CN106007899A - Method for preparing soybean organic fertilizer - Google Patents

Method for preparing soybean organic fertilizer Download PDF

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CN106007899A
CN106007899A CN201610315058.4A CN201610315058A CN106007899A CN 106007899 A CN106007899 A CN 106007899A CN 201610315058 A CN201610315058 A CN 201610315058A CN 106007899 A CN106007899 A CN 106007899A
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chinese medicine
semen glycines
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丁玉兰
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/30Microbial fungi; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/26Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • CCHEMISTRY; METALLURGY
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    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F3/00Fertilisers from human or animal excrements, e.g. manure
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F9/00Fertilisers from household or town refuse
    • C05F9/04Biological compost
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

Provided is a method for preparing soybean organic fertilizer. The soybean organic fertilizer is prepared from, by weight, animal manure, soybean straw, bean pulp, traditional Chinese medicine, microelements, urea, phosphatic fertilizer, potash fertilizer and humic acid. The traditional Chinese medicine comprises flos lonicerae, folium isatidis, radix euphorbiae lantu, Japanese thistle herb or root, chinaberry bark and root-bark, sun euphorbia herb and liquorice roots. The traditional Chinese medicine and the organic fertilizer are fermented, a traditional Chinese medicine fermentation concentrated solution is poured into the organic fertilizer, the mixture is stirred and mixed to be uniform, and drying is carried out at low temperature; nutrient content is detected, the urea, the phosphatic fertilizer, the potash fertilizer and the microelements are added to be mixed according to the content detecting result, and the materials are conveyed into a particle forming machine to be formed; humic acid is prepared in proportion and then added into the particles for coating; particles of coating are conveyed into an air-flowing type intermediate-temperature drying machine for drying, and the soybean organic fertilizer is obtained. The soybean organic fertilizer can improve the soil structure and increase soil fertility, and fertilizer and pesticide are gradually reduced year by year, so that the fertilizer and the pesticide are completely not used, and finally no-tillage work is achieved. Meanwhile, survival and propagation of microorganisms are inhibited, soilborne plant diseases and insect pests and successive cropping obstacles are relieved and gradually eliminated, the water seepage, water retention and ventilating capacity is enhanced, soil pelletization is promoted, the viable organism content is high, and the soybean organic fertilizer is environmentally friendly and free of residues.

Description

A kind of preparation method of Semen Glycines fertilizer
Technical field
The invention belongs to organic fertilizer technical field, particularly relate to the preparation method of a kind of Semen Glycines fertilizer.
Background technology
Semen Glycines originates in China, and all there is cultivation various places, the most extensively cultivate in all over the world.Semen Glycines is the important cereal crops of China One of, existing 5,000 years cultivation histories, ancient title bean, China northeast is main producing region, is that its seed a kind of contains abundant vegetable protein The crop of matter.Semen sojae atricolor is the most frequently used makees various bean product, squeeze Oleum Glycines, make soy sauce and extract protein.Bean dregs or wear into thick The Semen sojae atricolor of powder is also commonly used for poultry and livestock feed.
Semen Glycines is extremely wide, according to China's Semen Glycines climate regionalization, except High aititude, the high latitude of shortage of heat at China's planting range Degree area and annual precipitation are below 250 millimeters, again beyond the area of non-irrigated condition;Generally individually there is soybean planting.China is big Plain northeastward, concentration producing region, the Plain of Huanghua Area, Yangtze River Delta and the Jianghan Plain of bean.According to the requirement difference to temperature, point Spring Semen Glycines and two bions of summer Semen Glycines, different regions plantation dissimilar, in Heilungkiang, Jilin, Liaoning, the Inner Mongol plantation spring Semen Glycines, sowed spring 3~April, and 7~maturation in August, period of duration is short, about about 100 days;Huanghuai Area and the summer of the Yangtze river basin Big Semen Glycines district, sowed in the 5-6 month in summer, and the 9-10 month is ripe, period of duration about about 110 days, wherein, and northeast spring sowing Semen sojae atricolor and the Yellow River and Huai He River Sea Summer Soybean is two areas that Chinese soybean cultivated area is maximum, yield is the highest.
At present, people, when applying fertilizer to Semen Glycines, use the raw material such as chemical fertilizer, carbamide to topdress to Semen Glycines, although effect Good, but nutrition contained in chemical fertilizer, carbamide can not meet far away the nutritional need of Semen Glycines, easily causes Semen Glycines because lacking nutrition Blade face is yellow, growth is slow, and the Semen Glycines soybean pod born is few, and lightweight, premunition is poor, is more easy to various pest and disease damage.
Chemical fertilizer and pesticide play highly important effect in agricultural production, and chemical fertilizer accounts for the most raw in agricultural production The 50% of producing property expenditure, also brings the increases in grain production of 55% to developing country.Along with carrying of people's living standard and health perception Height, people pay much attention to the safety of agricultural product, increase demand nuisanceless, pollution-free food year by year.
