CN106757717A - A kind of antibiotic facing material and preparation method thereof - Google Patents
A kind of antibiotic facing material and preparation method thereof Download PDFInfo
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- CN106757717A CN106757717A CN201510367198.1A CN201510367198A CN106757717A CN 106757717 A CN106757717 A CN 106757717A CN 201510367198 A CN201510367198 A CN 201510367198A CN 106757717 A CN106757717 A CN 106757717A
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- facing material
- antibiotic facing
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Abstract
The invention provides a kind of antibiotic facing material and preparation method thereof, wherein antibiotic facing material includes following component by weight percentage：Protein cellulose viscose 25% 35%, chitin fiber 35% 45%, long-staple cotton 25% 35%.Protein cellulose viscose in antibiotic facing material of the invention contains appropriate protein and ten several amino acid, there is affine and health-care effect to the skin of human body, chitin fiber has the function such as antibacterial, antibacterial, health care, the antibiotic facing material obtained by protein cellulose viscose, chitin fiber and long wool cotton blend has soft and good moisture pick-up properties, has soft, skin care and antibacterial functions concurrently.
Description
Technical field
The present invention relates to field of textile, more particularly to a kind of antibiotic facing material and preparation method thereof.
Background technology
With the fast development of apparel industry, comfortableness, feature, fashion of the people to garment material
Property, security and the feature of environmental protection requirement it is growing.Therefore, breathed freely with soft feel, moisture absorption, protected
Skin health care and the exploitation of constitutionally stable functional fabric and application are a research of current fabric industry
Focus.How so that it is this area technical barrier urgently to be resolved hurrily that fabric has several functions concurrently.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of function of having soft, skin care and antibacterial concurrently
Property antibiotic facing material, to meet consumer to high-quality, the demand of comfortable and functional clothing.
In order to solve the above technical problems, the antibiotic facing material that the present invention is provided is included such as by weight percentage
Lower component：
Protein cellulose viscose 25%-35%,
Chitin fiber 35%-45%,
Long-staple cotton 25%-35%.
Protein cellulose viscose in antibiotic facing material of the invention contains appropriate protein and ten several amino
Acid, has affine and health-care effect to the skin of human body, and chitin fiber has antibacterial, antibacterial, guarantor
The function, the antibiotic facing material obtained by protein cellulose viscose, chitin fiber and long wool cotton blend such as strong
With soft and good moisture pick-up properties, soft, skin care and antibacterial functions are had concurrently.
Preferably, antibiotic facing material includes following component by weight percentage：30% protein cellulose viscose,
40% chitin fiber, 30% long-staple cotton.
Preferably, the protein cellulose viscose is silk fiber.
Present invention also offers a kind of preparation method of antibiotic facing material, it comprises the following steps：
1) it is (25-35) by blending ratio:(35-45):(25-35), yarn twist is 680-720 twists/m, is twisted with the fingers
Coefficient prepares protein cellulose viscose/chitin fiber/staple cotton blended yarn line for 110-130；
2) protein cellulose viscose/chitin fiber/staple cotton blended yarn line that will 1) obtain is woven,
Obtain blank fabric；
3) pre-treatment, dyeing treatment are carried out successively to the blank fabric for 2) obtaining, soaping is processed and fixed
Type treatment, that is, obtain antibiotic facing material.
Antibiotic facing material prepared by the method has soft without losing very refreshing style, and hygroscopicity
Can be good, have soft, skin care and antibacterial functions concurrently.
Preferably, the step 1) in protein cellulose viscose/chitin fiber/staple cotton blended yarn line
Line density be 21S-32S, obtained scribbled strength is big under this condition, is compiled by the scribbled
The fabric feeling knitted is endured with all one's will.It is highly preferred that protein cellulose viscose/chitin fiber/staple cotton blended yarn line
Line density be 21S。
Preferably, the step 2) it is specially：
Protein cellulose viscose/chitin fiber/staple cotton blended yarn the line that will 1) obtain is in 22-24 machines number
The many needle track large circle machines of one side on woven, one side tuck mesh blank fabric is obtained, in the condition
Lower obtained antibiotic facing material has good body bone.
