CN107586223A - A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function and preparation method thereof - Google Patents

A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function and preparation method thereof Download PDF

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CN107586223A
CN107586223A CN201710802826.3A CN201710802826A CN107586223A CN 107586223 A CN107586223 A CN 107586223A CN 201710802826 A CN201710802826 A CN 201710802826A CN 107586223 A CN107586223 A CN 107586223A
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parts
fertilizer
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biological compound
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曾清
吴运清
曹真真
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HENAN EZHONG FERTILIZER Co Ltd
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HENAN EZHONG FERTILIZER Co Ltd
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Abstract

It is as made from the raw material of following parts by weight the invention discloses a kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function and preparation method thereof:92 94 parts of particle cores fertilizer, 23 parts of Lauxite coating agent, 47 parts of complex micro organism fungicide.The present invention has the high-tower granulation biological compound fertilizer composition collocation of prevention and control pest and disease damage function reasonable, by the synergy of each nutrient, crop is promoted rationally to absorb the balance of nutrient, activating soil nutrient, improve soil texture, the soil weight is reduced, pathogen in effective prevention and control soil, strength growth-promoting root, suppress soil degradation, fertilizer conservation, the water holding capacity of soil are improved, while there are good prevention and control to act on to nematode and subterranean pest-insect, to realizing that agricultural sustainable development is significant.

Description

A kind of high-tower granulation biological compound fertilizer and its preparation with prevention and control pest and disease damage function Method
Technical field
The present invention relates to compound fertilizer field, and in particular to a kind of high-tower granulation biology with prevention and control pest and disease damage function is multiple Hefei and preparation method thereof.
Background technology
China is populous nation, a large agricultural country, and the population in the Liao Zhan worlds 22% is supported with the soil for accounting for the world 7%, Food problem is the major issue for being related to national economy forever.Existing 2,000,000,000 mu of the arable land in China, needs 1.5 hundred million tons of chemical fertilizer year, is the world Maximum chemical fertilizer importer and nitrogen fertilizer production state.Nevertheless, chemical fertilizer amount does not still meet the needs of agricultural development.Study carefully it Reason, key issue are that the utilization rate of chemical fertilizer is too low.According to investigations, the utilization rate of China's chemical fertilizer only has 35-40%, its remaining part Divide and the environmental problems such as water pollution, lake eutrophication are caused by soil fixing, or leaching.
Chemical fertilizer is developed into from farm manure in the prior art, the application of chemical fertilizer makes agricultural production have the development of leap, but changes Fertilizer pollution environment, hardened soil, destroys soil texture, many beneficial microbes in soil is gradually decreased or even is become extinct, so as to Decline soil fertility, the defects of crop quality deteriorates.In addition, the application of organic fertilizers material on the soil for applied chemical fertilizer, due to lacking Weary beneficial microorganism decomposition, prevents wherein nutrient to be absorbed from discharging by crop, thus utilization rate of fertilizer Low, fertilizer efficiency is poor.Have to use the amount of application for increasing chemical fertilizer to increase soil fertility, so go down for a long time, on the one hand certainly will be Soil hardening in family, soil granular structure destroy, and soil fertility is more declined, and on the other hand make farm investment cumulative year after year again.This With country advocated develop eco-agriculture, realize No-harmful apple orchard proposal run in the opposite direction.
Microorganism fertilizer is a kind of to cause crops to obtain the micro- of specific fertilizer effect with microbial life activity and its product Biological living product, it is in culture fertility, raising chemical fertilizer utilization ratio, the suppression harmful substance such as crops heavy metal and agricultural chemicals Absorption, purification and rehabilitating soil, promote the decomposed utilization of agricultural crop straw and municipal refuse, improve the side such as quality of agricultural product Face plays the role of irreplaceable.The effect of microbial manure plays mainly to be made by the synergy to traditional fertilizer, organic fertilizer Realized with, the improvement activation to soil, and the mode such as physiological action of microorganism.In the market agricultural Microbial bacterial agent is mainly single microorganism fungus kind, and the synergy of crops is weak, without the effect of prevention and control pest and disease damage, Crop yield effect is unsatisfactory.So it is a kind of good with prevention and control pest and disease damage function, effect of increasing production to be badly in need of exploitation at present Biologic compound fertilizer.
