CN108542850A - A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins - Google Patents
A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins Download PDFInfo
- Publication number
- CN108542850A CN108542850A CN201810644510.0A CN201810644510A CN108542850A CN 108542850 A CN108542850 A CN 108542850A CN 201810644510 A CN201810644510 A CN 201810644510A CN 108542850 A CN108542850 A CN 108542850A
- Authority
- CN
- China
- Prior art keywords
- parts
- indocalamus leaf
- total saposins
- preserving moisture
- protecting skin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones soapberry pericarp total saposins, sodium carboxymethylcellulose is dissolved in hot purified water, it is slowly stirred into gel-type vehicle, with lauryl sodium sulfate, sodium chloride mixes, pour into buffer solution, the stirring and dissolving in water bath with thermostatic control, it takes out, cooling, nipalgin is added, lanolin, winter jasmine extracting solution, citrus bark extract and indocalamus leaf Flavonoid extract, soapberry pericarp total saposins concentrate, it stirs evenly, buffer solution is added, again plus lemon juice, rose water stirs evenly, ultrasound, remove bubble, bottling, obtain antibacterial preserving moisture and protecting skin hand cleanser.Indocalamus leaf Flavonoid extract can be used as natural bacteriostatic agent, have good bacteriostasis property, and have unique indocalamus leaf fragrance；Using soapberry pericarp total saposins extracting solution as surfactant；Winter jasmine extracting solution has winter jasmine fragrance, can moisturize the skin moisturizing as sterilization bacteriostat；Citrus bark extract has good moisture-keeping efficacy, while having light fruit flavor.
Description
Technical field
The invention belongs to clean daily necessities fields, and in particular to a kind of addition indocalamus leaf flavones-soapberry pericarp total saposins
Antibacterial preserving moisture and protecting skin hand cleanser.
Background technology
Hand cleanser is a kind of emerging hand cleaning product, uses pump head nozzle, perfumed soap, fertilizer with traditional solid-like more
Soap is compared, and hand cleanser is not only easy to use, but also is also avoided the solids such as perfumed soap, soap and becomed easily infected by dirt on hand and thin
The defect of bacterium reduces the possibility of cross-infection, this makes hand cleanser increasingly by the great kindness of consumers in general.In early days,
The country does not focus on skin-care effect in hand cleanser this aspect, and hand cleanser products mostly only focus on decontamination biocidal efficacies, and
It is less paid close attention to whether to human skin fanout free region.In recent years, some natural extracts it is mild with its, it is non-stimulated, have sterilization,
Bacteriostasis efficacy and degradable feature, are just concerned by people.In recent years, some natural extracts it is mild with its, it is non-stimulated,
Have the characteristics that sterilization, bacteriostasis efficacy and degradable, is just concerned by people.The natural Huang of high-purity is extracted from plant
Letones cause the extensive concern of researcher, it has also become medicament research and development and the hot spot utilized.
Indocalamus leaf is the general name of grass family Bambusoideae Indocalamus Nakai leaves of plants, it contains multiple biological activities ingredient such as flavones, work
Property polysaccharide, vitamin, trace element, volatile oil, fragrance ingredient, tea polyphenols etc..Indocalamus leaf general flavone has to be removed in vivo certainly well
By base, anti-oxidant and aging, improve immunity, antibacterial, it is antiviral the effects that.
Winter jasmine is a kind of common Chinese herbal medicine, containing Flavonoid substances, has certain restraining and sterilizing bacteria effect, such as to large intestine bar
Bacterium, Pseudomonas aeruginosa, golden yellow glucose coccus, typhoid bacillus, bacillus enteritidis etc. have certain antibacterial activity.
Citrus is a kind of common fruit, in pericarp containing pectin, essential oil, flavonoids, terpenoid, glycoside, carbohydrate,
Vitamin etc. has certain moisturizing, anti-inflammatory, sterilization and bacteriostasis efficacy, and is easy to be biodegradable in the environment, will not be to ring
Border pollutes.Soapberry pericarp contains abundant saponin(e, has stronger surface-active and dirt-removing power, pericarp saponin(e bubble
Foam is abundant, and feel is fine and smooth, and smell faint scent can improve skin quality to no skin irritation, make skin exquisite luster, rich in bullet
Property, it is the raw material of ideal natural detergent.
