CN106256923B - Film formation device, film build method and substrate-placing platform - Google Patents

Film formation device, film build method and substrate-placing platform Download PDF

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Publication number
CN106256923B
CN106256923B CN201610425922.6A CN201610425922A CN106256923B CN 106256923 B CN106256923 B CN 106256923B CN 201610425922 A CN201610425922 A CN 201610425922A CN 106256923 B CN106256923 B CN 106256923B
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substrate
temperature
film
mounting portion
peripheral ring
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CN106256923A (en
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田中诚治
里吉务
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Tokyo Electron Ltd
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Tokyo Electron Ltd
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    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K71/00Manufacture or treatment specially adapted for the organic devices covered by this subclass
    • H10K71/10Deposition of organic active material
    • H10K71/16Deposition of organic active material using physical vapour deposition [PVD], e.g. vacuum deposition or sputtering
    • H10K71/164Deposition of organic active material using physical vapour deposition [PVD], e.g. vacuum deposition or sputtering using vacuum deposition
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/12Organic material
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/50Substrate holders
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67098Apparatus for thermal treatment
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67242Apparatus for monitoring, sorting or marking
    • H01L21/67248Temperature monitoring
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/683Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere for supporting or gripping

Abstract

A kind of film formation device of present invention offer, film build method and substrate-placing platform.Uniform film can be formed, and can only form film on substrate.The process chamber and processing gas feed mechanism that film formation device has substrate-placing platform, implements film process to substrate.Substrate-placing platform includes:Its upper surface becomes the mounting portion of the mounting surface of mounting substrate;The peripheral ring being arranged in a manner of the periphery for surrounding mounting portion;1st temperature regulation section of the 1st temperature that the temperature of mounting portion is adjusted to form a film using processing gas;The temperature of peripheral ring can be adjusted to the 2nd temperature regulation section of the 2nd temperature that can not be formed a film using processing gas, between mounting portion and peripheral ring, complete cycle it is provided with the gap functioned as insulation, mounting surface forms smaller than substrate, and gap is formed in a manner of being taken in peripheral ring beyond part complete cycle of substrate when substrate is placed into mounting surface.

Description

Film formation device, film build method and substrate-placing platform
Technical field
The film formation device of film, film build method are formed the present invention relates to processing gas is supplied to substrate and for forming a film The substrate-placing platform of device.
Background technology
Organic material film has been used in sealant for organic EL display device etc..It is known that there are as below methods:It is manufacturing When such organic material film, so that Organic Ingredients is evaporated using gasifier etc. and supplied into film forming room, make them on substrate Vapor deposition polymerize and forms organic film (such as patent document 1).
Existing technical literature
Patent document
Patent document 1:No. 4283910 bulletins of Japanese Patent
Invention content
Problems to be solved by the invention
But, in the case where being aggregated in formation organic material film on the substrate of large area using vapor deposition, it is difficult to equably It forms a film.In addition, forming film handling the indoor part other than substrate, it is shorter in this way that accordingly, there exist maintenance periods The problem of.
This problem is not limited to the case where forming organic material film using vapor deposition polymerization, is handled to process chamber supply Gas also largely exists in the case of carrying out film process.
Thus, the object of the present invention is to provide a kind of film formation device, film build method and it is used for such film formation device Substrate-placing platform, wherein supply processing gas and when being formed a film on substrate, uniform film can be formed, and can Film is only formed on substrate.
The solution to the problem
To solve the above-mentioned problems, the present invention provides a kind of film formation device comprising:Substrate-placing platform is used to load Substrate;Process chamber is used to implement film process to the substrate for being placed on the substrate-placing platform;Processing gas supply part, It is used to supply the processing gas of film process to the process chamber, and the film formation device is to the substrate on the substrate-placing platform Implement film process, which is characterized in that the substrate-placing platform includes:Mounting portion, upper surface become for loading substrate Mounting surface;Peripheral ring is arranged in a manner of surrounding the periphery of the mounting portion;1st temperature regulation section is used for the load The temperature for setting portion is adjusted to the 1st temperature to form a film using the processing gas;2nd temperature regulation section, be used for by The temperature of the peripheral ring is adjusted to the 2nd temperature that can not be formed a film using the processing gas, in the mounting portion and institute Between stating peripheral ring, complete cycle it is provided with as the insulation for inhibiting the heat exchange between the mounting portion and the peripheral ring The mounting surface in the gap functioned, the mounting portion forms smaller than the substrate, and the gap is in the substrate When being placed on the mounting surface substrate exceed from the mounting surface taken in the peripheral ring beyond part complete cycle Mode is formed.