The content of the invention
The invention provides a kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, biological compound fertilizer tool Have that prevention and control pest and disease damage function, effect of increasing production be good, excellent properties of high-efficiency environment friendly.
The invention also discloses the preparation method of the high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function.
The technical solution adopted by the present invention is as follows:
A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is made by the raw material of following parts by weight 's:Particle cores fertilizer 92-94 parts, Lauxite coating agent 2-3 parts, complex micro organism fungicide 4-7 parts;
The particle cores fertilizer is as made from the raw material of following parts by weight:Urea 500-530 parts, ammonium sulfate 60-80 parts, phosphorus Sour ammonium 100-130 parts, double superhosphate 40-60 parts, reinforcing agent 3-5 parts, pulullan polysaccharide 2-4 parts, potassium sulfate 220-240 Part, potassium dihydrogen phosphate 15-25 parts, ammonium molybdate 3-5 parts, magnesium sulfate 10-15 parts, rare earth element 0.05-0.5 parts, 10% imidacloprid Wettable powder 10-15 parts, AVM 3-5 parts;
The Lauxite coating agent is as made from the raw material of following parts by weight:Urea 18-28 parts, formaldehyde 27-29 parts, α-methylglucoside 1-3 parts, polyoxypropylene ethylene oxide glycerin ether 0.9-1.1 parts;
The complex micro organism fungicide be by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii according to 1:1-2:Made from 1.5-2.5 weight ratio.
Described, reinforcing agent is by nano-TiO2Modified SiO2Aeroge, α-ketoglutaric acid and ethylenediamine tetra-acetic acid are according to 1: 1.5-2:Made from 1-1.5 weight ratio.
Described, nano-TiO2Modified SiO2Aeroge is as made from following methods:By the 50% of glacial acetic acid total amount, titanium Acid butyl ester and ethanol are placed in triangular flask, are well mixed, add Nano-meter SiO_22Aeroge, ultrasonic 15min, obtains solution A;Remainder The glacial acetic acid of amount is added dropwise in solution A, is added dropwise, and is moved to magnetic stirring apparatus and is stirred 1-2h, still aging 24h at room temperature, Obtain white gels;5h will be dried in vacuo at 100 DEG C of white gels, be transferred to Muffle furnace roasting 6h, be cooled to room temperature, obtains nano-TiO2 Modified SiO2Aeroge.
Described, complex micro organism fungicide is as made from following steps:By coral Nocard's bacillus, the red false unit cell in marsh Bacterium and Acinetobacter baumannii activation after cultivate 15h at 25 DEG C in liquid seed culture medium respectively, then according to 1% inoculation Amount be transferred in sterilized big tank culture medium, 30 DEG C cultivate 20h after, by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii freezes and freeze-dried powder is made, obtain complex micro organism fungicide by weight being well mixed.
It is described, liquid seed culture medium be 5% sucrose, 2% peptone, 2% corn flour, 0.1% potassium dihydrogen phosphate, 0.05% sodium chloride and surplus sterilized water composition;The big tank culture medium be 5% peptone, 3% beef extract, 1% sucrose, 15% corn flour, 3% starch, 0.1% potassium chloride and surplus sterilized water composition.
Described, the pH of liquid seed culture medium and big tank culture medium is 6.5.
A kind of preparation method of the high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is prepared by following steps Obtain:
1) formula ratio Urea is melted to form urea melting liquid, then by ammonium sulfate, MAP, weight peroxophosphoric acid Calcium, reinforcing agent, pulullan polysaccharide, potassium sulfate, potassium dihydrogen phosphate, ammonium molybdate, magnesium sulfate, rare earth element, 10% imidacloprid are wettable Property pulvis and AVM be added thereto, be mixed to form slurry, then by the slurry be sent into granulation tower using tower solution granulation Technique is granulated to obtain particle cores fertilizer of the particle diameter in 2-3.5mm;
2) formaldehyde is added in reactive tank, adds the urea of 50% weight while stirring, add methyl glucose glucoside With polyoxypropylene ethylene oxide glycerin ether, sodium hydroxide regulation pH value 7.5,100 DEG C of reaction 40min are warming up to;Add residue 50% weight urea, phosphorus acid for adjusting pH value be 4,65 DEG C reaction 1h, obtain Lauxite coating agent;
3) particle cores fertilizer is placed in coating machine, Lauxite coating agent is carried out at a coating to particle cores fertilizer spraying Reason, water content is dried to less than 15%;Face powder aluminum coated steel is carried out to the particle after drying with complex micro organism fungicide again, obtained High-tower granulation biological compound fertilizer with prevention and control pest and disease damage function.