Fertilizer type used by current Semen Glycines plantation is a lot, and wherein Semen Glycines special fertilizer uses commercially mostly NPK compound fertilizer, it is mainly made up of the big inorganic elements of N, P, K tri-, can meet the growth needs of Semen Glycines at short notice.But it is long Phase use can make soil aggregate be destroyed, and easily causes soil compaction, soil property hardening, thus affects growth of soybean, to Huang Bean growth-promoting effect is inconspicuous.Though the most simple fertilizer is rich in organic matter, but nutrients release is slow, Semen Glycines absorb slow, Fertilizer efficiency is low, does not reaches active balance between various available nutrients.But due to fertilizer character, the combined influence of soil environment condition and The characteristic of chemical fertilizer self and unreasonable use, causes the problems such as utilization rate is low, the wasting of resources, environmental pollution.China at present Chemical fertilizer this season utilization rate nitrogen is 30~35%, and phosphorus is 10~20%, and potassium is 35~50%, and nitrogenous fertilizer this season utilization rate is flourishing less than the world Country 10~15%, and account for 30~50% by the nitrogen of the loss such as leaching, volatilization, this causes subsoil water eutrophication, vegetable The problems of ecological security such as middle nitrate nitrogen content exceeds standard, nitrous oxide emission amount increase.
At present Semen Glycines prevention and elimination of disease and pests is mainly with chemicals and the blended stirring of toxic pesticides, in being manured into soil or agriculture On crop, life-time service year in year out, substantial amounts of pesticide, cause insect to produce drug resistance, water source soil and crops are made Becoming to pollute, agricultural product quality declines, and pesticide residues exceed standard and have a strong impact on the physical and mental health of people and China Semen Glycines in international market Competitiveness.
Therefore, improve chemical fertilizer utilization ratio, reduce the environmental pollution that causes of chemical fertilizer application, develop and develop new-type fertilizer and get over More cause the common concern of society.
Summary of the invention
Present invention aims to the deficiency of above technology, solve that current chemical fertilizer is unreasonable to be used, cause utilization rate The problem of low, the wasting of resources, environmental pollution etc., it is provided that the preparation method of a kind of Semen Glycines fertilizer, this preparation method is simple, use Convenience, safety and environmental protection, pure ecology, noresidue, viable bacteria content height.
For reaching above-mentioned purpose, the technical solution used in the present invention is as follows:
A kind of preparation method of Semen Glycines fertilizer, it is characterised in that: it is to prepare according to the following steps: one, take following weight portion former Material: animal fecaluria 40-50, soybean stalks 25-35, bean cake 5-10, Chinese medicine 10-15, trace element 1-2, carbamide 10-15, phosphate fertilizer 15-20, potash fertilizer 5-10, humic acid 0.5-1.0;Two, Chinese medicine is Flos Lonicerae, Folium Isatidis, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), Radix Cirsii Japonici, Cortex Meliae, Herba Euphorbiae Helioscopiae, sweet Grass, adds ethanol solution intense fire by each Study on Supermicro-pulverization of Traditional Chinese Drugs and boils, and slow fire is incubated, cold filtration, concentrated filtrate, adds white sugar and boils Boiling, inoculates red tea fungus and yeast after cooling down to room temperature, through 96 ~ 120h fermentation to bacterium solution pH6-7, stops fermentation, by bacterium solution Cryoconcentration to 1g crude drug/gram;Three, the fermentation of fertilizer: weigh animal fecaluria, soybean stalks, bean cake in proportion, adds 1-3 The water of times amount, soaks 12-24h, is added thereto to 20-30kg and contains lactobacillus, phosphorus decomposing bacillus megaterium and bacillus subtilis Mixed bacteria liquid, 35 DEG C-55 DEG C, ferment 96-144h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Four, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40-60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide, phosphate fertilizer, potash fertilizer and trace element and mix;Five, pelletize: by thing Material is sent into agent grain forming machine and is shaped, a diameter of 2mm-6mm of thing grain after molding, and the time of material turnover forming machine is about 0.5-1min;Six, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule;Seven, cold drying: will be coated with The granule of layer is sent into air-flowing type middle temperature dehydrator and is dried, and obtains Semen Glycines fertilizer.
The preparation method of described a kind of Semen Glycines fertilizer, it is characterised in that: step 2 weighs the Chinese medicine gold silver of weight portion Flower 100-120, Folium Isatidis 100-120, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100-120, Radix Cirsii Japonici 80-100, Cortex Meliae 80-100, Herba Euphorbiae Helioscopiae 60-80, Radix Glycyrrhizae 40- 60, micronizing, the ethanol solution of 70%~the 80% of addition Chinese medicine gross weight 6~8 times amount, soak 30~60min, intense fire boils Boiling, slow fire insulation 30~60min, cool down Floor 12 filtered through gauze;Filtering residue adds 4~the ethanol solution of the 40% of 6 times amount~50% again, Intense fire boils, slow fire insulation 30~60min, cools down Floor 12 filtered through gauze, merges twice filtrate, concentration and recovery ethanol, use second Without stopping during ethanol concentrating in alcohol detector detection concentrated solution, add water in concentrated solution and make every milliliter of water crude drug Han 0.25g, with 100 Kg concentrated solutions are that unit adds white sugar 10~20Kg, and boil 3~5min, are cooled to room temperature, inoculation red tea fungus and yeast Bacterium (commercially available) preparation 20~25Kg, setting fermentation temperature 35~38 DEG C, standing for fermentation is cultivated 96~120h, is grown to pH6 ~ 7 white Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating.
The preparation method of described a kind of Semen Glycines fertilizer, it is characterised in that: the temperature of step 3 cold drying sets 50 DEG C-60 DEG C, the moisture of material is made to be down to 20-25% by original 50% standby.
