CN106316121A - Jun porcelain celeste blue glaze - Google Patents

Jun porcelain celeste blue glaze Download PDF

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Publication number
CN106316121A
CN106316121A CN201610680518.3A CN201610680518A CN106316121A CN 106316121 A CN106316121 A CN 106316121A CN 201610680518 A CN201610680518 A CN 201610680518A CN 106316121 A CN106316121 A CN 106316121A
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oxide
glaze
pottery
kiln
celeste
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CN201610680518.3A
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Chinese (zh)
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温书强
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Individual
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Glass Compositions (AREA)

Abstract

Jun porcelain celeste blue glaze is prepared from silicon dioxide, aluminum oxide, ferric oxide, titanium oxide, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, phosphorus pentoxide and copper oxide. The prepared jun porcelain celeste blue glaze is transparent, has third dimension, is good in liquidity, not prone to bubble and good in gloss, and the fired jun porcelain celeste blue glaze is bright and smooth in glaze color, has fewer cracks and is high in mechanical resistance.

Description

A kind of pottery celeste glaze
Technical field
The invention belongs to pottery manufacturing technology field, be specifically related to a kind of pottery celeste glaze.
Background technology
Pottery is thick for this with glaze, and at the bottom of its color or heavy glaze or in outstanding glaze or floating glaze table, the thick muddy work of glaze, glaze layer opalescence jade-like stone moistens, Being administrations with multiplied departments lives is intended to drip, and third dimension is extremely strong.Pottery is with transmutation as god, and natural transmutation is the elite place of pottery art, is also Pottery is rely the four seas of becoming famous, the rare part of porcelain woods of making a name.With executing a kind of glaze in firing, once burning till in multicoloured it is then " enter kiln of the same colour, kiln discharge ten thousand is color ".Protean transmutation effect, defines the mystery that colors changing hue is infinite, in red inner purple, purple During in dark blue, blue or green, residence is white, white general red, five colours imbibition, form a brightening, and have the title of ", without right, transmutation is unparalleled for pottery ".
Making pottery when, although present technology has been achieved for remarkable progress, but there are some defects, Pottery fires finished product in manufacturing process from selecting materials to, and period experiences tens of roads production process, accidentally also making of an operation All that has been achieved is spoiled for one-tenth, and this is also the reason that pottery yield all the time is extremely low.An ancient unit of weight glaze is one layer of decorative layer on pottery surface, is to determine The principal element that pottery glaze colours generates, utilizes natural raw mineral materials or adds some industrial chemicals and coordinate according to a certain percentage, Melt under high temperature reducing atmospheres effect and cover the rich jade-like stone in billet surface and moisten gloss and colorful vitreous body layer, tool There is abundant dicoration, increase the aesthetic feeling of pottery natural trend, make pottery have certain artistic value and enjoying value.
Pottery it is critical only that enamel, enamel transmutation color after being fired determines the value of pottery, white Pottery have bluish white, grey dawn, creamy white, beautiful white etc., blue pottery have sky blue, acid blue, powder are blue, sapphire blue, peacock blue.Glaze plasmogamy The difference of side, the color burnt out is the most variant, and when tradition fires pottery, is to execute one layer of glaze, according to kiln on element tire surface In fire environment an ancient unit of weight glaze generation transmutation, it may appear that some uncontrollable decorative pattern or color lumps, the finished product that burns out is more difficult joins To or configure complete.
In prior art, formula of pottery celeste glaze and preparation method thereof is the most little, and the pottery ultramarine glaze surface prepared There are crackle, glaze wearability and resistance to mechanical ability poor, beautiful sense deficiency.
Summary of the invention
In order to solve the problems referred to above, the present invention provides a kind of pottery celeste glaze.
The technical solution used in the present invention is:
A kind of pottery celeste glaze, it is made up of following raw materials according: silicon dioxide, aluminium oxide, ferrum oxide, titanium oxide, oxidation Calcium, magnesium oxide, potassium oxide, sodium oxide, phosphorus pentoxide, copper oxide.
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 60-80 part, aluminium oxide 10- 30 parts, ferrum oxide 1-3, titanium oxide 0.2-1, calcium oxide 8-10, magnesium oxide 0.5-1, potassium oxide 1-3, sodium oxide 1-3, five oxidations Two phosphorus 0.6-1, copper oxide 0.03-0.08 part.