In addition, the present invention provides a kind of substrate-placing platform, it is used to supply processing gas and film process is implemented to substrate Film formation device, which is characterized in that the substrate-placing platform includes:Mounting portion, upper surface become the mounting for loading substrate Face;Peripheral ring is arranged in a manner of surrounding the periphery of the mounting portion;1st temperature regulation section, by the temperature of the mounting portion Degree is adjusted to the 1st temperature to form a film using the processing gas;2nd temperature regulation section, by the peripheral ring Temperature is adjusted to the 2nd temperature that can not be formed a film using the processing gas, between the mounting portion and the peripheral ring, It is provided with to complete cycle as between for inhibiting the insulation of the heat exchange between the mounting portion and the peripheral ring to function The mounting surface of gap, the mounting portion forms smaller than the substrate, and the gap is in the substrate-placing to the load The mode taken beyond part complete cycle in the peripheral ring of the substrate exceeded from the mounting surface is formed when setting face.
Moreover, the present invention provides a kind of film build method, using film formation device in substrate-placing to load in the film build method It sets and supplies processing gas to process chamber and film process are implemented to substrate in the state of portion, the film formation device is in the process chamber Configured with substrate-placing platform, which includes:The mounting portion, upper surface become the mounting for loading substrate Face;Peripheral ring, to be wrapped across as the gap for inhibiting the insulation in its heat exchange between the mounting portion to function It is arranged with enclosing the mode complete cycle of the periphery of the mounting portion, which is characterized in that, which has following work Sequence:The substrate by complete cycle is covered to the gap and takes the work for being placed in the mounting surface in a manner of the peripheral ring Sequence;The process for the 1st temperature that the temperature of the mounting portion is adjusted to form a film using the processing gas;It will be described The temperature of peripheral ring is adjusted to can not be using the process for the 2nd temperature that the processing gas forms a film.
It can be set as such as lower structure:The substrate-placing platform has matrix, central portion of the mounting portion from described matrix It is protrusively provided upward, the peripheral ring is set to described matrix across heat-insulating material.
Preferably, the width beyond part of the substrate when the substrate-placing is to the mounting surface is unused Below the width for making the region of product.In this case, the width beyond part can be set as and be less than 10mm, the gap Width be 1mm~9mm.Preferably, the width beyond part is 5mm less than 10mm, the width in the gap Degree is 3mm~5mm.
Can also be also to have:Upper lid is arranged in a manner of covering the substrate-placing platform, is formed for dividing The process chamber;3rd temperature regulation section, by the temperature of the upper lid be adjusted to can not using the processing gas carry out at 3rd temperature of film.
It can be set as, also there is the spraying component being arranged in a manner of opposite with the mounting surface, it will be from the processing gas The processing gas that the supply of body supply part comes is sprayed from the spraying component.
Using organic system gas as the processing gas, can on the substrate be formed by vapor deposition polymerization organic Film.In this case, it can be set as, the organic film is polyurea film, is adjusted into trip temperature using the 1st temperature regulation section, So that the 1st temperature of the mounting portion become 100 DEG C hereinafter, using the 2nd temperature regulation section into trip temperature adjust, with The 2nd temperature of the peripheral ring is set to become 150 DEG C or more.