Preferably, the step 3) in pre-treatment technique it is specific as follows：
Pretreatment solution is first heated to 35 DEG C -45 DEG C, then it is 1 to control bath raio:(15-20) is put into blank
Fabric, and be incubated after pretreatment solution is warming up into 78 DEG C -82 DEG C with the heating rate of 2 DEG C/min
1h-1.5h, is then naturally cooling to room temperature, wherein, the component in the pretreatment solution is as follows：
Above-mentioned refining agent may preferably be high-efficiency refining agent MRN, and bleeding agent may preferably be bleeding agent
JFC-1, hydrogen peroxide bleaching stabilizer may preferably be waterglass.
Pre-treating technology under the conditions of this eliminate cotton seed hulls on blank fabric, cellulose commensal and
The greasy dirt impurity being stained with during weaving, the fabric strength loss after pre-treatment is small, with whiteness is good, feel
The features such as softness.
Preferably, the step 3) in dyeing treatment technique it is specific as follows：
Pure water is first heated to 18 DEG C -25 DEG C, successively in pure water add 1%owf reactive dye and
13-15g/L glauber salt, adds 13-15g/L glauber salt after 10min, 13-15g/L is added after 20min
Glauber salt, adds 6-7g/L soda ash to obtain dye liquor after 30min, then it is 1 to control bath raio:(15-20) is put into
Blank fabric, and add after dye liquor is warming up into 60 DEG C -65 DEG C with the heating rate of 1 DEG C/min
The soda ash of 12-14g/L, is incubated 1h-1.5h, is then naturally cooling to room temperature.
Dyeing handling process under the conditions of this has the advantages that dye-uptake is high, dyefastness is good.
Preferably, the step 3) in treatment of soaping technique it is specific as follows：
It is 1 that bath raio is controlled under normal temperature condition:Blank fabric is put into solution of soaping by (15-20), and with
The heating rate of 8-10 DEG C/min will soap after solution is warming up to 90 DEG C -95 DEG C and be incubated 14-16min, connect
And washed after being naturally cooling to room temperature, wherein, the component in the solution of soaping is as follows：
Soap powder 1.8-2.2g/L
Soda ash 1.8-2.2g/L.
The technique of the treatment of soaping under the conditions of this is so that antibiotic facing material has good color and luster and reflecting feel
Feature.
Preferably, blank fabric is by step 3) soap treatment after also by antibiotic finish process,
The technique of the antibiotic finish treatment is specific as follows：
It is 1 to control bath raio:(10-15) carries out antibacterial finishing agent dip finishing to blank fabric, wherein, institute
The concentration of antibacterial finishing agent is stated for 4-6%owf, the temperature of dip finishing is 58 DEG C -62 DEG C, dip finishing
Time be 43-48min.
Above-mentioned antibacterial finishing agent may preferably be antibacterial finishing agent JC-1 or FWY.
By the antibiotic facing material that antibiotic finish is processed, still there is excellent antibacterial work(after washing 50 times
Energy.
Specific embodiment
To enable above-mentioned purpose, the feature and advantage of invention more obvious understandable, below to tool of the invention
Body implementation method is described in detail.
Many details are elaborated in the following description in order to fully understand the present invention, but it is of the invention
Can also be different from other manner described here using other to implement, those skilled in the art can be not
Similar popularization is done in the case of running counter to intension of the present invention, therefore the present invention does not receive following public specific embodiment
Limitation.
Protein cellulose viscose and chitin fiber used in embodiments of the invention is by Suzhou perseverance light chemical fibre
Co., Ltd produces.
Tester used by the present invention is as follows：
Yarn property tester：YG061 type electronics single yarn tester, YG135G bar evenness
Tester, YG172 type yarn filoplume testers；
Fabric performance test instrument：HD026N+ type electronic fabrics strength tester, YG541B types are knitted
Thing pincher elasticity analyzer, Martindale's pilling wear resistant instrument, LLY-01 type electronics hardometer,
XDP-1 types fabric drapeometer, YG606G thermal resistance dampness testers.