The present invention has the high-tower granulation biological compound fertilizer nutrient formula of prevention and control pest and disease damage function reasonable, has and provides plant Balanced nutrients effect of growth, 10% imidacloprid wettable powder and AVM have good to nematode and subterranean pest-insect Prevention and control act on, and reinforcing agent and pulullan polysaccharide are obviously improved 10% imidacloprid wettable powder and AVM to nematode and ground The drug effect of lower insect, while 10% imidacloprid wettable powder and AVM play facilitation to plant growth;By more than Multiple components are well mixed to produce multi-element particle core fertilizer by high tower process units, then using Lauxite coating agent And complex micro organism fungicide carries out coating twice to particle cores fertilizer and handled;By increasing Alpha-Methyl in Lauxite coating agent Glycoside and polyoxypropylene ethylene oxide glycerin ether, the consistency of coating is improved, the mechanical property of gained coating is good, dissolution Degree is high, while can be effectively isolated complex micro organism fungicide and inorganic fertilizer, improves complex micro organism fungicide and the compound rear bacterium of chemical fertilizer The living environment of kind, significantly improve the survival rate of functional microbial microbial inoculum.Complex micro organism fungicide face powder aluminum coated steel, respectively Strain acts synergistically after liquid seed culture medium and big tank medium treatment, can suppress growth, the breeding of pathogen, Protective barrier is formed in root system, mitigates the generation of soil-borne disease to greatest extent, significantly improves stress resistance of plant and root system nutrition Absorb, while fully decompose phosphorus, potassium and the mineral matter of indissoluble in soil, improve utilization rate of fertilizer.
Beneficial effects of the present invention:
The present invention has the high-tower granulation biological compound fertilizer composition collocation of prevention and control pest and disease damage function reasonable, passes through each nutrition member The synergy of element, promote crop rationally to absorb the balance of nutrient, activating soil nutrient, improve soil texture, reduce The soil weight, pathogen in effective prevention and control soil, strength growth-promoting root, suppress soil degradation, improve fertilizer conservation, the water conservation energy of soil Power, while there are good prevention and control to act on to nematode and subterranean pest-insect, to realizing that agricultural sustainable development is significant.
Embodiment
With reference to specific embodiment, the present invention is further illustrated, but the present invention is not limited by following embodiments It is fixed.
AVM used in the present invention for white or yellow crystal, 150-155 DEG C of fusing point.
Coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii used in the present invention are commercially available prod.
Embodiment 1
A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is made by the raw material of following parts by weight 's:92 parts of particle cores fertilizer, 3 parts of Lauxite coating agent, 7 parts of complex micro organism fungicide;
The particle cores fertilizer is as made from the raw material of following parts by weight:530 parts of urea, 80 parts of ammonium sulfate, MAP 100 parts, 40 parts of double superhosphate, 3 parts of reinforcing agent, 2 parts of pulullan polysaccharide, 240 parts of potassium sulfate, 15 parts of potassium dihydrogen phosphate, molybdenum Sour 3 parts of ammonium, 15 parts of magnesium sulfate, 0.05 part of rare earth element, 15 parts of 10% imidacloprid wettable powder, 5 parts of AVM;
The Lauxite coating agent is as made from the raw material of following parts by weight:18 parts of urea, 29 parts of formaldehyde, Alpha-Methyl 3 parts of glycoside, 0.9 part of polyoxypropylene ethylene oxide glycerin ether;
The complex micro organism fungicide be by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii according to 1:1:Made from 2.5 weight ratio.
