material, multiple fundamentally to solve The problem of miscellaneous jacket and internal control shape core difficulty difficult processing removal;The present invention only introduces increasing in hot isostatic pressing manufacturing process The theory of material manufacture, emphasis is still hot isostatic pressing forming rather than increasing material manufacturing, required complex parts are quiet by heat etc. Pressing formation technique prepares rather than increasing material manufacturing obtains, which is only intended to prepare the hot isostatic pressing forming of stratiform Raw material are used for subsequent thermal hydrostatic pressing.
As it will be easily appreciated by one skilled in the art that the foregoing is merely illustrative of the preferred embodiments of the present invention, not to The limitation present invention, all within the spirits and principles of the present invention made by all any modification, equivalent and improvement etc., should all include Within protection scope of the present invention.

Claims (8)

1. a kind of hot isostatic pressing manufacturing process based on increasing material manufacturing, which is characterized in that thought of this method based on increasing material manufacturing The raw material that dusty material is shaped as hot isostatic pressing are replaced using layer structure material, and by using backing material and two Secondary hip treatment realizes the hot isostatic pressing forming of part to be formed.
2. the hot isostatic pressing manufacturing process based on increasing material manufacturing as described in claim 1, which is characterized in that the method includes Following steps:
S1 obtains the three-dimensional CAD model of part to be formed, and the three-dimensional CAD model for treating formation of parts carries out slicing treatment, obtains Each slicing layer and corresponding two-dimensional silhouette information, that chooses part to be formed prepares material as sliced materials, and according to two dimension Profile information is processed sliced materials and obtains all slicing layers;
S2 prepares thickness supporting layer identical with slicing layer, each slicing layer with the metal material less than part fusing point to be formed It is correspondingly arranged on a supporting layer, corresponding slicing layer is cut away according to the two-dimensional silhouette information of corresponding slicing layer in each supporting layer Shape so that each supporting layer is just nested on corresponding slicing layer;
The every layer of slicing layer processed is sequentially placed into the position of corresponding supporting layer cut away by S3, then according to be formed Assembled slice is sequentially overlapped acquisition three dimensional practicality by the priority ordering of part between layers, quiet to complete heat etc. The preparation of the raw material of pressing formation;
S4 processes corresponding jacket according to the three dimensional practicality exterior contour that superposition obtains, and by three dimensional practicality be put into jacket it Middle acquisition base at the beginning of the part with jacket, then by base at the beginning of the part with jacket as being heated in heating furnace, and in jacket Portion is vacuumized, and soldering and sealing is carried out after vacuumizing;
S5 carries out first time hip treatment to base at the beginning of the part with jacket, and jacket is removed after first time hot isostatic pressing;It will go Added except the three dimensional practicality of jacket is put into heating furnace of the temperature between backing material fusing point and formation of parts material melting point Heat obtains base among part after backing material is completely melt and is detached from slicing layer;
S6 takes out base among part, and carries out second of hip treatment to obtain required formation of parts.
3. the hot isostatic pressing manufacturing process based on increasing material manufacturing as claimed in claim 1 or 2, which is characterized in that described first For the temperature of secondary hot isostatic pressing in supporting layer fusing point hereinafter, pressure is 40MPa~200Mpa, the time is 2h~10h.
4. the hot isostatic pressing manufacturing process based on increasing material manufacturing as described in claim 1, which is characterized in that second of the heat The temperature of isostatic pressed is 0.5-0.8 times of part fusing point to be formed, and pressure is 40MPa~200MPa, and the time is 2h~10h.
5. the hot isostatic pressing manufacturing process based on increasing material manufacturing as described in claim 1, which is characterized in that the slicing layer Thickness is preferably 50 microns to 100 millimeters.
6. the hot isostatic pressing manufacturing process based on increasing material manufacturing as described in claim 1, which is characterized in that the supporting layer Fusing point is no more than 0.8 times of part material fusing point to be formed.
7. the hot isostatic pressing manufacturing process based on increasing material manufacturing as described in claim 1, which is characterized in that with jacket in S4 Just base is less than backing material fusing point to part in the heating temperature of heating furnace.
8. such as hot isostatic pressing manufacturing process of the claim 1-7 any one of them based on increasing material manufacturing, which is characterized in that jacket Internal vacuum degree is 10-3Pa~10-4Pa。
CN201810216847.1A 2018-03-16 2018-03-16 A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing Active CN108421980B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810216847.1A CN108421980B (en) 2018-03-16 2018-03-16 A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810216847.1A CN108421980B (en) 2018-03-16 2018-03-16 A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing

Publications (2)

Publication Number Publication Date
CN108421980A true CN108421980A (en) 2018-08-21
CN108421980B CN108421980B (en) 2019-07-19

Family

ID=63158270

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810216847.1A Active CN108421980B (en) 2018-03-16 2018-03-16 A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing

Country Status (1)

Country Link
CN (1) CN108421980B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110773735A (en) * 2019-10-31 2020-02-11 华中科技大学 Metal part near-net-shape forming method based on three-dimensional spray printing and hot isostatic pressing and product
CN111014930A (en) * 2019-12-23 2020-04-17 有研亿金新材料有限公司 Two-step hot isostatic pressing diffusion welding method for tungsten target assembly
CN111985059A (en) * 2020-08-04 2020-11-24 华中科技大学 Part forming method and system based on additive manufacturing and hot isostatic pressing
CN112427652A (en) * 2020-11-02 2021-03-02 中国航空制造技术研究院 Titanium alloy structural part and preparation method thereof
CN113056340A (en) * 2018-09-24 2021-06-29 沃斯贝茨公司 How to produce a cost-effective geometrically complex part
CN113088842A (en) * 2021-04-09 2021-07-09 于立豪 System and method for laminating alloy foils
CN113927034A (en) * 2021-07-21 2022-01-14 上海理工大学 Method for manufacturing vacuum self-packaging sheath for hot isostatic pressure powder metallurgy part
CN115121811A (en) * 2022-06-29 2022-09-30 中国航发动力股份有限公司 Welding method of powder-spreading 3D printer case and engine case
CN116329556A (en) * 2023-03-31 2023-06-27 中机新材料研究院(郑州)有限公司 Powder metallurgy preparation method of column product

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4247755A (en) * 1978-01-16 1981-01-27 Autoclave Engineers, Inc. High pressure autoclave
JPS6186469A (en) * 1984-10-03 1986-05-01 エヌオーケー株式会社 Manufacture of ceramic sintered body
CN1041914A (en) * 1988-10-14 1990-05-09 库特·海尔德 The method and apparatus of continuous producing zone rolled-up stock
CN1043805A (en) * 1988-08-30 1990-07-11 斯帕克斯公司 Generate the apparatus and method of three-dimensional body
CN102026752A (en) * 2008-03-20 2011-04-20 先进交互式材料科学有限公司 Net-shape or near net-shape powder isostatic pressing process
CN103111619A (en) * 2013-01-30 2013-05-22 华中科技大学 Hot isostatic pressing two-step forming method of high temperature alloy compact piece
CN105568185A (en) * 2014-10-11 2016-05-11 中国航空工业集团公司西安飞机设计研究所 Manufacturing method for titanium alloy sheet material

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4247755A (en) * 1978-01-16 1981-01-27 Autoclave Engineers, Inc. High pressure autoclave
JPS6186469A (en) * 1984-10-03 1986-05-01 エヌオーケー株式会社 Manufacture of ceramic sintered body
CN1043805A (en) * 1988-08-30 1990-07-11 斯帕克斯公司 Generate the apparatus and method of three-dimensional body
CN1041914A (en) * 1988-10-14 1990-05-09 库特·海尔德 The method and apparatus of continuous producing zone rolled-up stock
CN102026752A (en) * 2008-03-20 2011-04-20 先进交互式材料科学有限公司 Net-shape or near net-shape powder isostatic pressing process
CN103111619A (en) * 2013-01-30 2013-05-22 华中科技大学 Hot isostatic pressing two-step forming method of high temperature alloy compact piece
CN105568185A (en) * 2014-10-11 2016-05-11 中国航空工业集团公司西安飞机设计研究所 Manufacturing method for titanium alloy sheet material

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
许晓琴: "影响LOM 快速成型的加工效率的因素及对策研究", 《机械工程师》 *