Hand sanitizer formula is added using winter jasmine extracting solution as bactericidal active constituent, by citrus extracts in the present invention
In, it is prepared for a kind of new hand sanitizer with natural fragrance, can be had both while ensureing product decontamination, bactericidal
Mildly, the features such as non-stimulated, preserving moisture and protecting skin.
Invention content
The purpose of the present invention is for existing problem, provide a kind of addition indocalamus leaf flavones-soapberry pericarp total saposins
Antibacterial preserving moisture and protecting skin hand cleanser, according to this method prepare hand cleanser have very strong bactericidal performance and dirt-removing power,
And have the characteristics that preserving moisture and protecting skin and unique fragrance.
The present invention is achieved by the following technical solutions：
A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins, which is characterized in that including as follows
Step：
（1）The preparation of indocalamus leaf Flavonoid extract：
5-10 parts of indocalamus leafs are acquired, cleans and dries, smash it through 80 mesh sieve, 23-25h is impregnated in petroleum ether and removes depigmentation, by material
Liquor ratio 1:20（g/mL）A concentration of 60% extractant ethyl alcohol is added, 1-2h is extracted at 60-63 DEG C, filters, rotary evaporation concentration
Filtrate obtains indocalamus leaf Flavonoid extract to paste；
（2）The ultrasonic extraction process of soapberry pericarp total saposins：
It is 1 that solid-liquid ratio is pressed into 2-3 parts of soapberry pericarp powder:30 are added the ethanol solution that volume fraction is 90%, seal, shake
30-35min is placed after even, is placed into supersonic wave cleaning machine, ultrasonic extraction 80-90min, is filtered, is carried out with Rotary Evaporators
It is concentrated under reduced pressure, obtains soapberry pericarp total saposins concentrate；
（3）The preparation process of antibacterial preserving moisture and protecting skin hand cleanser：
2-4 parts of sodium carboxymethylcelluloses are dissolved in 40-60 parts of hot purified waters, gel-type vehicle is slowly stirred into, with 2-3 parts 12
Sodium alkyl sulfate, 0.5-0.6 parts of sodium chloride mixing, pour into 10-12 parts of buffer solutions, are stirred in 60-63 DEG C of water bath with thermostatic control molten
Solution is taken out, is cooled to 35 DEG C, and 0.1-0.2 parts of nipalgins, 0.1-0.2 parts of lanolin, winter jasmine extracting solution, orange peel is added and carries
Resulting material in object and (1), (2) is taken, is stirred evenly, 8-10 parts of buffer solutions are added, then add 1-2 portions of lemon juices, 20-25 parts of roses
Rare water stirs evenly, ultrasonic 1-2h, removes bubble, and bottling obtains antibacterial preserving moisture and protecting skin hand cleanser.
Further, step（2）In win ripe soapberry fruit, rinsed 2-3 times repeatedly with clear water, dry in the shade, divest fruit
Core leaves pericarp, and pericarp is shredded, and 5-6h is dried in 43-47 DEG C of baking oven, is crushed with pulverizer, and soapberry fruit peel powder is made
End；Ultrasonic power is 60-100W.
Further, step（3）The preparation of middle winter jasmine extracting solution：15-20 parts of winter jasmines are dried, are crushed, by feed liquid
Than 1:30（g/mL）It is added a concentration of 60% ethanol solution, after supersonic leaching 1-2h, stands 24-25h, take supernatant liquor, obtain
Winter jasmine extracting solution.
Further, step（3）The preparation of middle citrus bark extract：10-15 parts of orange peels are dried, are crushed,
Into the orange peel of crushing in mass ratio 1:10 are added hot water, after refluxing extraction 1-2h, stand 5-10min, by upper layer oil
Shape liquid is dried with anhydrous magnesium sulfate, and citrus bark extract is made.
Further, step（3）The preparation of middle lemon juice：Fresh Lemon is removed the peel, is obtained by filtration after squeezing out lemon juice
Fresh Lemon juice.
Further, step（3）The preparation of middle rose water：Into dry roseleaf 1:100 DEG C of boiling water is added in 15-20,
Stirring after impregnating 30-40min, filters to obtain rose water.
Further, step（3）Middle buffer solution refers to the citric acid-sodium citrate buffer that pH is 6.
The present invention has the following advantages compared with prior art：
（1）Using indocalamus leaf as raw material, add extractant ethyl alcohol to extract, prepare Flavonoid extract, can be used as natural bacteriostatic agent, has good
Bacteriostasis property, and there is unique indocalamus leaf fragrance, a kind of novel environment friendly, pollution-free, decontamination, antibacterial hand cleanser are prepared, more
There is the characteristics of mild, skin care.