Described, reinforcing agent is by nano-TiO2Modified SiO2Aeroge, α-ketoglutaric acid and ethylenediamine tetra-acetic acid are according to 1: 1.5:Made from 1 weight ratio.
Described, nano-TiO2Modified SiO2Aeroge is as made from following methods:By the 50% of glacial acetic acid total amount, titanium Acid butyl ester and ethanol are placed in triangular flask, are well mixed, add Nano-meter SiO_22Aeroge, ultrasonic 15min, obtains solution A;Remainder The glacial acetic acid of amount is added dropwise in solution A, is added dropwise, and is moved to magnetic stirring apparatus and is stirred 1-2h, still aging 24h at room temperature, Obtain white gels;5h will be dried in vacuo at 100 DEG C of white gels, be transferred to Muffle furnace roasting 6h, be cooled to room temperature, obtains nano-TiO2 Modified SiO2Aeroge.
Described, complex micro organism fungicide is as made from following steps:By coral Nocard's bacillus, the red false unit cell in marsh Bacterium and Acinetobacter baumannii activation after cultivate 15h at 25 DEG C in liquid seed culture medium respectively, then according to 1% inoculation Amount be transferred in sterilized big tank culture medium, 30 DEG C cultivate 20h after, by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii freezes and freeze-dried powder is made, obtain complex micro organism fungicide by weight being well mixed.
It is described, liquid seed culture medium be 5% sucrose, 2% peptone, 2% corn flour, 0.1% potassium dihydrogen phosphate, 0.05% sodium chloride and surplus sterilized water composition;The big tank culture medium be 5% peptone, 3% beef extract, 1% sucrose, 15% corn flour, 3% starch, 0.1% potassium chloride and surplus sterilized water composition.
Described, the pH of liquid seed culture medium and big tank culture medium is 6.5.
A kind of preparation method of the high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is prepared by following steps Obtain:
1) formula ratio Urea is melted to form urea melting liquid, then by ammonium sulfate, MAP, weight peroxophosphoric acid Calcium, reinforcing agent, pulullan polysaccharide, potassium sulfate, potassium dihydrogen phosphate, ammonium molybdate, magnesium sulfate, rare earth element, 10% imidacloprid are wettable Property pulvis and AVM be added thereto, be mixed to form slurry, then by the slurry be sent into granulation tower using tower solution granulation Technique is granulated to obtain particle cores fertilizer of the particle diameter in 2-3.5mm;
2) formaldehyde is added in reactive tank, adds the urea of 50% weight while stirring, add methyl glucose glucoside With polyoxypropylene ethylene oxide glycerin ether, sodium hydroxide regulation pH value 7.5,100 DEG C of reaction 40min are warming up to;Add residue 50% weight urea, phosphorus acid for adjusting pH value be 4,65 DEG C reaction 1h, obtain Lauxite coating agent;
3) particle cores fertilizer is placed in coating machine, Lauxite coating agent is carried out at a coating to particle cores fertilizer spraying Reason, water content is dried to less than 15%;Face powder aluminum coated steel is carried out to the particle after drying with complex micro organism fungicide again, obtained High-tower granulation biological compound fertilizer with prevention and control pest and disease damage function.
Embodiment 2
A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is made by the raw material of following parts by weight 's:93 parts of particle cores fertilizer, 2 parts of Lauxite coating agent, 5 parts of complex micro organism fungicide;
The particle cores fertilizer is as made from the raw material of following parts by weight:515 parts of urea, 70 parts of ammonium sulfate, MAP 115 parts, 50 parts of double superhosphate, 4 parts of reinforcing agent, 3 parts of pulullan polysaccharide, 230 parts of potassium sulfate, 20 parts of potassium dihydrogen phosphate, molybdenum Sour 4 parts of ammonium, 13 parts of magnesium sulfate, 0.3 part of rare earth element, 13 parts of 10% imidacloprid wettable powder, 4 parts of AVM;
The Lauxite coating agent is as made from the raw material of following parts by weight:24 parts of urea, 28 parts of formaldehyde, Alpha-Methyl 2 parts of glycoside, 1 part of polyoxypropylene ethylene oxide glycerin ether;
The complex micro organism fungicide be by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii according to 1:1.5:Made from 2 weight ratio.
