CN106234632A - A kind of Semen Arecae dried tofu and preparation method thereof - Google Patents
A kind of Semen Arecae dried tofu and preparation method thereof Download PDFInfo
- Publication number
- CN106234632A CN106234632A CN201610866680.4A CN201610866680A CN106234632A CN 106234632 A CN106234632 A CN 106234632A CN 201610866680 A CN201610866680 A CN 201610866680A CN 106234632 A CN106234632 A CN 106234632A
- Authority
- CN
- China
- Prior art keywords
- semen arecae
- dried tofu
- parts
- semen
- juice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C20/00—Cheese substitutes
- A23C20/02—Cheese substitutes containing neither milk components, nor caseinate, nor lactose, as sources of fats, proteins or carbohydrates
- A23C20/025—Cheese substitutes containing neither milk components, nor caseinate, nor lactose, as sources of fats, proteins or carbohydrates mainly containing proteins from pulses or oilseeds
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of Semen Arecae dried tofu, by the raw material of following parts by weight through bean defibrination, fruit is squeezed the juice, serosity boils, lower the temperature after add Gypsum Fibrosum, squeezing final vacuum packaging sterilization be prepared from: Semen sojae atricolor 80～90 parts, Semen phaseoli radiati 5～10 parts, Semen Arecae extract 0.01～5 parts, Gypsum Fibrosum 5～15 parts, crystal sugar 3～5 parts, Fructus Musae 2～5 parts, Fructus Mali pumilae 1～3 parts, Fructus Ananadis comosi 2～3 parts, Hylocereus undatus 3～6 parts.The Semen Arecae dried tofu obtained by preparation technology of the present invention is in good taste, and in the course of processing, with the addition of Semen Arecae effective ingredient, nutrient containing multiple needed by human body and benefit materials, while possessing Semen Arecae taste and characteristic, impart the helping digestion of Semen Arecae dried tofu of the present invention, removing food stagnancy, improve the effects such as constipation symptom.
Description
Technical field
The present invention relates to the technical field of food processing, be specifically related to Semen Arecae dried tofu and preparation method thereof.
Background technology
Fresh Semen Arecae (Areca catechu L) is the mature fruit of Palmae Betel nuts plant Semen Arecae.The whole world is about at present
There are 700,000,000 people's edible areca-nuts.Semen Arecae is liked by consumers in general equally deeply in China, is described as " the green arrow chewing gum of China ".
Semen Arecae also has abundant medical value, occupies (Semen Arecae, Fructus Alpiniae Oxyphyllae, Fructus Amomi, Ba Ji first of China's " four great Nan medicines "
My god), bitter in the mouth, pungent, warm, return stomach, large intestine channel.Nutrient containing multiple needed by human body and benefit materials, also contain many simultaneously
Planting pharmacological component, have the effects such as parasite killing, removing food stagnancy, diuretic, dehumidifying, preventing the attack (or recurrence) of malaria, " Chinese Pharmacopoeia " is gone through version and is all recorded, 2015 years
Version Semen Arecae one-tenth side kind has 55." side's arteries and veins is authentic " record Semen Arecae full vexed one-tenth sputum vomiter for the treatment of food stagnation: Semen Arecae, the Rhizoma Pinelliae, sand
Core, Semen Raphani, Fructus Hordei Germinatus, Rhizoma Zingiberis, each two money of the Rhizoma Atractylodis Macrocephalae, be decocted in water for oral dose." Prescriptions for Universal Relief " Semen Arecae dissipates and " detailed outline " is recorded Semen Arecae and controlled defecation not
Logical, also controlling the intestines and stomach has wet, and big constipation is puckery: Semen Arecae is to big person half piece.Decoct water mill one money with Radix Ophiopogonis, weight soup scald decoction being taken hot it.
Containing indispensable in the human life activities such as rich in protein, fat, vitamin and mineral in Semen sojae atricolor
Nutrition, compares with other food, and protein content is high, and the collocation of other nutrition the most relatively equalizes.Therefore, often eat
Bean product, it is possible to decrease the diseases such as cholesterolemia and prophylaxis of hypertension, arteriosclerosis and cardiovascular.Dried tofu is a kind of with a long history
Folk snack, tradition dried tofu be with single Semen sojae atricolor as raw material, the bean curd deep processing made is made, instant.Along with people
Growth in the living standard and the growing requirement to quality of life, the dried tofu that market is sold scarcely has health care merit
Effect, it is impossible to meet the diversified demand of consumer.