The effect of invention
According to the present invention, the 1st temperature that the temperature of mounting portion is adjusted to form a film using processing gas will be outer The temperature of chow ring is adjusted to the 2nd temperature that can not be formed a film using processing gas, therefore, it is possible to only form film on substrate. In addition, between mounting portion and peripheral ring, it is provided with as inhibiting the heat exchange between mounting portion and peripheral ring to complete cycle The gap that insulation functions, therefore, it is possible to prevent from directly transmitting from periphery circumferential direction mounting portion heat.Therefore, it is possible to load The temperature in portion controls the state in the heat affecting for inhibiting peripheral ring, but the temperature of substrate can be made uniformly to be formed uniform Film.In addition, keeping the upper surface of peripheral ring concordant with mounting surface, mounting surface is made to be configured smaller than substrate, moreover, gap is set as Substrate-placing to substrate when mounting surface peripheral part complete cycle take the size as the upper surface of peripheral ring, therefore, gap quilt Substrate covers, and can prevent processing gas from entering in gap.
Description of the drawings
Fig. 1 is the sectional view for the film formation device for indicating one embodiment of the present invention.
Fig. 2 is the vertical view of the thermoregulation mechanism for the film formation device for schematically showing Fig. 1.
Fig. 3 is the sectional view for indicating the partial enlargement of the substrate-placing platform of the film formation device of Fig. 1.
Reference sign
1, substrate-placing platform;2, upper lid;3, matrix;4, mounting portion;5, peripheral ring;6, gap;7, heat-insulating material;8, empty Between;9, shower plate;10, process chamber;13, processing gas feed mechanism;16, exhaust gear;17,18,19, temperature regulating medium stream Road;20, temperature regulating medium feed unit;25, control unit;100, film formation device;G, substrate.
Specific implementation mode
Hereinafter, the embodiments of the present invention will be described with reference to the drawings.
Fig. 1 is the sectional view for the film formation device for indicating one embodiment of the present invention, and Fig. 2 schematically shows Fig. 1 The vertical view of the thermoregulation mechanism of film formation device.
Film formation device 100 has:Substrate-placing platform 1 is used to load substrate G;Upper lid 2 is used to divide to be formed and use In the process chamber for carrying out film process to the substrate G for being placed on substrate-placing platform 1.
Substrate-placing platform 1 has:Plate-like matrix 3;It is arranged in such a way that the central portion from matrix 3 is outstanding upward Column and its upper surface become the mounting portion 4 of the mounting surface 4a for loading substrate G;It is set to matrix 3 across heat-insulating material 7 Peripheral ring 5 around mounting portion 4.The mounting surface 4a for forming the upper surface of mounting portion 4 forms smaller than substrate G.In this example, Substrate G and mounting surface 4a rectangular shapeds.
Peripheral ring 5 is arranged in a manner of surrounding the periphery of mounting portion 4 across gap 6, in the shape of a frame.Gap 6 is outer as inhibition The insulation of heat exchange between chow ring 5 and mounting portion 4 functions.The upper surface of peripheral ring 5 is concordant with mounting surface 4a.
When substrate G is placed on mounting surface 4a, what peripheral part as complete cycle exceeded from mounting surface 4a exceeds part, The size of gap 6 crosses gap 6 beyond part as substrate G and reaches the upper surface of peripheral ring 5, takes to complete cycle in peripheral ring 5 Upper surface as size.Thus, when substrate G is placed on mounting surface 4a, gap 6 is covered by substrate G.
Heat-insulating material 7 is in frame-shaped corresponding with peripheral ring 5, and inner peripheral surface and the periphery of mounting portion 4 are placed in contact with.It is adiabatic Material 7 is arranged to make between peripheral ring 5 and matrix 3 adiabatic, can it is preferable to use talcum, MACOR (registered trademark) Such lower ceramic material of thermal coefficient.In addition, the periphery of peripheral ring 5 and heat-insulating material 7 has reached the periphery of matrix 3 Position.
As shown in the enlarged drawing of Fig. 3, the width D 1 beyond part exceeded from the mounting surface 4a of substrate G is set as technology ensuring Outside and it is not used as the width in region of product or less.The width in the region outside the technology ensuring is typically 10mm or so, therefore, In this case, it is preferred that the width beyond part is less than 10mm.In addition, the width beyond part of the width D 2 in gap 6 and substrate G D1 correspondingly changes, and in the case where the width D 1 beyond part is less than 10mm, the width D 2 in gap 6 is 1mm~9mm or so. Preferably, the width D 1 beyond part of substrate G is 5mm less than 10mm, and the width D 2 in gap is 3mm~5mm.
