CN103288493A - Reddish-black jun porcelain glaze prepared by utilizing metal copper and iron and preparation method of reddish-black jun porcelain glaze - Google Patents
Reddish-black jun porcelain glaze prepared by utilizing metal copper and iron and preparation method of reddish-black jun porcelain glaze Download PDFInfo
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Abstract
The invention discloses a reddish-black jun porcelain glaze prepared by utilizing metal copper and iron and a preparation method of the reddish-black jun porcelain glaze, belonging to the preparation filed of ceramic glazes. The preparation method of the reddish-black jun porcelain glaze comprises the following steps of: (1), mixing the following components in percentage by weight: 45%-50% of feldspar, 20%-30% of quartz, 14%-17% of calcite, 5%-7% of talcum, 2.5%-3.5% of kaolin and 2.9%-3.5% of calcium phosphate, so as to obtain a material mixture, and adding and sufficiently mixing the following materials (based on the total weight of the material mixture): 0.3%-2% of ZnO, 1.5%-4% of SnO2, 0.2%-2% of Fe, 0.1%-1.5% of Cu, 0.1%-0.5% of cellulose and 0.5%-1.5% of sodium tripolyphosphate, so as to obtain a glaze mixture; (2), carrying out wet-process ball-milling on the glaze mixture to obtain glaze pulp; (3), applying the glaze pulp on a biscuit firing billet for firing for 20 minutes-40minutes in a neutral or weak oxidative atmosphere, and cooling to obtain the reddish-black jun porcelain glaze. The preparation method of the reddish-black jun porcelain glaze is simple and easy to implement, board in firing temperature range and easily controllable in firing atmosphere. And the reddish-black jun porcelain glaze obtained by the preparation method disclosed by the invention is simple in composition, smooth and flat in glazed surface, high in stability and bright in reddish-black color.
Description
Technical field
The invention belongs to the ceramic glaze preparation field, relate to a kind of preparation method of pottery glaze, be specifically related to a kind of metallic copper, iron reddish black pottery glaze that is equipped with and preparation method thereof of utilizing.
Background technology
The pottery glaze is a kind of very famous and precious glaze.General pottery glaze is to add the mineral that contain copper and iron in parent glaze, uses initial oxidation, and the atmosphere of back reduction is fired and formed.But the extremely difficult control of the condition that these atmosphere require, thus fire pottery " ten kilns nine do not become ", the saying of " saw type in three minutes, saw in five minutes and to burn till, two minutes see fortune ", it is big to this shows that pottery burns till difficulty.
Along with the raising of detection technique in modern age, some scholars have carried out deep research to microstructure and the transmutation mechanism of pottery in ancient times, draw an ancient unit of weight glaze and be under the reducing atmosphere phase-splitting painted with multiple coloring mechanism such as oxide coloring.Reducing atmosphere is compared under the oxidizing atmosphere and is burnt till, owing to be that incomplete combustion and energy consumption are high and pollute greatly, cost is relatively also high, and does not meet the needs of current international community energy-saving and emission-reduction, needs technological improvement and raising badly.
Summary of the invention
The object of the present invention is to provide a kind of metallic copper, iron reddish black pottery glaze that is equipped with and preparation method thereof of utilizing, this method prescription is formed simple, and firing range is wide, and firing atmosphere is easily controlled, and the product glaze that makes is smooth smooth, and color is vivid, and color development is stable.
The present invention is achieved through the following technical solutions:
A kind of reddish black pottery glaze in massfraction, comprises following component: SiO
258.47～63.68%, Al
2O
38.99～10.20%, CaO14.91～17.94%, MgO2.22～3.03%, K
2O0.22～0.50%, Na
2O3.08～3.46%, Ca
3(PO
4)
22.59～3.5%, ZnO0.28～2%, SnO
21.4～4%, CuO0.12～1.76%, Fe
2O
30.28～2.88%.
A kind of reddish black pottery glaze, fired by following raw material and to form: 45～50% feldspar, 20～30% quartz, 14～17% calcite, 5～7% talcum, 2.5 the compound that～3.5% kaolin and 2.9～3.5% calcium phosphate are formed also comprises the ZnO that accounts for compound total mass 0.3～2%, 1.5～4%SnO
2, 0.2～2% Fe, 0.1～1.5% Cu, 0.1～0.5% Mierocrystalline cellulose and 0.5～1.5% tripoly phosphate sodium STPP.
