CN107033209B - 一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 - Google Patents
一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 Download PDFInfo
- Publication number
- CN107033209B CN107033209B CN201710388435.1A CN201710388435A CN107033209B CN 107033209 B CN107033209 B CN 107033209B CN 201710388435 A CN201710388435 A CN 201710388435A CN 107033209 B CN107033209 B CN 107033209B
- Authority
- CN
- China
- Prior art keywords
- water
- dietary fiber
- soluble dietary
- mogroside
- microwave drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000013325 dietary fiber Nutrition 0.000 title claims abstract description 66
- 229930189775 mogroside Natural products 0.000 title claims abstract description 66
- 238000000034 method Methods 0.000 title claims abstract description 61
- 238000000605 extraction Methods 0.000 title claims abstract description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 98
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 64
- 241001409321 Siraitia grosvenorii Species 0.000 claims abstract description 53
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 claims abstract description 53
- 238000001728 nano-filtration Methods 0.000 claims abstract description 51
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 34
- 239000012528 membrane Substances 0.000 claims abstract description 27
- 239000012466 permeate Substances 0.000 claims abstract description 24
- 239000012465 retentate Substances 0.000 claims abstract description 24
- 238000004587 chromatography analysis Methods 0.000 claims abstract description 21
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 239000012530 fluid Substances 0.000 claims abstract description 13
- 238000005119 centrifugation Methods 0.000 claims abstract description 7
- 238000010828 elution Methods 0.000 claims abstract description 5
- 238000001035 drying Methods 0.000 claims description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
- 229910052799 carbon Inorganic materials 0.000 claims description 20
- 235000021022 fresh fruits Nutrition 0.000 claims description 20
- 238000001914 filtration Methods 0.000 claims description 17
- 239000000284 extract Substances 0.000 claims description 16
- 239000007787 solid Substances 0.000 claims description 14
- 239000002023 wood Substances 0.000 claims description 9
- 235000015203 fruit juice Nutrition 0.000 claims description 5
- 229930182470 glycoside Natural products 0.000 abstract description 18
- 150000002338 glycosides Chemical class 0.000 abstract description 18
- 238000004519 manufacturing process Methods 0.000 abstract description 12
- 239000000047 product Substances 0.000 abstract description 5
- 239000003905 agrochemical Substances 0.000 abstract description 2
- 238000001816 cooling Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 12
- 239000012535 impurity Substances 0.000 description 11
- 239000012153 distilled water Substances 0.000 description 8
- 229940023032 activated charcoal Drugs 0.000 description 7
- 239000003513 alkali Substances 0.000 description 7
- 235000009508 confectionery Nutrition 0.000 description 7
- 235000009815 Momordica Nutrition 0.000 description 6
- 241000218984 Momordica Species 0.000 description 6
- 244000269722 Thea sinensis Species 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 6
- 239000000447 pesticide residue Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- TWFZGCMQGLPBSX-UHFFFAOYSA-N Carbendazim Natural products C1=CC=C2NC(NC(=O)OC)=NC2=C1 TWFZGCMQGLPBSX-UHFFFAOYSA-N 0.000 description 4
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 4
- 239000006013 carbendazim Substances 0.000 description 4
- JNPZQRQPIHJYNM-UHFFFAOYSA-N carbendazim Chemical compound C1=C[CH]C2=NC(NC(=O)OC)=NC2=C1 JNPZQRQPIHJYNM-UHFFFAOYSA-N 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 230000002255 enzymatic effect Effects 0.000 description 4
- 238000004128 high performance liquid chromatography Methods 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- GHBNZZJYBXQAHG-KUVSNLSMSA-N (2r,3r,4s,5s,6r)-2-[[(2r,3s,4s,5r,6r)-6-[[(3s,8s,9r,10r,11r,13r,14s,17r)-17-[(2r,5r)-5-[(2s,3r,4s,5s,6r)-4,5-dihydroxy-3-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-6-[[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@H](CC[C@@H](C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]6[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O6)O)O5)O)CC4)(C)C)=CC[C@H]3[C@]2(C)CC1)C)C(C)(C)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O GHBNZZJYBXQAHG-KUVSNLSMSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000004811 liquid chromatography Methods 0.000 description 3
- TVJXHJAWHUMLLG-UHFFFAOYSA-N mogroside V Natural products CC(CCC(OC1OC(COC2OC(CO)C(O)C(O)C2OC3OC(CO)C(O)C(O)C3O)C(O)C(O)C1O)C(C)(C)O)C4CCC5(C)C6CC=C7C(CCC(OC8OC(COC9OC(CO)C(O)C(O)C9O)C(O)C(O)C8O)C7(C)C)C6(C)C(O)CC45C TVJXHJAWHUMLLG-UHFFFAOYSA-N 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
- 229920001100 Polydextrose Polymers 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- HEBKCHPVOIAQTA-NGQZWQHPSA-N d-xylitol Chemical compound OC[C@H](O)C(O)[C@H](O)CO HEBKCHPVOIAQTA-NGQZWQHPSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000008101 lactose Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000001259 polydextrose Substances 0.000 description 2
- 229940035035 polydextrose Drugs 0.000 description 2
- 235000013856 polydextrose Nutrition 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZMYFCFLJBGAQRS-IRXDYDNUSA-N (2R,3S)-epoxiconazole Chemical compound C1=CC(F)=CC=C1[C@@]1(CN2N=CN=C2)[C@H](C=2C(=CC=CC=2)Cl)O1 ZMYFCFLJBGAQRS-IRXDYDNUSA-N 0.000 description 1
- QNBTYORWCCMPQP-JXAWBTAJSA-N (Z)-dimethomorph Chemical compound C1=C(OC)C(OC)=CC=C1C(\C=1C=CC(Cl)=CC=1)=C/C(=O)N1CCOCC1 QNBTYORWCCMPQP-JXAWBTAJSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 239000005761 Dimethomorph Substances 0.000 description 1
- 239000005767 Epoxiconazole Substances 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 240000006053 Garcinia mangostana Species 0.000 description 1
- 235000017048 Garcinia mangostana Nutrition 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000003851 azoles Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000010812 external standard method Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000005374 membrane filtration Methods 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 235000021096 natural sweeteners Nutrition 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- UWVQIROCRJWDKL-UHFFFAOYSA-N oxadixyl Chemical compound CC=1C=CC=C(C)C=1N(C(=O)COC)N1CCOC1=O UWVQIROCRJWDKL-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 210000004885 white matter Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J17/00—Normal steroids containing carbon, hydrogen, halogen or oxygen, having an oxygen-containing hetero ring not condensed with the cyclopenta(a)hydrophenanthrene skeleton
- C07J17/005—Glycosides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Sustainable Development (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (30)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710388435.1A CN107033209B (zh) | 2017-05-27 | 2017-05-27 | 一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710388435.1A CN107033209B (zh) | 2017-05-27 | 2017-05-27 | 一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN107033209A CN107033209A (zh) | 2017-08-11 |
CN107033209B true CN107033209B (zh) | 2019-03-26 |
Family
ID=59539062
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710388435.1A Active CN107033209B (zh) | 2017-05-27 | 2017-05-27 | 一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107033209B (zh) |
Families Citing this family (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107602653B (zh) * | 2017-10-09 | 2020-06-16 | 晨光生物科技集团股份有限公司 | 一种从鲜罗汉果中提取罗汉果甜苷的方法 |
CN108094772A (zh) * | 2017-12-08 | 2018-06-01 | 桂林莱茵生物科技股份有限公司 | 一种罗汉果果汁及其制备方法 |
CN108294142A (zh) * | 2018-04-08 | 2018-07-20 | 湖南艾达伦科技有限公司 | 一种红茶轻饮及其制备方法 |
CN108606287A (zh) * | 2018-04-08 | 2018-10-02 | 湖南艾达伦科技有限公司 | 一种草莓果酱及其制备方法 |
CN108514010A (zh) * | 2018-04-08 | 2018-09-11 | 湖南艾达伦科技有限公司 | 一种泡芙及其制备方法 |
CN108308323A (zh) * | 2018-04-08 | 2018-07-24 | 湖南艾达伦科技有限公司 | 一种绿茶轻饮及其制备方法 |
CN108208088A (zh) * | 2018-04-08 | 2018-06-29 | 湖南艾达伦科技有限公司 | 一种卡仕达酱及制备方法 |
CN108323665A (zh) * | 2018-04-08 | 2018-07-27 | 湖南艾达伦科技有限公司 | 一种罗汉果轻饮及其制备方法 |
CN108402129A (zh) * | 2018-04-08 | 2018-08-17 | 湖南艾达伦科技有限公司 | 一种罗汉果蛋糕及其制备方法 |
CN108606122A (zh) * | 2018-04-08 | 2018-10-02 | 湖南艾达伦科技有限公司 | 一种罗汉果菊花轻饮及其制备方法 |
CN108514011A (zh) * | 2018-04-08 | 2018-09-11 | 湖南艾达伦科技有限公司 | 一种香草奶油酱及其制备方法 |
CN108184958A (zh) * | 2018-04-08 | 2018-06-22 | 湖南艾达伦科技有限公司 | 一种蔓越莓饼干及其制备方法 |
CN108185104A (zh) * | 2018-04-08 | 2018-06-22 | 湖南艾达伦科技有限公司 | 一种抹茶慕斯及制备方法 |
CN108514008A (zh) * | 2018-04-08 | 2018-09-11 | 湖南艾达伦科技有限公司 | 一种罗汉果吐司及制备方法 |
CN108606149A (zh) * | 2018-04-08 | 2018-10-02 | 湖南艾达伦科技有限公司 | 一种罗汉果冰激凌的制备方法 |
CN108371268A (zh) * | 2018-04-08 | 2018-08-07 | 湖南艾达伦科技有限公司 | 一种罗汉果甜橙饮料及其制备方法 |
CN108497248A (zh) * | 2018-04-11 | 2018-09-07 | 湖南华诚生物资源股份有限公司 | 一种罗汉果浓缩汁及罗汉果果粉的制备方法 |
CN108516996B (zh) * | 2018-05-24 | 2020-10-16 | 湖南华诚生物资源股份有限公司 | 罗汉果益生元的提取方法及同时提取罗汉果甜苷v的方法 |
CN109247561A (zh) * | 2018-09-06 | 2019-01-22 | 湖南绿蔓生物科技股份有限公司 | 一种从罗汉果中制备罗汉果甜味组合物的方法及其应用 |
CN109320400B (zh) * | 2018-09-30 | 2021-08-10 | 湖南华诚生物资源股份有限公司 | 一种从罗汉果甜苷生产废液中提取天然甘露醇的方法 |
CN110521993A (zh) * | 2019-08-13 | 2019-12-03 | 湖南艾达伦科技有限公司 | 罗汉果苷甜味和风味组合物及其制备方法与应用 |
CN111588043B (zh) * | 2020-06-05 | 2023-11-10 | 邵阳华诚绿果生物科技有限公司 | 一种基于罗汉果废弃物的膳食纤维的制备方法 |
CN111543530B (zh) * | 2020-06-22 | 2023-06-02 | 湖南华诚生物资源股份有限公司 | 一种低热量的罗汉果甜茶轻饮的制备方法 |
CN116784468A (zh) * | 2022-03-16 | 2023-09-22 | 桂林莱茵生物科技股份有限公司 | 一种甜味组合物及其制备方法和用途 |
CN114634545B (zh) * | 2022-04-19 | 2023-02-24 | 湖南华诚生物资源股份有限公司 | 一种脱除农药残留的罗汉果甜苷的规模化生产方法 |
CN115124585B (zh) * | 2022-08-02 | 2024-05-28 | 湖南华诚生物资源股份有限公司 | 一种罗汉果提取物的清洁生产方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1683387A (zh) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN101007042A (zh) * | 2007-02-06 | 2007-08-01 | 桂林莱茵生物科技股份有限公司 | 一种脱色、脱苦的罗汉果提取物的制备方法 |
CN106306991A (zh) * | 2016-08-23 | 2017-01-11 | 湖南华诚生物资源股份有限公司 | 一种同时去除罗汉果提取物中农残和塑化剂的方法 |
CN106617115A (zh) * | 2017-02-20 | 2017-05-10 | 湖南华诚生物资源股份有限公司 | 从罗汉果生产废液中分离可溶性膳食纤维的方法 |
-
2017
- 2017-05-27 CN CN201710388435.1A patent/CN107033209B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1683387A (zh) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN101007042A (zh) * | 2007-02-06 | 2007-08-01 | 桂林莱茵生物科技股份有限公司 | 一种脱色、脱苦的罗汉果提取物的制备方法 |
CN106306991A (zh) * | 2016-08-23 | 2017-01-11 | 湖南华诚生物资源股份有限公司 | 一种同时去除罗汉果提取物中农残和塑化剂的方法 |
CN106617115A (zh) * | 2017-02-20 | 2017-05-10 | 湖南华诚生物资源股份有限公司 | 从罗汉果生产废液中分离可溶性膳食纤维的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN107033209A (zh) | 2017-08-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN107033209B (zh) | 一种同时提取无农残罗汉果甜苷和水溶性膳食纤维的方法 | |
CN106588616B (zh) | 一种姜黄素的制备方法 | |
CN102276679B (zh) | 一种从油茶饼粕减压沸腾提取高纯度茶皂素的方法 | |
CN104086614B (zh) | 一种适用于工业生产的罗汉果提取物的制备方法 | |
CN106279339B (zh) | 一种高纯度罗汉果苷v的分离纯化方法 | |
Wang et al. | Separation and purification of amygdalin from thinned bayberry kernels by macroporous adsorption resins | |
CN107216228B (zh) | 一种低共熔溶剂及用于提取大黄中蒽醌的方法 | |
CN108176079B (zh) | 一种甘草提取物的脱色方法 | |
CN107235949A (zh) | 一种无塑化剂花青素提取物的提取方法 | |
CN101485705A (zh) | 熟三七和熟三七标准提取物和其应用 | |
CN109053821B (zh) | 从罗汉果叶中提取茶多酚、总氨基酸、黄酮化合物的方法 | |
CN106242953A (zh) | 一种从丹凤牡丹籽壳中制备白藜芦醇的方法 | |
CN105053952B (zh) | 一种无苦涩味的陈皮提取物的加工工艺 | |
CN104610417B (zh) | 一种从山楂中提取熊果酸和齐墩果酸的方法 | |
Zheng et al. | Purification characteristics and parameters optimization of anthocyanin extracted from blueberry | |
CN109021046B (zh) | 一种从罗汉果茎叶中同时提取槲皮苷和山萘苷的方法 | |
CN103446195A (zh) | 银杏叶提取物的制备方法 | |
CN103880806A (zh) | 一种从蓝莓中提取花青素的方法 | |
CN107098942A (zh) | 一种亚临界水萃取萝卜叶中山奈苷的方法 | |
CN104892717B (zh) | 一种罗汉果甜苷v的工业级制备液相色谱分离方法 | |
CN108864238A (zh) | 从罗汉果提取渣中提取罗汉果籽油及β-谷甾醇的方法 | |
CN104910223A (zh) | 一种橄榄苦苷的制备方法 | |
CN105712896A (zh) | 一种从玛咖中高效制备玛咖酰胺单体的方法 | |
CN113603742B (zh) | 一种罗汉果甜苷v的制备方法 | |
CN104610418A (zh) | 一种从锁阳中提取熊果酸的方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for simultaneous extraction of Mogroside and water soluble dietary fiber from Siraitia grosvenorii Effective date of registration: 20210422 Granted publication date: 20190326 Pledgee: CITIC Bank Changsha branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2021980002898 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231127 Granted publication date: 20190326 Pledgee: CITIC Bank Changsha branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2021980002898 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for simultaneous extraction of mogroside and water-soluble dietary fiber from Momordica grosvenorii without pesticide residues Granted publication date: 20190326 Pledgee: Agricultural Bank of China Limited Changsha Wangcheng District sub branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2024980000707 |