At present, there is not yet the relevant report of the dried tofu of Semen Arecae composition and taste.
Summary of the invention
It is an object of the invention to provide a kind of interpolation Semen Arecae composition in the dried tofu course of processing so that it is Semen Arecae dried tofu reaches
Aid digestion, be conducive to improving effect of constipation symptom.
To achieve these goals, the technical scheme is that a kind of Semen Arecae dried tofu of offer, by following parts by weight
Raw material adds Gypsum Fibrosum after bean defibrination, mashing off, cooling, and squeezing, the packaging sterilization of stew in soy sauce final vacuum are prepared from: Semen sojae atricolor 80～95
Part, Semen phaseoli radiati 5～10 parts, Semen Arecae extract 0.01～5 parts, Gypsum Fibrosum 3～10 parts；Refined salt 0.1～2 parts, Jiang Ding 0.2～2 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi)
0.1～1 part, anistree 0.5～1 part, Fructus Piperis 1～2 parts, Flos Caryophylli 1～3 parts, fragrant 0.5～2 part of mattress, soy sauce 1～2 parts, Herba Alii fistulosi 0.5～1
Part, monosodium glutamate 0.5～2 parts；
The preparation method of described Semen Arecae extract is as follows:
A, fresh areca nuts is sorted, clean up, broken, squeezing, it is thus achieved that clear juice and Semen Arecae residue；
B, edible ethanol is added in clear juice, stand overnight, take supernatant, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, it is thus achieved that fruit juice carries
Take liquid；
D, Semen Arecae residue add its weight 3～10 times of water and cellulase carries out biological cracking, cellulase after mixing
Final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～12000rpm, obtain
Obtain residue extracting solution；
E, juice extraction liquid merge with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids, powder
Broken, inspection, obtain Semen Arecae extract.
Another object of the present invention is to provide the preparation method of a kind of Semen Arecae dried tofu, comprise the following steps:
(1) prepared by Semen Arecae extract:
A, squeezing are extracted: sorted by fresh areca nuts, clean up, broken, carry out squeezing with physical method and obtain fruit juice, really
Juice obtains clear juice through processing；Merge Semen Arecae residue, stand-by；
B, removal tannin: edible ethanol is added in clear juice, make ethanol final concentration of 45～85% after mixing, stand
Overnight, supernatant is taken, it is thus achieved that juice solution；
C, removal part biological alkali: juice solution concentrate under reduced pressure at low temperature removes ethanol, the juice solution after concentration is by solid
Xiang Zhu, and with 1～10 times of volume of water drip washing solid column, collect all liq, it is thus achieved that juice extraction liquid；Described solid phase column built with
Arecoline molecular brand polymer as fixing phase；
D, residue extract: add its weight 3～10 times of water in Semen Arecae residue and cellulase carries out biological cracking, after mixing
Cellulase final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～
12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 30～120 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: by Semen sojae atricolor, Semen phaseoli radiati clean after, be positioned in clear water immersion 8～10 hours after pull out, add Semen sojae atricolor and
The water of Semen phaseoli radiati gross weight 5～6 times carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 2～5 minutes, stops heating；It is cooled to 50～75
DEG C time, add Gypsum Fibrosum, stand to obtain bean brain, by broken brain, upper plate, squeezing, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 70～80 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.4～0.5%, time 5～6 minutes,
Then repeatedly being cleaned by dried tofu clear water good for tenderization, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce,
Herba Alii fistulosi, monosodium glutamate mixing bittern, add dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；
Wherein, during stew in soy sauce otherwise stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) be vacuum-packed, sterilizing i.e. obtains Semen Arecae dried tofu.
Further, in described step (3), the squeezing time is 10～20 minutes；
Further, the sterilization in described step (6) refers to: the dried tofu that vacuum packet is installed is placed in pot, uniformly, entirely
After portion is well placed, sterilize 10 minutes after rising to 90 DEG C.
Further, the stripping and slicing in described step (3), including: with being manually or mechanically cut into, thickness is uniform, sheet shape is whole
Neat dried tofu.
Semen Arecae dried tofu of the present invention and preparation method thereof has a following beneficial effect:
1, the present invention uses fresh areca nuts Technology in Pressing, and whole nutrition that maximum possible is absorbed when retaining betel quid chewing become
Point；Use precipitate with ethanol mode to remove the tannin in press juice, reduce it and bring the astringent taste in follow-up food, thus improve mouthfeel；
Utilize enzyme biology cracking mode that press residue is extracted further, having in comprehensive extraction Semen Arecae crude fibre cell simultaneously
Effect nutritional labeling.
2, the present invention uses molecular imprinting technique, it is intended to remove the dangerous factor of part in Semen Arecae, is retaining Semen Arecae effect
While position and special flavor, weaken its cytotoxicity produced.
3, fresh areca nuts is rapidly transformed into Semen Arecae extract dry powder by the present invention, solves the problem that fresh fruit is difficult to preserve；Bin
Bulky extract dry powder is prepared overall process and is all carried out at low temperature, at utmost protects functional component.
4, the Semen Arecae dried tofu obtained by preparation technology of the present invention is in good taste, and with the addition of Semen Arecae in the course of processing and have
Effect composition (Semen Arecae extract), the nutrient containing multiple needed by human body and benefit materials, possessing Semen Arecae taste and characteristic
While, impart the helping digestion of Semen Arecae dried tofu of the present invention, removing food stagnancy, improve the effects such as constipation symptom.
Detailed description of the invention
Embodiment 1
Semen Arecae dried tofu of the present invention have help digestion, the effect such as removing food stagnancy；And be prepared from by the raw material of following parts by weight: Semen sojae atricolor
80kg, Semen phaseoli radiati 10kg, Semen Arecae extract 0.5kg, Gypsum Fibrosum 10kg, refined salt 1kg, Jiang Ding 2kg, Cortex cinnamomi japonici (Ramulus Cinnamomi) 0.5kg, anistree 0.5kg, recklessly
Green pepper 1kg, Flos Caryophylli 1kg, mattress perfume (or spice) 1kg, soy sauce 1kg, Herba Alii fistulosi 0.5kg, monosodium glutamate 0.5kg；
The preparation method of Semen Arecae dried tofu of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 6000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 65% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 8 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 5 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.25%, Fructus Citri Limoniae acid for adjusting pH value 4.8, supersound extraction 3h, centrifugal 6000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 60 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after Semen sojae atricolor 80kg, Semen phaseoli radiati 10kg being cleaned, pulls out after being positioned in clear water immersion 8 hours, adds 5 times
Water carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 5 minutes, stops heating；When being cooled to 50 DEG C, add
Enter Gypsum Fibrosum 10kg, stand to obtain bean brain, by broken brain, upper plate, squeezing 10 minutes, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 70 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.4%, 5 minutes time, then that tenderization is good
Dried tofu clear water repeatedly clean, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce,
Herba Alii fistulosi, monosodium glutamate mixing bittern, add dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；
Wherein, during stew in soy sauce otherwise stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) vacuum packaging, the dried tofu that vacuum packet is installed is placed in pot, uniformly, be all well placed after, rise to 90 DEG C
Rear sterilization 10 minutes, obtains Semen Arecae dried tofu.
According to the present embodiment 1 preparation Semen Arecae dried tofu, through 45 people (there is dyspepsia or constipation symptom) be not added with Semen Arecae
Common dried tofu compare edible, observe after edible six days continuously, the people's indigestion symptom eating Semen Arecae dried tofu is obviously improved,
And appetite increases；Having constipation symptom person, times of defecation to increase, constipation symptom has certain improvement.
Embodiment 2
Semen Arecae dried tofu of the present invention have help digestion, the effect such as removing food stagnancy；And be prepared from by the raw material of following parts by weight: Semen sojae atricolor
90kg, Semen phaseoli radiati 5kg, Semen Arecae extract 1kg, Gypsum Fibrosum 4kg, refined salt 1kg, Jiang Ding 2kg, Cortex cinnamomi japonici (Ramulus Cinnamomi) 0.5kg, anistree 1kg, Fructus Piperis 1kg,
Flos Caryophylli 1.5kg, mattress perfume (or spice) 0.5kg, soy sauce 1kg, Herba Alii fistulosi 1kg, monosodium glutamate 0.5kg；
The preparation method of Semen Arecae dried tofu of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 12000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 75% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 10 times of bodies
Hydrops drip washing solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is built with the arecoline as fixing phase
Molecular brand polymer；
D, residue extract: add 7 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.5%, Fructus Citri Limoniae acid for adjusting pH value 4.5, supersound extraction 6h, centrifugal 12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 100 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after Semen sojae atricolor 90kg, Semen phaseoli radiati 5kg being cleaned, pulls out after being positioned in clear water immersion 9 hours, adds 5 times
Water carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 5 minutes, stops heating；When being cooled to 60 DEG C, add
Enter Gypsum Fibrosum 4kg, stand to obtain bean brain, by broken brain, upper plate, squeezing 10 minutes, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 80 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.5%, 5 minutes time, then that tenderization is good
Dried tofu clear water repeatedly clean, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce,
Herba Alii fistulosi, monosodium glutamate mixing bittern, add dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；
Wherein, during stew in soy sauce otherwise stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) vacuum packaging, the dried tofu that vacuum packet is installed is placed in pot, uniformly, be all well placed after, rise to 90 DEG C
Rear sterilization 10 minutes, obtains Semen Arecae dried tofu.
According to the present embodiment 2 preparation Semen Arecae dried tofu, through 45 people (there is dyspepsia or constipation symptom) be not added with Semen Arecae
Common dried tofu compare edible, observe after edible six days continuously, the people's indigestion symptom eating Semen Arecae dried tofu all eliminates,
And appetite increases；Having constipation symptom person, times of defecation showed increased, constipation symptom is all improved in varying degrees.
Embodiment 3
Semen Arecae dried tofu of the present invention have help digestion, the effect such as removing food stagnancy；And be prepared from by the raw material of following parts by weight: Semen sojae atricolor
85kg, Semen phaseoli radiati 8kg, Semen Arecae extract 3kg, Gypsum Fibrosum 4kg；Refined salt 1kg, Jiang Ding 1kg, Cortex cinnamomi japonici (Ramulus Cinnamomi) 1kg, anistree 0.5kg, Fructus Piperis 1kg,
Flos Caryophylli 1kg, mattress perfume (or spice) 0.5kg, soy sauce 1kg, Herba Alii fistulosi 0.5kg, monosodium glutamate 0.5kg；
The preparation method of Semen Arecae dried tofu of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 9000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 50% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 5 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 8 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.4%, Fructus Citri Limoniae acid for adjusting pH value 4.8, supersound extraction 3h, centrifugal 6000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 60 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after Semen sojae atricolor 85kg, Semen phaseoli radiati 8kg being cleaned, pulls out after being positioned in clear water immersion 8 hours, adds 6 times
Water carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 5 minutes, stops heating；When being cooled to 75 DEG C, add
Enter Gypsum Fibrosum 4kg, stand to obtain bean brain, by broken brain, upper plate, squeezing 10 minutes, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 80 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.5%, 5 minutes time, then that tenderization is good
Dried tofu clear water repeatedly clean, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce,
Herba Alii fistulosi, monosodium glutamate mixing bittern, add dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；
Wherein, during stew in soy sauce otherwise stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) vacuum packaging, the dried tofu that vacuum packet is installed is placed in pot, uniformly, be all well placed after, rise to 90 DEG C
Rear sterilization 10 minutes, obtains Semen Arecae dried tofu.
According to the present embodiment 3 preparation Semen Arecae dried tofu, through 45 people (there is dyspepsia or constipation symptom) be not added with Semen Arecae
Common dried tofu compare edible, observe after edible six days continuously, the people's indigestion symptom eating Semen Arecae dried tofu all eliminates,
And appetite increases；Having constipation symptom person, times of defecation significantly to increase, constipation symptom all has clear improvement.
Embodiment 4
Semen Arecae dried tofu of the present invention have help digestion, the effect such as removing food stagnancy；And be prepared from by the raw material of following parts by weight: Semen sojae atricolor
95kg, Semen phaseoli radiati 7kg, Semen Arecae extract 0.8kg, Gypsum Fibrosum 6kg；Refined salt 1kg, Jiang Ding 1kg, Cortex cinnamomi japonici (Ramulus Cinnamomi) 1kg, anistree 0.5kg, Fructus Piperis
1kg, Flos Caryophylli 1kg, mattress perfume (or spice) 1kg, soy sauce 1kg, Herba Alii fistulosi 1kg, monosodium glutamate 0.5kg；
The preparation method of Semen Arecae dried tofu of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 12000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 70% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 6 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 6 times of water of Semen Arecae residue weight in Semen Arecae residue and cellulase carries out biological cracking, mixing
Rear cellulase final concentration of 0.5%, Fructus Citri Limoniae acid for adjusting pH value 4.5, supersound extraction 4h, centrifugal 12000rpm, it is thus achieved that residue carries
Take liquid；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 100 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after Semen sojae atricolor 95kg, Semen phaseoli radiati 7kg being cleaned, pulls out after being positioned in clear water immersion 10 hours, adds 6 times
Water carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 5 minutes, stops heating；When being cooled to 75 DEG C, add
Enter Gypsum Fibrosum 6kg, stand to obtain bean brain, by broken brain, upper plate, squeezing 10 minutes, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 80 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.5%, 5 minutes time, then that tenderization is good
Dried tofu clear water repeatedly clean, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce,
Herba Alii fistulosi, monosodium glutamate mixing bittern, add dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；
Wherein, during stew in soy sauce otherwise stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) vacuum packaging, the dried tofu that vacuum packet is installed is placed in pot, uniformly, be all well placed after, rise to 90 DEG C
Rear sterilization 10 minutes, obtains Semen Arecae dried tofu.
According to the present embodiment 4 preparation Semen Arecae dried tofu, through 45 people (there is dyspepsia or constipation symptom) be not added with Semen Arecae
Common dried tofu compare edible, observe after edible six days continuously, the people's indigestion symptom eating Semen Arecae dried tofu all eliminates,
And appetite increases；Having constipation symptom person, times of defecation significantly to increase, constipation symptom all has clear improvement.
Process of the test:
(1) total polyphenols in spectrophotometry Semen Arecae extract of the present invention is used:
Main agents and instrument: gallic acid (biochemical reagents, National Institute for Food and Drugs Control)；Methanol；7.5% carbon
Acid sodium solution；Forint phenol test solution；DUV 2450 type ultraviolet-uisible spectrophotometer (Japan's Shimadzu).
1) linear test is to be not added with gallic acid as blank, uses spectrophotography to measure absorbance at 765nm wavelength,
With gallic acid concentration (mg/ml) as abscissa, absorbance (A) is vertical coordinate, draws standard curve, calculates linear regression side
Journey.
2) result calculates
According to the equation of linear regression of gallic acid, calculate the polyphenol concentration C in determined need testing solution1.Semen Arecae
In extract, polyphenol is with mass fraction W1Meter, numerical value represents with %:
w1The mass fraction of weight polyphenol fraction in test sample；
C1Weight polyphenol fraction concentration in need testing solution, unit is mg/mL；
V1The dilution volume of need testing solution, unit is milliliter (mL)；
m1 -The sample weighting amount of test sample, unit is milligram (mg)；
D extension rate.
Statistical result is as shown in table 1:
In table 1 Semen Arecae extract of the present invention, Determination of Polyphenols compares with traditional extraction data
(2) total polysaccharides in spectrophotometry Semen Arecae extract of the present invention is used
Main agents and instrument: glucose (biochemical reagents, National Institute for Food and Drugs Control)；5% phenol solution；Dense
Sulfuric acid solution；DUV 2450 type ultraviolet-uisible spectrophotometer (Japan's Shimadzu).
1) linear test is to be not added with glucose as blank, uses spectrophotography to measure absorbance at 490nm wavelength, with
Concentration of glucose (mg/ml) is abscissa, and absorbance (A) is vertical coordinate, draws standard curve, calculates equation of linear regression.
2) result calculates
According to the equation of linear regression of glucose, calculate the polysaccharide concentration C in determined need testing solution2.Semen Arecae carries
Take in thing polysaccharide with mass fraction W2Meter, numerical value represents with %:
w2The mass fraction of polysaccharide component in test sample；
C2Polysaccharide component concentration in need testing solution, unit is mg/mL；
V2The dilution volume of need testing solution, unit is milliliter (mL)；
m2The sample weighting amount of test sample, unit is milligram (mg)；
D extension rate；
Statistical result is as shown in table 2:
In table 2 Semen Arecae extract of the present invention, total polysaccharides content compares with traditional extraction data
Tables 1 and 2 data show, compared with conventional Semen Arecae extract, the present invention prepares in gained Semen Arecae extract effective
Composition (polyphenol and polysaccharide) content is higher.
(3) in vitro toxicity experiment (human mouth mucosa model of keratinocytes)
Key instrument and reagent: human mouth mucosa keratinocyte (KC) serum-free medium (K-SFM), KC trains completely
Support base, DMEM culture medium, mouse-anti human keratin antibody and mouse-anti people's vimentin monoclonal antibody, SABC SABC reagent
Box, fluorescence microscope.
Experimental technique: the KC of In vitro culture is randomly divided into 3 groups: negative control group: K-SFM+KC；Conventional Semen Arecae extract
Process group (AW): AW+KC；Semen Arecae extract process group of the present invention: embodiment (1,2,3,4)+KC.
Testing index: fluorescence microscope cell number.Apoptosis percentage rate=apoptotic cell/total cell number × 100%.
Statistical result is as shown in table 3:
Four embodiments of table 3 present invention compare with traditional extraction KC apoptosis rate data
Table 3 data draw, conventional Semen Arecae extract (being cut by fresh areca nuts, ethanol extraction) has substantially induction KC apoptosis
Effect, embodiment 1,2,3,4 Semen Arecae extract (use molecular imprinting technique remove part arecoline) can substantially reduce KC
Apoptosis rate, with negative control group (without Semen Arecae intervention) without significant difference.Hence it is demonstrated that the present invention uses the molecular imprinting technique to go
Except part arecoline in fresh areca nuts, its cytotoxicity produced can be weakened so that it is reduce infringement human mouth mucosa structure wind
Danger, it is ensured that the edible safety of Semen Arecae product.
(4) high performance liquid chromatography (HPLC) method is used to measure the arecoline content in Semen Arecae extract of the present invention.
Japan's highly effective liquid phase chromatographic system (Japan's HITACHI series)；With strong cation exchange bonded silica gel as filler
(SCX-strong cation-exchanging resin post)；With acetonitrile-phosphoric acid solution (2 → 1000, strong ammonia solution regulation pH value is to 3.8) (55:
45) for flowing phase；Detection wavelength is 215nm.
Statistical result is as follows:
Embodiment 1: arecoline content 0.16%；Embodiment 2: arecoline content 0.14%；Embodiment 3: arecoline content
0.15%；Embodiment 4: arecoline content 0.13%.
The outer toxicity test result of coalition, uses the Semen Arecae extract of the present invention to prepare Semen Arecae dried tofu, and keeping, Semen Arecae is only
While special local flavor, it is possible to substantially weaken its cytotoxicity produced, while possessing Semen Arecae taste and characteristic, impart this
The helping digestion of invention Semen Arecae dried tofu, removing food stagnancy, improve the effects such as constipation symptom.
The above disclosed presently preferred embodiments of the present invention that is only, can not limit the right of the present invention with this certainly
Scope, the equivalent variations therefore made according to the claims in the present invention, still fall within the scope that the present invention is contained.
Claims (4)
1. a Semen Arecae dried tofu, it is characterised in that added stone after bean defibrination, mashing off, cooling by the raw material of following parts by weight
Cream, squeezing, stew in soy sauce final vacuum packaging, sterilization be prepared from: Semen sojae atricolor 80～95 parts, Semen phaseoli radiati 5～10 parts, Semen Arecae extract 0.01～
5 parts, Gypsum Fibrosum 3～10 parts；Refined salt 0.1～2 parts, Jiang Ding 0.2～2 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 0.1～1 part, anistree 0.5～1 part, Fructus Piperis 1～2
Part, Flos Caryophylli 1～3 parts, fragrant 0.5～2 part of mattress, soy sauce 1～2 parts, Herba Alii fistulosi 0.5～1 part, monosodium glutamate 0.5～2 parts；
The preparation method of described Semen Arecae extract is as follows:
A, fresh areca nuts is sorted, clean up, broken, squeezing, it is thus achieved that clear juice and Semen Arecae residue；
B, edible ethanol is added in clear juice, stand overnight, take supernatant, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, it is thus achieved that juice extraction liquid；
Adding its weight 3～10 times of water in d, Semen Arecae residue and cellulase carries out biological cracking, after mixing, cellulase is the denseest
Degree is 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～12000rpm, it is thus achieved that residual
Slag extracting solution；
E, juice extraction liquid merge with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids, pulverize,
Inspection, obtains Semen Arecae extract.
2. the preparation method of Semen Arecae dried tofu as claimed in claim 1, it is characterised in that comprise the following steps:
(1) prepared by Semen Arecae extract:
A, squeezing are extracted: sorted by fresh areca nuts, clean up, broken, carry out squeezing with physical method and obtain fruit juice, fruit juice warp
Cross process and obtain clear juice；Merge Semen Arecae residue, stand-by；
B, removal tannin: edible ethanol is added in clear juice, make ethanol final concentration of 45～85% after mixing, stood
At night, take supernatant, it is thus achieved that juice solution；
C, removal part biological alkali: juice solution concentrate under reduced pressure at low temperature removes ethanol, and the juice solution after concentration passes through solid phase column,
And with 1～10 times of volume of water drip washing solid column, collect all liq, it is thus achieved that juice extraction liquid；Described solid phase column is built with conduct
The arecoline molecular brand polymer of fixing phase；
D, residue extract: add its weight 3～10 times of water in Semen Arecae residue and cellulase carries out biological cracking, fine after mixing
Dimension element enzyme final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～
12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids,
Cross 30～120 mesh to pulverize, inspection, obtain Semen Arecae extract；
(2) defibrination: after Semen sojae atricolor, Semen phaseoli radiati are cleaned, pull out after being positioned in clear water immersion 8～10 hours, add Semen sojae atricolor and Semen phaseoli radiati
The water of gross weight 5～6 times carries out defibrination, filter cleaner, obtains raw soya-bean milk；
(3) prepared by dried tofu: raw soya-bean milk big fire boiled, and after keeping boiling 2～5 minutes, stops heating；It is cooled to 50～75 DEG C
Time, add Gypsum Fibrosum, stand to obtain bean brain, by broken brain, upper plate, squeezing, stripping and slicing, dry, it is thus achieved that dried tofu；
(4) tenderization: with 70～80 DEG C, concentration is the sodium carbonate liquor tenderization dried tofu of 0.4～0.5%, time 5～6 minutes, then
Repeatedly being cleaned by dried tofu clear water good for tenderization, the aqueous alkali staying dried tofu surface is the most clean, and dewatering is standby；
(5) stew in soy sauce: by proportioning by Semen Arecae extract, refined salt, Jiang Ding, Cortex cinnamomi japonici (Ramulus Cinnamomi), anise, Fructus Piperis, Flos Caryophylli, mattress perfume, soy sauce, Herba Alii fistulosi, taste
Essence mixing bittern, adds dried tofu after the salt twice-cooked stir-frying made being boiled, big fire changes boiling with soft fire 30 minutes after boiling 40 minutes；Wherein,
During stew in soy sauce however stop stirring, make dried tofu stew in soy sauce uniform, pull cooling out；
(6) be vacuum-packed, sterilizing i.e. obtains Semen Arecae dried tofu.
3. the preparation method of Semen Arecae dried tofu as claimed in claim 2, it is characterised in that: in described step (3), the squeezing time is
10～20 minutes.