Described, reinforcing agent is by nano-TiO2Modified SiO2Aeroge, α-ketoglutaric acid and ethylenediamine tetra-acetic acid are according to 1: 1.8:Made from 1.3 weight ratio.
Remaining is the same as embodiment 1.
Embodiment 3
A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, is made by the raw material of following parts by weight 's:94 parts of particle cores fertilizer, 3 parts of Lauxite coating agent, 4 parts of complex micro organism fungicide;
The particle cores fertilizer is as made from the raw material of following parts by weight:500 parts of urea, 60 parts of ammonium sulfate, MAP 130 parts, 60 parts of double superhosphate, 5 parts of reinforcing agent, 4 parts of pulullan polysaccharide, 220 parts of potassium sulfate, 25 parts of potassium dihydrogen phosphate, molybdenum Sour 5 parts of ammonium, 10 parts of magnesium sulfate, 0.5 part of rare earth element, 10 parts of 10% imidacloprid wettable powder, 3 parts of AVM;
The Lauxite coating agent is as made from the raw material of following parts by weight:28 parts of urea, 27 parts of formaldehyde, Alpha-Methyl 1 part of glycoside, 1.1 parts of polyoxypropylene ethylene oxide glycerin ether;
The complex micro organism fungicide be by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii according to 1:2:Made from 1.5 weight ratio.
Described, reinforcing agent is by nano-TiO2Modified SiO2Aeroge, α-ketoglutaric acid and ethylenediamine tetra-acetic acid are according to 1: 2:1.5 weight ratio made from.
Remaining is the same as embodiment 1.
Comparative example 1
A kind of high-tower granulation biological compound fertilizer, it is as made from the raw material of following parts by weight:Particle cores fertilizer 93 parts, ureaformaldehyde tree 2 parts of fat coating agent, 5 parts of complex micro organism fungicide;
The particle cores fertilizer is as made from the raw material of following parts by weight:515 parts of urea, 70 parts of ammonium sulfate, MAP 115 parts, 50 parts of double superhosphate, 230 parts of potassium sulfate, 20 parts of potassium dihydrogen phosphate, 4 parts of ammonium molybdate, 13 parts of magnesium sulfate, rare earth member 0.3 part of element, 13 parts of 10% imidacloprid wettable powder, 4 parts of AVM;
The Lauxite coating agent is as made from the raw material of following parts by weight:24 parts of urea, 28 parts of formaldehyde, Alpha-Methyl 2 parts of glycoside, 1 part of polyoxypropylene ethylene oxide glycerin ether;
The complex micro organism fungicide be by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii according to 1:1.5:Made from 2 weight ratio.
Remaining is the same as embodiment 1.
Comparative example 2
A kind of high-tower granulation biological compound fertilizer, it is as made from the raw material of following parts by weight:Particle cores fertilizer 93 parts, ureaformaldehyde tree 2 parts of fat coating agent;
The particle cores fertilizer is as made from the raw material of following parts by weight:515 parts of urea, 70 parts of ammonium sulfate, MAP 115 parts, 50 parts of double superhosphate, 230 parts of potassium sulfate, 20 parts of potassium dihydrogen phosphate, 4 parts of ammonium molybdate, 13 parts of magnesium sulfate, rare earth member 0.3 part of element, 13 parts of 10% imidacloprid wettable powder, 4 parts of AVM;
The Lauxite coating agent is as made from the raw material of following parts by weight:24 parts of urea, 28 parts of formaldehyde, Alpha-Methyl 2 parts of glycoside, 1 part of polyoxypropylene ethylene oxide glycerin ether;
Remaining is the same as embodiment 1.
Apple application effect example
Experimental field:It is chosen within 2015 Henan Province somewhere apple cooperative society apple orchard to be tested, tests soil productivity Situation is:PH value is:5.3, organic matter 13.5g/kg, alkali-hydrolyzable nitrogen 63.4mg/kg, rapid available phosphorus 29mg/kg, available potassium 43.8mg/ kg.Land leveling, soil fertility are uniform.
