CN108752050A - Your porcelain tea-dust glaze of one kind and preparation method thereof - Google Patents
Your porcelain tea-dust glaze of one kind and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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Abstract
Your a kind of porcelain tea-dust glaze of present invention offer and preparation method thereof, by the raw material components of following parts by weight：Black feldspar 3-7 parts, 2-4 parts of gold soil, 28-32 parts of dolomite, 11-15 parts of quartz, 12-16 parts of calcite, 0.5-1.5 parts of talcum, 0.5-1 parts of agate, 5-7 parts of bone ash.Tea-dust glaze glaze colours prepared by the present invention is deep dignified, great ancient meaning, breaches your modern porcelain based on celadon, and the situation that other glaze are rare, increases the new glaze colours of your porcelain, good publicity effect is played to the popularization of your culture of porcelain.
Description
Technical field
The present invention relates to your a kind of porcelain production field, a kind of your porcelain tea-dust glaze and its manufacture craft are specifically related to.
Background technology
Tea-dust glaze is one of kind important in Ancient Times in China iron crystalline glaze, belongs to high temperature yellow glaze, is burnt through high temperature reduction flame
At.Tea-dust glaze began to burn in the Tang Dynasty, and Yao county kiln at that time was once largely fired, Tang and Song Dynasty time, Shanxi Huiyuan kiln and northern area one
The kiln for burning black glaze a bit also has burning to make.Common product holds pot, cylinder, alms bowl bottle, tank, small cup etc.And the imitative burning in Qing Dynasty Jing Dezhen is then
It is very successful, suddenly become rare color glaze kind.The tea-dust glaze majority of Jing Dezhen Qing Dynasty firing is to chisel device to display porcelain.From
Material object handed down from ancient times sees, is common with Yongzheng and Qianrong's period product, partially yellow in the majority of Yongzheng's tea-dust glaze, Qianrong's tea-dust glaze is then inclined
Green is in the majority.
And traditional Ruyao is well-known to fire celadon, there is the glaze colours such as reddish black, sky blue, pea green, bluish white.Your modern porcelain fires work
The then burning process of rare tea dust glaze colours in skill.
Invention content
For the burning process of the rare tea dust glaze colours of your current modern porcelain, by research and development repeatedly for many years, the present invention
A kind of your porcelain tea-dust glaze and preparation method thereof is provided, your porcelain of tea-dust glaze can be burnt out, enrich the kind of your enamel color.
The technical proposal of the invention is realized in this way：Your a kind of porcelain tea-dust glaze, by the raw material group of following parts by weight
Point：Black feldspar 3-7 parts, 2-4 parts of gold soil, 28-32 parts of dolomite, 11-15 parts of quartz, 12-16 parts of calcite, talcum 0.5-
1.5 parts, 0.5-1 parts of agate, 5-7 parts of bone ash.
What technical scheme of the present invention can be realized in：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：5 parts of black feldspar, 3 parts of gold soil, 30 parts of dolomite,
13 parts of quartz, 14 parts of calcite, 1 part of talcum, 0.8 part of agate, 6 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
At angle；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
Time 12-16 hour.
Preferably, the embryo material in the step 4 is Tang mouthful soil, wind scoop soil and kaolin.
Preferably, the glaze of leaching twice in the step 8 is respectively to soak for the first time 1-2 seconds glaze time, second of leaching glaze time
3-4 seconds.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1 hour to 1.5 hours used time；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
2 hours to 3.5 hours；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 2 hours to 3 hours；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 6.5 small
Up to 7.5 hours；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
Preferably, the step 6）In the Temperature fall time be 12 hours.
The beneficial effects of the invention are as follows：Tea-dust glaze glaze colours prepared by the present invention is deep dignified, and great ancient meaning breaches existing
For your porcelain based on celadon, and the situation that other glaze are rare, the new glaze colours of your porcelain is increased, your popularization of culture of porcelain is played
Good publicity effect.
