CN106831806A - 一种水溶性芝麻素的制备方法 - Google Patents
一种水溶性芝麻素的制备方法 Download PDFInfo
- Publication number
- CN106831806A CN106831806A CN201710069415.8A CN201710069415A CN106831806A CN 106831806 A CN106831806 A CN 106831806A CN 201710069415 A CN201710069415 A CN 201710069415A CN 106831806 A CN106831806 A CN 106831806A
- Authority
- CN
- China
- Prior art keywords
- sesamin
- water
- sesame
- soluble
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PEYUIKBAABKQKQ-AFHBHXEDSA-N (+)-sesamin Chemical compound C1=C2OCOC2=CC([C@H]2OC[C@H]3[C@@H]2CO[C@@H]3C2=CC=C3OCOC3=C2)=C1 PEYUIKBAABKQKQ-AFHBHXEDSA-N 0.000 title claims abstract description 72
- PEYUIKBAABKQKQ-UHFFFAOYSA-N epiasarinin Natural products C1=C2OCOC2=CC(C2OCC3C2COC3C2=CC=C3OCOC3=C2)=C1 PEYUIKBAABKQKQ-UHFFFAOYSA-N 0.000 title claims abstract description 72
- VRMHCMWQHAXTOR-CMOCDZPBSA-N sesamin Natural products C1=C2OCOC2=CC([C@@H]2OC[C@@]3(C)[C@H](C=4C=C5OCOC5=CC=4)OC[C@]32C)=C1 VRMHCMWQHAXTOR-CMOCDZPBSA-N 0.000 title claims abstract description 72
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 235000003434 Sesamum indicum Nutrition 0.000 claims abstract description 42
- 241000207961 Sesamum Species 0.000 claims abstract description 34
- 235000012054 meals Nutrition 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 239000012528 membrane Substances 0.000 claims abstract description 12
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 5
- 238000004108 freeze drying Methods 0.000 claims abstract description 4
- 238000000926 separation method Methods 0.000 claims abstract description 4
- 239000000243 solution Substances 0.000 claims description 25
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 22
- 239000000284 extract Substances 0.000 claims description 17
- 239000000047 product Substances 0.000 claims description 16
- 229960000583 acetic acid Drugs 0.000 claims description 10
- 239000012065 filter cake Substances 0.000 claims description 10
- -1 hydroxypropyl cyclodextrin Chemical compound 0.000 claims description 10
- 108090000526 Papain Proteins 0.000 claims description 9
- 239000004365 Protease Substances 0.000 claims description 9
- 229940055729 papain Drugs 0.000 claims description 9
- 235000019834 papain Nutrition 0.000 claims description 9
- 102000012479 Serine Proteases Human genes 0.000 claims description 8
- 108010022999 Serine Proteases Proteins 0.000 claims description 8
- 239000012153 distilled water Substances 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- 239000012362 glacial acetic acid Substances 0.000 claims description 8
- 108010059892 Cellulase Proteins 0.000 claims description 6
- 229940106157 cellulase Drugs 0.000 claims description 6
- 102000004190 Enzymes Human genes 0.000 claims description 5
- 108090000790 Enzymes Proteins 0.000 claims description 5
- 229940088598 enzyme Drugs 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000001976 enzyme digestion Methods 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 239000004375 Dextrin Substances 0.000 claims description 3
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 15
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract description 8
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract description 8
- 238000011084 recovery Methods 0.000 abstract description 7
- 239000001913 cellulose Substances 0.000 abstract description 4
- 229920002678 cellulose Polymers 0.000 abstract description 4
- 231100000331 toxic Toxicity 0.000 abstract description 3
- 230000002588 toxic effect Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 2
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical group O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 abstract description 2
- 238000000638 solvent extraction Methods 0.000 abstract 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 8
- 244000000231 Sesamum indicum Species 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000000605 extraction Methods 0.000 description 6
- 235000011803 sesame oil Nutrition 0.000 description 6
- 239000008159 sesame oil Substances 0.000 description 6
- 239000012535 impurity Substances 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 3
- 230000014509 gene expression Effects 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 206010020772 Hypertension Diseases 0.000 description 2
- 240000006240 Linum usitatissimum Species 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000287 crude extract Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 238000005374 membrane filtration Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 238000000108 ultra-filtration Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 206010006187 Breast cancer Diseases 0.000 description 1
- 208000026310 Breast neoplasm Diseases 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical group COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- 208000004930 Fatty Liver Diseases 0.000 description 1