Embodiment 1
1) it is 30 by blending ratio:40:30, yarn twist is 680 twists/m, and twist factor is 110, and line is close
Spend is 21SPrepare protein cellulose viscose/chitin fiber/staple cotton blended yarn line；
2) protein cellulose viscose/chitin fiber/staple cotton blended yarn line that will 1) obtain is in machines No. 22
The many needle track large circle machines of one side on woven, one side tuck mesh blank fabric is obtained, four during braiding
Pin, four tunnels one are circulated, wherein, 1,2 road odd number pin tucks, even number pin lopping, 3,4 road odd number pins
Lopping, even number pin tuck, and braiding is circulated with this.
3) pre-treating technology：
Pretreatment solution is first heated to 40 DEG C, then it is 1 to control bath raio:20 are put into blank fabric, and with
Be warming up to pretreatment solution after 80 DEG C and be incubated 1h by the heating rate of 2 DEG C/min, is then naturally cooling to
Room temperature, wherein, the component in the pretreatment solution is as follows：
Scouring enzyme 7g/L,
High-efficiency refining agent MRN 6g/L,
The 13g/L of penetrating agent JFC -1,
Hydrogen peroxide 5g/L,
Sodium carbonate 5g/L,
Waterglass 1g/L.
Dyeing handling process：
Pure water is first heated to 20 DEG C, 1%owf reactive dye and 15g/L units is added in pure water successively
Bright powder, adds 15g/L glauber salt after 10min, 13g/L glauber salt, 30min are added after 20min
7g/L soda ash is added to obtain dye liquor afterwards, then it is 1 to control bath raio:20 are put into blank fabric, and with 1 DEG C/min
Heating rate by dye liquor be warming up to after 65 DEG C add 14g/L soda ash, be incubated 1h, then naturally drop
Warm to room temperature.
Soap handling process：
It is 1 that bath raio is controlled under normal temperature condition:Blank fabric is put into solution of soaping by 20, and with 9 DEG C/min
Heating rate will soap after solution is warming up to 95 DEG C and be incubated 15min, after being then naturally cooling to room temperature
Washing, wherein, the component in the solution of soaping is as follows：
Soap powder 2g/L
Soda ash 2g/L.
Antibiotic finish handling process：
It is 1 to control bath raio:10 pairs of blank fabrics carry out antibacterial finishing agent FWY dip finishings, wherein,
The concentration of the antibacterial finishing agent FWY is 5%owf, and the temperature of dip finishing is 60 DEG C, is impregnated whole
The time of reason is 45min.
After testing, the total amino acid content of antibiotic facing material obtained in embodiment 1 is 0.0737g/100g, egg
White matter is 1.0g/100g, and surface fabric contains amino acid and protein, has pro-skin skin-protecting function concurrently.
As shown in table 1, it is mixed that what embodiment 1 was obtained prepares protein cellulose viscose/chitin fiber/long-staple cotton
Yarn is with reference to country GB/T 3916-1997 yarn tension failures performance, FZ/T 01069-2007 yarns
The standards such as lines are dry, FZ/T 01086-2000 Yarn filoplumes, strength and extension property respectively to yarn, bar are done
The performances such as irregularity, filoplume are detected, higher by the visible yarn breaking force of testing result,
Yarn undercoat plumage is more, while more than 3mm filoplumes are little.
As shown in table 2, implement 1 antibiotic facing material for obtaining and participate in FZ/T 70010-2006 knitted fabrics square
The measure of meter Chong Liang, measure, the FZ7002-1991 knitted fabrics of GB/T 3820-1997 textile thickness
Loop density measurement standard measurement fabric Gram Mass, thickness and loop density, show fabric more
Abundant, loop density is larger.