Test method and material:Experimental cultivar is Fuji apple, and the age of tree 7 years is each to handle test tree 20, size growing way base This is consistent, area per hill 15m2, roll over 667m230 plants of plantation.Experiment sets 5 processing, and the processing method of each treatment group is in fruit Tree early growth period is made base manure trench digging row replacement and is manured into soil, and each treatment group dose is identical, and wherein T1 is that to apply the present invention real Apply the high-tower granulation biological compound fertilizer treatment group of the preparation of example 1;T2 is that the high-tower granulation biology prepared using the embodiment of the present invention 2 is multiple Hefei treatment group;T3 is the high-tower granulation biological compound fertilizer treatment group prepared using the embodiment of the present invention 3;T4 is to apply to contrast High-tower granulation biological compound fertilizer control group prepared by example 1;T5 is that the high-tower granulation biological compound fertilizer prepared using comparative example 2 compares Group.The each treatment group all same of other field management.Pluck whole fruits weigh statistics yield, and to it is each processing group selection 4 The identical apple tree of tree vigo(u)r plucks whole fruits, and classification is weighed statistics yield, and the solubility of fruit is determined with portable saccharous detector Solid content, and scene is measured tree vigo(u)r.Result of the test is as shown in table 1.
The different disposal group fruit morphology character analysis statistical result of table 1
From the result of above-mentioned table 1 as can be seen that the present invention high-tower granulation biological compound fertilizer obvious effect of increasing production, and from It can be obtained in fruit morphology analysis, it is per plant number, mean fruit weight, every after fertilizer of the present invention compared with T5 groups 667m2Yield is significantly increased, and rate of growth may be up to 54.5%, and effect of increasing production is fairly obvious.And T1-T3 treatment group fruits are solvable Property solid content is also of a relatively high.
The present invention is investigated the pest and disease damage of above-mentioned different disposal group fruit tree, and a situation arises and is counted, and statistical result is such as Shown in table 2 below -3.
The different disposal group apple disease situation statistical result of table 2
Remarks:Prevention effect=(T5 control groups diseased fruit rate-treatment group diseased fruit rate)/T5 control group diseased fruit rate × 100%.
The different disposal group apple insect pest situation statistical result of table 3
Remarks:Prevention effect=(T5 control groups diseased fruit rate-treatment group diseased fruit rate)/T5 control group diseased fruit rate × 100%.
Find out from table 2 and table 3:Apple pest species is various, and field generally occurs, trial zone apple prevalence pest and disease damage master Will based on apple marssonina leaf spot, apple anthracnose, aphid, aphid, leaf roller, small heart-eating peach worm etc., also have a small number of apples by Eelworm harm.Under the conditions of identical pest management, for T1-T3 compared with T5, the prevention effect of apple marssonina leaf spot reaches 36.9%, Apple anthracnose prevention effect reaches 45.8%, has reached 31.3% to the preventive effect of the sucking pests such as aphid, aleyrodid, mite class, Control of nematode effect reaches 34.3%, therefore, compared with control treatment group T5, pest and disease damage incidence after Fertilizer application of the invention Significantly reduce, thus fruit significantly increases production and commodity rate significantly improves.
Soybean application effect example
High-tower granulation biology prepared by the embodiment 1-3 high-tower granulation biological compound fertilizers prepared and comparative example 1-2 is compound Soy bean test field of the fertilizer before soybean planting is tested, and is equally divided into 5 groups, every group 10 mu, every piece of experimental plot Fertilizer application amount For 41kg/ mus, other conditions are identical, statistics soybean yields, downy mildew, root rot disease rate.Result of the test is as described in Table 4
The application effect result of the test of table 4
Project Per mu yield (kg/ mus) Downy mildew disease rate (%) Root rot disease rate (%)
Embodiment 1 218 6.5 7.8
Embodiment 2 223 5.9 7.6
Embodiment 3 220 6.3 8.2
Comparative example 1 189 14.2 17.9
Comparative example 2 170 14.8 18.7
Remarks:When counting downy mildew, root rot disease rate, the soil of 100 square metres of areas in experimental plot, system are randomly selected Meter wherein downy mildew, root rot disease rate plant quantity.