- 206010019708 Hepatic steatosis Diseases 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 102000003929 Transaminases Human genes 0.000 description 1
- 108090000340 Transaminases Proteins 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000035614 depigmentation Effects 0.000 description 1
- 239000012259 ether extract Substances 0.000 description 1
- 208000010706 fatty liver disease Diseases 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 210000002865 immune cell Anatomy 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229930013686 lignan Natural products 0.000 description 1
- 150000005692 lignans Chemical class 0.000 description 1
- 235000009408 lignans Nutrition 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000011552 rat model Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 238000010898 silica gel chromatography Methods 0.000 description 1
- 231100000240 steatosis hepatitis Toxicity 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 241000712461 unidentified influenza virus Species 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
- C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
- C07D493/04—Ortho-condensed systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710069415.8A CN106831806B (zh) | 2017-02-08 | 2017-02-08 | 一种水溶性芝麻素的制备方法 |
Applications Claiming Priority (1)
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CN201710069415.8A CN106831806B (zh) | 2017-02-08 | 2017-02-08 | 一种水溶性芝麻素的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN106831806A true CN106831806A (zh) | 2017-06-13 |
CN106831806B CN106831806B (zh) | 2018-12-21 |
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CN201710069415.8A Active CN106831806B (zh) | 2017-02-08 | 2017-02-08 | 一种水溶性芝麻素的制备方法 |
Country Status (1)
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2019196340A (ja) * | 2018-05-10 | 2019-11-14 | 亀井 淳三 | セサミノールとシクロデキストリンとの包接複合体及びその製造方法 |
CN110464850A (zh) * | 2018-05-10 | 2019-11-19 | 有限会社农业科学 | 芝麻素与环糊精的包接复合物及其制造方法 |
CN113461703A (zh) * | 2021-08-16 | 2021-10-01 | 内蒙古泓兴生物科技有限公司 | 由芝麻制备芝麻素的方法以及芝麻素 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101092421A (zh) * | 2006-06-20 | 2007-12-26 | 白心亮 | 一种芝麻素提取新工艺 |
CN101245071A (zh) * | 2008-03-21 | 2008-08-20 | 河南工业大学 | 从芝麻油中提取芝麻木酚素的方法 |
JP2010024240A (ja) * | 2009-10-30 | 2010-02-04 | Tsujido Chemical Corp | 包接体およびその製造方法 |
CN102086209A (zh) * | 2010-12-14 | 2011-06-08 | 刘勇 | 一种利用芝麻饼粕提取芝麻素的方法 |
CN105726576A (zh) * | 2016-02-04 | 2016-07-06 | 刘玉财 | 一种用于心绞痛缓释期治疗的片剂及其制备方法 |
-
2017
- 2017-02-08 CN CN201710069415.8A patent/CN106831806B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101092421A (zh) * | 2006-06-20 | 2007-12-26 | 白心亮 | 一种芝麻素提取新工艺 |
CN101245071A (zh) * | 2008-03-21 | 2008-08-20 | 河南工业大学 | 从芝麻油中提取芝麻木酚素的方法 |
JP2010024240A (ja) * | 2009-10-30 | 2010-02-04 | Tsujido Chemical Corp | 包接体およびその製造方法 |
CN102086209A (zh) * | 2010-12-14 | 2011-06-08 | 刘勇 | 一种利用芝麻饼粕提取芝麻素的方法 |
CN105726576A (zh) * | 2016-02-04 | 2016-07-06 | 刘玉财 | 一种用于心绞痛缓释期治疗的片剂及其制备方法 |
Non-Patent Citations (1)
Title |
---|
张世卿 等: "芝麻素研究进展", 《氨基酸和生物资源》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2019196340A (ja) * | 2018-05-10 | 2019-11-14 | 亀井 淳三 | セサミノールとシクロデキストリンとの包接複合体及びその製造方法 |
CN110464850A (zh) * | 2018-05-10 | 2019-11-19 | 有限会社农业科学 | 芝麻素与环糊精的包接复合物及其制造方法 |
CN110464849A (zh) * | 2018-05-10 | 2019-11-19 | 龟井淳三 | 芝麻素酚与环糊精的包接复合物及其制备方法 |
JP7079931B2 (ja) | 2018-05-10 | 2022-06-03 | 淳三 亀井 | セサミノールとシクロデキストリンとの包接複合体及びその製造方法 |
CN113461703A (zh) * | 2021-08-16 | 2021-10-01 | 内蒙古泓兴生物科技有限公司 | 由芝麻制备芝麻素的方法以及芝麻素 |
Also Published As
Publication number | Publication date |
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CN106831806B (zh) | 2018-12-21 |
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Denomination of invention: A preparation method of water soluble Sesamin Effective date of registration: 20210222 Granted publication date: 20181221 Pledgee: Agricultural Bank of China Limited Helingeer County sub branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY Co.,Ltd. Registration number: Y2021150000016 |
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Denomination of invention: A preparation method of water-soluble Sesamin Effective date of registration: 20220330 Granted publication date: 20181221 Pledgee: Agricultural Bank of China Limited Helingeer County sub branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Registration number: Y2022150000027 |
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Denomination of invention: A preparation method of water-soluble sesamin Effective date of registration: 20231101 Granted publication date: 20181221 Pledgee: China Minsheng Banking Corp Hohhot branch Pledgor: INNER MONGOLIA CHANGHUI BIOTECHNOLOGY CO.,LTD. Registration number: Y2023150000154 |
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