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 70 parts, aluminium oxide 20 parts, Ferrum oxide 2, titanium oxide 0.6, calcium oxide 9, magnesium oxide 0.8, potassium oxide 2, sodium oxide 2, phosphorus pentoxide 0.8, copper oxide 0.05 Part.
The present invention also provides for the preparation method of a kind of pottery celeste glaze:
(1) glazing: make glaze slip become vaporific by compressed air, be sprayed on the most uniformly on base substrate, relies on the water absorption of base substrate to make Glaze is adsorbed on base substrate;Or base substrate is immersed and takes out a moment in the glaze slip of celeste glaze, utilize the water absorption of base substrate, make glaze slip equal Even is attached to billet surface;
(2) in the glaze firing oxidizing flame stage: after glazing, base substrate is loaded saggar, by saggar loading of kiln, then kiln temperature is gradually risen from 0 DEG C To 1040 DEG C, the chimney casket plate controlling ventilation is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, in saggar, base substrate and kiln Organic substances in moisture and glaze etc. are discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
The invention has the beneficial effects as follows: the glaze of the pottery celeste glaze that the present invention makes is the most penetrating, has third dimension, flowing Property good, the most easy to foaming, good luster, and fire pottery celeste glaze glaze colours jade-like stone profit, crackle is few, and resistance to mechanical ability is strong.
Detailed description of the invention
A kind of pottery celeste glaze, it is made up of following raw materials according: silicon dioxide, aluminium oxide, ferrum oxide, titanium oxide, oxygen Change calcium, magnesium oxide, potassium oxide, sodium oxide, phosphorus pentoxide, copper oxide.
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 60-80 part, aluminium oxide 10- 30 parts, ferrum oxide 1-3, titanium oxide 0.2-1, calcium oxide 8-10, magnesium oxide 0.5-1, potassium oxide 1-3, sodium oxide 1-3, five oxidations Two phosphorus 0.6-1, copper oxide 0.03-0.08 part.
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 70 parts, aluminium oxide 20 parts, Ferrum oxide 2, titanium oxide 0.6, calcium oxide 9, magnesium oxide 0.8, potassium oxide 2, sodium oxide 2, phosphorus pentoxide 0.8, copper oxide 0.05 Part.
The present invention also provides for the preparation method of a kind of pottery celeste glaze:
(1) glazing: make glaze slip become vaporific by compressed air, be sprayed on the most uniformly on base substrate, relies on the water absorption of base substrate to make Glaze is adsorbed on base substrate;Or base substrate is immersed and takes out a moment in the glaze slip of celeste glaze, utilize the water absorption of base substrate, make glaze slip equal Even is attached to billet surface;
(2) in the glaze firing oxidizing flame stage: after glazing, base substrate is loaded saggar, by saggar loading of kiln, then kiln temperature is gradually risen from 0 DEG C To 1040 DEG C, the chimney casket plate controlling ventilation is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, in saggar, base substrate and kiln Organic substances in moisture and glaze etc. are discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
Embodiment 1
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 70 parts, aluminium oxide 20 parts, oxidation Ferrum 2, titanium oxide 0.6, calcium oxide 9, magnesium oxide 0.8, potassium oxide 2, sodium oxide 2, phosphorus pentoxide 0.8, copper oxide 0.05 part.
The present invention also provides for the preparation method of a kind of pottery celeste glaze:
(1) glazing: make glaze slip become vaporific by compressed air, be sprayed on the most uniformly on base substrate, relies on the water absorption of base substrate to make Glaze is adsorbed on base substrate;Or base substrate is immersed and takes out a moment in the glaze slip of celeste glaze, utilize the water absorption of base substrate, make glaze slip equal Even is attached to billet surface;
(2) in the glaze firing oxidizing flame stage: after glazing, base substrate is loaded saggar, by saggar loading of kiln, then kiln temperature is gradually risen from 0 DEG C To 1040 DEG C, the chimney casket plate controlling ventilation is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, in saggar, base substrate and kiln Organic substances in moisture and glaze etc. are discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
Embodiment 2
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 60 parts, aluminium oxide 10 parts, oxidation Ferrum 1, titanium oxide 0.2, calcium oxide 8, magnesium oxide 0.5, potassium oxide 1, sodium oxide 1, phosphorus pentoxide 0.6, copper oxide 0.03 part.
Embodiment 3
A kind of pottery celeste glaze, it is prepared by the raw materials in: silicon dioxide 80 parts, aluminium oxide 30 parts, oxidation Ferrum 3, titanium oxide 1, calcium oxide 10, magnesium oxide 1, potassium oxide 3, sodium oxide 3, phosphorus pentoxide 1, copper oxide 0.08 part.