A kind of metallic copper, iron method that is equipped with reddish black pottery glaze utilized may further comprise the steps:
1) in massfraction, the feldspar with 45～50%, 20～30% quartz, 14～17% calcite, 5～7% talcum is after 2.5～3.5% kaolin and 2.9～3.5% calcium phosphate mix, obtain compound, add the ZnO of compound total mass 0.3～2% again, 1.5～4%SnO
2, 0.2～2% Fe, 0.1～1.5% Cu, 0.1～0.5% Mierocrystalline cellulose and 0.5～1.5% tripoly phosphate sodium STPP fully behind the mixing, obtain mixing glaze;
2) will mix glaze through wet ball grinding, and fully obtain glaze slip behind the ball milling, regulating glaze slip proportion is 1.57～1.67g/cm
3
3) glaze slip is executed uniformly applied on biscuit, after the drying, in neutrality or weak oxide atmosphere, fire under 1250～1300 ℃, behind insulation 20～40min, cooling obtains reddish black pottery glaze.
Described wet ball grinding is by mixing glaze: the mass ratio of ball: water=1:2:0.8, and compound, ball and water packed into carry out ball milling in the ball mill.
Described abundant ball milling is for being finely ground to 250 orders.
Described abundant ball milling is fine grinding 20～40min.
Described firing in chamber type electric resistance furnace carried out.
The described furnace cooling that is cooled to.
Compared with prior art, the present invention has following beneficial technical effects:
The present invention utilizes metallic copper, the iron preparation method who is equipped with reddish black pottery glaze, modulation by prescription, utilize the parvafacies mechanism that melt produces in the glaze sintering process to carry out painted, glass melt produces phase-splitting in the glaze firing process, the oxidation in neutrality or weak oxide atmosphere of a spot of elemental metals copper obtains cupric oxide, the oxidation in neutrality or weak oxide atmosphere of a spot of elemental metals iron obtains a spot of iron protoxide and ferric oxide, cupric oxide is present in the microfacies rather than in the whole glassy phase, therefore can improve the concentration of iron ion and cupric ion in the microfacies, make a spot of metal simple-substance produce bigger tinting strength, also avoided its over oxidation and that glaze colours is transferred to is yellowish green, and glaze firing is carried out under neutrality or weak oxide atmosphere, compare with the reducing atmosphere of routine, energy consumption and pollution all reduce.This preparation method is simple, and firing range is wide, and firing atmosphere is easily controlled.
By the reddish black pottery glaze that present method prepares, prescription is formed simple, and smooth smooth, the stability height of glaze has vivid Celeste color.
Embodiment
The present invention is described in further detail below in conjunction with specific embodiment, and the explanation of the invention is not limited.
The employed raw material chemical constitution of the embodiment of the invention, as shown in table 1:
Table 1 raw material chemical constitution (wt%)
Embodiment 1
Utilize metallic copper, the iron method that is equipped with reddish black pottery glaze, may further comprise the steps:
1) with mass percent, the feldspar with 50%, 20% quartz, 17% calcite, 7% talcum, 3% calcium phosphate, 3% kaolin obtains compound after mixing, and adds the ZnO of compound total mass 0.5% again, 2% SnO
2, 1% Fe, 0.5% Cu, 0.3% Mierocrystalline cellulose and 1% tripoly phosphate sodium STPP, fully mixing obtains mixing glaze;
2) by by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water to be packed into carry out wet ball grinding in the ball mill, fine grinding 30min to 250 order obtains glaze slip, and adjusting glaze slip proportion is 1.65g/cm
3
3) glaze slip is executed uniformly applied on biscuit, after the drying, in chamber type electric resistance furnace, with neutrality or weak oxide atmosphere, fire under 1280 ℃, behind the insulation 20min, furnace cooling obtains reddish black pottery glaze.
Embodiment 2
Utilize metallic copper, the iron method that is equipped with reddish black pottery glaze, may further comprise the steps:
1) with mass percent, the feldspar with 50%, 25% quartz, 14% calcite, 5% talcum, 2.9% calcium phosphate, 3.1% kaolin obtains compound after mixing, and adds the ZnO of compound total mass 0.9% again, 1.5% SnO
2, 2% Fe, 1.5% Cu, 0.3% Mierocrystalline cellulose and 1% tripoly phosphate sodium STPP, fully mixing obtains mixing glaze;
2) by by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water to be packed into carry out wet ball grinding in the ball mill, fine grinding 30min to 250 order obtains glaze slip, and adjusting glaze slip proportion is 1.57g/cm
3
3) glaze slip is executed uniformly applied on biscuit, after the drying, in chamber type electric resistance furnace, with neutrality or weak oxide atmosphere, fire under 1260 ℃, behind the insulation 30min, furnace cooling obtains reddish black pottery glaze.