4. the preparation method of Semen Arecae dried tofu as claimed in claim 2, it is characterised in that: the sterilization in described step (6) refers to:
The dried tofu that vacuum packet is installed is placed in pot, uniformly, be all well placed after, after rising to 90 DEG C sterilize 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610866680.4A CN106234632A (en) | 2016-09-30 | 2016-09-30 | A kind of Semen Arecae dried tofu and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610866680.4A CN106234632A (en) | 2016-09-30 | 2016-09-30 | A kind of Semen Arecae dried tofu and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106234632A true CN106234632A (en) | 2016-12-21 |
Family
ID=57612170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610866680.4A Pending CN106234632A (en) | 2016-09-30 | 2016-09-30 | A kind of Semen Arecae dried tofu and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106234632A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106805164A (en) * | 2017-02-07 | 2017-06-09 | 海口椰语堂餐饮文化有限公司 | A kind of preparation method of old salt cumquat lemon powder |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103444889A (en) * | 2013-07-29 | 2013-12-18 | 马鞍山市黄池食品（集团）有限公司 | Spicy dried deep-fried bean curd and preparation method thereof |
| CN104472720A (en) * | 2014-12-10 | 2015-04-01 | 马鞍山市采石矶食品有限公司 | Dried bean curd for invigorating stomach, promoting digestion and preserving health and processing method thereof |
| CN105831266A (en) * | 2016-03-24 | 2016-08-10 | 镇远乐豆坊食品有限公司 | Spicy-and-hot dried bean curd and preparation method thereof |
-
2016
- 2016-09-30 CN CN201610866680.4A patent/CN106234632A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103444889A (en) * | 2013-07-29 | 2013-12-18 | 马鞍山市黄池食品（集团）有限公司 | Spicy dried deep-fried bean curd and preparation method thereof |
| CN104472720A (en) * | 2014-12-10 | 2015-04-01 | 马鞍山市采石矶食品有限公司 | Dried bean curd for invigorating stomach, promoting digestion and preserving health and processing method thereof |
| CN105831266A (en) * | 2016-03-24 | 2016-08-10 | 镇远乐豆坊食品有限公司 | Spicy-and-hot dried bean curd and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106805164A (en) * | 2017-02-07 | 2017-06-09 | 海口椰语堂餐饮文化有限公司 | A kind of preparation method of old salt cumquat lemon powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102987196A (en) | Blood-fat-reducing thick honey juice and preparation method thereof | |
| CN104041644A (en) | Bowel relaxing tea and preparation method thereof | |
| CN101449844B (en) | Polygonatum odoratum juice | |
| CN103504044A (en) | Formula and production method for dark plum refreshing and palate-cleansing tea | |
| CN110179080A (en) | Dragon fruit jujube compound nectar and preparation method thereof | |
| CN107115460A (en) | David's-harp compound granules and preparation method thereof | |
| CN105145992A (en) | Blood-pressure-reducing antipyretic health beverage and making method thereof | |
| CN105831262A (en) | Antitumor red bean curd | |
| CN104273265A (en) | Tonic and healthy ginseng herbal tea beverage and preparation method thereof | |
| CN106234632A (en) | A kind of Semen Arecae dried tofu and preparation method thereof | |
| CN105533737B (en) | A kind of black garlic oral solution and its preparation method and application containing Folium Artemisiae Argyi extract | |
| CN109329428A (en) | A kind of jasmine flower green tea milk tea and preparation method thereof | |
| CN103960401B (en) | A kind of Chinese olive green tea instant drinks and its preparation method | |
| CN106616126A (en) | Functional radix glehniae drink and preparation method thereof | |
| CN100393241C (en) | Health-care products containing American ginseng and red ginseng and their preparation | |
| CN106635726A (en) | Healthcare fruit vinegar and preparation method thereof | |
| CN106615363A (en) | Slimming health-care tea and preparation method thereof | |
| CN106260011A (en) | A kind of Semen Arecae dried bean curd and preparation method thereof | |
| CN109043028A (en) | The instant tea and preparation method thereof of U.S. rattan fruit shell | |
| CN109287916A (en) | A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage | |
| CN103749763A (en) | Qi-invigorating and yin-nourishing herbal tea and preparation method thereof | |
| CN106722016A (en) | A kind of person in middle and old age's instant type health care polished glutinous rice powder and preparation method thereof | |
| KR20030059432A (en) | A red ginseng sipjeondaebo bean jelly and the preparing method thereof | |
| CN107183450A (en) | A kind of preparation method of persimmon leaf health care beverage | |
| CN106234671A (en) | Maize health preserving Tea containing traditional Chinese medicine beverage and preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161221 |