As shown in table 3, the antibiotic facing material that embodiment 1 is obtained spins with reference to country GB/T 19976-2005
The measure of fabric bursting strength, the measure of GB/T 4802-2008 textile fabric pilling performances,
The measure of GB/T 3819-1997 textile wrinkle recovery properties, GB/T 18318-2001 textile fabrics
The measure of bending length, measure, the GB/T of GB/T 23329-2009 textile fabric drapability
The measure of 5453-1997 textile fabric gas permeabilities, GB/T 11048-2008 textile physiological comforts
The standard such as measure of thermal resistance and dampness under limit, test the antibiotic facing material physical and mechanical properties and
Wearability, from the table, the bursting strength of fabric is higher, and anti-fluffing and anti-pilling performance is good, fabric
Good permeability, with preferable hot wet migration energy.
As shown in table 4, it is Bacteria Detection knot after the antibiotic facing material that obtains of embodiment 1 is washed through 50 times
Really, from the table, antibiotic facing material still has good fungistatic effect after being washed through 50 times.
1 protein cellulose viscose of the table/linear energy of chitin fiber/staple cotton blended yarn
The antibiotic facing material basic parameter of table 2
The antibiotic facing material physical and mechanical properties of table 3 and wearability
The anti-microbial property of fabric after the arrangement of table 4
Embodiment 2
1) it is 35 by blending ratio:35:30, yarn twist is 720 twists/m, and twist factor is 130, and line is close
Spend is 32SPrepare protein cellulose viscose/chitin fiber/staple cotton blended yarn line；
2) protein cellulose viscose/chitin fiber/staple cotton blended yarn line that will 1) obtain is in machines No. 24
The many needle track large circle machines of one side on woven, one side tuck mesh blank fabric is obtained, four during braiding
Pin, four tunnels one are circulated, wherein, 1,2 road odd number pin tucks, even number pin lopping, 3,4 road odd number pins
Lopping, even number pin tuck, and braiding is circulated with this.
3) pre-treating technology：
Pretreatment solution is first heated to 40 DEG C, then it is 1 to control bath raio:15 are put into blank fabric, and with
Be warming up to pretreatment solution after 80 DEG C and be incubated 1h by the heating rate of 2 DEG C/min, is then naturally cooling to
Room temperature, wherein, the component in the pretreatment solution is as follows：
Scouring enzyme 6.8g/L,
High-efficiency refining agent MRN 5.8g/L,
The 13g/L of penetrating agent JFC -1,
Hydrogen peroxide 5g/L,
Sodium carbonate 5g/L,
Waterglass 1g/L.
Dyeing handling process：
Pure water is first heated to 20 DEG C, 1%owf reactive dye and 13g/L units is added in pure water successively
Bright powder, adds 13g/L glauber salt after 10min, 14g/L glauber salt, 30min are added after 20min
6g/L soda ash is added to obtain dye liquor afterwards, then it is 1 to control bath raio:15 are put into blank fabric, and with 1 DEG C/min
Heating rate by dye liquor be warming up to after 60 DEG C add 12g/L soda ash, be incubated 1h, then naturally drop
Warm to room temperature.
Soap handling process：
It is 1 that bath raio is controlled under normal temperature condition:Blank fabric is put into solution of soaping by 15, and with 9 DEG C/min
Heating rate will soap after solution is warming up to 90 DEG C and be incubated 15min, after being then naturally cooling to room temperature
Washing, wherein, the component in the solution of soaping is as follows：
Soap powder 1.8g/L
Soda ash 1.8g/L.
Antibiotic finish handling process：
It is 1 to control bath raio:10 pairs of blank fabrics carry out antibacterial finishing agent JC-1 dip finishings, wherein, institute
The concentration of antibacterial finishing agent JC-1 is stated for 5%owf, the temperature of dip finishing is 60 DEG C, dip finishing
Time be 45min.
After testing, the total amino acid content of antibiotic facing material obtained in embodiment 2 is 0.0648g/100g, egg
White matter is 0.9g/100g, and surface fabric contains amino acid and protein, has pro-skin skin-protecting function concurrently.