Soapberry pericarp total saposins concentrate is prepared using ultrasonic extraction, is made with soapberry pericarp total saposins extracting solution
It is reliable and stable using ultrasonic method extraction total saponin of sapindusmukerossi for surfactant, the energy is saved, using soapberry pericarp total saposins
Extracting solution prepares new hand sanitizer, and hand cleanser ecological, environmental protective prepared by total saponin of sapindusmukerossi has the exploitation of soapberry certain
Directive significance.
（2）It is prepared for winter jasmine extracting solution, can be used as sterilization bacteriostat, not only containing in winter jasmine extracting solution can inhibit
The natural bacteriostatic ingredient of bacterial growth, and there is unique fragrance and color and luster, while winter jasmine extracting solution also has moist skin
Skin and antistatic property have winter jasmine fragrance, moistening effect good.
Citrus bark extract has good moisture-keeping efficacy, is added into hand cleanser, can improve the moisture retention of hand cleanser,
Make product that there is light fruit flavor simultaneously.Lemon juice, rose water are added in hand cleanser, gained hand cleanser has good anti-
Bacterium property and cleaning function, and preferable nursing role can be played to hand skin.
Specific implementation mode
Embodiment 1
A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins, which is characterized in that including as follows
Step：
（1）The preparation of indocalamus leaf Flavonoid extract：
5 parts of indocalamus leafs are acquired, cleans and dries, smash it through 80 mesh sieve, 23h is impregnated in petroleum ether and removes depigmentation, by solid-liquid ratio 1:
20（g/mL）A concentration of 60% extractant ethyl alcohol is added, 1h is extracted at 60-63 DEG C, filters, rotary evaporation concentrates filtrate to cream
Shape obtains indocalamus leaf Flavonoid extract；
（2）The ultrasonic extraction process of soapberry pericarp total saposins：
It is 1 that solid-liquid ratio is pressed into 2 parts of soapberry pericarp powder:30 are added the ethanol solution that volume fraction is 90%, seal, shake up
After place 30min, place into supersonic wave cleaning machine, ultrasonic extraction 80min, filter, be concentrated under reduced pressure with Rotary Evaporators,
Obtain soapberry pericarp total saposins concentrate；
（3）The preparation process of antibacterial preserving moisture and protecting skin hand cleanser：
2 parts of sodium carboxymethylcelluloses are dissolved in 40 parts of hot purified waters, gel-type vehicle is slowly stirred into, with 2 parts of dodecyl sulphur
Sour sodium, 0.5 part of sodium chloride mixing, pour into 10 parts of buffer solutions, the stirring and dissolving in 60-63 DEG C of water bath with thermostatic control is taken out, is cooled to
35 DEG C, gains in 0.1 part of nipalgin, 0.1 part of lanolin, winter jasmine extracting solution, citrus bark extract and (1), (2) are added
Material, stirs evenly, and 8 parts of buffer solutions is added, then 1 portion of lemon juice, 20 parts of rose waters is added to stir evenly, and ultrasonic 1h removes bubble,
Bottling, obtains antibacterial preserving moisture and protecting skin hand cleanser.
Further, step（2）In win ripe soapberry fruit, rinsed 2 times, dried in the shade repeatedly with clear water, divest fruit stone
Pericarp is left, pericarp is shredded, 5h is dried in 43-47 DEG C of baking oven, is crushed with pulverizer, soapberry pericarp powder is made；It is super
Acoustical power is 60W.
Further, step（3）The preparation of middle winter jasmine extracting solution：15 parts of winter jasmines are dried, are crushed, by solid-liquid ratio 1:
30（g/mL）It is added a concentration of 60% ethanol solution, after supersonic leaching 1h, stands for 24 hours, take supernatant liquor, obtain winter jasmine and carry
Take liquid.
Further, step（3）The preparation of middle citrus bark extract：10 parts of orange peels are dried, are crushed,
Into the orange peel of crushing in mass ratio 1:10 are added hot water, after refluxing extraction 1h, 5min are stood, by upper layer oily liquids
It is dried with anhydrous magnesium sulfate, citrus bark extract is made.
Further, step（3）The preparation of middle lemon juice：Fresh Lemon is removed the peel, is obtained by filtration after squeezing out lemon juice
Fresh Lemon juice.
Further, step（3）The preparation of middle rose water：Into dry roseleaf 1:15 are added 100 DEG C of boiling water, stir
After mixing, impregnating 30min, rose water is filtered to obtain.