The preparation method of described a kind of Semen Glycines fertilizer, it is characterised in that: step 4 trace element include S, Mg, Zn, B, Fe, Mo, Cu etc..
The preparation method of described a kind of Semen Glycines fertilizer, it is characterised in that: step 6 coating time period is 1-2min.
The preparation method of described a kind of Semen Glycines fertilizer, it is characterised in that: step 7 cold drying temperature setting 40 DEG C- 50 DEG C, the moisture of material is made to be down to 10%-15% by original 20-25%.
Fertilizer of the present invention have suppression harmful microbe existence with breeding, alleviate and successive elimination soil-borne disease insect pest and Continuous cropping obstacle, infiltration, water conservation, venting capability strengthen, and promote soil granular, and viable bacteria content is high, green noresidue.The present invention Have the beneficial effects that improve in soil potassium improves 10%, phosphorus improves 30.8%, and full nitrogen improves 18.5%;The Chinese medicine added and life Thing probiotics, has obvious inhibiting effect to the Fusarium spp. causing Semen Glycines root rot, can significantly reduce its biological activity, prevents harnessing the Yellow River Radix Sophorae Tonkinensis maize ear rot effect is obvious, and viable bacteria content is high, and content is in 2.30-4.62 × 10 after measured8cfu/g。
Fusarium spp. Antibacterial Activity: use mycelial growth rate method, often process and be repeated 3 times, be processed as with non-adding medicine Blank group, with thiophanate-methyl for antibiotic matched group.Measure colony diameter by decussation method, take the flat of 3 repetitions Average.Suppression ratio (I) is calculated by equation below.Wherein, C is straight for comparison bacterium colony in I (%)=[(C-T)/(C-0.4)] × 100 Footpath, T is for processing colony diameter.
Concentration (EC in virulence regression equation and suppression is obtained with SPSS13.0 software50), the results are shown in Table 1.
Virulence regression equation and the EC50 result of bacteriostatic activity respectively organized by table 1
Group Virulence regression equation r EC50(mg/mL)
Chinese medicine fermented liquid Y=2.118x±2.348 0.998 14.81±2.78
Organic fertilizer fermentation liquid Y=2.215x±1.625 0.932 36.73±4.69
Chinese medicine+organic fertilizer liquid Y=2.486x±1.768 0.971 19.12±2.24
Thiophanate-methyl Y=1.536x±3.091 0.985 15.76±2.89
As can be seen from the table, Fusarium spp. is all had necessarily by Chinese medicine fermented liquid, organic fertilizer fermentation liquid, Chinese medicine+organic fertilizer fermentation liquid Inhibitory action, wherein the EC50 of Chinese medicine fermented liquid and thiophanate-methyl are suitable, illustrate that Chinese medicine fermented liquid causes by Fusarium spp. Semen Glycines root rot there is obvious inhibitory action, Semen Glycines root rot can be prevented and treated with substitute antibiotics.Chinese prescription of the present invention Having the functions such as bacteriostasis and sterilization, parasite killing, antiviral, modern pharmacology shows: in Fang, Flos Lonicerae, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), Radix Cirsii Japonici etc. have significantly Antibacterial and bactericidal action, Folium Isatidis, Herba Euphorbiae Helioscopiae have stronger antivirus action, can treat virus infect caused by tissue injury, Cortex Meliae has pest-resistant effect, and Radix Glycyrrhizae is to make medicine, make all medicines return through effect.
To the organic fertilizer in embodiment, with reference to organic fertilizer (NY525-2012), detecting, acquired results is shown in Table 2;
Table 2, organic fertilizer testing result in embodiment
The content of organic matter of the organic fertilizer of the present invention is all more than 45% as can be seen from Table 2, total nutrient more than 5.0%, water Dividing less than 15%, pH5.9-7.5, all above index all meets organic fertilizer (NY525-2012) standard.
Detailed description of the invention
Embodiment 1
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 30min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filtering residue Add again 4 times amount 40% ethanol solution, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 10Kg, and boil 3min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 20Kg, set fermentation temperature 35 DEG C, and standing for fermentation cultivates 96h, grows white bacterium to pH6.2 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Semen Glycines straw Stalk 25, bean cake 5 add the water of 1 times amount, soak 12h, are added thereto to 20kg and contain lactobacillus, phosphorus decomposing bacillus megaterium and withered The mixed bacteria liquid of grass bacillus, 35 DEG C, ferment 96h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40 mesh, and detection is supported Divide content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu and enter Row mixing;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 2mm of thing grain after molding, material passes in and out into The time of type machine is about 0.5 minute;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 40 DEG C, makes material Moisture 11.2%, obtain Semen Glycines fertilizer, viable count is 0.28 hundred million cfu/g.
Embodiment 2
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 30min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filtering residue Add again 4 times amount 40% ethanol solution, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 15Kg, and boil 4min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 20Kg, set fermentation temperature 36 DEG C, and standing for fermentation cultivates 110h, grows white to pH6.5 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh the animal excreta of weight portion Urine 45, soybean stalks 30, bean cake 7, add the water of 2 times amount, soaks 18h, and being added thereto to 25kg, to contain lactobacillus, phosphorus decomposing huge Bacillus cereus and the mixed bacteria liquid of bacillus subtilis, 36 DEG C, ferment 112h, to growing white hypha, stops fermentation, adds Chinese medicine and sends out Ferment concentrated solution, is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach To 60 mesh, detect nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material being sent into agent grain forming machine and is shaped, the thing grain after molding is a diameter of 4mm, material turnover forming machine time be about 1 minute;Five, coating: add after humic acid is prepared in proportion in above-mentioned granule Carry out coating 1min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 45 DEG C, making the moisture 13.4% of material, obtain Semen Glycines fertilizer, viable count is 0.3 hundred million cfu/g.
Embodiment 3
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 300min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 40% of 4 times amount again, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20Kg in units of 100 Kg concentrated solutions, and boils 5min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25Kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 110h, grows white to pH6.8 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Huang Beanstalk stalk 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to lactobacillus, phosphorus decomposing bacillus megaterium and hay Bacillus, 35 DEG C-55 DEG C, ferment 96-144h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, and stirring is mixed Close uniformly, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, detects nutrient Content, according to content detection result, adds carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu and carries out Mixing;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 5mm of thing grain after molding, material turnover molding The time of machine is about 0.5 minute;Five, coating: add after humic acid is prepared in proportion and carry out coating 2min in above-mentioned granule; Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes the water of material Dividing and be down to 11.8%, obtain Semen Glycines fertilizer, viable count is 0.41 hundred million cfu/g.
Embodiment 4
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 40% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 20Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 120h, grows white bacterium to pH7 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Semen Glycines straw Stalk 25, bean cake 5 add the water of 2 times amount, soak 18h, are added thereto to 20kg and contain lactobacillus, phosphorus decomposing bacillus megaterium and withered The mixed bacteria liquid 40 DEG C of grass bacillus, ferment 128h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40 mesh, and detection is supported Divide content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu Mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 5mm of thing grain after molding, material passes in and out The time of forming machine is about 0.5 minute;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 40 DEG C, makes material Moisture be down to 12.5%, obtain Semen Glycines fertilizer, viable count is 0.32 hundred million cfu/g.
Embodiment 5
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 80% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 50% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 15Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 35 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.4 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to 25kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid 45 DEG C of bacillus subtilis, ferment 96h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material enters The time going out forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 12.8%, obtain Semen Glycines fertilizer, viable count is 0.31 hundred million cfu/g.
Embodiment 6
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 80, Cortex Meliae 80, Herba Euphorbiae Helioscopiae 60, Radix Glycyrrhizae 40, micronizing, add Chinese medicine gross weight The ethanol solution of the 80% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 50% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 36 DEG C, and standing for fermentation cultivates 108h, grows white bacterium to pH7 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines straw Stalk 35, bean cake 10 add the water of 3 times amount, soak 24h, be added thereto to 30kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 55 DEG C, ferment 96h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40 mesh, detection Nutrient content, according to content detection result, adds carbamide 15, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu Mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 3mm of thing grain after molding, material passes in and out The time of forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1.5min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes thing The moisture of material is down to 10.9%, obtains Semen Glycines fertilizer, and viable count is 0.38 hundred million cfu/g.
Embodiment 7
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 30min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filtering residue Add again 4 times amount 40% ethanol solution, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 10Kg, and boil 3min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 20Kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.2 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Semen Glycines Straw 25, bean cake 5 add the water of 1 times amount, soak 24h, be added thereto to 20kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 35 DEG C of fermentation 120h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 50 mesh, detection Nutrient content, according to content detection result, adds carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu Mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material passes in and out The time of forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating 2min in above-mentioned granule; Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes the water of material Dividing and be down to 10.8%, obtain Semen Glycines fertilizer, viable count is 0.29 hundred million cfu/g.
Embodiment 8
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 30min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filtering residue Add again 4 times amount 40% ethanol solution, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 15Kg, and boil 4min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white truffle to pH7 Till, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, soybean stalks 25, bean cake 5 adds the water of 3 times amount, soaks 24h, is added thereto to 25kg and contains lactobacillus, phosphorus decomposing bacillus megaterium and hay The mixed bacteria liquid of bacillus, 45 DEG C, ferment 106h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40-60 mesh, detection Nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material enters The time going out forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 450 DEG C, makes thing The moisture of material is down to 10.2%, obtains Semen Glycines fertilizer, and viable count is 0.3 hundred million cfu/g.
Embodiment 9
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 70% of 6 times amount, soaks 30min, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze;Filtering residue Adding the ethanol solution of 4 times amount 40% again, intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze, merges twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 35 DEG C, and standing for fermentation cultivates 120h, grows white to pH6.3 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Semen Glycines Straw 25, bean cake 5 add the water of 1 times amount, soak 24h, be added thereto to 30kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 50 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, detection Nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material enters The time going out forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 9.5%, obtain Semen Glycines fertilizer, viable count is 0.39 hundred million cfu/g.
Embodiment 10
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 80% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 50% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 10Kg, and boil 3min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 36 DEG C, and standing for fermentation cultivates 120h, grows white to pH6.5 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to 20kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 35 DEG C of fermentation 144h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material The time of turnover forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion in above-mentioned granule and be coated with Layer 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes thing The moisture of material is down to 10.2%, obtains Semen Glycines fertilizer, and viable count is 0.31 hundred million cfu/g.
Embodiment 11
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 80% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 50% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 15Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 108h, grows white bacterium to pH7 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines straw Stalk 35, bean cake 10 add the water of 3 times amount, soak 24h, be added thereto to 25kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 40 DEG C of fermentation 136h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, detection Nutrient content, according to content detection result, adds carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu Mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material passes in and out The time of forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 14.1%, obtain Semen Glycines fertilizer, viable count is 0.33 hundred million cfu/g.
Embodiment 12
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight The ethanol solution of the 80% of 8 times amount, soaks 60min, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze;Filtering residue Add again 6 times amount 50% ethanol solution, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20Kg, and boil 5min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white bacterium to pH6.4 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines straw Stalk 35, bean cake 10 add the water of 3 times amount, soak 24h, be added thereto to 30kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, detection Nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material enters The time going out forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 11.9%, obtain Semen Glycines fertilizer, viable count is 0.45 hundred million cfu/g.
Embodiment 13
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 6 times amount 70% ethanol solution, soak 30min, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 40% of 4 times amount again, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 10Kg in units of 100 Kg concentrated solutions, and boils 3min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 20Kg, set fermentation temperature 35 DEG C, and standing for fermentation cultivates 120h, grows white to pH6.3 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Huang Beanstalk stalk 25, bean cake 5 add the water of 1 times amount, soak 12h, are added thereto to 20kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 35 DEG C of fermentation 128h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material The time of turnover forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 40 DEG C, makes material Moisture be down to 10.3%, obtain Semen Glycines fertilizer, viable count is 0.33 hundred million cfu/g.
Embodiment 14
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 6 times amount 70% ethanol solution, soak 30min, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 40% of 4 times amount again, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 15Kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25kg, set fermentation temperature 36 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.6 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Huang Beanstalk stalk 25, bean cake 5 add the water of 1 times amount, soak 24h, are added thereto to 25kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 5mm of thing grain after molding, material enters The time going out forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture 12.1%, obtain Semen Glycines fertilizer, viable count is 0.35 hundred million cfu/g.
Embodiment 15
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 6 times amount 70% ethanol solution, soak 30min, intense fire boils, slow fire insulation 30min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 40% of 4 times amount again, and intense fire boils, slow fire insulation 30min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20kg in units of 100 Kg concentrated solutions, and boils 5min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25Kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.5 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Huang Beanstalk stalk 25, bean cake 5 add the water of 1 times amount, soak 24h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 55 DEG C, ferment 120h, to growing white hypha, stops fermentation, adds herb fermenting and concentrates Liquid, is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, Detection nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material The time of turnover forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 450 DEG C, makes thing The moisture of material is down to 10.1%, obtains Semen Glycines fertilizer, and viable count is 0.44 hundred million cfu/g.
Embodiment 16
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 8 times amount 80% ethanol solution, soak 60min, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 50% of 6 times amount again, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 10Kg in units of 100 Kg concentrated solutions, and boils 3min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 20Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white to pH6.2 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to lactobacillus, phosphorus decomposing bacillus megaterium and hay bar Bacterium, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, be uniformly mixed, low temperature It is dried;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, detects nutrient content, according to containing Amount testing result, adds carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu and mixes;Four, make Grain: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, the time of material turnover forming machine is about For 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating 2min in above-mentioned granule;Six, cold drying: The granule of coating being sent into air-flowing type middle temperature dehydrator be dried, temperature sets 40 DEG C, makes the moisture of material be down to 13.8%, Obtaining Semen Glycines fertilizer, viable count is 0.32 hundred million cfu/g.
Embodiment 17
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 8 times amount 80% ethanol solution, soak 60min, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 50% of 6 times amount again, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 15Kg in units of 100 Kg concentrated solutions, and boils 5min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 20Kg, set fermentation temperature 35 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.3 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Huang Beanstalk stalk 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to 25kg and contain lactobacillus, phosphorus decomposing huge spore bar Bacterium and the mixed bacteria liquid of bacillus subtilis, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting and concentrate Liquid, is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, Detection nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material The time of turnover forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 40 DEG C, makes material Moisture be down to 12.5%, obtain Semen Glycines fertilizer, viable count is 0.37 hundred million cfu/g.
Embodiment 18
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 8 times amount 80% ethanol solution, soak 60min, intense fire boils, slow fire insulation 60min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 50% of 6 times amount again, and intense fire boils, slow fire insulation 60min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20Kg in units of 100kg concentrated solution, and boils 5min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 96h, grows white to pH6.2 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 35, bean cake 10 add the water of 3 times amount, soak 24h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 3mm of thing grain after molding, material enters The time going out forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 10.4%, obtain Semen Glycines fertilizer, viable count is 0.35 hundred million cfu/g.
Embodiment 19
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 15kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 22Kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 110h, grows white to pH6.0 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Huang Beanstalk stalk 25, bean cake 7 add the water of 2 times amount, soak 18h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 35 DEG C of fermentation 144h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 50 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 12, phosphate fertilizer 17, potash fertilizer 7 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 5mm of thing grain after molding, material enters The time going out forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1.5min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 45 DEG C, makes thing The moisture of material is down to 11.6%, obtains Semen Glycines fertilizer, and viable count is 0.38 hundred million cfu/g.
