CN108559656A - A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell - Google Patents
A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/044—Hydroxides or bases
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
- C11D3/323—Amides; Substituted amides urea or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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Abstract
The invention discloses a kind of plant type antibacterial bacteriostatic liquid detergents with pomelo fragrant smell, deionized water is heated, surfactant is added while stirring, cool down again, lauric acid diethyl amide, urea and sodium cellulose glycolate stirring and dissolving is added, Wedelia trilobata volatile oil, ginger extract, Chinese cassia tree extracting solution, tangerine essential oil, pomelo peel soaked extracting solution and wormwood volatile oil is added, it stirs evenly, pH is adjusted with trisodium citrate and sodium hydrate aqueous solution, sodium chloride is added, side edged shakes up, and is got product until sticky.Using the volatile oil of extraction by steam distillation Wedelia trilobata aerial part, the miscellaneous bacteria that wedelia chinensis volatile oil is cultivated to Escherichia coli and naturally has apparent bactericidal effect, can be used as the preservative and fungicide of liquid detergent.Ginger extract is prepared by absolute ethyl alcohol mechanical shaking extraction, ginger extract has inhibiting effect to Gram-negative bacteria and gram-positive bacteria, and the bacteriostatic activity of ginger extract is strong, and thermal stability is good.
Description
Technical field
The invention belongs to clean daily necessities fields, and in particular to a kind of plant type antibacterial bacteriostatic with pomelo fragrant smell
Liquid detergent.
Background technology
As the fast development of urban and rural economies and the level of cultural life are continuously improved, the consciousness enhancing of people's sanitation and hygiene,
Tableware, kitchen tools and veterinary antibiotics are cleaned and are sterilized and are more paid attention to.But commercially available clean dose of quality problems of meal protrude, qualification rate
It is low, largely limit the sound development of tableware detergent.It is increasingly extensive with the mutually contacts of people, give various infections
The propagation of disease increases chance, wherein being had a good chance by what tableware for food and drink infected, so research and development antibacterial tableware cleaning
Essence has larger Social benefit and economic benefit.Antibacterial tableware detergent is mainly by surfactant, bacteriostatic agent and various
Auxiliary combination forms.
The present invention prepares Chinese cassia tree extracting solution by steam distillation, is imitated to the antibacterial of miscellaneous bacteria in Escherichia coli and air
Fruit is good, and uses it for preparing in Antibiotic liquid detergent, to develop a kind of antibacterial, the preferable plant type of dirt-removing power wash it is clean
Essence.Chinese cassia tree extracting solution is the by-product for extracting cinnamon essential oil process, and effective antipathogenic composition is cinnamic acid, can be used as antibacterial activity
Ingredient is added in various products.It contains abundant limonene in orange peel, is widely present in the natural plants of nature
Monocycle list mushroom has very strong degreasing and sterilizing ability.The present invention will extract D- limonenes in orange peel and be configured to natural plant
Object type Antibiotic liquid detergent, and its bactericidal effect is studied.Wormwood is a kind of traditional Chinese medicine with peat-reek, volatilization
Oil has anti-inflammatory, antibacterial and an effectiveness such as antiviral, and natural plant Antibiotic liquid detergent has been made in this research oil compounding that will end, to open
Send out new and effective natural plant Antibiotic liquid detergent a kind of.
Invention content
The purpose of the present invention is for existing problem, provide a kind of plant type antibacterial suppression with pomelo fragrant smell
Bacterium liquid detergent, the liquid detergent dirt-removing power prepared according to this method is strong, has very strong bactericidal performance, and clear with shaddock
Fragrance taste.
The present invention is achieved by the following technical solutions：
A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell, which is characterized in that include the following steps：
（1）The extraction of Wedelia trilobata volatile oil：
The aerial part of 5-10 parts of Wedelia trilobatas is acquired, dust removal is cleaned, dries in the shade, shredded, with extraction by steam distillation 2-
After 3h, add sodium chloride to being saturated, stood after stirring, separate oil reservoir, dried with anhydrous sodium sulfate, obtains Wedelia trilobata volatilization
Oil；
（2）The preparation of ginger extract：
5-10 parts of fresh gingers are smashed to pieces with mortar, 1:The absolute ethyl alcohol mechanical shaking extraction 3- that volume fraction is 90-95% is added in 3-4
4h is extracted 2-3 times altogether, is merged extracting solution, is filtered, is then concentrated at 48-52 DEG C, obtain ginger extract；
（3）The preparation of plant type Antibiotic liquid detergent：
280-320 parts of deionized waters are heated to 44-46 DEG C, surfactant are added while stirring, then be cooled to 34-36 DEG C,
5-7 parts of lauric acid diethyl amides, 15-20 parts of urea and 1-2 parts of sodium cellulose glycolate stirring and dissolvings are added, trilobated leaf is added
Wedelia chinensis volatile oil, ginger extract, Chinese cassia tree extracting solution, tangerine essential oil, pomelo peel soaked extracting solution and wormwood volatile oil, are stirred
It mixes uniformly, it is 7.5 to adjust pH with trisodium citrate and sodium hydrate aqueous solution, and 20-25 parts of sodium chloride are added, and side edged shakes up,
It is got product until sticky.
Further, step（3）The preparation of middle Chinese cassia tree extracting solution：
Cassia is broken for 40 mesh, into 15-20 parts of cassia powder 1:Distilled water is added in 20-25, adds auxiliary agent sodium chloride,
Ebuillition of heated 1-2h obtains the Chinese cassia tree extracting solution that mass fraction is 15-20%.
Further, step（3）The ethyl alcohol and ultrasonic extraction of middle tangerine essential oil：
Fresh complete orange peel is cleaned with clear water, dipping pretreatment is anti-in the VC solution that mass fraction is 0.15-0.3%
Then block is dried to Shui in 43-47 DEG C of baking oven and divides Han Liang≤14%, crushed through pulverizer, 40 mesh sieve is crossed, to 5-10 parts
Solid-liquid ratio 1 is pressed in dry orange peel powder:Absolute ethyl alcohol is added in 5-6g/mL, and after ultrasonic extraction 1-2d, decompression water bath with thermostatic control distillation obtains
Tangerine essential oil.
Further, step（3）Middle pomelo peel soaked extracting solution：
By fresh grapefruit peeling, remove the white wooden dipper in pomelo peel, solid-liquid ratio 1 is pressed into 10-15 parts of pomelo peels:30-35 is added dense
Degree is the ethanol solution of 20-25%, is protected from light immersion one week, obtains pomelo peel soaked extracting solution.
Further, step（3）The extraction of middle wormwood volatile oil：
Acquisition wormwood aerial part is cleaned, dries in the shade, is shredded, and the broken extraction by steam distillation 2-3h of 8-10 parts of wormwoods is added
Sodium chloride powder stands after stirring to being saturated, separates oil reservoir, dried with anhydrous sodium sulfate, obtain wormwood volatile oil.
Further, step（3）Middle surfactant is by 16-20 parts of fatty alcohol polyoxyethylene ether, 22-26 parts of dodecyls
Benzene sulfonic acid sodium salt, 30-40 parts of sodium sulfate of polyethenoxy ether of fatty alcohol compositions.
The present invention has the following advantages compared with prior art：
（1）Using the volatile oil of extraction by steam distillation Wedelia trilobata aerial part, itself and other components are compounded, system
At plant type Antibiotic liquid detergent, the miscellaneous bacteria that wedelia chinensis volatile oil is cultivated to Escherichia coli and naturally has apparent bactericidal effect, can
Preservative and fungicide as liquid detergent.
Using the volatile oil of extraction by steam distillation wormwood aerial part, is compounded with other substances, be prepared for plant
The volatile oil of type Antibiotic liquid detergent, wormwood has apparent bactericidal effect to the miscellaneous bacteria cultivated under Escherichia coli and natural conditions, Chinese mugwort
The volatile oil of grass has good bactericidal effect, is a kind of efficient, safety, natural plant antiseptic, can be used as liquid detergent
Preservative and fungicide.
（2）Ginger extract is prepared by absolute ethyl alcohol mechanical shaking extraction, ginger extract is blue to Gram-negative bacteria and leather
Family name's positive bacteria has inhibiting effect, and the bacteriostatic activity of ginger extract is strong, and has good thermal stability.
Using Chinese cassia tree as raw material, Chinese cassia tree extracting solution is prepared by steam distillation, the good anti-bacterial effect of Chinese cassia tree extracting solution is right
Miscellaneous bacteria has good inhibition, Chinese cassia tree to take liquid that can inhibit the growth of bacterium, can also inhibit bud in Escherichia coli and air
Itself and other components compounding are prepared liquid detergent by the growth of spore and mould, and dirt-removing power is strong.
（3）Using orange peel as raw material, using ethyl alcohol and ultrasonic wave extraction tangerine essential oil, natural citrus peel essential oil is added
Plant type liquid detergent dirt-removing power is good, and has biocidal property to Escherichia coli, mould, staphylococcus aureus, especially to big
The inhibiting effect of enterobacteria is most strong.
It uses pomelo peel for raw material, uses ethanol solution as leachate, extract the ethanol solution containing D- citric acids, have
There is good bactericidal effect, is a kind of safety and efficient natural plant type antiseptic, can be used as the fungicide and table of liquid detergent
The plant type Antibiotic liquid detergent with pomelo fragrant smell is made in face activating agent.
Specific implementation mode
Embodiment 1
A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell, which is characterized in that include the following steps：
（1）The extraction of Wedelia trilobata volatile oil：
The aerial part of 5 parts of Wedelia trilobatas is acquired, dust removal is cleaned, dries in the shade, is shredded, after extraction by steam distillation 2h,
Add sodium chloride to being saturated, is stood after stirring, separate oil reservoir, dried with anhydrous sodium sulfate, obtain Wedelia trilobata volatile oil；
（2）The preparation of ginger extract：
5 parts of fresh gingers are smashed to pieces with mortar, 1:3 are added the absolute ethyl alcohol mechanical shaking extraction 3h that volume fraction is 90%, extract 2 altogether
It is secondary, merge extracting solution, is filtered, is then concentrated at 48-52 DEG C, obtain ginger extract；
（3）The preparation of plant type Antibiotic liquid detergent：
280 parts of deionized waters are heated to 44-46 DEG C, surfactant are added while stirring, then be cooled to 34-36 DEG C, are added 5
Wedelia trilobata volatilization is added in part lauric acid diethyl amide, 15 parts of urea and 1 part of sodium cellulose glycolate stirring and dissolving
Oil, ginger extract, Chinese cassia tree extracting solution, tangerine essential oil, pomelo peel soaked extracting solution and wormwood volatile oil, stir evenly, and use
It is 7.5 that trisodium citrate and sodium hydrate aqueous solution, which adjust pH, 20 parts of sodium chloride is added, side edged shakes up, until sticky
It gets product.
Further, step（3）The preparation of middle Chinese cassia tree extracting solution：
Cassia is broken for 40 mesh, into 15 parts of cassia powder 1:20 are added distilled water, add auxiliary agent sodium chloride, heating boiling
1h is risen, the Chinese cassia tree extracting solution that mass fraction is 15% is obtained.
Further, step（3）The ethyl alcohol and ultrasonic extraction of middle tangerine essential oil：
Fresh complete orange peel is cleaned with clear water, the anti-block of dipping pretreatment in the VC solution that mass fraction is 0.15%
Change, Shui is then dried in 43-47 DEG C of baking oven and divides Han Liang≤14%, is crushed through pulverizer, 40 mesh sieve is crossed, to 5 parts of dry orange peel powder
In press solid-liquid ratio 1:Absolute ethyl alcohol is added in 5g/mL, and after ultrasonic extraction 1d, decompression water bath with thermostatic control distillation obtains tangerine essential oil.
Further, step（3）Middle pomelo peel soaked extracting solution：
By fresh grapefruit peeling, remove the white wooden dipper in pomelo peel, solid-liquid ratio 1 is pressed into 10 parts of pomelo peels:30 are added a concentration of 20%
Ethanol solution, be protected from light immersion one week, obtain pomelo peel soaked extracting solution.
Further, step（3）The extraction of middle wormwood volatile oil：
Acquisition wormwood aerial part is cleaned, dries in the shade, is shredded, and by the broken extraction by steam distillation 2h of 8 parts of wormwoods, sodium chloride is added
Powder stands after stirring to being saturated, separates oil reservoir, dried with anhydrous sodium sulfate, obtain wormwood volatile oil.
Further, step（3）Middle surfactant is by 16 parts of fatty alcohol polyoxyethylene ether, 22 parts of dodecyl benzene sulfonic acid
Sodium, 30 parts of sodium sulfate of polyethenoxy ether of fatty alcohol compositions.
Embodiment 2
A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell, which is characterized in that include the following steps：
（1）The extraction of Wedelia trilobata volatile oil：
The aerial part of 10 parts of Wedelia trilobatas is acquired, dust removal is cleaned, dries in the shade, is shredded, after extraction by steam distillation 3h,
Add sodium chloride to being saturated, is stood after stirring, separate oil reservoir, dried with anhydrous sodium sulfate, obtain Wedelia trilobata volatile oil；
（2）The preparation of ginger extract：
10 parts of fresh gingers are smashed to pieces with mortar, 1:4 are added the absolute ethyl alcohol mechanical shaking extraction 4h that volume fraction is 95%, extract 3 altogether
It is secondary, merge extracting solution, is filtered, is then concentrated at 48-52 DEG C, obtain ginger extract；
（3）The preparation of plant type Antibiotic liquid detergent：
320 parts of deionized waters are heated to 44-46 DEG C, surfactant are added while stirring, then be cooled to 34-36 DEG C, are added 7
Wedelia trilobata volatilization is added in part lauric acid diethyl amide, 20 parts of urea and 2 parts of sodium cellulose glycolate stirring and dissolvings
Oil, ginger extract, Chinese cassia tree extracting solution, tangerine essential oil, pomelo peel soaked extracting solution and wormwood volatile oil, stir evenly, and use
It is 7.5 that trisodium citrate and sodium hydrate aqueous solution, which adjust pH, 25 parts of sodium chloride is added, side edged shakes up, until sticky
It gets product.
Further, step（3）The preparation of middle Chinese cassia tree extracting solution：
Cassia is broken for 40 mesh, into 20 parts of cassia powder 1:25 are added distilled water, add auxiliary agent sodium chloride, heating boiling
2h is risen, the Chinese cassia tree extracting solution that mass fraction is 20% is obtained.
Further, step（3）The ethyl alcohol and ultrasonic extraction of middle tangerine essential oil：
Fresh complete orange peel is cleaned with clear water, the anti-block of dipping pretreatment in the VC solution that mass fraction is 0.3%
Change, Shui is then dried in 43-47 DEG C of baking oven and divides Han Liang≤14%, is crushed through pulverizer, 40 mesh sieve is crossed, to 10 parts of dry orange peels
Solid-liquid ratio 1 is pressed in powder:Absolute ethyl alcohol is added in 6g/mL, and after ultrasonic extraction 2d, decompression water bath with thermostatic control distillation obtains tangerine essential oil.
Further, step（3）Middle pomelo peel soaked extracting solution：
By fresh grapefruit peeling, remove the white wooden dipper in pomelo peel, solid-liquid ratio 1 is pressed into 15 parts of pomelo peels:35 are added a concentration of 25%
Ethanol solution, be protected from light immersion one week, obtain pomelo peel soaked extracting solution.
Further, step（3）The extraction of middle wormwood volatile oil：
Acquisition wormwood aerial part is cleaned, dries in the shade, is shredded, and by the broken extraction by steam distillation 3h of 10 parts of wormwoods, chlorination is added
Sodium powder end stands after stirring to being saturated, separates oil reservoir, dried with anhydrous sodium sulfate, obtain wormwood volatile oil.
Further, step（3）Middle surfactant is by 20 parts of fatty alcohol polyoxyethylene ether, 26 parts of dodecyl benzene sulfonic acid
Sodium, 40 parts of sodium sulfate of polyethenoxy ether of fatty alcohol compositions.
Comparative example 1
This comparative example 1 compared with Example 1, in step（3）In ginger extract is not added, method and step in addition to this is equal
It is identical.
Comparative example 2
This comparative example 2 compared with Example 2, in step（3）In tangerine essential oil is not added, method and step in addition to this is equal
It is identical.
Control group
Application No. is：A kind of sterilizing skin-protective powdery liquid detergent disclosed in 201710383295.
In order to compare the dirt-removing power and bactericidal performance of liquid detergent produced by the present invention, to above-described embodiment 1, implement
Example 2, comparative example 1,2 method of comparative example correspond to liquid detergent obtained, are done the wash once with clear water after cleaning porcelain service plate,
The liquid detergent residual quantity for detecting every plate records cleaning effect as follows：
Table 1
Ginger extract and tangerine essential oil are not added in comparative example 1 it can be seen from upper table 1 and comparative example 2, it is multiple
Weaken with liquid detergent antibacterial obtained and dirt-removing power；Press down with very strong sterilization antibacterial by liquid detergent made from the method for the present invention
Bacterium performance, dirt-removing power is strong, has pomelo fragrant smell, Low-foam and easily cleaning, stability is strong, safe to use, great popularization
Use value and the market competitiveness.
Claims (6)
1. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell, which is characterized in that include the following steps：
（1）The extraction of Wedelia trilobata volatile oil：
The aerial part of 5-10 parts of Wedelia trilobatas is acquired, dust removal is cleaned, dries in the shade, shredded, with extraction by steam distillation 2-
After 3h, add sodium chloride to being saturated, stood after stirring, separate oil reservoir, dried with anhydrous sodium sulfate, obtains Wedelia trilobata volatilization
Oil；
（2）The preparation of ginger extract：
5-10 parts of fresh gingers are smashed to pieces with mortar, 1:The absolute ethyl alcohol mechanical shaking extraction 3- that volume fraction is 90-95% is added in 3-4
4h is extracted 2-3 times altogether, is merged extracting solution, is filtered, is then concentrated at 48-52 DEG C, obtain ginger extract；
（3）The preparation of plant type Antibiotic liquid detergent：
280-320 parts of deionized waters are heated to 44-46 DEG C, surfactant are added while stirring, then be cooled to 34-36 DEG C,
5-7 parts of lauric acid diethyl amides, 15-20 parts of urea and 1-2 parts of sodium cellulose glycolate stirring and dissolvings are added, trilobated leaf is added
Wedelia chinensis volatile oil, ginger extract, Chinese cassia tree extracting solution, tangerine essential oil, pomelo peel soaked extracting solution and wormwood volatile oil, are stirred
It mixes uniformly, it is 7.5 to adjust pH with trisodium citrate and sodium hydrate aqueous solution, and 20-25 parts of sodium chloride are added, and side edged shakes up,
It is got product until sticky.
2. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell according to claim 1, feature exist
In step（3）The preparation of middle Chinese cassia tree extracting solution：
Cassia is broken for 40 mesh, into 15-20 parts of cassia powder 1:Distilled water is added in 20-25, adds auxiliary agent sodium chloride,
Ebuillition of heated 1-2h obtains the Chinese cassia tree extracting solution that mass fraction is 15-20%.
3. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell according to claim 1, feature exist
In step（3）The ethyl alcohol and ultrasonic extraction of middle tangerine essential oil：
Fresh complete orange peel is cleaned with clear water, dipping pretreatment is anti-in the VC solution that mass fraction is 0.15-0.3%
Then block is dried to Shui in 43-47 DEG C of baking oven and divides Han Liang≤14%, crushed through pulverizer, 40 mesh sieve is crossed, to 5-10 parts
Solid-liquid ratio 1 is pressed in dry orange peel powder:Absolute ethyl alcohol is added in 5-6g/mL, and after ultrasonic extraction 1-2d, decompression water bath with thermostatic control distillation obtains
Tangerine essential oil.
4. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell according to claim 1, feature exist
In step（3）Middle pomelo peel soaked extracting solution：
By fresh grapefruit peeling, remove the white wooden dipper in pomelo peel, solid-liquid ratio 1 is pressed into 10-15 parts of pomelo peels:30-35 is added dense
Degree is the ethanol solution of 20-25%, is protected from light immersion one week, obtains pomelo peel soaked extracting solution.
5. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell according to claim 1, feature exist
In step（3）The extraction of middle wormwood volatile oil：
Acquisition wormwood aerial part is cleaned, dries in the shade, is shredded, and the broken extraction by steam distillation 2-3h of 8-10 parts of wormwoods is added
Sodium chloride powder stands after stirring to being saturated, separates oil reservoir, dried with anhydrous sodium sulfate, obtain wormwood volatile oil.
6. a kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell according to claim 1, feature exist
In step（3）Middle surfactant is by 16-20 parts of fatty alcohol polyoxyethylene ether, 22-26 parts of neopelexes, 30-40
Part sodium sulfate of polyethenoxy ether of fatty alcohol composition.
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| CN110699197A (en) * | 2019-09-18 | 2020-01-17 | 重庆第二师范学院 | Preparation method and preparation system of pepper degerming soap |
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