Further, step（3）Middle buffer solution refers to the citric acid-sodium citrate buffer that pH is 6.
Embodiment 2
A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins, which is characterized in that including as follows
Step：
（1）The preparation of indocalamus leaf Flavonoid extract：
10 parts of indocalamus leafs are acquired, cleans and dries, smash it through 80 mesh sieve, 25h is impregnated in petroleum ether and removes depigmentation, by solid-liquid ratio 1:
20（g/mL）A concentration of 60% extractant ethyl alcohol is added, 2h is extracted at 60-63 DEG C, filters, rotary evaporation concentrates filtrate to cream
Shape obtains indocalamus leaf Flavonoid extract；
（2）The ultrasonic extraction process of soapberry pericarp total saposins：
It is 1 that solid-liquid ratio is pressed into 3 parts of soapberry pericarp powder:30 are added the ethanol solution that volume fraction is 90%, seal, shake up
After place 35min, place into supersonic wave cleaning machine, ultrasonic extraction 90min, filter, be concentrated under reduced pressure with Rotary Evaporators,
Obtain soapberry pericarp total saposins concentrate；
（3）The preparation process of antibacterial preserving moisture and protecting skin hand cleanser：
4 parts of sodium carboxymethylcelluloses are dissolved in 60 parts of hot purified waters, gel-type vehicle is slowly stirred into, with 3 parts of dodecyl sulphur
Sour sodium, 0.6 part of sodium chloride mixing, pour into 12 parts of buffer solutions, the stirring and dissolving in 60-63 DEG C of water bath with thermostatic control is taken out, is cooled to
35 DEG C, gains in 0.2 part of nipalgin, 0.2 part of lanolin, winter jasmine extracting solution, citrus bark extract and (1), (2) are added
Material, stirs evenly, and 10 parts of buffer solutions is added, then 2 portions of lemon juices, 25 parts of rose waters is added to stir evenly, and ultrasonic 2h removes degassing
Bubble, bottling, must wash antibacterial preserving moisture and protecting skin hand liquid.
Further, step（2）In win ripe soapberry fruit, rinsed 3 times, dried in the shade repeatedly with clear water, divest fruit stone
Pericarp is left, pericarp is shredded, 6h is dried in 43-47 DEG C of baking oven, is crushed with pulverizer, soapberry pericarp powder is made；It is super
Acoustical power is 100W.
Further, step（3）The preparation of middle winter jasmine extracting solution：20 parts of winter jasmines are dried, are crushed, by solid-liquid ratio 1:
30（g/mL）It is added a concentration of 60% ethanol solution, after supersonic leaching 2h, stands 25h, take supernatant liquor, obtain winter jasmine and carry
Take liquid.
Further, step（3）The preparation of middle citrus bark extract：15 parts of orange peels are dried, are crushed,
Into the orange peel of crushing in mass ratio 1:10 are added hot water, after refluxing extraction 2h, 10min are stood, by upper layer oily liquid
Body is dried with anhydrous magnesium sulfate, and citrus bark extract is made.
Further, step（3）The preparation of middle lemon juice：Fresh Lemon is removed the peel, is obtained by filtration after squeezing out lemon juice
Fresh Lemon juice.
Further, step（3）The preparation of middle rose water：Into dry roseleaf 1:20 are added 100 DEG C of boiling water, stir
After mixing, impregnating 40min, rose water is filtered to obtain.
Further, step（3）Middle buffer solution refers to the citric acid-sodium citrate buffer that pH is 6.
Comparative example 1
This comparative example 1 compared with Example 1, in step（3）In indocalamus leaf Flavonoid extract is not added, method and step in addition to this
All same.
Comparative example 2
This comparative example 2 compared with Example 2, in step（3）In soapberry pericarp total saposins concentrate is not added, in addition to this
Method and step all same.
Control group
Application No. is：A kind of method for producing hand cleanser using red building disclosed in 2017104381557.