There is upper lid 2 side wall 2a and roof 2b, side wall 2a to be supported on air-tight state across containment member (not shown) The upper surface of peripheral ring 5.Space 8 is provided with shower plate 9 in the lower section of roof 2b, is surrounded by side wall 2a and shower plate 9 Part becomes process chamber 10.In addition it is also possible to be set as directly supporting the construction of upper lid 2 by matrix 3.In this case, periphery Ring 5 and heat-insulating material 7 are formed than the periphery of matrix 3 in a manner of in the inner part by their periphery.
Be formed with the gas introducing port 11 for reaching space 8 in the center of roof 2b, gas introducing port 11 via piping 12 with Processing gas feed mechanism 13 connects.Also, the processing gas from processing gas feed mechanism 13 reaches empty via piping 12 Between 8, sprayed from many a gas ejection hole 9a for being set to shower plate 9 into process chamber 10.Gas ejection hole 9a both can be equal It is configured at the region opposite with substrate G of shower plate 9 evenly, configures while specific pattern can also be described.
By so supplying processing gas into process chamber 10, scheduled film is formed on substrate G.At this point, by from Process gases feed mechanism 13 uses scheduled organic system gas as processing gas, vapor deposition can be utilized to be aggregated in shape on substrate G At organic film.It is formed by organic film as using vapor deposition polymerization, as representative, polyurea film can be enumerated.Forming polyureas When film, processing gas is supplied with the state for making diisocyanate and diamine gasify using gasifier etc..Thereby, it is possible to make them Vapor deposition polymerize and forms polyurea film on substrate G.
It is formed with exhaust outlet 14 in the lower part of the side wall 2a of upper lid 2, exhaust outlet 14 is connect with exhaust piping 15.It is being vented It is provided with the exhaust gear 16 being made of vacuum pump and pressure-control valve etc. in piping 15, can will be kept into process chamber 10 Scheduled vacuum atmosphere.In the case where forming polyurea film by diisocyanate and diamine, by the pressure control in process chamber 10 10Torr (1333Pa) is made hereinafter, being controlled preferably to 0.2Torr~2.0Torr (26.7Pa~266Pa).
In addition, although not shown, but it is formed with the input/output port for input and output substrate G in the side wall 2a of upper lid 2, The input/output port can be opened and closed by switching mechanisms such as gate valves.
Be internally provided with the 1st temperature regulating medium flow path 17 in mounting portion 4, by make the 1st temperature regulating medium to this 1st temperature regulating medium flow path 17 circulates, the temperature of mounting portion 4 to be adjusted.It is carried out using the 1st temperature regulating medium Temperature is adjusted, so that the substrate G for being placed on mounting surface 4a becomes the 1st temperature T1 that can be formed a film.It is formed using vapor deposition polymerization In the case of organic film, needing the 1st temperature T1 is formed using vapor deposition polymerization as low as the temperature for the degree that can be deposited In the case of polyurea film, the 1st temperature T1 is controlled so as to that 100 DEG C or less of vapor deposition polymerization can be carried out, is preferably 50 DEG C~100 ℃。
Be internally provided with the 2nd temperature regulating medium flow path 18 in peripheral ring 5, by make the 2nd temperature regulating medium to this 2nd temperature regulating medium flow path 18 circulates, the temperature of peripheral ring 5 to be adjusted.It will be outer using the 2nd temperature regulating medium The temperature of chow ring 5 is adjusted to that the 2nd temperature T2 of film can not be formed on its surface.The case where forming organic film using vapor deposition polymerization Under, need the 2nd temperature T2 to be up to the temperature for the degree that can not be deposited, using vapor deposition polymerization form polyurea film in the case of into Trip temperature is adjusted so that the temperature of peripheral ring 5 become can not carry out vapor deposition 150 DEG C or more of polymerization, be preferably 150 DEG C~ 180℃。
It is provided with the 3rd temperature regulating medium flow path 19 on the roof 2b of upper lid 2, by making the 3rd temperature regulating medium It circulates to the 3rd temperature regulating medium flow path 19, the temperature of upper lid 2 to be adjusted.Utilize the 3rd temperature regulating medium It is adjusted into trip temperature, so that upper lid 2 becomes the 3rd temperature T3 that can not form film in its inner wall.It is formed using vapor deposition polymerization In the case of organic film, the 3rd temperature T3 needs the temperature for the degree for being up to not to be deposited, and is formed using vapor deposition polymerization In the case of polyurea film, the temperature of upper lid 2 is controlled so as to effectively form 150 DEG C of film or more, preferably 150 DEG C ~180 DEG C.