Embodiment 3
Utilize metallic copper, the iron method that is equipped with reddish black pottery glaze, may further comprise the steps:
1) with mass percent, the feldspar with 45%, 30% quartz, 14% calcite, 5% talcum, 3.5% calcium phosphate, 2.5% kaolin obtains compound after mixing, and adds the ZnO of compound total mass 1.5% again, 2.5% SnO
2, 0.2% Fe, 0.1% Cu, 0.1% Mierocrystalline cellulose and 0.5% tripoly phosphate sodium STPP, fully mixing obtains mixing glaze;
2) by by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water to be packed into carry out wet ball grinding in the ball mill, fine grinding 35min to 250 order obtains glaze slip, and adjusting glaze slip proportion is 1.67g/cm
3
3) glaze slip is executed uniformly applied on biscuit, after the drying, in chamber type electric resistance furnace, with neutrality or weak oxide atmosphere, fire under 1300 ℃, behind the insulation 20min, furnace cooling obtains reddish black pottery glaze.
Embodiment 4
Utilize metallic copper, the iron method that is equipped with reddish black pottery glaze, may further comprise the steps:
1) with mass percent, the feldspar with 45%, 30% quartz, 14% calcite, 5% talcum, 3.3% calcium phosphate, 2.7% kaolin obtains compound after mixing, and adds the ZnO of compound total mass 0.3% again, 4% SnO
2, 1.5% Fe, 0.7% Cu, 0.2% Mierocrystalline cellulose and 1% tripoly phosphate sodium STPP, fully mixing obtains mixing glaze;
2) by by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water to be packed into carry out wet ball grinding in the ball mill, fine grinding 20min to 250 order obtains glaze slip, and adjusting glaze slip proportion is 1.64g/cm
3
3) glaze slip is executed uniformly applied on biscuit, with neutrality or weak oxide atmosphere, fire under 1290 ℃ in chamber type electric resistance furnace dry back, and behind the insulation 40min, furnace cooling obtains reddish black pottery glaze.
Embodiment 5
Utilize metallic copper, the iron method that is equipped with reddish black pottery glaze, may further comprise the steps:
1) with mass percent, the feldspar with 47%, 25.5% quartz, 15% calcite, 6% talcum, 3% calcium phosphate, 3.5% kaolin obtains compound after mixing, and adds the ZnO of compound total mass 2% again, 1.5% SnO
2, 1% Fe, 1% Cu, 0.5% Mierocrystalline cellulose and 1.5% tripoly phosphate sodium STPP, fully mixing obtains mixing glaze;
2) by by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water to be packed into carry out wet ball grinding in the ball mill, fine grinding 40min to 250 order obtains glaze slip, and adjusting glaze slip proportion is 1.60g/cm
3
3) glaze slip is executed uniformly applied on biscuit, with neutrality or weak oxide atmosphere, fire under 1250 ℃ in chamber type electric resistance furnace dry back, and behind the insulation 35min, furnace cooling obtains reddish black pottery glaze.
The chemical constitution of the reddish black pottery glaze that above-described embodiment 1～5 is prepared is as shown in table 2:
The chemical constitution (wt%) of the reddish black pottery glaze that table 2 embodiment of the invention makes
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| SiO 2 | 58.78 | 58.47 | 62.00 | 61.42 | 63.68 |
| Al 2O 3 | 9.31 | 9.0 | 9.21 | 8.99 | 10.20 |
| CaO | 15.19 | 17.94 | 14.91 | 15.08 | 15.07 |
| MgO | 2.39 | 2.22 | 2.67 | 3.03 | 2.23 |
| K 2O | 0.50 | 0.27 | 0.41 | 0.22 | 0.23 |
| Na 2O | 3.46 | 3.17 | 3.08 | 3.26 | 3.10 |
| Ca 3（PO 4） 2 | 2.88 | 2.61 | 3.5 | 2.59 | 2.60 |
| ZnO | 2.0 | 0.28 | 1.43 | 0.28 | 1.0 |
| SnO 2 | 2.52 | 1.40 | 2.39 | 4.0 | 1.41 |
| Fe 2O 3 | 2.37 | 2.88 | 0.28 | 0.79 | 0.30 |
| CuO | 0.60 | 1.76 | 0.12 | 0.34 | 0.18 |
In sum, the present invention utilizes in the glaze firing process phase-splitting and metallic copper in the glaze, metallic iron heat-tinting, the oxidation in neutrality or weak oxide atmosphere of a spot of elemental metals copper obtains cupric oxide, the oxidation in neutrality or weak oxide atmosphere of a spot of elemental metals iron obtains a spot of iron protoxide and ferric oxide, and iron protoxide very easily is oxidized to ferric oxide; Cupric oxide is present in the microfacies rather than in the whole glassy phase, therefore can improve that the concentration of iron ion and cupric ion makes a spot of elemental metals oxidation produce bigger artistic effect in the microfacies, the reddish black pottery glaze glaze fit that makes is good, firing range is wide, firing atmosphere is easy to control, save energy, color development is stable, and color is vivid.This reddish black pottery glaze is applicable to artistic porcelain, porcelain modelled after an antique, household china.