Embodiment 20
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 90, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 60, micronizing, add Chinese medicine gross weight The ethanol solution of the 75% of 7 times amount, soaks 45min, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze;Filtering residue Add again 5 times amount 45% ethanol solution, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 kg concentrated solutions, add white sugar 15Kg, and boil 4min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 23Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white bacterium to pH6.3 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 45, Semen Glycines straw Stalk 28, bean cake 8 add the water of 2 times amount, soak 20h, are added thereto to 27kg and contain lactobacillus, phosphorus decomposing bacillus megaterium and withered The mixed bacteria liquid of grass bacillus, 55 DEG C of fermentation 96h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 50 mesh, and detection is supported Divide content, according to content detection result, add carbamide 11, phosphate fertilizer 16, potash fertilizer 6 and trace element S, Mg, Zn, B, Fe, Mo, Cu and enter Row mixing;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 3mm of thing grain after molding, material passes in and out into The time of type machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating 1.5min in above-mentioned granule; Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 45 DEG C, makes the water of material Dividing and be down to 13.1%, obtain Semen Glycines fertilizer, viable count is 0.32 hundred million cfu/g.
Embodiment 21
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 100, Folium Isatidis 100, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 80, Radix Glycyrrhizae 50, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 14Kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 24kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white to pH6.2 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 33, bean cake 8 add the water of 2 times amount, soak 14h, be added thereto to 30kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 45 DEG C of fermentation 108h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 50 mesh, detection Nutrient content, according to content detection result, adds carbamide 13, phosphate fertilizer 18, potash fertilizer 7 and trace element S, Mg, Zn, B, Fe, Mo, Cu Mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material passes in and out The time of forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1.5min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 45 DEG C, makes thing The moisture of material is down to 11.0%, obtains Semen Glycines fertilizer, and viable count is 0.45 hundred million cfu/g.
Embodiment 22
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 100, Cortex Meliae 100, Herba Euphorbiae Helioscopiae 70, Radix Glycyrrhizae 45, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 23Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 108h, grows white to pH6.8 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 40, Huang Beanstalk stalk 33, bean cake 7 add the water of 2 times amount, soak 18h, are added thereto to 28kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 35 DEG C of fermentation 144h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 14, phosphate fertilizer 17, potash fertilizer 8 and trace element S, Mg, Zn, B, Fe, Mo, Cu mixes;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material enters The time going out forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes material Moisture be down to 12.2%, obtain Semen Glycines fertilizer, viable count is 0.35 hundred million cfu/g.
Embodiment 23
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 100, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 65, Radix Glycyrrhizae 55, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 22Kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white to pH6.1 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 45, Semen Glycines Straw 33, bean cake 8 add the water of 2 times amount, soak 18h, be added thereto to 26kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 38 DEG C, ferment 120h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 50 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 4mm of thing grain after molding, material The time of turnover forming machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion in above-mentioned granule and be coated with Layer 2min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes thing The moisture of material is down to 12.7%, obtains Semen Glycines fertilizer, and viable count is 0.36 hundred million cfu/g.
Embodiment 24
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 110, Folium Isatidis 110, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 110, Radix Cirsii Japonici 100, Cortex Meliae 90, Herba Euphorbiae Helioscopiae 65, Radix Glycyrrhizae 55, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20Kg in units of 100 Kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 106h, grows white to pH6.3 Till color truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Huang Beanstalk stalk 32, bean cake 7 add the water of 2 times amount, soak 18h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium With the mixed bacteria liquid of bacillus subtilis, 45 DEG C, ferment 120h, to growing white hypha, stops fermentation, adds herb fermenting and concentrates Liquid, is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, Detection nutrient content, according to content detection result, add carbamide 13, phosphate fertilizer 18, potash fertilizer 7 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material The time of turnover forming machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule 1.5min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes thing The moisture of material is down to 10.6%, obtains Semen Glycines fertilizer, and viable count is 0.46 hundred million cfu/g.
Embodiment 25
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 95, Cortex Meliae 95, Herba Euphorbiae Helioscopiae 75, Radix Glycyrrhizae 45, micronizing, add Chinese medicine gross weight The ethanol solution of the 75% of 7 times amount, soaks 45min, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze;Filtering residue Add again 5 times amount 45% ethanol solution, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20Kg, and boil 4min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white bacterium to pH6.6 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 42, Semen Glycines straw Stalk 30, bean cake 6 add the water of 2 times amount, soak 18h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium and withered The mixed bacteria liquid of grass bacillus, 42 DEG C of fermentation 120h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, and detection is supported Divide content, according to content detection result, add carbamide 12, phosphate fertilizer 16, potash fertilizer 7 and trace element S, Mg, Zn, B, Fe, Mo, Cu and enter Row mixing;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 3mm of thing grain after molding, material passes in and out into The time of type machine is about 0.5min;Five, coating: add after humic acid is prepared in proportion and carry out coating 2min in above-mentioned granule; Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes the water of material Dividing and be down to 10.2%, obtain Semen Glycines fertilizer, viable count is 0.38 hundred million cfu/g.
