CN106223071B - 一种棉/麻混纺织物的节水染色工艺 - Google Patents

一种棉/麻混纺织物的节水染色工艺 Download PDF

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CN106223071B
CN106223071B CN201610606260.2A CN201610606260A CN106223071B CN 106223071 B CN106223071 B CN 106223071B CN 201610606260 A CN201610606260 A CN 201610606260A CN 106223071 B CN106223071 B CN 106223071B
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柳伯强
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Abstract

一种棉/麻混纺织物的节水染色工艺,将染色预处理、染色和软化皂洗放在同一液体中进行,用水量约为常规方法的30%,节水效果非常好;在预处理残液中加入盐酸并共煮,清除残液中的过氧化氢,消除其对后续染色的影响;通过配制专用的染液达到良好的染色效果,其中加入微量花生油不但可以增强染液与棉织物的染色效果,而且也利于后续的皂洗环节对颜色的固定;本发明的节水染色工艺,染色效果好,棉和麻的染色均匀性好,棉织物具有非常好的色牢度,尤其是浅色,效果更佳。

Description

一种棉/麻混纺织物的节水染色工艺
技术领域
本发明涉及纺织印染技术领域,尤其涉及一种棉/麻混纺织物的节水染色工艺。
背景技术
棉纤维在纺织工业中占有重要的地位,大约占纤维总产量的65%。目前应用在棉纤维染色方面的最重要、最有潜力的染料是活性染料。活性染料与棉纤维通过共价键结合,从根本上解决了染色纤维湿处理牢度差的问题。同时因为活性染料具有色谱齐全,色泽鲜艳,应用工艺简便,适用性强,价格相对便宜等优点,近些年它已成为棉纤维用染料中产量和产值最大的染料。
在传统的纯棉织物染色工艺中,需要将纯棉织物先进行漂白处理,取出烘干后,然后再重新配置染色液对织物进行染色,耗水量非常大,已经逐渐无法满足国家对纺织行业节水、降耗的要求。
发明内容
为了解决背景技术中的问题,本发明提供一种棉/麻混纺织物的节水染色工艺。
一种棉/麻混纺织物的节水染色工艺,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为30-40min,加入过氧化氢和稳定剂,在60-70℃条件下处理15-20min;
B、将纯棉织物取出后进行水洗、30-40℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持5-8min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至70-80℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶(20-35),时间为45-60min;
E、在染液中加入柔软剂并调节pH值至微酸性,在80-90℃下处理25-30min;
F、加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物。
优选的,所述的步骤A中,过氧化氢的加入量为0.5-2%,稳定剂的加入量为0.1-0.3%。
优选的,所述的步骤C中,盐酸的加入量为0.2-0.5g/L。
优选的,所述的步骤C中,配制染液所需加入的各种原料的量为:
EDTA 1-3g/L
渗透剂 2-6g/L
花生油 0.02-0.05g/L
碳酸氢钠 10-20g/L
硅酸钠 5-8g/L
活性染料 1-5%(o.w.f.)。
所述的步骤E中,所述的柔软剂的加入量为15-30g/L。
优选的,所述的步骤F中,所述的低温皂洗剂的加入量为2-5g/L。
本发明的有益之处在于:
1、将染色预处理、染色和软化皂洗放在同一液体中进行,用水量约为常规方法的30%,节水效果非常好;
2、在预处理残液中加入盐酸并共煮,清除残液中的过氧化氢,消除其对后续染色的影响;
3、通过配制专用的染液达到良好的染色效果,其中加入微量花生油不但可以增强染液与棉织物的染色效果,而且也利于后续的皂洗环节对颜色的固定;
4、本发明的节水染色工艺,染色效果好,棉和麻的染色均匀性好,棉织物具有非常好的色牢度,尤其是浅色,效果更佳。
具体实施方式
实施例1
一种棉/麻混纺织物的节水染色工艺,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为35min,加入过氧化氢和稳定剂,在65℃条件下处理20min;
B、将纯棉织物取出后进行水洗、35℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持7min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至75℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶30,时间为50min;
E、在染液中加入柔软剂并调节pH值至微酸性,在80-90℃下处理25-30min;
F、加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物。
所述的步骤A中,过氧化氢的加入量为0.5-2%,稳定剂的加入量为0.1-0.3%。
稳定剂为潍坊瑞光化工三合一精练酶RG-420。
所述的步骤C中,盐酸的加入量为0.4g/L。
所述的步骤C中,配制染液所需加入的各种原料的量为:
EDTA 2g/L
渗透剂4g/L
花生油0.03g/L
碳酸氢钠15g/L
硅酸钠7g/L
活性染料1.5%(o.w.f.)。
所述的渗透剂为潍坊瑞光化工耐碱渗透剂。
所述的活性染料为江苏振扬染料活性黄FG 100%。
所述的步骤E中,所述的柔软剂的加入量为20g/L;所述的柔软剂为嘉宏科技改性氨基硅油Goon1202。
所述的步骤F中,所述的低温皂洗剂的加入量为3g/L。
所述的低温皂洗剂为庄杰化工ZJ-RH18。
实施例2
一种棉/麻混纺织物的节水染色工艺,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为40min,加入过氧化氢和稳定剂,在60℃条件下处理20min;
B、将纯棉织物取出后进行水洗、30℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持8min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至70℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶35,时间为45min;
E、在染液中加入柔软剂并调节pH值至微酸性,在80-90℃下处理25-30min;
F、加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物。
所述的步骤A中,过氧化氢的加入量为2%,稳定剂的加入量为0.1%。
稳定剂为潍坊瑞光化工三合一精练酶RG-420。
所述的步骤C中,盐酸的加入量为0.5g/L。
所述的步骤C中,配制染液所需加入的各种原料的量为:
EDTA 1g/L
渗透剂 6g/L
花生油 0.02g/L
碳酸氢钠 20g/L
硅酸钠 5g/L
活性染料 5%(o.w.f.)。
所述的渗透剂为潍坊瑞光化工 耐碱渗透剂。
所述的活性染料为江苏振扬染料活性黄FG 100%。
所述的步骤E中,所述的柔软剂的加入量为30g/L;所述的柔软剂为嘉宏科技改性氨基硅油Goon1202。
所述的步骤F中,所述的低温皂洗剂的加入量为2g/L。
所述的低温皂洗剂为庄杰化工ZJ-RH18。
实施例3
一种棉/麻混纺织物的节水染色工艺,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为30min,加入过氧化氢和稳定剂,在70℃条件下处理15min;
B、将纯棉织物取出后进行水洗、40℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持5min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至80℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶20,时间为60min;
E、在染液中加入柔软剂并调节pH值至微酸性,在80-90℃下处理25-30min;
F、加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物。
所述的步骤A中,过氧化氢的加入量为0.5%,稳定剂的加入量为0.3%。
稳定剂为潍坊瑞光化工三合一精练酶RG-420。
所述的步骤C中,盐酸的加入量为0.2g/L。
所述的步骤C中,配制染液所需加入的各种原料的量为:
EDTA 3g/L
渗透剂 2g/L
花生油 0.05g/L
碳酸氢钠 10g/L
硅酸钠 8g/L
活性染料 1%(o.w.f.)。
所述的渗透剂为潍坊瑞光化工 耐碱渗透剂。
所述的活性染料为江苏振扬染料 活性黄FG 100%。
所述的步骤E中,所述的柔软剂的加入量为15g/L;所述的柔软剂为嘉宏科技改性氨基硅油Goon1202。
所述的步骤F中,所述的低温皂洗剂的加入量为5g/L。
所述的低温皂洗剂为庄杰化工ZJ-RH18。
下面对实施例1-3的方法染色的纯棉面料进行检测,得到如下数据:
由对比参数及检测数据可以知道,使用本发明的染色方法,不但可以节省大量的水,同时织物的色牢度好,棉和麻的染色均匀性好,各批次染色的色差小。
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。