From temperature regulating medium feed unit 20 respectively to the 1st~the 3rd temperature regulating medium flow path 17~19 supply the 1st~ 3rd temperature regulating medium.Temperature regulating medium feed unit 20 has the 1st temperature regulating medium to the 1st temperature regulating medium The 1st temperature regulating medium supply unit (CH1) 20a that flow path 17 supplies, by the 2nd temperature regulating medium to the 2nd temperature regulating medium The 2nd temperature regulating medium supply unit (CH2) 20b that flow path 18 supplies, by the 3rd temperature regulating medium to the 3rd temperature regulating medium The 3rd temperature regulating medium supply unit (CH3) 20c that flow path 19 supplies.
1st temperature regulating medium supply unit (CH1) 20a supplies the adjusting of the 1st temperature with to the 1st temperature regulating medium flow path 17 The supplying tubing 21a of medium, the return piping 21b (figures that the 1st temperature regulating medium is returned from the 1st temperature regulating medium flow path 17 2) it connects, the 1st temperature regulating medium is recycled to the 1st temperature regulating medium flow path 17 and is supplied.It is situated between in addition, the 1st temperature is adjusted Matter supply unit (CH1) 20a controls the temperature of the 1st temperature regulating medium at the 1st temperature T1.
2nd temperature regulating medium supply unit (CH2) 20b supplies the adjusting of the 2nd temperature with to the 2nd temperature regulating medium flow path 18 The supplying tubing 22a of medium, the return piping 22b (figures that the 2nd temperature regulating medium is returned from the 2nd temperature regulating medium flow path 18 2) it connects, the 2nd temperature regulating medium is recycled to the 2nd temperature regulating medium flow path 18 and is supplied.It is situated between in addition, the 2nd temperature is adjusted Matter supply unit (CH2) 20b controls the temperature of the 2nd temperature regulating medium at the 2nd temperature T2.
3rd temperature regulating medium supply unit (CH3) 20c supplies the adjusting of the 3rd temperature with to the 3rd temperature regulating medium flow path 19 The supplying tubing 23a of medium, the return piping 23b (figures that the 3rd temperature regulating medium is returned from the 3rd temperature regulating medium flow path 19 2) it connects, the 3rd temperature regulating medium is recycled to the 3rd temperature regulating medium flow path 19 and is supplied.It is situated between in addition, the 3rd temperature is adjusted Matter supply unit (CH3) 20c controls the temperature of the 3rd temperature regulating medium at the 3rd temperature T3.
In addition, temperature regulating medium feed unit 20 can also be opposite 2nd temperature regulating medium flow path 18 and the 3rd temperature The temperature regulating medium for adjusting 19 supply of medium flow path carries out temperature controlled unit together.In addition, in Fig. 1,2, schematically The the 1st~the 3rd temperature regulating medium flow path 17~19 is described on ground, actually their temperature to be adjusted to the side of scheduled temperature Formula is configured to proper shape.
Film formation device 100 has the control unit 25 controlled for each constituting portion to film formation device 100.Control unit 25 With microprocessor (computer), to processing gas feed mechanism 13, exhaust gear 16, temperature regulating medium feed unit 20 Etc. being controlled.Control unit 25 executes scheduled processing processing procedure, has and stores the promising control executed needed for scheduled processing processing procedure Parameter processed, storage part, input part and the display etc. for handling processing procedure.
In thus configured film formation device 100, it will be transported in process chamber 10 from substrate input/output port (not shown) Substrate G the mounting surface 4a of mounting portion 4 is placed in a manner of taking in external rings 5 with covering gap 6 and complete cycle, utilize air exhauster Structure 16 will be kept into scheduled vacuum state in process chamber 10.Then, by from temperature regulating medium feed unit 20 to the 1st temperature Degree adjusts medium flow path 17, the 2nd temperature regulating medium flow path 18, the 3rd temperature regulating medium flow path 19 and is supplied respectively to the 1st temperature tune Medium, the 2nd temperature regulating medium, the 3rd temperature regulating medium are saved, the temperature of mounting portion 4 is adjusted to the 1st temperature of film forming The temperature of peripheral ring 5 and upper lid 2 is adjusted to the 2nd temperature T2 and the 3rd temperature T3 that can not form a film by T1 respectively.In addition, 2nd temperature T2 and the 3rd temperature T3 can also be identical.
In this state, it is supplied into process chamber 10 from processing gas feed mechanism 13 via piping 12 and shower plate 9 Processing gas forms scheduled film on the surface of substrate G.
For example, as processing gas, using scheduled organic system gas, vapor deposition can be utilized to be aggregated on substrate and be formed with Machine film.Polyurea film is formed as in the case of organic film polymerizeing using vapor deposition, is by the pressure control in process chamber 10 10Torr (1333Pa) is hereinafter, be preferably controlled to 0.2Torr~2.0Torr (26.7Pa~266Pa), as processing gas, It is supplied to process chamber 10 in the state of so that diisocyanate and diamine has been gasified using gasifier etc., makes them on substrate G Vapor deposition polymerization.
In this case, the 1st temperature T1 as the temperature of mounting portion 4 is the temperature as low as the degree that can be deposited Degree, in the case where forming polyurea film, 100 DEG C are adjusted to hereinafter, excellent using the 1st temperature regulating medium by the temperature of mounting portion 4 Select 50 DEG C~100 DEG C.On the other hand, the 3rd of the temperature as the 2nd temperature T2 of the temperature of peripheral ring 5 and as upper lid 2 Temperature T3 is up to the temperature for the degree that can not be deposited, and in the case where forming polyurea film, is utilized respectively the adjusting of the 2nd temperature The temperature of peripheral ring 5 and upper lid 2 is adjusted to 150 DEG C or more by medium and the 3rd temperature regulating medium, preferably 150 DEG C~ 180℃。
Thereby, it is possible to only form a film on the surface of substrate G, the periphery in the periphery for being set to mounting portion 4 can be inhibited The surface of ring 5, the inner wall of upper lid 2 form film.
But, the case where the mounting portion 4 and 5 temperature of peripheral ring that so will abut against are adjusted to respectively different temperature respectively Under, if mounting portion 4 and peripheral ring 5 contact, mounting portion 4 is easy to exchange heat with peripheral ring 5, the temperature control of mounting portion 4 It reduces, it is difficult to uniform film is formed on substrate G.Especially, if substrate G enlargements, tendency become apparent.
In contrast, in the present embodiment, in the mounting portion 4 including mounting surface 4a and being provided with work between peripheral ring 5 For the gap 6 of insulation, it is therefore possible to prevent directly carrying out hot transmission from peripheral ring 5 to mounting portion 4.Especially, gap 6 reaches Top makes mounting surface 4a and the upper surface of peripheral ring 5 effectively completely cut off, thus mutual temperature will not generate between them it is dry It relates to.Moreover, inhibiting to transmit to the heat of mounting portion 4 from peripheral ring 5 via the matrix 3 of substrate-placing platform 1 using heat-insulating material 7. Therefore, it is possible to control the temperature of mounting portion 4 in the state of inhibiting the heat affecting from peripheral ring 5, the temperature of substrate G can be made Degree uniformly forms uniform film.