As shown in table 5, it is mixed that what embodiment 2 was obtained prepares protein cellulose viscose/chitin fiber/long-staple cotton
Yarn is with reference to country GB/T 3916-1997 yarn tension failures performance, FZ/T 01069-2007 yarns
The standards such as lines are dry, FZ/T 01086-2000 Yarn filoplumes, strength and extension property respectively to yarn, bar are done
The performances such as irregularity, filoplume are detected, higher by the visible yarn breaking force of testing result,
Yarn undercoat plumage is more, while more than 3mm filoplumes are little.
As shown in table 6, implement 2 antibiotic facing materials for obtaining and participate in FZ/T 70010-2006 knitted fabrics square
The measure of meter Chong Liang, measure, the FZ7002-1991 knitted fabrics of GB/T 3820-1997 textile thickness
Loop density measurement standard measurement fabric Gram Mass, thickness and loop density, show fabric more
Abundant, loop density is larger.
As shown in table 7, the antibiotic facing material that embodiment 2 is obtained spins with reference to country GB/T 19976-2005
The measure of fabric bursting strength, the measure of GB/T 4802-2008 textile fabric pilling performances,
The measure of GB/T 3819-1997 textile wrinkle recovery properties, GB/T 18318-2001 textile fabrics
The measure of bending length, measure, the GB/T of GB/T 23329-2009 textile fabric drapability
The measure of 5453-1997 textile fabric gas permeabilities, GB/T 11048-2008 textile physiological comforts
The standard such as measure of thermal resistance and dampness under limit, test the antibiotic facing material physical and mechanical properties and
Wearability, from the table, the bursting strength of fabric is higher, and anti-fluffing and anti-pilling performance is good, fabric
Good permeability, with preferable hot wet migration energy.
As shown in table 8, it is Bacteria Detection knot after the antibiotic facing material that obtains of embodiment 2 is washed through 50 times
Really, from the table, antibiotic facing material still has good fungistatic effect after being washed through 50 times.
5 protein cellulose viscoses of the table/linear energy of chitin fiber/staple cotton blended yarn
The antibiotic facing material basic parameter of table 6
The antibiotic facing material physical and mechanical properties of table 7 and wearability
The anti-microbial property of fabric after the arrangement of table 8
Although present invention combination above example is described, the present invention is not limited to above-mentioned
Embodiment, and be only defined by the appended claims, those of ordinary skill in the art easily can enter to it
Row modifications and variations, but and without departing from essential idea of the invention and scope.
Claims (10)
1. a kind of antibiotic facing material, it is characterised in that by weight percentage including following component：
Protein cellulose viscose 25%-35%,
Chitin fiber 35%-45%,
Long-staple cotton 25%-35%.
2. antibiotic facing material according to claim 1, it is characterised in that wrap by weight percentage
Include following component：30% protein cellulose viscose, 40% chitin fiber, 30% long-staple cotton.
3. antibiotic facing material according to claim 1, it is characterised in that the protein cellulose viscose
It is silk fiber.
4. a kind of preparation method of antibiotic facing material, it is characterised in that comprise the following steps：
1) it is (25-35) by blending ratio:(35-45):(25-35), yarn twist is 680-720 twists/m, is twisted with the fingers
Coefficient prepares protein cellulose viscose/chitin fiber/staple cotton blended yarn line for 110-130；
2) protein cellulose viscose/chitin fiber/staple cotton blended yarn line that will 1) obtain is woven,
Obtain blank fabric；
3) pre-treatment, dyeing treatment are carried out successively to the blank fabric for 2) obtaining, soaping is processed and fixed
Type treatment, that is, obtain antibiotic facing material.
5. preparation method according to claim 4, it is characterised in that the step 1) in
The line density of protein cellulose viscose/chitin fiber/staple cotton blended yarn line is 21S-32S。
6. preparation method according to claim 4, it is characterised in that the step 2) it is specific
For：
Protein cellulose viscose/chitin fiber/staple cotton blended yarn the line that will 1) obtain is in 22-24 machines number
The many needle track large circle machines of one side on woven, obtain one side tuck mesh blank fabric.