Specific implementation mode
Below by several groups of embodiments, invention is further explained, these preferred embodiments are not with any side
The formula limitation present invention, under the premise of without departing substantially from the technology of the present invention solution, to the ordinary skill of the invention done
Personnel's any modifications or changes easy to implement are both fallen within the claims in the present invention protection domain.
Embodiment 1：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：3 parts of black feldspar, 2 parts of gold soil, 28 parts of dolomite,
11 parts of quartz, 12 parts of calcite, 0.5 part of talcum, 0.5 part of agate, 5 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
12 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1 hour used time；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
2 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 2 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 6.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
Embodiment 2：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：7 parts of black feldspar, 4 parts of gold soil, 32 parts of dolomite,
15 parts of quartz, 16 parts of calcite, 1.5 parts of talcum, 1 part of agate, 7 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
12 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1 hour used time；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
2 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 2 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 6.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
Embodiment 3：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：5 parts of black feldspar, 3 parts of gold soil, 30 parts of dolomite,
13 parts of quartz, 14 parts of calcite, 1 part of talcum, 0.8 part of agate, 6 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
12 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1 hour used time；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
2 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 2 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 6.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
Embodiment 4：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：3 parts of black feldspar, 2 parts of gold soil, 28 parts of dolomite,
11 parts of quartz, 12 parts of calcite, 0.5 part of talcum, 0.5 part of agate, 5 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
16 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1.5 hours used times；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
3.5 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 3 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 7.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
Embodiment 5：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：7 parts of black feldspar, 4 parts of gold soil, 32 parts of dolomite,
15 parts of quartz, 16 parts of calcite, 1.5 parts of talcum, 1 part of agate, 7 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
16 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1.5 hours used times；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
3.5 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 3 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 7.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
Embodiment 6：
Your a kind of porcelain tea-dust glaze, by the raw material components of following parts by weight：5 parts of black feldspar, 3 parts of gold soil, 30 parts of dolomite,
13 parts of quartz, 14 parts of calcite, 1 part of talcum, 0.8 part of agate, 6 parts of bone ash.
The present invention production method be：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, wipes the impurity such as floating ash, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
It at angle, prevents biscuit sucking too fast, avoids product glaze in sintering procedure, peeling phenomenon；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
16 hours time.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is Tang mouthful soil, wind scoop soil and kaolin to state the embryo material in step 4.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
It is respectively to soak for the first time 1-2 seconds glaze time to state the glaze of leaching twice in step 8, second of 3-4 seconds glaze time of leaching.
In concrete operations, the sintering procedure in the step 9 is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1.5 hours used times；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
3.5 hours, this process was oxidation process, and oxidation process is to keep product gentle such as beautiful effect；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 3 hours, this process is oxidation insulating process, aoxidizes insulating process and oxygen
Change process is the same also for the effect for keeping the gentle such as jade of product；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 7.5 small
When, this process is reduction process, and reduction process is to preferably make product porcelain；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
It is the basic embodiment of the present invention above, further can be improved, improved and limited on the basis of above：Institute
State step 6）In the Temperature fall time be 12 hours.
It should be noted that embodiments described above is to the illustrative and not limiting of technical solution of the present invention, affiliated skill
The equivalent replacement of the those of ordinary skill in art field or other modifications for being made according to the prior art are as long as no beyond the present invention
The thinking and range of technical solution should be included in right of the presently claimed invention within the scope of.
Claims (7)
1. your a kind of porcelain tea-dust glaze, it is characterised in that：Raw material composition including following parts by weight：Black feldspar 3-7 parts, gold
It is 2-4 parts native, 28-32 parts of dolomite, 11-15 parts of quartz, 12-16 parts of calcite, 0.5-1.5 parts of talcum, 0.5-1 parts of agate,
5-7 parts of bone ash.
2. your a kind of porcelain tea-dust glaze according to claim 1, it is characterised in that：Raw material group including following parts by weight
At：5 parts of black feldspar, 3 parts of gold soil, 30 parts of dolomite, 13 parts of quartz, 14 parts of calcite, 1 part of talcum, 0.8 part of agate, bone
6 parts of ash.
3. a kind of production method of your porcelain tea-dust glaze according to claim 1, which is characterized in that include the following steps：
Step 1：By above-mentioned parts by weight sorting, raw material is placed into oxidation 3-5 months, rejects impurity, is broken into graininess mixing
Proportioning, it is spare；
Step 2：120 mesh sieve is crossed into preliminary mixture material fine grinding in step 1, removes the iron that swims in slurry with magnet, as
Glaze；
Step 3：The Baume of glaze in step 2 is measured into concentration, adds water that glaze concentration is adjusted to 55 ° of summer Baume degrees, winter
Season 60 ° of Baume degrees, it is spare；
Step 4：Material base is placed on ventilation oxidation 3-5 months by scaffolding, after proportioning after mashing, pugging processing, throwing at
Green body is made in type, spare；
Step 5：Spare green body in step 4 is placed into 1-2 days summer, 3-4 days winter carried out cutting base, cut be positioned over after base it is logical
Naturally dry at wind slightly dips in water polishing base face with sponge, spare；
Step 6：Spare green body in step 5 is entered into kiln biscuiting, 800 DEG C -900 DEG C of firing temperature, firing time 5-6 hour burns
Temperature fall after the completion of system takes out green body, and inspection is hairless to prepare glazing after being ill；
Step 7：Spare glaze material stirring in step 3 is uniform, mix up concentration；The rib of biscuit is wiped with writing brush or hairbrush slightly humidification water
At angle；
Step 8：Biscuit is soaked into glaze at twice, soaks naturally dry after glaze, to having glazing position defective to carry out reclaim, repairing glaze；
Step 9：Spare green body in step 8 is put into kiln and carries out high-temperature firing, firing temperature is 950 DEG C -1200 DEG C, is fired
Time 12-16 hour.
4. the production method of your porcelain tea-dust glaze according to claim 3, it is characterised in that：Embryo material in the step 4
For Tang mouthful soil, wind scoop soil and kaolin.
5. the production method of your porcelain tea-dust glaze according to claim 3, it is characterised in that：In the step 8 twice
It is respectively to soak for the first time 1-2 seconds glaze time to soak glaze, soaks 3-4 seconds glaze time for the second time.
6. the production method of your porcelain tea-dust glaze according to claim 3, it is characterised in that：Firing in the step 9
Process is as follows：
1）Wicket stays seam, by room temperature to 500 DEG C, 1 hour to 1.5 hours used time；
2）When temperature reaches 500 DEG C, upper wicket, is warming up to 800 DEG C by 500 DEG C, slightly closes a floodgate when temperature rises to 800 DEG C, the used time
2 hours to 3.5 hours；
3）950 DEG C are warming up to by 800 DEG C, preceding fire heat preservation 2 hours to 3 hours；
4）Combined floodgate makes to be changed into reducing atmosphere in kiln, and is gradually heating to 1200 DEG C, and the entire fire reduction process that turns is 6.5 small
Up to 7.5 hours；
5）Turn to keep the temperature 0.5 hour after the completion of fiery reduction process；
6）Fire of operating a switch carries out Temperature fall；
7）When temperature drops to 200 DEG C or less, wicket opens digit seam, kiln is down to after 150 DEG C with the door open, when being down to 100 DEG C
It can kiln discharge.
7. the production method of your porcelain tea-dust glaze according to claim 6, it is characterised in that：The step 6）In nature
Temperature fall time is 12 hours.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111704360A (en) * | 2020-07-13 | 2020-09-25 | 张玉凤 | Antique Ru porcelain green glaze and manufacturing method thereof |
| CN112374756A (en) * | 2020-10-16 | 2021-02-19 | 龙泉市同契青瓷工作室 | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze |
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| CN112374756A (en) * | 2020-10-16 | 2021-02-19 | 龙泉市同契青瓷工作室 | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze |
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