In addition, in the case where being provided with such gap 6, if processing gas enters gap 6, there are following bad feelings Condition:Insulation effect can not be obtained by film forming as the reason of particle or gap 6 is interior, but in the present embodiment, make peripheral ring 5 upper surface is concordant with mounting surface 4a, and the mounting surface 4a as the upper surface of mounting portion 4 is made to be configured smaller than substrate G, and And the slave mounting surface 4a that the size in gap 6 is set as to the substrate G when substrate G is placed on mounting surface 4a exceed exceed part The size as the upper surface of peripheral ring 5 is taken to complete cycle, therefore, it is possible to prevent such unfavorable condition.I.e., on by being set as Such structure is stated, when substrate G is placed on mounting surface 4a, part is exceeded existing for the complete cycle in mounting surface 4a of substrate G It takes in peripheral ring 5, to which gap 6 is shielded, can prevent processing gas from entering in gap 6.
Moreover, substrate G outer peripheral portion there are technology ensuring outside and be not used as the region of product, therefore, as long as will surpass The width D 1 for going out part is set as the width in the region hereinafter, the yield rate of product will not then reduced.
The width in the region outside technology ensuring is typically 10mm or so, it is therefore preferable that the width D 1 beyond part is less than 10mm.In addition, the width D 2 in gap 6 and the width D 1 beyond part of substrate G correspondingly change, in the width D 1 beyond part In the case of 10mm, the width D 2 in gap 6 is 1mm~9mm or so.In addition, between mounting table 4 and peripheral ring 5 From the viewpoint of insulation effect, the width D 2 in gap 6 there is also preferred range, it is comprehensive these, then preferable substrate G exceeds portion Point width D 1 be 5mm less than 10mm, the width D 2 in gap is 3mm~5mm.
In addition, the present invention is not limited to the above embodiment, various modifications can be carried out.For example, in above-mentioned embodiment party In formula, following situation is shown:Substrate is aggregated in using vapor deposition as processing gas by using scheduled organic system gas The case where upper formation organic film, the case where especially forming polyurea film, but it is not limited to this, can be applied to make such as CVD The whole circumstances to be formed a film with processing gas.
In addition, in the above-described embodiment, show using temperature regulating medium to mounting portion, peripheral ring etc. into trip temperature The case where adjusting, but it is self-evident, other temperature controlling units such as resistance type heater can also be used.
Moreover, in the above-described embodiment, the case where shape to the mounting surface of substrate and mounting portion is rectangular shape It is illustrated, but is certainly not limited to this.

Claims (15)

1. a kind of film formation device comprising:
Substrate-placing platform is used to load substrate;
Process chamber is used to implement film process to the substrate for being placed on the substrate-placing platform;
Processing gas supply part is used to supply the processing gas of film process, the film formation device pair to the process chamber Substrate on the substrate-placing platform implements film process, which is characterized in that
The substrate-placing platform includes:
Mounting portion, upper surface become the mounting surface for loading substrate;
Peripheral ring is arranged in a manner of surrounding the periphery of the mounting portion;
1st temperature regulation section is used to be adjusted to form a film using the processing gas by the temperature of the mounting portion The 1st temperature;
2nd temperature regulation section is used to be adjusted to not form a film using the processing gas by the temperature of the peripheral ring The 2nd temperature,
Between the mounting portion and the peripheral ring, it is provided with as inhibiting the mounting portion and the periphery to complete cycle The gap that the insulation of heat exchange between ring functions,
The mounting surface of the mounting portion forms smaller than the substrate, and the gap is in the substrate-placing to the load The mode taken beyond part complete cycle in the peripheral ring of the substrate exceeded from the mounting surface is formed when setting face.
2. film formation device according to claim 1, which is characterized in that
The substrate-placing platform has matrix, and the mounting portion is protrusively provided upward from the central portion of described matrix, described Peripheral ring is set to described matrix across heat-insulating material.
3. film formation device according to claim 1 or 2, which is characterized in that
The width beyond part of the substrate when the substrate-placing is to the mounting surface is the region for being not used as product Width below.