7. preparation method according to claim 4, it is characterised in that the step 3) in
The technique of pre-treatment is specific as follows：
Pretreatment solution is first heated to 35 DEG C -45 DEG C, then it is 1 to control bath raio:(15-20) is put into blank
Fabric, and be incubated after pretreatment solution is warming up into 78 DEG C -82 DEG C with the heating rate of 2 DEG C/min
1h-1.5h, is then naturally cooling to room temperature, wherein, the component in the pretreatment solution is as follows：
8. preparation method according to claim 4, it is characterised in that the step 3) in
The technique for dyeing treatment is specific as follows：
Pure water is first heated to 18 DEG C -25 DEG C, successively in pure water add 1%owf reactive dye and
13-15g/L glauber salt, adds 13-15g/L glauber salt after 10min, 13-15g/L is added after 20min
Glauber salt, adds 6-7g/L soda ash to obtain dye liquor after 30min, then it is 1 to control bath raio:(15-20) is put into
Blank fabric, and add after dye liquor is warming up into 60 DEG C -65 DEG C with the heating rate of 1 DEG C/min
The soda ash of 12-14g/L, is incubated 1h-1.5h, is then naturally cooling to room temperature.
9. preparation method according to claim 4, it is characterised in that the step 3) in
Soap treatment technique it is specific as follows：
It is 1 that bath raio is controlled under normal temperature condition:Blank fabric is put into solution of soaping by (15-20), and with
The heating rate of 8-10 DEG C/min will soap after solution is warming up to 90 DEG C -95 DEG C and be incubated 14-16min, connect
And washed after being naturally cooling to room temperature, wherein, the component in the solution of soaping is as follows：
Soap powder 1.8-2.2g/L
Soda ash 1.8-2.2g/L.
10. preparation method according to claim 4, it is characterised in that blank fabric is by step
Also processed by antibiotic finish after rapid treatment of soaping 3), the technique of the antibiotic finish treatment is specific
It is as follows：
It is 1 to control bath raio:(10-15) carries out antibacterial finishing agent dip finishing to blank fabric, wherein, institute
The concentration of antibacterial finishing agent is stated for 4-6%owf, the temperature of dip finishing is 58 DEG C -62 DEG C, dip finishing
Time be 43-48min.
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| CN107988687A (en) * | 2017-12-04 | 2018-05-04 | 佛山市亨特纺织有限公司 | A kind of wired double side weft knitting knitting fabric of viscose |
| CN108166191A (en) * | 2018-03-09 | 2018-06-15 | 宁波市鄞州凤林纺织整理有限公司 | A kind of knitting fabric antibacterial deodourizing technique |
| CN109338540A (en) * | 2018-11-28 | 2019-02-15 | 湖北中天科技有限公司 | A kind of antibacterial blended yarn and preparation method thereof |
| CN109487543A (en) * | 2018-11-12 | 2019-03-19 | 北京阿尔法针织有限公司 | A kind of knitting of knitted fabric |
| CN110016750A (en) * | 2019-04-15 | 2019-07-16 | 中山市仕春纺织印染实业有限公司 | A kind of garment material with bacteriostasis |
| CN110079916A (en) * | 2019-04-09 | 2019-08-02 | 于洪海 | A kind of textile fabric and its manufacture craft of included massage efficacy |
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| CN108166191A (en) * | 2018-03-09 | 2018-06-15 | 宁波市鄞州凤林纺织整理有限公司 | A kind of knitting fabric antibacterial deodourizing technique |
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| CN109487543B (en) * | 2018-11-12 | 2021-05-11 | 北京阿尔法针织有限公司 | Knitting process of knitted fabric |
| CN109338540A (en) * | 2018-11-28 | 2019-02-15 | 湖北中天科技有限公司 | A kind of antibacterial blended yarn and preparation method thereof |
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