Embodiment 26
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 85, Cortex Meliae 85, Herba Euphorbiae Helioscopiae 75, Radix Glycyrrhizae 55, micronizing, add Chinese medicine gross weight The ethanol solution of the 75% of 7 times amount, soaks 45min, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze;Filtering residue Add again 5 times amount 45% ethanol solution, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze, merge twice filter Liquid, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milli Rise water crude drug Han 0.25g, in units of 100 Kg concentrated solutions, add white sugar 20kg, and boil 4min, be cooled to room temperature, inoculate red Tea bacterium and yeast (commercially available) preparation 25kg, set fermentation temperature 38 DEG C, and standing for fermentation cultivates 96h, grows white bacterium to pH6.6 Till block, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 45, Semen Glycines straw Stalk 30, bean cake 7 add the water of 2 times amount, soak 18h, are added thereto to 30kg and contain lactobacillus, phosphorus decomposing bacillus megaterium and withered The mixed bacteria liquid of grass bacillus, 39 DEG C of fermentation 108h, to growing white hypha, stop fermentation, add herb fermenting concentrated solution, stirring Mix homogeneously, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, and detection is supported Divide content, according to content detection result, add carbamide 10, phosphate fertilizer 15, potash fertilizer 5 and trace element S, Mg, Zn, B, Fe, Mo, Cu and enter Row mixing;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 2mm of thing grain after molding, material passes in and out into The time of type machine is about 1min;Five, coating: add after humic acid is prepared in proportion and carry out coating 1.5min in above-mentioned granule; Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 45 DEG C, makes the water of material Dividing and be down to 10.9%, obtain Semen Glycines fertilizer, viable count is 0.36 hundred million cfu/g.
Embodiment 27
The preparation method of a kind of Semen Glycines fertilizer, comprises the following steps: one, the fermentation of Chinese medicine: weigh the Chinese medicine gold silver of weight portion Spend 120, Folium Isatidis 120, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 120, Radix Cirsii Japonici 100, Cortex Meliae 95, Herba Euphorbiae Helioscopiae 65, Radix Glycyrrhizae 55, micronizing, add Chinese medicine gross weight Measure 7 times amount 75% ethanol solution, soak 45min, intense fire boils, slow fire insulation 45min, cool down Floor 12 filtered through gauze;Filter Slag adds the ethanol solution of the 45% of 5 times amount again, and intense fire boils, slow fire insulation 45min, cools down Floor 12 filtered through gauze, merges twice Filtrate, concentration and recovery ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, adding water in concentrated solution, it is every to make Milliliter water crude drug Han 0.25g, adds white sugar 20kg in units of 100 kg concentrated solutions, and boils 4min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 25kg, set fermentation temperature 37 DEG C, and standing for fermentation cultivates 108h, grows white to pH7 Till truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating;Two, the fermentation of fertilizer: weigh animal fecaluria 50, Semen Glycines Straw 35, bean cake 7 add the water of 2 times amount, soak 20h, be added thereto to 30kg contain lactobacillus, phosphorus decomposing bacillus megaterium and The mixed bacteria liquid of bacillus subtilis, 45 DEG C, ferment 120h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, It is uniformly mixed, cold drying;Three, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide 15, phosphate fertilizer 20, potash fertilizer 10 and trace element S, Mg, Zn, B, Fe, Mo, Cu mix;Four, pelletize: material is sent into agent grain forming machine and is shaped, a diameter of 6mm of thing grain after molding, material The time of turnover forming machine is about 0.8min;Five, coating: add after humic acid is prepared in proportion in above-mentioned granule and be coated with Layer 1.5min;Six, cold drying: the granule of coating being sent into air-flowing type middle temperature dehydrator and is dried, temperature sets 50 DEG C, makes The moisture of material is down to 10.5%, obtains Semen Glycines fertilizer, and viable count is 0.45 hundred million cfu/g.
The above, the only detailed description of the invention of the present invention, but protection scope of the present invention is not limited thereto, and any Those familiar with the art, in the technical scope that the invention discloses, can readily occur in change or replace, should contain Cover within protection scope of the present invention.

Claims (6)

1. the preparation method of a Semen Glycines fertilizer, it is characterised in that: it is to prepare according to the following steps: one, take following weight portion Raw material: animal fecaluria 40-50, soybean stalks 25-35, bean cake 5-10, Chinese medicine 10-15, trace element 1-2, carbamide 10-15, phosphorus Fertile 15-20, potash fertilizer 5-10, humic acid 0.5-1.0;Two, Chinese medicine be Flos Lonicerae, Folium Isatidis, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), Radix Cirsii Japonici, Cortex Meliae, Herba Euphorbiae Helioscopiae, Radix Glycyrrhizae, adds ethanol solution intense fire by each Study on Supermicro-pulverization of Traditional Chinese Drugs and boils, and slow fire is incubated, cold filtration, concentrated filtrate, adds white sugar and boils Boiling, inoculates red tea fungus and yeast after cooling down to room temperature, through 96 ~ 120h fermentation to bacterium solution pH6-7, stops fermentation, by bacterium solution Cryoconcentration to 1g crude drug/gram;Three, the fermentation of fertilizer: weigh animal fecaluria, soybean stalks, bean cake in proportion, adds 1-3 The water of times amount, soaks 12-24h, is added thereto to 20-30kg and contains lactobacillus, phosphorus decomposing bacillus megaterium and bacillus subtilis Mixed bacteria liquid, 35 DEG C-55 DEG C, ferment 96-144h, to growing white hypha, stops fermentation, adds herb fermenting concentrated solution, stir Mix mix homogeneously, cold drying;Four, dispensing: dried material is sent into pulverizer, makes fineness of materials reach 40-60 mesh, inspection Survey nutrient content, according to content detection result, add carbamide, phosphate fertilizer, potash fertilizer and trace element and mix;Five, pelletize: by thing Material is sent into agent grain forming machine and is shaped, a diameter of 2mm-6mm of thing grain after molding, and the time of material turnover forming machine is about 0.5-1min;Six, coating: add after humic acid is prepared in proportion and carry out coating in above-mentioned granule;Seven, cold drying: will be coated with The granule of layer is sent into air-flowing type middle temperature dehydrator and is dried, and obtains Semen Glycines fertilizer.