In order to compare the dirt-removing power and bactericidal performance of hand cleanser produced by the present invention, to above-described embodiment 1, implement
Example 2, comparative example 1,2 method of comparative example correspond to hand cleanser obtained, with reference to professional standard to the soil removal efficiency of hand cleanser
It is tested with bacteriostasis antibiosis performance, test result record is as follows：
Table 1
Indocalamus leaf Flavonoid extract and soapberry pericarp are not added in comparative example 1 it can be seen from upper table 1 and comparative example 2
Total saposins concentrate compounds hand cleanser antibacterial bacteriostatic ability and dirt-removing power obtained and weakens；It is washed by made from the method for the present invention
Hand liquid has very strong sterilization antibacterial bacteriostatic performance, and dirt-removing power is strong, and has the characteristics that preserving moisture and protecting skin and unique fragrance, low
Easy cleaning is steeped, stability is strong, safe to use, great popularizing value and the market competitiveness.
Claims (7)
1. a kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins, which is characterized in that including such as
Lower step：
（1）The preparation of indocalamus leaf Flavonoid extract：
5-10 parts of indocalamus leafs are acquired, cleans and dries, smash it through 80 mesh sieve, 23-25h is impregnated in petroleum ether and removes depigmentation, by material
Liquor ratio 1:20（g/mL）A concentration of 60% extractant ethyl alcohol is added, 1-2h is extracted at 60-63 DEG C, filters, rotary evaporation concentration
Filtrate obtains indocalamus leaf Flavonoid extract to paste；
（2）The ultrasonic extraction process of soapberry pericarp total saposins：
It is 1 that solid-liquid ratio is pressed into 2-3 parts of soapberry pericarp powder:30 are added the ethanol solution that volume fraction is 90%, seal, shake
30-35min is placed after even, is placed into supersonic wave cleaning machine, ultrasonic extraction 80-90min, is filtered, is carried out with Rotary Evaporators
It is concentrated under reduced pressure, obtains soapberry pericarp total saposins concentrate；
（3）The preparation process of antibacterial preserving moisture and protecting skin hand cleanser：
2-4 parts of sodium carboxymethylcelluloses are dissolved in 40-60 parts of hot purified waters, gel-type vehicle is slowly stirred into, with 2-3 parts 12
Sodium alkyl sulfate, 0.5-0.6 parts of sodium chloride mixing, pour into 10-12 parts of buffer solutions, are stirred in 60-63 DEG C of water bath with thermostatic control molten
Solution is taken out, is cooled to 35 DEG C, and 0.1-0.2 parts of nipalgins, 0.1-0.2 parts of lanolin, winter jasmine extracting solution, orange peel is added and carries
Resulting material in object and (1), (2) is taken, is stirred evenly, 8-10 parts of buffer solutions are added, then add 1-2 portions of lemon juices, 20-25 parts of roses
Rare water stirs evenly, ultrasonic 1-2h, removes bubble, and bottling obtains antibacterial preserving moisture and protecting skin hand cleanser.
2. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（2）In win ripe soapberry fruit, rinsed 2-3 times, dried in the shade repeatedly with clear water, divested fruit stone and stay
Lower pericarp, pericarp is shredded, 5-6h is dried in 43-47 DEG C of baking oven, is crushed with pulverizer, and soapberry pericarp powder is made；It is super
Acoustical power is 60-100W.
3. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（3）The preparation of middle winter jasmine extracting solution：
15-20 parts of winter jasmines are dried, are crushed, by solid-liquid ratio 1:30（g/mL）A concentration of 60% ethanol solution, ultrasound leaching is added
After taking 1-2h, 24-25h is stood, supernatant liquor is taken, obtains winter jasmine extracting solution.
4. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（3）The preparation of middle citrus bark extract：
10-15 parts of orange peels are dried, are crushed, into the orange peel of crushing in mass ratio 1:10 are added hot water, refluxing extraction 1-
After 2h, 5-10min is stood, upper layer oily liquids is dried with anhydrous magnesium sulfate, citrus bark extract is made.
5. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（3）The preparation of middle lemon juice：Fresh Lemon is removed the peel, squeeze out be obtained by filtration after lemon juice it is fresh
Lemon juice.
6. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（3）The preparation of middle rose water：Into dry roseleaf 1:100 DEG C of boiling water is added in 15-20, stirs
After mixing, impregnating 30-40min, rose water is filtered to obtain.
