CN106260011A - A kind of Semen Arecae dried bean curd and preparation method thereof - Google Patents
A kind of Semen Arecae dried bean curd and preparation method thereof Download PDFInfo
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- CN106260011A CN106260011A CN201610860960.4A CN201610860960A CN106260011A CN 106260011 A CN106260011 A CN 106260011A CN 201610860960 A CN201610860960 A CN 201610860960A CN 106260011 A CN106260011 A CN 106260011A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
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Abstract
The invention discloses a kind of Semen Arecae dried bean curd, by the raw material of following parts by weight through defibrination, mashing off, order halogen, squeeze, pickle, be vacuum-packed after sterilize and make: Semen sojae atricolor 80～95 parts, Semen Arecae extract 0.01～5 parts, salt 8～10 parts, Bulbus Allii 1～3 parts, Rhizoma Zingiberis Recens 1～5 parts, Sal 1～3 parts, Fericarpium Citri Limoniae 1～2 parts, defatted milk powder 3～7 parts, tangerine peel powder 0.1～0.7 part, Fructus Foeniculi 0.5～1 part, pepper powder 0.1～0.5 part, star aniseed powder 0.1～0.6 part, Cortex cinnamomi japonici powder 0.5～0.7 part；The Semen Arecae dried bean curd obtained by preparation technology of the present invention is in good taste, and in the course of processing, with the addition of Semen Arecae effective ingredient, nutrient containing multiple needed by human body and benefit materials, while possessing Semen Arecae taste and characteristic, impart the helping digestion of Semen Arecae dried bean curd of the present invention, removing food stagnancy, improve the effects such as constipation symptom.
Description
Technical field
The present invention relates to the technical field of food processing, be specifically related to Semen Arecae dried bean curd and preparation method thereof.
Background technology
Fresh Semen Arecae (Areca catechu L) is the mature fruit of Palmae Betel nuts plant Semen Arecae.The whole world is about at present
There are 700,000,000 people's edible areca-nuts.Semen Arecae is liked by consumers in general equally deeply in China, is described as " the green arrow chewing gum of China ".
Semen Arecae also has abundant medical value, occupies (Semen Arecae, Fructus Alpiniae Oxyphyllae, Fructus Amomi, Ba Ji first of China's " four great Nan medicines "
My god), bitter in the mouth, pungent, warm, return stomach, large intestine channel.Nutrient containing multiple needed by human body and benefit materials, also contain many simultaneously
Planting pharmacological component, have the effects such as parasite killing, removing food stagnancy, diuretic, dehumidifying, preventing the attack (or recurrence) of malaria, " Chinese Pharmacopoeia " is gone through version and is all recorded, 2015 years
Version Semen Arecae one-tenth side kind has 55." side's arteries and veins is authentic " record Semen Arecae full vexed one-tenth sputum vomiter for the treatment of food stagnation: Semen Arecae, the Rhizoma Pinelliae, sand
Core, Semen Raphani, Fructus Hordei Germinatus, Rhizoma Zingiberis, each two money of the Rhizoma Atractylodis Macrocephalae, be decocted in water for oral dose." Prescriptions for Universal Relief " Semen Arecae dissipates and " detailed outline " is recorded Semen Arecae and controlled defecation not
Logical, also controlling the intestines and stomach has wet, and big constipation is puckery: Semen Arecae is to big person half piece.Decoct water mill one money with Radix Ophiopogonis, weight soup scald decoction being taken hot it.
Containing indispensable in the human life activities such as rich in protein, fat, vitamin and mineral in Semen sojae atricolor
Nutrition, compares with other food, and protein content is high, and the collocation of other nutrition the most relatively equalizes.Therefore, often eat
Bean product, it is possible to decrease the diseases such as cholesterolemia and prophylaxis of hypertension, arteriosclerosis and cardiovascular.Dried bean curd is adding again of bean curd
Work goods, nutritious, containing substantial amounts of protein, fat, carbohydrate, possibly together with multiple needed by human body such as calcium, phosphorus, ferrum
Mineral, the lecithin contained in dried bean curd can remove the cholesterol being attached in blood vessel wall, prevents sclerosis of blood vessels, prevents the heart
Angiopathy, cardioprotection.
At present, there is not yet the relevant report of the dried bean curd of Semen Arecae composition and taste.
Summary of the invention
It is an object of the invention to provide a kind of interpolation Semen Arecae composition in the dried bean curd course of processing so that it is Semen Arecae dried bean curd
Reach aid digestion, be conducive to improving effect of constipation symptom.
To achieve these goals, the technical scheme is that a kind of Semen Arecae dried bean curd of offer, by following parts by weight
Raw material through defibrination, mashing off, order halogen, squeeze, pickle, be vacuum-packed after sterilize and be prepared from: Semen sojae atricolor 80～95 parts, Semen Arecae extract
Thing 0.01～5 parts, salt 8～10 parts, Bulbus Allii 1～3 parts, Rhizoma Zingiberis Recens 1～5 parts, Sal 1～3 parts, Fericarpium Citri Limoniae 1～2 parts, defatted milk powder 3
～7 parts, tangerine peel powder 0.1～0.7 part, Fructus Foeniculi 0.5～1 part, pepper powder 0.1～0.5 part, star aniseed powder 0.1～0.6 part, Cortex cinnamomi japonici (Ramulus Cinnamomi)
Powder 0.5～0.7 part；
The preparation method of described Semen Arecae extract is as follows:
A, fresh areca nuts is sorted, clean up, broken, squeezing, it is thus achieved that clear juice and Semen Arecae residue；
B, edible ethanol is added in clear juice, stand overnight, take supernatant, it is thus achieved that juice solution；
C, juice solution use concentrate under reduced pressure at low temperature to remove ethanol, and the juice solution after concentration passes through solid phase column, it is thus achieved that really
Juice extracting solution；
D, Semen Arecae residue add its weight 3～10 times of water and cellulase carries out biological cracking, cellulase after mixing
Final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～12000rpm, obtain
Obtain residue extracting solution；
E, juice extraction liquid merge with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids, powder
Broken, inspection, obtain Semen Arecae extract.
Another object of the present invention is to provide the preparation method of Semen Arecae dried bean curd, comprises the following steps:
(1) prepared by Semen Arecae extract:
A, squeezing are extracted: sorted by fresh areca nuts, clean up, broken, carry out squeezing with physical method and obtain fruit juice, really
Juice obtains clear juice through processing；Merge Semen Arecae residue, stand-by；
B, removal tannin: edible ethanol is added in clear juice, make ethanol final concentration of 45～85% after mixing, stand
Overnight, supernatant is taken, it is thus achieved that juice solution；
C, removal part biological alkali: juice solution uses concentrate under reduced pressure at low temperature to remove ethanol, and the juice solution after concentration leads to
Cross solid phase column, and with 1～10 times of volume of water drip washing solid column, collect all liq, it is thus achieved that juice extraction liquid；In described solid phase column
Equipped with the arecoline molecular brand polymer as fixing phase；
D, residue extract: add its weight 3～10 times of water in Semen Arecae residue and cellulase carries out biological cracking, after mixing
Cellulase final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～
12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 30～120 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor, pulls out after being positioned in clear water immersion 8～10 hours, adds Semen sojae atricolor weight 5～6 times
Water carry out defibrination, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 50～75 DEG C, add salt and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: by Semen Arecae extract, Bulbus Allii, Rhizoma Zingiberis Recens, Sal, Fericarpium Citri Limoniae, defatted milk powder, tangerine peel powder, Fructus Foeniculi, Pericarpium Zanthoxyli
After face, star aniseed powder, Cortex cinnamomi japonici powder mix homogeneously, it is coated uniformly on fritter bean curd surface, pickles 1～3 hour；
(7) be vacuum-packed, sterilizing i.e. obtains Semen Arecae dried bean curd.