Described above is only the preferred embodiment of the present invention, it should be pointed out that:For the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications It should be regarded as protection scope of the present invention.

Claims (7)

1. a kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function, it is characterised in that be by following parts by weight Made from raw material:Particle cores fertilizer 92-94 parts, Lauxite coating agent 2-3 parts, complex micro organism fungicide 4-7 parts;
The particle cores fertilizer is as made from the raw material of following parts by weight:Urea 500-530 parts, ammonium sulfate 60-80 parts, phosphoric acid one Ammonium 100-130 parts, double superhosphate 40-60 parts, reinforcing agent 3-5 parts, pulullan polysaccharide 2-4 parts, potassium sulfate 220-240 parts, phosphorus Acid dihydride potassium 15-25 parts, ammonium molybdate 3-5 parts, magnesium sulfate 10-15 parts, rare earth element 0.05-0.5 parts, 10% imidacloprid wettable Pulvis 10-15 parts, AVM 3-5 parts;
The Lauxite coating agent is as made from the raw material of following parts by weight:Urea 18-28 parts, formaldehyde 27-29 parts, α-first Base glycoside 1-3 parts, polyoxypropylene ethylene oxide glycerin ether 0.9-1.1 parts;
The complex micro organism fungicide is according to 1 by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii:1- 2:Made from 1.5-2.5 weight ratio.
2. there is the high-tower granulation biological compound fertilizer of prevention and control pest and disease damage function according to claim 1, it is characterised in that described Reinforcing agent is by nano-TiO2Modified SiO2Aeroge, α-ketoglutaric acid and ethylenediamine tetra-acetic acid are according to 1:1.5-2:1-1.5 weight Made from amount ratio.
3. there is the high-tower granulation biological compound fertilizer of prevention and control pest and disease damage function according to claim 2, it is characterised in that described Nano-TiO2Modified SiO2Aeroge is as made from following methods:The 50% of glacial acetic acid total amount, butyl titanate and ethanol are placed in Triangular flask, it is well mixed, adds Nano-meter SiO_22Aeroge, ultrasonic 15min, obtains solution A;The glacial acetic acid of remainder amount is added dropwise In solution A, it is added dropwise, moves to magnetic stirring apparatus and stir 1-2h at room temperature, still aging 24h, obtain white gels;White is solidifying 5h is dried in vacuo at 100 DEG C of glue, Muffle furnace roasting 6h is transferred to, is cooled to room temperature, obtains nano-TiO2Modified SiO2Aeroge.
4. there is the high-tower granulation biological compound fertilizer of prevention and control pest and disease damage function according to claim 3, it is characterised in that described Complex micro organism fungicide is as made from following steps:By coral Nocard's bacillus, Rhodopseudomonas palustris and Boydii not lever 15h is cultivated at 25 DEG C in liquid seed culture medium respectively after bacterium activation, is then transferred to according to 1% inoculum concentration sterilized big In tank culture medium, after 30 DEG C are cultivated 20h, by coral Nocard's bacillus, Rhodopseudomonas palustris and Acinetobacter baumannii by weight Amount is lyophilized that freeze-dried powder is made than well mixed, obtains complex micro organism fungicide.
5. there is the high-tower granulation biological compound fertilizer of prevention and control pest and disease damage function according to claim 4, it is characterised in that described Liquid seed culture medium is 5% sucrose, 2% peptone, 2% corn flour, 0.1% potassium dihydrogen phosphate, 0.05% sodium chloride and remaining Measure sterilized water composition;The big tank culture medium be 5% peptone, 3% beef extract, 1% sucrose, 15% corn flour, 3% starch, 0.1% potassium chloride and surplus sterilized water composition.
6. there is the high-tower granulation biological compound fertilizer of prevention and control pest and disease damage function according to claim 5, it is characterised in that described The pH of liquid seed culture medium and big tank culture medium is 6.5.