Claims (3)

1. a pottery celeste glaze, it is characterised in that: it is made up of following raw materials according: silicon dioxide, aluminium oxide, ferrum oxide, Titanium oxide, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, phosphorus pentoxide, copper oxide.
A kind of pottery celeste glaze the most according to claim 1, it is characterised in that: it is to be prepared by the raw materials in : silicon dioxide 60-80 part, aluminium oxide 10-30 part, ferrum oxide 1-3, titanium oxide 0.2-1, calcium oxide 8-10, magnesium oxide 0.5- 1, potassium oxide 1-3, sodium oxide 1-3, phosphorus pentoxide 0.6-1, copper oxide 0.03-0.08 part.
A kind of pottery celeste glaze the most according to claim 1, it is characterised in that: it is to be prepared by the raw materials in : silicon dioxide 70 parts, aluminium oxide 20 parts, ferrum oxide 2, titanium oxide 0.6, calcium oxide 9, magnesium oxide 0.8, potassium oxide 2, sodium oxide 2, phosphorus pentoxide 0.8, copper oxide 0.05 part.
CN201610680518.3A 2016-08-18 2016-08-18 Jun porcelain celeste blue glaze Pending CN106316121A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610680518.3A CN106316121A (en) 2016-08-18 2016-08-18 Jun porcelain celeste blue glaze

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Application Number Priority Date Filing Date Title
CN201610680518.3A CN106316121A (en) 2016-08-18 2016-08-18 Jun porcelain celeste blue glaze

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108752050A (en) * 2018-06-19 2018-11-06 张玉凤 Your porcelain tea-dust glaze of one kind and preparation method thereof
CN109399929A (en) * 2018-12-12 2019-03-01 湖南德兴瓷业有限公司 Transmutation blue glaze and preparation method thereof
CN115196950A (en) * 2022-06-17 2022-10-18 瑞尔(浙江)品牌管理有限责任公司 Secret color porcelain raw material and firing method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103288493A (en) * 2013-05-29 2013-09-11 陕西科技大学 Reddish-black jun porcelain glaze prepared by utilizing metal copper and iron and preparation method of reddish-black jun porcelain glaze

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103288493A (en) * 2013-05-29 2013-09-11 陕西科技大学 Reddish-black jun porcelain glaze prepared by utilizing metal copper and iron and preparation method of reddish-black jun porcelain glaze

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
(美)布莱恩·泰勒: "《釉 釉料及陶瓷颜色配制手册》", 30 November 2015 *
徐建华等: "《陶瓷花釉与装饰技术》", 30 April 2011 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108752050A (en) * 2018-06-19 2018-11-06 张玉凤 Your porcelain tea-dust glaze of one kind and preparation method thereof
CN109399929A (en) * 2018-12-12 2019-03-01 湖南德兴瓷业有限公司 Transmutation blue glaze and preparation method thereof
CN115196950A (en) * 2022-06-17 2022-10-18 瑞尔(浙江)品牌管理有限责任公司 Secret color porcelain raw material and firing method

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Application publication date: 20170111

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