Further, the sterilization of described step (7) refers to, the dried bean curd that vacuum packet is installed is placed in pot, uniformly, entirely
After portion is well placed, sterilize 10 minutes after rising to 90 DEG C.
Semen Arecae dried bean curd of the present invention and preparation method thereof has a following beneficial effect:
1, the present invention uses fresh areca nuts Technology in Pressing, and whole nutrition that maximum possible is absorbed when retaining betel quid chewing become
Point；Use precipitate with ethanol mode to remove the tannin in press juice, reduce it and bring the astringent taste in follow-up food, thus improve mouthfeel；
Utilize enzyme biology cracking mode that press residue is extracted further, having in comprehensive extraction Semen Arecae crude fibre cell simultaneously
Effect nutritional labeling.
2, the present invention uses molecular imprinting technique, it is intended to remove the dangerous factor of part in Semen Arecae, is retaining Semen Arecae effect
While position and special flavor, weaken its cytotoxicity produced.
3, fresh areca nuts is rapidly transformed into Semen Arecae extract dry powder by the present invention, solves the problem that fresh fruit is difficult to preserve；Bin
Bulky extract dry powder is prepared overall process and is all carried out at low temperature, at utmost protects functional component.
4, the Semen Arecae dried bean curd obtained by preparation technology of the present invention is in good taste, and with the addition of Semen Arecae in the course of processing
Effective ingredient (Semen Arecae extract), the nutrient containing multiple needed by human body and benefit materials, possessing Semen Arecae taste and spy
While color, impart the helping digestion of Semen Arecae dried bean curd of the present invention, removing food stagnancy, improve the effects such as constipation symptom.
Detailed description of the invention
Embodiment 1
Semen Arecae dried bean curd of the present invention have help digestion, the effect such as removing food stagnancy, and be prepared from by the raw material of following parts by weight: big
Bean 80kg, Semen Arecae extract 0.1kg, salt 9kg, Bulbus Allii 1kg, Rhizoma Zingiberis Recens 2kg, Sal 1kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 4kg, old
Corium farinosum 0.2kg, Fructus Foeniculi 0.5kg, pepper powder 0.3kg, star aniseed powder 0.2kg, Cortex cinnamomi japonici powder 0.5kg；
The preparation method of Semen Arecae dried bean curd of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 6000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 65% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 8 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 5 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.25%, Fructus Citri Limoniae acid for adjusting pH value 4.8, supersound extraction 3h, centrifugal 6000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 60 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor 80kg, pulls out after being positioned in clear water immersion 8 hours, and the water adding 5 times grinds
Slurry, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 50 DEG C, add salt 9kg and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: the fritter bean curd of preparation in step (5) is placed in case, by Semen Arecae extract 0.1kg, Bulbus Allii 1kg,
Rhizoma Zingiberis Recens 2kg, Sal 1kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 4kg, tangerine peel powder 0.2kg, Fructus Foeniculi 0.5kg, pepper powder 0.3kg, anistree
Powder 0.2kg, after Cortex cinnamomi japonici powder 0.5kg mix homogeneously, is coated uniformly on fritter bean curd surface, pickles 2 hours.
(7) be vacuum-packed, sterilizing i.e. obtains described a kind of Semen Arecae dried bean curd.
The sterilization of described step (7) refers to, the dried bean curd that vacuum packet is installed is placed in pot, uniformly, is all well placed
After, sterilize 10 minutes after rising to 90 DEG C.
According to the present embodiment 1 preparation Semen Arecae dried bean curd, through 45 people (there is dyspepsia or constipation symptom) be not added with Bin
Bulky common beancurd is dry to be compared edible, observes after the most edible six days, and the people's indigestion symptom eating Semen Arecae dried bean curd has
Improved, and appetite is increased；Having constipation symptom person, times of defecation to increase, constipation symptom makes moderate progress.
Embodiment 2
Semen Arecae dried bean curd of the present invention have help digestion, the effect such as removing food stagnancy, and be prepared from by the raw material of following parts by weight: big
Bean 90kg, Semen Arecae extract 1kg, salt 10kg, Bulbus Allii 2kg, Rhizoma Zingiberis Recens 3kg, Sal 2kg, Fericarpium Citri Limoniae 2kg, defatted milk powder 5kg, old
Corium farinosum 0.3kg, Fructus Foeniculi 0.6kg, pepper powder 0.2kg, star aniseed powder 0.4kg, Cortex cinnamomi japonici powder 0.6kg；
The preparation method of Semen Arecae dried bean curd of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 8000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 75% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 10 times of bodies
Hydrops drip washing solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is built with the arecoline as fixing phase
Molecular brand polymer；
D, residue extract: add 7 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.5%, Fructus Citri Limoniae acid for adjusting pH value 4.5, supersound extraction 6h, centrifugal 12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 100 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor 90kg, pulls out after being positioned in clear water immersion 10 hours, and the water adding 6 times grinds
Slurry, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 60 DEG C, add salt 10kg and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: the fritter bean curd of preparation in step (5) is placed in case, by Semen Arecae extract 1kg, Bulbus Allii 2kg, Rhizoma Zingiberis Recens
3kg, Sal 2kg, Fericarpium Citri Limoniae 2kg, defatted milk powder 5kg, tangerine peel powder 0.3kg, Fructus Foeniculi 0.6kg, pepper powder 0.2kg, star aniseed powder
0.4kg, after Cortex cinnamomi japonici powder 0.6kg mix homogeneously, is coated uniformly on fritter bean curd surface, pickles 2 hours.
(7) be vacuum-packed, sterilizing i.e. obtains described a kind of Semen Arecae dried bean curd.
The sterilization of described step (7) refers to, the dried bean curd that vacuum packet is installed is placed in pot, uniformly, is all well placed
After, sterilize 10 minutes after rising to 90 DEG C.
According to the present embodiment 2 preparation Semen Arecae dried bean curd, through 45 people (there is dyspepsia or constipation symptom) be not added with Bin
Bulky common beancurd is dry to be compared edible, observes after the most edible six days, and the people's indigestion symptom eating Semen Arecae dried bean curd is complete
Portion eliminates, and appetite increases；Having constipation symptom person, times of defecation showed increased, constipation symptom is all improved in varying degrees.
Embodiment 3
Semen Arecae dried bean curd of the present invention have help digestion, the effect such as removing food stagnancy, and be prepared from by the raw material of following parts by weight: big
Bean 95kg, Semen Arecae extract 3kg, salt 8kg, Bulbus Allii 3kg, Rhizoma Zingiberis Recens 5kg, Sal 3kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 6kg, Pericarpium Citri Reticulatae
Powder 0.4kg, Fructus Foeniculi 0.8kg, pepper powder 0.4kg, star aniseed powder 0.5kg, Cortex cinnamomi japonici powder 0.7kg；
The preparation method of Semen Arecae dried bean curd of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, take fresh areca nuts 100kg, sorting, clean up, broken, squeezing, pressed liquor is centrifuged 9000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 50% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 5 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 8 times of water of its weight in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.4%, Fructus Citri Limoniae acid for adjusting pH value 4.8, supersound extraction 3h, centrifugal 6000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 60 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor 95kg, pulls out after being positioned in clear water immersion 10 hours, and the water adding 6 times grinds
Slurry, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 70 DEG C, add salt 8kg and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: the fritter bean curd of preparation in step (5) is placed in case, by Semen Arecae extract 3kg, Bulbus Allii 3kg, Rhizoma Zingiberis Recens
5kg, Sal 3kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 6kg, tangerine peel powder 0.4kg, Fructus Foeniculi 0.8kg, pepper powder 0.4kg, star aniseed powder
0.5kg, after Cortex cinnamomi japonici powder 0.7kg mix homogeneously, is coated uniformly on fritter bean curd surface, pickles 3 hours.
(7) be vacuum-packed, sterilizing i.e. obtains described a kind of Semen Arecae dried bean curd.
The sterilization of described step (7) refers to, the dried bean curd that vacuum packet is installed is placed in pot, uniformly, is all well placed
After, sterilize 10 minutes after rising to 90 DEG C.
According to the present embodiment 3 preparation Semen Arecae dried bean curd, through 45 people (there is dyspepsia or constipation symptom) be not added with Bin
Bulky common beancurd is dry to be compared edible, observes after the most edible six days, and the people's indigestion symptom eating Semen Arecae dried bean curd is complete
Portion eliminates, and appetite increases；Having constipation symptom person, times of defecation significantly to increase, constipation symptom all has clear improvement.
Embodiment 4
Semen Arecae dried bean curd of the present invention have help digestion, the effect such as removing food stagnancy, and be prepared from by the raw material of following parts by weight: big
Bean 85kg, Semen Arecae extract 5kg, salt 8kg, Bulbus Allii 1kg, Rhizoma Zingiberis Recens 1kg, Sal 1kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 3kg, Pericarpium Citri Reticulatae
Powder 0.3kg, Fructus Foeniculi 0.6kg, pepper powder 0.3kg, star aniseed powder 0.6kg, Cortex cinnamomi japonici powder 0.7kg；
The preparation method of Semen Arecae dried bean curd of the present invention comprises the following steps:
(1) prepared by Semen Arecae extract:
A, taking fresh areca nuts 100kg sorting, clean up, broken, squeezing, pressed liquor is centrifuged 12000rpm, it is thus achieved that clarification
Fruit juice, merges Semen Arecae residue, stand-by；
B, edible ethanol is added in clear juice, make ethanol final concentration of 70% after mixing, stand overnight, take supernatant
Liquid, it is thus achieved that juice solution；
C, juice solution concentrate under reduced pressure at low temperature remove ethanol, and the juice solution after concentration passes through solid phase column, and with 6 times of volumes
Water wash solid column, collects all liq, it is thus achieved that juice extraction liquid；Described solid phase column is divided built with the arecoline as fixing phase
Sub-brand polymer；
D, residue extract: add 6 times of water of Semen Arecae residue weight in Semen Arecae residue and cellulase carries out biological cracking, mixing
Rear cellulase final concentration of 0.5%, Fructus Citri Limoniae acid for adjusting pH value 4.5, supersound extraction 4h, centrifugal 12000rpm, it is thus achieved that residue carries
Take liquid；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solid
Thing, crosses 100 mesh and pulverizes, and inspection obtains Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor 85kg, pulls out after being positioned in clear water immersion 10 hours, and the water adding 6 times grinds
Slurry, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 75 DEG C, add salt 8kg and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: the fritter bean curd of preparation in step (5) is placed in case, by Semen Arecae extract 5kg, Bulbus Allii 1kg, Rhizoma Zingiberis Recens
1kg, Sal 1kg, Fericarpium Citri Limoniae 1kg, defatted milk powder 3kg, tangerine peel powder 0.3kg, Fructus Foeniculi 0.6kg, pepper powder 0.3kg, star aniseed powder
0.6kg, after Cortex cinnamomi japonici powder 0.7kg mix homogeneously, is coated uniformly on fritter bean curd surface, pickles 3 hours.
(7) be vacuum-packed, sterilizing i.e. obtains described a kind of Semen Arecae dried bean curd.
The sterilization of described step (7) refers to, the dried bean curd that vacuum packet is installed is placed in pot, uniformly, is all well placed
After, sterilize 10 minutes after rising to 90 DEG C.
According to the present embodiment 4 preparation Semen Arecae dried bean curd, through 45 people (there is dyspepsia or constipation symptom) be not added with Bin
Bulky common beancurd is dry to be compared edible, observes after the most edible six days, and the people's indigestion symptom eating Semen Arecae dried bean curd is complete
Portion eliminates, and appetite increases；Having constipation symptom person, times of defecation significantly to increase, constipation symptom all has clear improvement.
Process of the test:
(1) total polyphenols in spectrophotometry Semen Arecae extract of the present invention is used:
Main agents and instrument: gallic acid (biochemical reagents, National Institute for Food and Drugs Control)；Methanol；7.5% carbon
Acid sodium solution；Forint phenol test solution；DUV 2450 type ultraviolet-uisible spectrophotometer (Japan's Shimadzu).
1) linear test is to be not added with gallic acid as blank, uses spectrophotography to measure absorbance at 765nm wavelength,
With gallic acid concentration (mg/ml) as abscissa, absorbance (A) is vertical coordinate, draws standard curve, calculates linear regression side
Journey.
2) result calculates
According to the equation of linear regression of gallic acid, calculate the polyphenol concentration C in determined need testing solution1.Semen Arecae
In extract, polyphenol is with mass fraction W1Meter, numerical value represents with %:
w1The mass fraction of weight polyphenol fraction in test sample；
C1Weight polyphenol fraction concentration in need testing solution, unit is mg/mL；
V1The dilution volume of need testing solution, unit is milliliter (mL)；
m1 -The sample weighting amount of test sample, unit is milligram (mg)；
D extension rate.
Statistical result is as shown in table 1:
In table 1 Semen Arecae extract of the present invention, Determination of Polyphenols compares with traditional extraction data
(2) total polysaccharides in spectrophotometry Semen Arecae extract of the present invention is used
Main agents and instrument: glucose (biochemical reagents, National Institute for Food and Drugs Control)；5% phenol solution；Dense
Sulfuric acid solution；DUV 2450 type ultraviolet-uisible spectrophotometer (Japan's Shimadzu).
1) linear test is to be not added with glucose as blank, uses spectrophotography to measure absorbance at 490nm wavelength, with
Concentration of glucose (mg/ml) is abscissa, and absorbance (A) is vertical coordinate, draws standard curve, calculates equation of linear regression.
2) result calculates
According to the equation of linear regression of glucose, calculate the polysaccharide concentration C in determined need testing solution2.Semen Arecae carries
Take in thing polysaccharide with mass fraction W2Meter, numerical value represents with %:
w2The mass fraction of polysaccharide component in test sample；
C2Polysaccharide component concentration in need testing solution, unit is mg/mL；
V2The dilution volume of need testing solution, unit is milliliter (mL)；
m2The sample weighting amount of test sample, unit is milligram (mg)；
D extension rate；
Statistical result is as shown in table 2:
In table 2 Semen Arecae extract of the present invention, total polysaccharides content compares with traditional extraction data
Tables 1 and 2 data show, compared with conventional Semen Arecae extract, the present invention prepares in gained Semen Arecae extract effective
Composition (polyphenol and polysaccharide) content is higher.
(3) in vitro toxicity experiment (human mouth mucosa model of keratinocytes)
Key instrument and reagent: human mouth mucosa keratinocyte (KC) serum-free medium (K-SFM), KC trains completely
Support base, DMEM culture medium, mouse-anti human keratin antibody and mouse-anti people's vimentin monoclonal antibody, SABC SABC reagent
Box, fluorescence microscope.
Experimental technique: the KC of In vitro culture is randomly divided into 3 groups: negative control group: K-SFM+KC；Conventional Semen Arecae extract
Process group (AW): AW+KC；Semen Arecae extract process group of the present invention: embodiment (1,2,3,4)+KC.
Testing index: fluorescence microscope cell number.Apoptosis percentage rate=apoptotic cell/total cell number × 100%.
Statistical result is as shown in table 3:
Four embodiments of table 3 present invention compare with traditional extraction KC apoptosis rate data
Table 3 data draw, conventional Semen Arecae extract (being cut by fresh areca nuts, ethanol extraction) has substantially induction KC apoptosis
Effect, embodiment 1,2,3,4 Semen Arecae extract (use molecular imprinting technique remove part arecoline) can substantially reduce KC
Apoptosis rate, with negative control group (without Semen Arecae intervention) without significant difference.Hence it is demonstrated that the present invention uses the molecular imprinting technique to go
Except part arecoline in fresh areca nuts, its cytotoxicity produced can be weakened so that it is reduce infringement human mouth mucosa structure wind
Danger, it is ensured that the edible safety of Semen Arecae product.
(4) high performance liquid chromatography (HPLC) method is used to measure the arecoline content in Semen Arecae extract of the present invention.
Japan's highly effective liquid phase chromatographic system (Japan's HITACHI series)；With strong cation exchange bonded silica gel as filler
(SCX-strong cation-exchanging resin post)；With acetonitrile-phosphoric acid solution (2 → 1000, strong ammonia solution regulation pH value is to 3.8) (55:
45) for flowing phase；Detection wavelength is 215nm.
Statistical result is as follows:
Embodiment 1: arecoline content 0.16%；Embodiment 2: arecoline content 0.14%；Embodiment 3: arecoline content
0.15%；Embodiment 4: arecoline content 0.13%.
The outer toxicity test result of coalition, uses Semen Arecae extract of the present invention to prepare Semen Arecae dried bean curd, and keeping, Semen Arecae is only
While special local flavor, it is possible to substantially weaken its cytotoxicity produced, while possessing Semen Arecae taste and characteristic, impart this
The helping digestion of invention Semen Arecae dried bean curd, removing food stagnancy, improve the effects such as constipation symptom.
The above disclosed presently preferred embodiments of the present invention that is only, can not limit the right of the present invention with this certainly
Scope, the equivalent variations therefore made according to the claims in the present invention, still fall within the scope that the present invention is contained.
Claims (3)
1. a Semen Arecae dried bean curd, it is characterised in that: by the raw material of following parts by weight through defibrination, mashing off, order halogen, squeeze, salt down
Sterilize after system, vacuum packaging and be prepared from: Semen sojae atricolor 80～95 parts, Semen Arecae extract 0.01～5 parts, salt 8～10 parts, Bulbus Allii 1
～3 parts, Rhizoma Zingiberis Recens 1～5 parts, Sal 1～3 parts, Fericarpium Citri Limoniae 1～2 parts, defatted milk powder 3～7 parts, tangerine peel powder 0.1～0.7 part, Fructus Foeniculi
0.5～1 part, pepper powder 0.1～0.5 part, star aniseed powder 0.1～0.6 part, Cortex cinnamomi japonici powder 0.5～0.7 part；
The preparation method of described Semen Arecae extract is as follows:
A, fresh areca nuts is sorted, clean up, broken, squeezing, it is thus achieved that clear juice and Semen Arecae residue；
B, edible ethanol is added in clear juice, stand overnight, take supernatant, it is thus achieved that juice solution；
C, juice solution use concentrate under reduced pressure at low temperature to remove ethanol, and the juice solution after concentration passes through solid phase column, it is thus achieved that fruit juice carries
Take liquid；
Adding its weight 3～10 times of water in d, Semen Arecae residue and cellulase carries out biological cracking, after mixing, cellulase is the denseest
Degree is 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～12000rpm, it is thus achieved that residual
Slag extracting solution；
E, juice extraction liquid merge with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids, pulverize, inspection,
Obtain Semen Arecae extract.