7. a kind of antibacterial preserving moisture and protecting skin of addition indocalamus leaf flavones-soapberry pericarp total saposins according to claim 1 is washed one's hands
Liquid, which is characterized in that step（3）Middle buffer solution refers to the citric acid-sodium citrate buffer that pH is 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810644510.0A CN108542850A (en) | 2018-06-21 | 2018-06-21 | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810644510.0A CN108542850A (en) | 2018-06-21 | 2018-06-21 | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108542850A true CN108542850A (en) | 2018-09-18 |
Family
ID=63492727
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810644510.0A Pending CN108542850A (en) | 2018-06-21 | 2018-06-21 | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108542850A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110339133A (en) * | 2019-08-21 | 2019-10-18 | 浙江理工大学 | A kind of preparation method of green bacteriostatic hand sanitizer |
| WO2022058343A3 (en) * | 2020-09-17 | 2022-04-21 | Givaudan Sa | Preservative and antimicrobial compositions |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102671017A (en) * | 2012-04-27 | 2012-09-19 | 湖北长友现代农业股份有限公司 | Method for simultaneously preparing indocalamus leaf volatile oil, total flavone and total polysaccharide |
| CN104288026A (en) * | 2014-09-27 | 2015-01-21 | 张乔木 | Hand sanitizer and preparation method thereof |
| CN108078815A (en) * | 2017-12-01 | 2018-05-29 | 吴义峰 | A kind of disposable hand cleanser of natural bacteriostatic and preparation method thereof |
-
2018
- 2018-06-21 CN CN201810644510.0A patent/CN108542850A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102671017A (en) * | 2012-04-27 | 2012-09-19 | 湖北长友现代农业股份有限公司 | Method for simultaneously preparing indocalamus leaf volatile oil, total flavone and total polysaccharide |
| CN104288026A (en) * | 2014-09-27 | 2015-01-21 | 张乔木 | Hand sanitizer and preparation method thereof |
| CN108078815A (en) * | 2017-12-01 | 2018-05-29 | 吴义峰 | A kind of disposable hand cleanser of natural bacteriostatic and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 吉瑞冬等: "箬叶黄酮抑菌洗手液的研制", 《化工技术与开发》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110339133A (en) * | 2019-08-21 | 2019-10-18 | 浙江理工大学 | A kind of preparation method of green bacteriostatic hand sanitizer |
| WO2022058343A3 (en) * | 2020-09-17 | 2022-04-21 | Givaudan Sa | Preservative and antimicrobial compositions |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105754768B (en) | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof | |
| CN103756808A (en) | Natural washing liquid without preservative and preparation method of natural wash liquid | |
| KR102019443B1 (en) | Dishwashing detergent composition comprising eco-friendly complex mixture and methods for manufacturing the same | |
| CN105012224A (en) | Natural shampoo and preparation method thereof | |
| CN108096117A (en) | A kind of composition and its preparation method and application | |
| CN107937176A (en) | A kind of high-efficiency antioxidant anti-acne handmade soap | |
| CN102247309A (en) | Shampoo with a mint tea fragrance, and preparation method thereof | |
| KR102226774B1 (en) | Detergent comprising the extract of astragalus membranaceus, polydonati rhizoma and pine leaf, and the method of manufacturing thereof | |
| CN108542850A (en) | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins | |
| CN103385837B (en) | Myrica rubra leaf proanthocyanidin toning lotion and preparation method of myrica rubra leaf proanthocyanidin toning lotion | |
| CN109010178B (en) | Shower gel and production process thereof | |
| CN111110574A (en) | Wet tissue with three-in-one functions of cleaning, sterilizing and moisturizing and preparation method thereof | |
| KR20160105187A (en) | A kitchen antimicrobial detergent containing an eco-friendly antimicrobial agent | |
| CN102451111A (en) | Natural bacteriostasis hand cleanser and its preparation method | |
| CN104207998B (en) | A kind of Flos Sophorae handwashing liquid and preparation method thereof | |
| CN104721121A (en) | Skin care type cosmetic | |
| CN103860438B (en) | The whitening scrubbing cream that a kind of pomelo peel is made | |
| CN106344430A (en) | Konjac glucomannan shower gel and preparation method thereof | |
| KR101539744B1 (en) | A kitchen antimicrobial detergent containing an eco-friendly antimicrobial agent for preventing atopic dermatitis | |
| CN105419381A (en) | Purification method of natural dyestuff of mulberries | |
| CN102949311B (en) | Additive-free children bath liquid and preparation method thereof | |
| CN105687023A (en) | Beauty-retaining whitening facial cleanser and preparation method thereof | |
| CN107184467A (en) | A kind of hair care exterior-applied article being made of Lignum Xanthoceratis extract and preparation method thereof | |
| CN107805559A (en) | A kind of preparation method of high-efficiency antioxidant anti-acne handmade soap | |
| CN113388460A (en) | Faint scent type perfumed soap containing peony flowers and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180918 |