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113056340B (en) * 2018-09-24 2023-12-05 沃斯贝茨公司 How to produce a geometrically complex part with high cost effectiveness
CN113056340A (en) * 2018-09-24 2021-06-29 沃斯贝茨公司 How to produce a cost-effective geometrically complex part
CN110773735A (en) * 2019-10-31 2020-02-11 华中科技大学 Metal part near-net-shape forming method based on three-dimensional spray printing and hot isostatic pressing and product
CN111014930A (en) * 2019-12-23 2020-04-17 有研亿金新材料有限公司 Two-step hot isostatic pressing diffusion welding method for tungsten target assembly
CN111985059A (en) * 2020-08-04 2020-11-24 华中科技大学 Part forming method and system based on additive manufacturing and hot isostatic pressing
CN111985059B (en) * 2020-08-04 2022-07-19 华中科技大学 Part forming method and system based on additive manufacturing and hot isostatic pressing
CN112427652A (en) * 2020-11-02 2021-03-02 中国航空制造技术研究院 Titanium alloy structural part and preparation method thereof
CN113088842A (en) * 2021-04-09 2021-07-09 于立豪 System and method for laminating alloy foils
CN113927034A (en) * 2021-07-21 2022-01-14 上海理工大学 Method for manufacturing vacuum self-packaging sheath for hot isostatic pressure powder metallurgy part
CN115121811A (en) * 2022-06-29 2022-09-30 中国航发动力股份有限公司 Welding method of powder-spreading 3D printer case and engine case
CN115121811B (en) * 2022-06-29 2024-03-12 中国航发动力股份有限公司 Welding method of powder-spreading 3D printer casing and engine casing
CN116329556A (en) * 2023-03-31 2023-06-27 中机新材料研究院(郑州)有限公司 Powder metallurgy preparation method of column product
CN116329556B (en) * 2023-03-31 2024-04-05 中机新材料研究院(郑州)有限公司 Processing equipment and preparation method of column product

Also Published As

Publication number Publication date
CN108421980B (en) 2019-07-19

Similar Documents

Publication Publication Date Title
CN108421980B (en) A kind of hot isostatic pressing manufacturing process based on increasing material manufacturing
US11426792B2 (en) Method for manufacturing objects using powder products
CN111618298B (en) Efficient collaborative additive manufacturing method for multi-material and variable-rigidity structure
CN102941343B (en) Quick manufacturing method of titanium-aluminum alloy composite part
CN105170978B (en) Linkage interface has the homogeneity jacket high temperature insostatic pressing (HIP) manufacturing process of gradient structure
CN103949639A (en) Method for preparing Nb-Si based superhigh-temperature alloy by SLM (selective laser melting) technology
CN109396434B (en) Method for preparing titanium alloy part based on selective laser melting technology
CN104419846B (en) Mallory sharton alloy target and preparation method thereof
US20130039799A1 (en) Method of Making Near-Net Shapes From Powdered Metals
CN111215855B (en) Titanium/nickel alloy part based on explosive welding and laser additive manufacturing and preparation method
EP3085472B1 (en) Method of manufacturing a turbine blisk through hot isostatic pressing using a metal core
CN107127343A (en) A kind of electron beam increasing material manufacturing method of nickel-base alloy structural member
JP2022105482A (en) Method for manufacturing interposed straight groove annular member
CN109365826A (en) The compound increasing material manufacturing process of dissimilar material thrust chamber
CN103834923B (en) The making method of tungsten titanium target material
CN104174848A (en) Powder hot isostatic pressing molding method of titanium alloy automobile connecting shaft rod
CN105312563A (en) Manufacturing method for nickel-based double-alloy integral blade disc
CN113414406B (en) Method for improving density of magnesium/magnesium alloy part manufactured by selective laser melting additive
CN112570730B (en) High-precision selective laser melting forming method for cooling body part
CN102503083A (en) Isostatic pressing near-net-shape forming method easy for removing mold core for manufacturing glass
CN115488342B (en) Short-process preparation method of dissimilar metal integral She Panzeng and other materials
EP3427869A1 (en) Additive manufacturing methods and related components
TWI604902B (en) Engine Turbine rotor casting method
CN104668549A (en) Alloy powder and laser adding material manufacturing process applying same
Węgrzyn The Use of Additive Manufacturing for Production of Commercial Airplane Power Plants Components: A Review

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant