CN107903050A - 一种基于五球连磨***的瓷质砖的制备工艺 - Google Patents

一种基于五球连磨***的瓷质砖的制备工艺 Download PDF

Info

Publication number
CN107903050A
CN107903050A CN201711317551.0A CN201711317551A CN107903050A CN 107903050 A CN107903050 A CN 107903050A CN 201711317551 A CN201711317551 A CN 201711317551A CN 107903050 A CN107903050 A CN 107903050A
Authority
CN
China
Prior art keywords
balls
system based
porcelain tiles
preparation process
imitation rock
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711317551.0A
Other languages
English (en)
Inventor
陈晓宣
黄大平
周海龙
洪敏�
周伟峰
薛细亮
吴谋胜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong Crown Star Ceramic Enterprise Co Ltd
Original Assignee
Guangdong Crown Star Ceramic Enterprise Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangdong Crown Star Ceramic Enterprise Co Ltd filed Critical Guangdong Crown Star Ceramic Enterprise Co Ltd
Priority to CN201711317551.0A priority Critical patent/CN107903050A/zh
Publication of CN107903050A publication Critical patent/CN107903050A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/85—Coating or impregnation with inorganic materials
    • C04B41/86—Glazes; Cold glazes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567—Treatment time

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Finishing Walls (AREA)

Abstract

本发明涉及陶瓷领域，具体地说，涉及一种基于五球连磨***的瓷质砖的制备工艺，所述的工艺包括：步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；步骤2：压坯，将球磨后的原料压坯成为预设规格；步骤3：干燥，将压坯后的砖体通过干燥窑干燥；所述的干燥工艺参数为160‑200℃下干燥40‑60min。步骤4：施釉，在干燥后的坯体表面布施釉层和印花；步骤5：烧制；烧制工艺为1190‑1220℃，烧制时间60‑70min。其中，所述的原料由以下组分组成：SiO2 65‑68％；Al2O3 18‑21％；Fe2O3≤1.0；CaO+MgO 1‑2％；K2O+Na2O 5.5‑7％；烧失量4‑7％；本发明的目的是提供一种基于五球连磨***的瓷质砖的制备工艺，通过该工艺制备得到的瓷质砖吸水率能够控制在0.02％以下。

Description

一种基于五球连磨***的瓷质砖的制备工艺
技术领域
本发明涉及陶瓷领域，具体地说，涉及一种基于五球连磨***的瓷质砖的制备工艺。
背景技术
瓷质砖具有天然石材的质感，而且更具有高光性、高硬度、高耐磨、高抗污性、吸水率低，色差少以及规格多样化和色彩丰富的优点，是室内、厨房、卫浴间常用的墙面和地面材料。
现有的瓷质砖国标要求吸水率要控制在0.5％以下，但是，针对于瓷质砖的吸水率，客户的要求更为严苛，如果能够控制在0.02％以下，则产品竞争力更大。
发明内容
本发明的目的是提供一种基于五球连磨***的瓷质砖的制备工艺，通过该工艺制备得到的瓷质砖吸水率能够控制在0.02％以下。
本发明提供的技术方案为：一种基于五球连磨***的瓷质砖的制备工艺，所述的工艺包括：
步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；
步骤2：压坯，将球磨后的原料压坯成为预设规格；
步骤3：干燥，将压坯后的砖体通过干燥窑干燥；
步骤4：施釉，在干燥后的坯体表面布施釉层和印花；
步骤5：烧制；
其中，所述的原料由以下组分组成：
SiO2 65-68％；Al2O3 18-21％；Fe2O3≤1.0；CaO+MgO 1-2％；K2O+Na2O 5.5-7％；烧失量4-7％。
在上述的基于五球连磨***的瓷质砖的制备工艺中，所述的原料在五个球磨罐的球磨时间为1.4-1.8h。
在上述的基于五球连磨***的瓷质砖的制备工艺中，所述的原料在五个球磨罐的球磨时间为1.5h
在上述的基于五球连磨***的瓷质砖的制备工艺中，所述的干燥温度为160-200℃。
在上述的基于五球连磨***的瓷质砖的制备工艺中，所述的烧制工艺为1190-1220℃，烧制时间60-70min。
有益效果：
本发明采用五球连磨技术，辅以原材料的进一步优选，使烧制出来的瓷质砖吸水率达到0.02％以下。
本发明实现了原料的标准化，通过五球连磨技术，使物料充分混合，标准化程度高。
并且为产能的提高提供了保障，并且保证了产品质量的恒定，降低了占地面积。
具体实施方式
下面结合具体实施方式，对本发明的技术方案作进一步的详细说明，但不构成对本发明的任何限制。
实施例一
一种基于五球连磨***的瓷质砖的制备工艺，所述的工艺包括：
步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；
步骤2：压坯，将球磨后的原料压坯成为预设规格；
步骤3：干燥，将压坯后的砖体通过干燥窑干燥；所述的干燥工艺参数为160-200℃下干燥40-60min。
步骤4：施釉，在干燥后的坯体表面布施釉层和印花；
步骤5：烧制；烧制工艺为1190-1220℃，烧制时间70min。
其中，所述的原料由以下组分组成：
SiO2 67.5％；Al2O3 19％；Fe2O3≤1.0；CaO+MgO 1.5％；K2O+Na2O 6％；烧失量5％。
所述的原料在五个球磨罐的球磨时间为1.5h。
实施例二
一种基于五球连磨***的瓷质砖的制备工艺，所述的工艺包括：
步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；
步骤2：压坯，将球磨后的原料压坯成为预设规格；
步骤3：干燥，将压坯后的砖体通过干燥窑干燥；所述的干燥工艺参数为160-200℃下干燥40-60min。
步骤4：施釉，在干燥后的坯体表面布施釉层和印花；
步骤5：烧制；烧制工艺为1190-1220℃，烧制时间60min。
其中，所述的原料由以下组分组成：
SiO2 65％；Al2O3 21％；Fe2O3≤1.0；CaO+MgO 2％；K2O+Na2O 7％；烧失量4％。
所述的原料在五个球磨罐的球磨时间为1.6h。
实施例三
一种基于五球连磨***的瓷质砖的制备工艺，所述的工艺包括：
步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；
步骤2：压坯，将球磨后的原料压坯成为预设规格；
步骤3：干燥，将压坯后的砖体通过干燥窑干燥；所述的干燥工艺参数为160-200℃下干燥40-60min。
步骤4：施釉，在干燥后的坯体表面布施釉层和印花；
步骤5：烧制；烧制工艺为1190-1220℃，烧制时间64min。
其中，所述的原料由以下组分组成：
SiO2 68％；Al2O3 19％；Fe2O3≤1.0；CaO+MgO 1％；K2O+Na2O 5.5％；烧失量6.5％。
所述的原料在五个球磨罐的球磨时间为1.4h。
测试结果
实施例1-3的吸水率均低于0.01％。并且，上述实施例1-3采用五球连磨技术，也达到了原料的标准化、生产的稳定化、占地面积的优化的目的。
上述实施例为本发明较佳的实施方式，但本发明的实施方式并不受上述实施例的限制，其它的任何未背离本发明的精神实质与原理下所作的改变、修饰、替代、组合、简化，均应为等效的置换方式，都包含在本发明的保护范围之内。

Claims (5)

1.一种基于五球连磨***的瓷质砖的制备工艺，其特征在于：所述的工艺包括：
步骤1：球磨，将原料注入串联的五个球磨罐中进行球磨；
步骤2：压坯，将球磨后的原料压坯成为预设规格；
步骤3：干燥，将压坯后的砖体通过干燥窑干燥；
步骤4：施釉，在干燥后的坯体表面布施釉层和印花；
步骤5：烧制；
其中，所述的原料由以下组分组成：
SiO2 65-68％；Al2O3 18-21％；Fe2O3≤1.0；CaO+MgO 1-2％；K2O+Na2O 5.5-7％；烧失量4-7％。
2.根据权利要求1所述的基于五球连磨***的瓷质砖的制备工艺，其特征在于：所述的原料在五个球磨罐的球磨时间为1.4-1.8h。
3.根据权利要求1所述的基于五球连磨***的瓷质砖的制备工艺，其特征在于：所述的原料在五个球磨罐的球磨时间为1.5h。
4.根据权利要求1所述的基于五球连磨***的瓷质砖的制备工艺，其特征在于：所述的干燥温度为160-200℃。
5.根据权利要求1所述的基于五球连磨***的瓷质砖的制备工艺，其特征在于：所述的烧制工艺为1190-1220℃，烧制时间60-70min。
CN201711317551.0A 2017-12-12 2017-12-12 一种基于五球连磨***的瓷质砖的制备工艺 Pending CN107903050A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711317551.0A CN107903050A (zh) 2017-12-12 2017-12-12 一种基于五球连磨***的瓷质砖的制备工艺

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711317551.0A CN107903050A (zh) 2017-12-12 2017-12-12 一种基于五球连磨***的瓷质砖的制备工艺

Publications (1)

Publication Number Publication Date
CN107903050A true CN107903050A (zh) 2018-04-13

Family

ID=61865298

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711317551.0A Pending CN107903050A (zh) 2017-12-12 2017-12-12 一种基于五球连磨***的瓷质砖的制备工艺

Country Status (1)

Country Link
CN (1) CN107903050A (zh)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101224980A (zh) * 2008-01-28 2008-07-23 关锐华 一种瓷质通体仿古砖的生产方法
CN101284729A (zh) * 2008-06-04 2008-10-15 关锐华 一种瓷质通体抛光金碧石砖的生产方法
CN103693942A (zh) * 2013-11-27 2014-04-02 广东家美陶瓷有限公司 低温快速烧成陶瓷砖及生产工艺
CN106747479A (zh) * 2016-12-26 2017-05-31 广东博晖机电有限公司 一种可线上配料的陶瓷原料湿法制粉生产线及其工作方式

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101224980A (zh) * 2008-01-28 2008-07-23 关锐华 一种瓷质通体仿古砖的生产方法
CN101284729A (zh) * 2008-06-04 2008-10-15 关锐华 一种瓷质通体抛光金碧石砖的生产方法
CN103693942A (zh) * 2013-11-27 2014-04-02 广东家美陶瓷有限公司 低温快速烧成陶瓷砖及生产工艺
CN106747479A (zh) * 2016-12-26 2017-05-31 广东博晖机电有限公司 一种可线上配料的陶瓷原料湿法制粉生产线及其工作方式

Similar Documents

Publication Publication Date Title
CN107032772B (zh) 一种透光陶瓷砖及其制备方法
CN104591687B (zh) 广色域喷墨釉饰陶瓷地砖及其生产工艺
CN107216127B (zh) 德化珍珠白瓷器及其制备工艺
CN100469734C (zh) 一种超薄瓷质抛光砖及其制作工艺
CN102503365A (zh) 玉青白胎瓷器的制作工艺
CN104130032B (zh) 一种抛釉砖的制造方法及其产品
CN105218170B (zh) 一种高硬度高耐磨免抛光铁系微晶玻璃陶瓷复合板及其制备方法
CN101747089A (zh) 一种汝窑玛瑙釉及其加工方法和应用
CN104016667A (zh) 一种中温镁质强化瓷的制备方法及其制得的产品
CN104211446A (zh) 一种仿天然石材砖的制备方法
CN107857475A (zh) 一种白瓷釉料
CN101786844B (zh) 一种轻质保温砖及其制造方法
CN110228993A (zh) 一种具有内面非裂纹釉的裂纹青瓷化妆品瓶加工工艺
CN108892478B (zh) 一种低温瓷及其制备方法
CN103708811B (zh) 抛光砖及其制备方法和应用
CN107382065B (zh) 一种青瓷秘色釉及其制备方法和秘色釉瓷
CN113402265A (zh) 一种白底黑花釉瓷及其制备方法
CN107244908B (zh) 一种高白仿玉石抛光砖砖坯及其瓷砖制备方法
CN108726871A (zh) 绿釉陶瓷工艺品的制备方法
CN105294091B (zh) 一种同窑炉烧制双规格仿古砖的生产方法
CN106518008A (zh) 一种高强度瓷绝缘子及其制备方法
CN107903050A (zh) 一种基于五球连磨***的瓷质砖的制备工艺
CN108046603A (zh) 一种一式多类的陶瓷砖的制作方法
CN103086697B (zh) 一种高钙陶瓷及其制备工艺
KR101262809B1 (ko) 주입성형이 가능한 분청소지 조성물 및 이를 이용한 분청도자기의 제조방법

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180413