The preparation method of a kind of Semen Glycines fertilizer the most according to claim 1, it is characterised in that: step 2 weighs weight portion Flos lonicerae 100-120, Folium Isatidis 100-120, Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 100-120, Radix Cirsii Japonici 80-100, Cortex Meliae 80-100, Herba Euphorbiae Helioscopiae 60- 80, Radix Glycyrrhizae 40-60, micronizing, add Chinese medicine gross weight 6~8 times amount 70%~80% ethanol solution, soak 30~ 60min, intense fire boils, slow fire insulation 30~60min, cools down Floor 12 filtered through gauze;Filtering residue add 4 again~the 40% of 6 times amount~ The ethanol solution of 50%, intense fire boils, slow fire insulation 30~60min, cools down Floor 12 filtered through gauze, merges twice filtrate, concentrates Reclaim ethanol, concentrate without stopping during ethanol with in ethanol detector detection concentrated solution, add water in concentrated solution and make every milliliter of water contain 0.25g crude drug, adds white sugar 10~20Kg in units of 100 Kg concentrated solutions, and boils 3~5min, be cooled to room temperature, inoculation Red tea fungus and yeast (commercially available) preparation 20~25Kg, setting fermentation temperature 35~38 DEG C, standing for fermentation cultivation 96~120h, extremely Till pH6 ~ 7 grow white truffle, cryoconcentration bacterium solution to 1g crude drug/gram, stop concentrating.
The preparation method of a kind of Semen Glycines fertilizer the most according to claim 1, it is characterised in that: step 3 cold drying Temperature sets 50 DEG C-60 DEG C, makes the moisture of material be down to 20-25% by original 50% standby.
The preparation method of a kind of Semen Glycines fertilizer the most according to claim 1, it is characterised in that: step 4 trace element bag Include S, Mg, Zn, B, Fe, Mo, Cu etc..
The preparation method of a kind of Semen Glycines fertilizer the most according to claim 1, it is characterised in that: step 6 coating time period is 1-2min。
The preparation method of a kind of Semen Glycines fertilizer the most according to claim 1, it is characterised in that: step 7 cold drying temperature Degree sets 40 DEG C-50 DEG C, makes the moisture of material be down to 10%-15% by original 20-25%.
CN201610315058.4A 2016-05-13 2016-05-13 Method for preparing soybean organic fertilizer Pending CN106007899A (en)

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Publication number Priority date Publication date Assignee Title
US20180237355A1 (en) * 2017-02-23 2018-08-23 Produquímica Indústria e Comaércio S.A. Multi-nutrient granular fertilizer compositions and methods of using the same
CN108707022A (en) * 2018-07-13 2018-10-26 芜湖三月禾园艺设计有限公司 Antibacterial fermentation fertilizer of one kind and preparation method thereof
CN113508877A (en) * 2021-07-20 2021-10-19 齐齐哈尔医学院 Preparation method of compound fermented feed for dairy cows
CN113632669A (en) * 2021-07-21 2021-11-12 海南大学 Method for preventing and treating green soy bean root rot

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CN104557208A (en) * 2015-01-16 2015-04-29 山东省农作物种质资源中心 Soybean special fertilizer as well as preparation method and fertilization method thereof

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Publication number Priority date Publication date Assignee Title
CN104557208A (en) * 2015-01-16 2015-04-29 山东省农作物种质资源中心 Soybean special fertilizer as well as preparation method and fertilization method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20180237355A1 (en) * 2017-02-23 2018-08-23 Produquímica Indústria e Comaércio S.A. Multi-nutrient granular fertilizer compositions and methods of using the same
US10519072B2 (en) * 2017-02-23 2019-12-31 Produquímica Indústria E Comércio S.A. Multi-nutrient granular fertilizer compositions and methods of using the same
US10696604B2 (en) 2017-02-23 2020-06-30 Produquímica Indústria E Comércio S.A. Granular fertilizers comprising macronutrients and micronutrients, and processes for manufacture thereof
US10865158B2 (en) 2017-02-23 2020-12-15 Compass Minerals América do Sul Indústria e Comércio S.A. Granular fertilizers comprising macronutrients and micronutrients, and processes for manufacture thereof
CN108707022A (en) * 2018-07-13 2018-10-26 芜湖三月禾园艺设计有限公司 Antibacterial fermentation fertilizer of one kind and preparation method thereof
CN113508877A (en) * 2021-07-20 2021-10-19 齐齐哈尔医学院 Preparation method of compound fermented feed for dairy cows
CN113632669A (en) * 2021-07-21 2021-11-12 海南大学 Method for preventing and treating green soy bean root rot

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Application publication date: 20161012