CN107156835A - 一种含葡萄渣提取物的高活性缓释型乳清蛋白粉及其制备方法 - Google Patents
一种含葡萄渣提取物的高活性缓释型乳清蛋白粉及其制备方法 Download PDFInfo
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Abstract
本发明公开了一种含葡萄渣提取物的乳清蛋白粉的制备方法,包括如下步骤:(1)葡萄渣采用射频加热灭酶灭菌后加纤维素酶酶解,然后加入30~70%乙醇溶液,于30~50℃条件超声提取,将所得提取物离心取上清液,将所得上清液浓缩得葡萄渣提取物;(2)将所得葡萄渣提取物与乳清蛋白粉及去离子水混匀后均质处理,然后经喷雾冷冻干燥即得。本发明使用微胶囊技术,选取葡萄渣提取物为芯材,乳清蛋白为壁材,进行包埋,得到含葡萄渣提取物乳清蛋白粉,既稳定地保留葡萄渣提取物的生物活性,又丰富了目前乳清蛋白粉的风味和营养。
Description
技术领域
本发明属于食品加工技术领域,具体涉及一种含葡萄渣提取物的高活性缓释型乳清蛋白粉及其制备方法。
背景技术
葡萄是一种营养价值很高的食用浆果,目前的利用方式除了新鲜食用之外主要以葡萄酿酒、榨葡萄汁进行利用,而在生产过程中,会产生约20%的葡萄渣,其主要成分为葡萄皮和籽,这些废弃物因被大量丢弃而造成生态环境污染,或作为肥料利用而造成资源的浪费。葡萄渣中包含葡萄皮和籽丰富的营养物质,包括花青素、白藜芦醇、酒石酸、原花青素、膳食纤维等生理活性物质,有强抗氧化性、抗衰老、抗病菌、预防癌症和心血管疾病的有益活性功能。因而有效利用葡萄渣,充分提取葡萄渣中活性物质,既是对生态环境的保护,又提高了葡萄渣的利用价值,提高其经济效益。
乳清蛋白是制作干酪过程中产生的副产物精炼而成的,摄入人体中,非常容易被消化吸收,代谢效率高,因而有很高的生物利用价值,同时乳清蛋白中还含有丰富的生物活性物质,包括β-乳球蛋白、α-乳白蛋白、乳铁蛋白、生长因子等,是人体必需氨基酸、支链氨基酸、钙类补充的丰富来源,并能抗菌、抗病毒、调节人体免疫、降低血脂含量,适合于乳糖不耐人群补充乳蛋白。而且乳化性能好,口感细腻,干燥成粉时性质较稳定,适用于多种食品加工体系。
发明内容
本发明提供一种含葡萄渣提取物的高活性缓释型乳清蛋白粉及其制备方法,得到的产品较好保存了葡萄渣提取物的活性和风味,有丰富口感。
一种含葡萄渣提取物的乳清蛋白粉的制备方法,包括如下步骤:
(1)葡萄渣采用射频加热灭酶灭菌后加纤维素酶酶解,然后加入30~70%乙醇溶液,于30~50℃条件下超声提取,将所得提取物离心取上清液,将所得上清液浓缩得葡萄渣提取物;
(2)将所得葡萄渣提取物与乳清蛋白粉及去离子水混匀后均质处理,然后经喷雾冷冻干燥即得。
考虑葡萄渣的提取物因抗氧化性强而易受高温、光照等外部条件影响而变质失效,因而本发明使用微胶囊技术,选取葡萄渣提取物为芯材,乳清蛋白为壁材,进行混合均质包埋,得到含葡萄渣提取物缓释型乳清蛋白粉,以乳清蛋白包埋葡萄渣活性成分,隔绝了活性成分与外界的空气、水和光照的影响,既稳定地保留葡萄渣提取物的生物活性并使其缓慢释放,延长缓释有效期40%,又丰富了目前乳清蛋白粉的风味和营养。
本发明选取合适的葡萄渣、对其进行射频加热杀菌灭酶、纤维素酶解-超声波辅助提取活性成分、离心、减压浓缩、与壁材溶液混合、搅拌、均质、喷雾冷冻干燥和铝箔纸真空包装。本发明得到的产品较好地保留葡萄渣中营养活性成分,并在储存的过程中缓慢释放,比起单一的乳清蛋白粉包含更多的营养与风味,可直接食用,也可广泛添加到各种食品体系如冰淇淋、糖果和饼干中。
葡萄渣选取新鲜酿酒或榨葡萄汁后葡萄渣。优选地,射频加热的条件为:25~30MHz射频加热10~20min。进一步地,为27.12MHz射频加热10~20min。
优选地,纤维素酶的加入量为每千克葡萄渣加入5~10g纤维素酶计,酶解时间为1~1.5h。
优选地,加入30~70%乙醇溶液时酶解产物与30~70%乙醇溶液的质量比为1:(10~20),超声提取条件为:超声波15~25kHz辅助提取30~60min,功率为100w~150w。
优选地,离心条件为:4000~5000rpm离心5~10min。
经40℃减压干燥浓缩约至原溶液的1/10,优选地,所述葡萄渣提取物粗品的浓度5%~10%。
优选地,步骤(2)中葡萄渣提取物与乳清蛋白粉及去离子水的质量比为5~15:15~25:65~75。
进一步优选地,葡萄渣提取物与乳清蛋白粉及去离子水的质量比为10:20:70。
优选地,葡萄渣提取物与乳清蛋白粉及去离子水混合后600~1000rpm磁力搅拌5~7min;均质条件为:8000~12000rpm均质5~10min。
优选地,喷雾冷冻干燥条件为:使用20~40psi压缩空气进行进料雾化,进料速度为20ml/min,经液氮冷冻成小冰晶后,于-25~-15℃下冻干至恒重。
本发明还提供一种如所述制备方法制备得到的含葡萄渣提取物的乳清蛋白粉。
与现有技术相比,本发明具有如下有益效果:
(1)使用射频加热对葡萄渣进行灭酶杀菌,在此过程中温度变化较小,在较低的温度中更为有效地杀灭葡萄渣中的危害菌和酶类。
(2)使用纤维酶解-超声波辅助提取葡萄渣中的活性成分,减少纤维素阻碍溶剂对葡萄渣中活性物质的提取,之后使用超声波辅助后期提取,加快提取所需时间、提高提取效率。以本发明中的方法进行提取白藜芦醇得率可达0.6%,原花青素得率可达5%,与一般提取相比有所提升。
(3)使用乳清蛋白粉作为壁材包裹葡萄渣缓释型提取物,既保护了其中的活性物质,生物活性保留和有效释放期延长40%;又丰富了乳清蛋白粉的营养和风味。乳清蛋白较为稳定,包埋性好,在牛奶中资源丰富获取容易。
(4)使用喷雾冷冻干燥对乳化后的混合液进行干燥,在低温条件下保护好乳清蛋白和葡萄渣提取物的活性功能成分,同时使用喷雾干燥使得到的乳清蛋白粉颗粒较为细致,同时也大大减少了冻干所需时间和能耗。所得的乳清蛋白粉颗粒饱满,平均粒径小于0.15mm,与直接进行冻干相比时间缩短约20%~40%。葡萄渣提取物在浸提后浓缩可直接作为包埋的芯材溶液,省去了过程中彻底干燥后再配置新溶液的步骤,降低了生产成本,同时减少了过程中可能产生的对活性物质的伤害。各处理步骤及处理手段之间相互协同,共同提高产品的性能,且尽可能降低生产成本。
具体实施方式
通过以下实施例进一步具体阐述本发明,其目的是为了更加具体详细了解本发明而不以限制本发明为目的,实验所用设备为生产车间或实验室常用设备。
实施例1
选取新鲜酿酒或榨葡萄汁后葡萄渣使用27.12MHz射频加热10min杀菌灭酶,按每千克葡萄渣加入5g纤维素酶,酶解1h后,加入40%乙醇溶液,料液比为1:15,于30℃条件下,超声波20kHz辅助提取30min,功率为150w后离心4000rpm,10min得到上清液,经40℃减压干燥浓缩约至原溶液的1/10,之后按每10g葡萄渣提取物加入至20g乳清蛋白粉和70g去离子水的混合液中,使用磁力搅拌器在转速600rpm,搅拌7min,再使用高速均质机,均质条件为12000rpm,均质7min后使用20psi压缩空气进行进料雾化,进料速度为20ml/min,经液氮冷冻成小冰晶后,收集于-15℃下冻干至恒重,最后用铝箔袋真空包装。
本实施例得到的乳清蛋白粉中葡萄渣混合物的包埋率超过90%,经检测其中多酚含量为26mg/g,在常温避光的相同储存条件下,本发明中的葡萄渣活性成分在储存100天后的多酚含量仍高于18mg/g,下降率低于30%,稳定性优于一般葡萄渣粉状产品。同时所得的产品带有淡淡葡萄的风味,使大众更加容易接受。
实施例2
选取新鲜酿酒或榨葡萄汁后葡萄渣使用27.12MHz射频加热20min杀菌灭酶,按每千克葡萄渣加入10g纤维素酶,酶解1h后,加入70%乙醇溶液,料液比为1:15,于40℃条件下,超声波20kHz辅助提取60min,功率为100w后离心5000rpm,5min得到上清液,经40℃减压干燥浓缩约至原溶液的1/10,之后按每10g葡萄渣提取物加入至20g乳清蛋白粉和70g去离子水的混合液中,使用磁力搅拌器在转速1000rpm,搅拌5min,再使用高速均质机,均质条件为8000rpm,均质5min后使用40psi压缩空气进行进料雾化,进料速度为20ml/min,经液氮冷冻成小冰晶后,收集于-25℃下冻干至恒重,最后用铝箔袋真空包装。
本实施例得到的乳清蛋白粉中葡萄渣混合物的包埋率超过90%,经检测其中多酚含量为25mg/g,在常温避光的相同储存条件下,本发明中的葡萄渣活性成分在储存100天后的多酚含量仍高于18mg/g,下降率低于30%,稳定性优于一般葡萄渣粉状产品。同时所得的产品带有淡淡葡萄的风味,使大众更加容易接受。
以上所述仅为本发明专利的具体实施案例,但本发明专利的技术特征并不局限于此,任何相关领域的技术人员在本发明的领域内,所作的变化或修饰皆涵盖在本发明的专利范围之中。
Claims (10)
1.一种含葡萄渣提取物的高活性缓释型乳清蛋白粉的制备方法,其特征在于,包括如下步骤:
(1)葡萄渣采用射频加热灭酶灭菌后加纤维素酶酶解,然后加入30%~70%乙醇溶液,于30~50℃条件下超声提取,将所得提取物离心取上清液,将所得上清液浓缩得葡萄渣提取物;
(2)将所得葡萄渣提取物与乳清蛋白粉及去离子水混匀后均质处理,然后经喷雾冷冻干燥即得。
2.根据权利要求1所述制备方法,其特征在于,射频加热的条件为:25~30MHz射频加热10~20min。
3.根据权利要求1所述制备方法,其特征在于,纤维素酶的加入量为每千克葡萄渣加入5~10g纤维素酶计,酶解时间为1~1.5h。
4.根据权利要求1所述制备方法,其特征在于,加入30~70%乙醇溶液时酶解产物与30~70%乙醇溶液的质量比为1:(10~20),超声提取条件为:超声波15~25kHz辅助提取30~60min,功率为100w~150w。
5.根据权利要求1所述制备方法,其特征在于,离心条件为:4000~5000rpm离心5~10min。
6.根据权利要求1所述制备方法,其特征在于,所述葡萄渣提取物的质量分数为5%~10%。
7.根据权利要求1所述制备方法,其特征在于,步骤(2)中葡萄渣提取物与乳清蛋白粉及去离子水的质量比为5~15:15~25:65~75。
8.根据权利要求1所述制备方法,其特征在于,葡萄渣提取物与乳清蛋白粉及去离子水混合后600~1000rpm磁力搅拌5~7min;均质条件为:8000~12000rpm均质5~10min。
9.根据权利要求1所述制备方法,其特征在于,喷雾冷冻干燥条件为:使用20~40psi压缩空气进行进料雾化,进料速度为15~25ml/min,经液氮冷冻成小冰晶后,于-25~-15℃下冻干至恒重。
10.一种如权利要求1~9任一权利要求所述制备方法制备得到的含葡萄渣提取物的高活性缓释型乳清蛋白粉。
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CN114951239A (zh) * | 2022-05-25 | 2022-08-30 | 成都工业学院 | 一种回收酿酒工艺中葡萄渣制备衍生品原料的方法 |
CN114951239B (zh) * | 2022-05-25 | 2023-11-21 | 成都工业学院 | 一种回收酿酒工艺中葡萄渣制备衍生品原料的方法 |
CN114951125B (zh) * | 2022-05-25 | 2024-05-14 | 楚天科技股份有限公司 | 立式胶塞清洗机用于验证的有线探头安装方法及装置 |
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