Claims (8)
1. a reddish black pottery glaze is characterized in that, in massfraction, comprises following component: SiO
258.47～63.68%, Al
2O
38.99～10.20%, CaO14.91～17.94%, MgO2.22～3.03%, K
2O0.22～0.50%, Na
2O3.08～3.46%, Ca
3(PO
4)
22.59～3.5%, ZnO0.28～2%, SnO
21.4～4%, CuO0.12～1.76%, Fe
2O
30.28～2.88%.
2. reddish black pottery glaze, it is characterized in that, in massfraction, fired by following raw material and to form: 45～50% feldspar, 20～30% quartz, 14～17% calcite, 5～7% talcum, 2.5 the compound that～3.5% kaolin and 2.9～3.5% calcium phosphate are formed also comprises the ZnO that accounts for compound total mass 0.3～2%, 1.5～4%SnO
2, 0.2～2% Fe, 0.1～1.5% Cu, 0.1～0.5% Mierocrystalline cellulose and 0.5～1.5% tripoly phosphate sodium STPP.
3. one kind is utilized metallic copper, the iron method that is equipped with reddish black pottery glaze, it is characterized in that, may further comprise the steps:
1) in massfraction, the feldspar with 45～50%, 20～30% quartz, 14～17% calcite, 5～7% talcum is after 2.5～3.5% kaolin and 2.9～3.5% calcium phosphate mix, obtain compound, add the ZnO of compound total mass 0.3～2% again, 1.5～4%SnO
2, 0.2～2% Fe, 0.1～1.5% Cu, 0.1～0.5% Mierocrystalline cellulose and 0.5～1.5% tripoly phosphate sodium STPP fully behind the mixing, obtain mixing glaze;
2) will mix glaze through wet ball grinding, and fully obtain glaze slip behind the ball milling, regulating glaze slip proportion is 1.57～1.67g/cm
3
3) glaze slip is executed uniformly applied on biscuit, after the drying, in neutrality or weak oxide atmosphere, fire under 1250～1300 ℃, behind insulation 20～40min, cooling obtains reddish black pottery glaze.
4. according to right 3 described a kind of metallic copper, iron methods that are equipped with reddish black pottery glaze utilized, it is characterized in that described wet ball grinding is by mixing glaze: the mass ratio of ball: water=1:2:0.8, compound, ball and water packed into carry out ball milling in the ball mill.
5. according to right 3 described a kind of metallic copper, iron methods that are equipped with reddish black pottery glaze utilized, it is characterized in that described abundant ball milling is for being finely ground to 250 orders.
6. according to right 3 described a kind of metallic copper, iron methods that are equipped with reddish black pottery glaze utilized, it is characterized in that described abundant ball milling is fine grinding 20～40min.
7. according to right 3 described a kind of metallic copper, iron methods that are equipped with reddish black pottery glaze utilized, it is characterized in that described firing in chamber type electric resistance furnace carried out.
8. according to right 7 described a kind of metallic copper, iron methods that are equipped with reddish black pottery glaze utilized, it is characterized in that the described furnace cooling that is cooled to.
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| CN107056054A (en) * | 2017-05-24 | 2017-08-18 | 禹州市神器钧窑有限公司 | A kind of blue or green glaze of pottery |
| CN107602152A (en) * | 2017-09-28 | 2018-01-19 | 禹州市正玉钧窑有限公司 | A kind of pottery is with bluish white glaze and the technique for preparing pottery with bluish white glaze using pottery |
| CN107602152B (en) * | 2017-09-28 | 2021-04-13 | 禹州市正玉钧窑有限公司 | Green and white glaze for Jun porcelain and process for preparing Jun porcelain by using green and white glaze for Jun porcelain |
| CN107555797A (en) * | 2017-10-16 | 2018-01-09 | 禹州市锦丰源瓷业有限公司 | A kind of imitation Song-Dynasty-style typeface an ancient unit of weight orchid glaze |
| CN112408787A (en) * | 2020-11-27 | 2021-02-26 | 浙江省长兴县新华陶器有限公司 | Ecological green glaze and firing method thereof |
| CN112408787B (en) * | 2020-11-27 | 2022-07-22 | 浙江省长兴县新华陶器有限公司 | Ecological green glaze and firing method thereof |
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