2. the preparation method of Semen Arecae dried bean curd as claimed in claim 1, it is characterised in that comprise the following steps:
(1) prepared by Semen Arecae extract:
A, squeezing are extracted: sorted by fresh areca nuts, clean up, broken, carry out squeezing with physical method and obtain fruit juice, fruit juice warp
Cross process and obtain clear juice；Merge Semen Arecae residue, stand-by；
B, removal tannin: edible ethanol is added in clear juice, make ethanol final concentration of 45～85% after mixing, stood
At night, take supernatant, it is thus achieved that juice solution；
C, removal part biological alkali: juice solution uses concentrate under reduced pressure at low temperature to remove ethanol, the juice solution after concentration is by solid
Xiang Zhu, and with 1～10 times of volume of water drip washing solid column, collect all liq, it is thus achieved that juice extraction liquid；Described solid phase column built with
Arecoline molecular brand polymer as fixing phase；
D, residue extract: add its weight 3～10 times of water in Semen Arecae residue and cellulase carries out biological cracking, fiber after mixing
Element enzyme final concentration of 0.01%～0.8%, Fructus Citri Limoniae acid for adjusting pH value 3～6, supersound extraction 1～6h, centrifugal 6000～
12000rpm, it is thus achieved that residue extracting solution；
E, dehydration: juice extraction liquid merges with residue extracting solution, use concentrate under reduced pressure at low temperature to be dehydrated, obtain solids,
Cross 30～120 mesh to pulverize, inspection, obtain Semen Arecae extract；
(2) defibrination: after being cleaned by Semen sojae atricolor, pulls out after being positioned in clear water immersion 8～10 hours, adds Semen sojae atricolor weight 5～the water of 6 times
Carry out defibrination, filter cleaner, obtain raw soya-bean milk；
(3) mashing off: after raw soya-bean milk big fire is boiled 10 minutes, stops heating；
(4) order halogen: when step (3) is cooled to 50～75 DEG C, add salt and carry out putting into bulk；
(5) squeezing: use bean curd press to be pressed into fritter bean curd of uniform size to ordering the goods after halogen；
(6) pickle: by Semen Arecae extract, Bulbus Allii, Rhizoma Zingiberis Recens, Sal, Fericarpium Citri Limoniae, defatted milk powder, tangerine peel powder, Fructus Foeniculi, pepper powder, eight
After angle powder, Cortex cinnamomi japonici powder mix homogeneously, it is coated uniformly on fritter bean curd surface, pickles 1～3 hour；
(7) be vacuum-packed, sterilizing i.e. obtains Semen Arecae dried bean curd.
3. the preparation method of Semen Arecae dried bean curd as claimed in claim 2, it is characterised in that the sterilization of described step (7) refers to,
The dried bean curd that vacuum packet is installed is placed in pot, uniformly, be all well placed after, after rising to 90 DEG C sterilize 10 minutes.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104026248A (en) * | 2014-06-20 | 2014-09-10 | 南京海鲸食品厂 | Flavored dried bean curd and preparing process thereof |
| CN104026249A (en) * | 2014-06-20 | 2014-09-10 | 南京海鲸食品厂 | Fumigated dried bean curd and processing technology thereof |
| CN104472720A (en) * | 2014-12-10 | 2015-04-01 | 马鞍山市采石矶食品有限公司 | Dried bean curd for invigorating stomach, promoting digestion and preserving health and processing method thereof |
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2016
- 2016-09-30 CN CN201610860960.4A patent/CN106260011A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104026248A (en) * | 2014-06-20 | 2014-09-10 | 南京海鲸食品厂 | Flavored dried bean curd and preparing process thereof |
| CN104026249A (en) * | 2014-06-20 | 2014-09-10 | 南京海鲸食品厂 | Fumigated dried bean curd and processing technology thereof |
| CN104472720A (en) * | 2014-12-10 | 2015-04-01 | 马鞍山市采石矶食品有限公司 | Dried bean curd for invigorating stomach, promoting digestion and preserving health and processing method thereof |
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Application publication date: 20170104 |