4. film formation device according to claim 3, which is characterized in that
The width beyond part is less than 10mm, and the width in the gap is 1mm~9mm.
5. film formation device according to claim 4, which is characterized in that
The width beyond part is 5mm less than 10mm, and the width in the gap is 3mm~5mm.
6. film formation device according to claim 1 or 2, which is characterized in that
The film formation device also has:Upper lid is arranged in a manner of covering the substrate-placing platform, for dividing described in formation Process chamber;3rd temperature regulation section, be used for by the temperature of the upper lid be adjusted to can not using the processing gas carry out at 3rd temperature of film.
7. film formation device according to claim 1 or 2, which is characterized in that
The film formation device also has the spraying component being arranged in a manner of opposite with the substrate-placing face, will be from the processing gas The processing gas that the supply of body supply part comes is sprayed from the spraying component.
8. film formation device according to claim 1 or 2, which is characterized in that
As the processing gas, using organic system gas, organic film is formed on the substrate using vapor deposition polymerization.
9. film formation device according to claim 8, which is characterized in that
The organic film is polyurea film, is adjusted into trip temperature using the 1st temperature regulation section, so that the mounting portion is described 1st temperature becomes 100 DEG C hereinafter, being adjusted into trip temperature using the 2nd temperature regulation section, so that described the of the peripheral ring 2 temperature become 150 DEG C or more.
10. a kind of substrate-placing platform, it is used to supply processing gas and implements the film formation devices of film process to substrate, feature It is,
The substrate-placing platform includes:
Mounting portion, upper surface become the mounting surface for loading substrate;
Peripheral ring is arranged in a manner of surrounding the periphery of the mounting portion;
The temperature of the mounting portion is adjusted to the form a film using the processing gas the 1st by the 1st temperature regulation section Temperature;
The temperature of the peripheral ring is adjusted to the can not form a film using the processing gas the 2nd by the 2nd temperature regulation section Temperature,
Between the mounting portion and the peripheral ring, it is provided with as inhibiting the mounting portion and the periphery to complete cycle The gap that the insulation of heat exchange between ring functions,
The mounting surface of the mounting portion forms smaller than the substrate, and the gap is in the substrate-placing to the load The mode taken beyond part complete cycle in the peripheral ring of the substrate exceeded from the mounting surface is formed when setting face.
11. substrate-placing platform according to claim 10, which is characterized in that
The substrate-placing platform also has matrix, and the mounting portion is protrusively provided upward from the central portion of described matrix, described Peripheral ring is set to described matrix across heat-insulating material.
12. the substrate-placing platform according to claim 10 or 11, which is characterized in that
The width beyond part of the substrate when the substrate-placing is to the mounting surface is the region for being not used as product Width below.
13. substrate-placing platform according to claim 12, which is characterized in that
The width beyond part is less than 10mm, and the width in the gap is 1mm~9mm.
14. substrate-placing platform according to claim 13, which is characterized in that
The width beyond part is 5mm less than 10mm, and the width in the gap is 3mm~5mm.
15. a kind of film build method, in the film build method, using film formation device to place in the state that substrate-placing is to mounting portion It manages room supply processing gas and film process is implemented to substrate, which is configured with substrate-placing in the process chamber Platform, the substrate-placing platform include:The mounting portion, upper surface become the mounting surface for loading substrate;Peripheral ring, with every It and surrounds the outer of the mounting portion in the gap that the insulation of its heat exchange between the mounting portion functions as inhibition The mode complete cycle in week it is arranged, which is characterized in that,
The film build method has following process:
The substrate by complete cycle is covered to the gap and takes the work for being placed in the mounting surface in a manner of the peripheral ring Sequence;
The process for the 1st temperature that the temperature of the mounting portion is adjusted to form a film using the processing gas;
The temperature of the peripheral ring is adjusted to can not be using the process for the 2nd temperature that the processing gas forms a film.
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JP2017002385A (en) 2017-01-05
KR20160148471A (en) 2016-12-26

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