Claims (6)

1.一种棉/麻混纺织物的节水染色工艺,其特征在于,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为30-40min,加入过氧化氢和稳定剂,在60-70℃条件下处理15-20min;
B、将纯棉织物取出后进行水洗、30-40℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持5-8min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至70-80℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶(20-35),时间为45-60min;
E、在染液中加入柔软剂并调节pH值至微酸性,在80-90℃下处理25-30min;
F、加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物;
步骤C中,配制染液所需加入的各种原料的量为:
EDTA 1-3g/L
渗透剂 2-6g/L
花生油 0.02-0.05g/L
碳酸氢钠 10-20g/L
硅酸钠 5-8g/L
活性染料 1-5%(o.w.f.)。
2.如权利要求1所述的棉/麻混纺织物的节水染色工艺,其特征在于,所述的步骤A中,过氧化氢的加入量为0.5-2%,稳定剂的加入量为0.1-0.3%。
3.如权利要求1所述的棉/麻混纺织物的节水染色工艺,其特征在于,所述的步骤C中,盐酸的加入量为0.2-0.5g/L。
4.如权利要求1所述的棉/麻混纺织物的节水染色工艺,其特征在于,所述的步骤E中,所述的柔软剂的加入量为15-30g/L。
5.如权利要求1所述的棉/麻混纺织物的节水染色工艺,其特征在于,所述的步骤F中,所述的低温皂洗剂的加入量为2-5g/L。
6.如权利要求1所述的棉/麻混纺织物的节水染色工艺,其特征在于,包括以下步骤:
A、将纯棉织物加入容器中进行预处理:沸水煮,时间为35min,加入过氧化氢和稳定剂,在65℃条件下处理20min;
B、将纯棉织物取出后进行水洗、35℃烘干;
C、在预处理残液中加入0.1mol/L的盐酸并加热至沸腾,保持7min;加入活性染料,并加入EDTA、渗透剂、花生油、缓染剂、碳酸氢钠和硅酸钠,加热至75℃,得到染液;
D、将干燥后的纯棉织物放入染液中染色,浴比为1∶30,时间为50min;
E、在染液中加入低温皂洗剂,将染色后纯棉织物进行皂洗,在温度40-50℃下处理10-15min后,取出,经清洗、低温烘干,得到染色纯棉织物;
所述的步骤A中,过氧化氢的加入量为0.5-2%,稳定剂的加入量为0.1-0.3%;
稳定剂为潍坊瑞光化工三合一精练酶RG-420;
所述的步骤C中,盐酸的加入量为0.4g/L;
所述的步骤C中,配制染液所需加入的各种原料的量为:
EDTA 2g/L
渗透剂 4g/L
花生油 0.03g/L
碳酸氢钠 15g/L
硅酸钠 7g/L
活性染料 1.5%(o.w.f.);
所述的渗透剂为潍坊瑞光化工耐碱渗透剂;
所述的活性染料为江苏振扬染料活性黄 FG 100%;
所述的步骤E中,所述的柔软剂的加入量为20g/L;所述的柔软剂为嘉宏科技改性氨基硅油Goon1202;
所述的步骤F中,所述的低温皂洗剂的加入量为3g/L;
所述的低温皂洗剂为庄杰化工ZJ-RH18。
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