A kind of 7. preparation of the high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function any one of claim 1-6 Method, it is characterised in that be prepared by following steps:
1) formula ratio Urea is melted to form urea melting liquid, then by ammonium sulfate, MAP, double superhosphate, increasing Strong agent, pulullan polysaccharide, potassium sulfate, potassium dihydrogen phosphate, ammonium molybdate, magnesium sulfate, rare earth element, 10% imidacloprid wettable powder It is added thereto with AVM, is mixed to form slurry, then makes slurry feeding granulation tower using tower solution prilling Grain obtains particle cores fertilizer of the particle diameter in 2-3.5mm;
2) formaldehyde is added in reactive tank, adds the urea of 50% weight while stirring, added methyl glucose glucoside and gather Oxypropylene ethylene oxide glycerin ether, sodium hydroxide regulation pH value 7.5, it is warming up to 100 DEG C of reaction 40min;Add remaining The urea of 50% weight, phosphorus acid for adjusting pH value are 4,65 DEG C of reaction 1h, obtain Lauxite coating agent;
3) particle cores fertilizer is placed in coating machine, Lauxite coating agent carries out a coating processing to particle cores fertilizer spraying, dries Do to water content and be less than 15%;Face powder aluminum coated steel is carried out to the particle after drying with complex micro organism fungicide again, obtained with anti- The high-tower granulation biological compound fertilizer of disease-control insect pest function.
CN201710802826.3A 2017-09-08 2017-09-08 A kind of high-tower granulation biological compound fertilizer with prevention and control pest and disease damage function and preparation method thereof Pending CN107586223A (en)

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CN108191574A (en) * 2018-02-28 2018-06-22 河北百禾丰化肥有限公司 A kind of complex microorganism multielement coating enhanced fertilizer and its manufacturing method
CN108314547A (en) * 2018-04-20 2018-07-24 史丹利化肥遂平有限公司 A kind of complex microorganism coating type depot fertilizer and preparation method thereof
CN109734531A (en) * 2019-03-16 2019-05-10 刘超 It is a kind of for prevent and treat ginkgo leaf yellow leaf it is withered medicine fertilizer and its fertilizing method
WO2019153776A1 (en) * 2018-02-09 2019-08-15 郑州高富肥料有限公司 Multi-coating-structure controlled-release fertilizer and preparation method therefor
WO2019153775A1 (en) * 2018-02-09 2019-08-15 郑州高富肥料有限公司 Sustained-release and controlled-release fertilizer having core-shell structure and preparation method therefor
CN110386842A (en) * 2018-04-20 2019-10-29 联发生物科技股份有限公司 Fertilizer granules and preparation method thereof
CN111410578A (en) * 2020-03-25 2020-07-14 云南恒卓农业科技有限公司 Pesticide bacterial fertilizer for preventing and treating diseases and pests of potatoes and preparation method thereof
CN111517891A (en) * 2020-05-06 2020-08-11 云南泵龙马铃薯种植有限公司 Special fertilizer for potatoes

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019153776A1 (en) * 2018-02-09 2019-08-15 郑州高富肥料有限公司 Multi-coating-structure controlled-release fertilizer and preparation method therefor
WO2019153775A1 (en) * 2018-02-09 2019-08-15 郑州高富肥料有限公司 Sustained-release and controlled-release fertilizer having core-shell structure and preparation method therefor
CN108191574A (en) * 2018-02-28 2018-06-22 河北百禾丰化肥有限公司 A kind of complex microorganism multielement coating enhanced fertilizer and its manufacturing method
CN108314547A (en) * 2018-04-20 2018-07-24 史丹利化肥遂平有限公司 A kind of complex microorganism coating type depot fertilizer and preparation method thereof
CN110386842A (en) * 2018-04-20 2019-10-29 联发生物科技股份有限公司 Fertilizer granules and preparation method thereof
CN109734531A (en) * 2019-03-16 2019-05-10 刘超 It is a kind of for prevent and treat ginkgo leaf yellow leaf it is withered medicine fertilizer and its fertilizing method
CN111410578A (en) * 2020-03-25 2020-07-14 云南恒卓农业科技有限公司 Pesticide bacterial fertilizer for preventing and treating diseases and pests of potatoes and preparation method thereof
CN111517891A (en) * 2020-05-06 2020-08-11 云南泵龙马铃薯种植有限公司 Special fertilizer for potatoes

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