CN105970671B - A kind of dye applies integrated dyeing, stamp paste composition and its application - Google Patents
A kind of dye applies integrated dyeing, stamp paste composition and its application Download PDFInfo
- Publication number
- CN105970671B CN105970671B CN201610580392.2A CN201610580392A CN105970671B CN 105970671 B CN105970671 B CN 105970671B CN 201610580392 A CN201610580392 A CN 201610580392A CN 105970671 B CN105970671 B CN 105970671B
- Authority
- CN
- China
- Prior art keywords
- disperse
- red
- type
- blue
- dyeing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6131—Addition products of hydroxyl groups-containing compounds with oxiranes
- D06P1/6133—Addition products of hydroxyl groups-containing compounds with oxiranes from araliphatic or aliphatic alcohols
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Coloring (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The present invention relates to textile dyeing, printing technique, specifically a kind of hydrophobic textile material dye applies integrated dyeing, stamp paste composition and its application.Dyeing, stamp paste composition are consisting of dyeing, stamp thickened pulp 1-25%, thickener 0.5-10%, pH adjusting agent 0.05-3% and water 62-98.45%.The advantages of dyeing and stamp of the slurry of the present invention for hydrophobic textile materials can take into account dyeing, stamp and pigment dyeing, stamp, while guaranteeing high distillation, washing and dry, fastness to wet rubbing, again with gay colours, soft feel, while also can avoid the generation of high-concentration waste water during traditional disperse dyeing, stamp, it is dyeing, the Printing of a kind of clean and environmental protection.
Description
Technical field
The present invention relates to textile dyeing, printing technique, specifically a kind of hydrophobic textile material dye applies one dye
Material dyeing, stamp paste composition and its application.
Background technique
Textile dyeing, stamp generally can be divided into two kinds of dyeing, stamp and pigment dyeing, stamp.Dyeing, print
Flower be usually dyed by the molecular separating force or active group of dyestuff itself with fibration, stamp.Pigment dyeing, stamp
It is to be combined in a manner of physical adhesion with fabric the adhesive in pigment dyeing, printing paste.Usually dye printing
The dyeing that obtains afterwards, Printing are more environmentally friendly, and content of formaldehyde is low, and bright, color fastness is preferable, while soft, stamp
Position is tack-free；Pigment printing simple process, stamp is at low cost, generates substantially without the three wastes.
Conventional dyes dyeing, printing technology are general are as follows: and textile → stamp → drying → decatize → washing → reduction washes →
Soap → washing → dry → arrange → stamp finished product.It usually requires that dye dosage 1- is added in conventional dyes dyeing, printing paste
The auxiliary agents such as sodium alginate, sodium lignin sulfonate, naphthalene sulfonic acid-formaldehyde condensation product, dispersing agent, levelling agent, the bleeding agent of 1.5 times of amounts produce
Product, these auxiliary agents dyeing, stamp process after the completion of need wash, reduction wash and soap and etc. make its from fiber surface shell
From hence into dyeing, printing waste water.During conventional dyes dyeing simultaneously, stamp, the dye-uptake of dyestuff is generally
The dyestuff of 90-95%, remaining 5-10% are present in fiber surface after the completion of dyeing, stamp in the form of loose colour, and washing is gone back
Original can also enter in dyeing waste water during washing and soaping.These enter dyeing, the auxiliary agent in printing waste water and dyestuff just
The high COD and high chroma of dyeing waste water are caused, processing difficulty is larger, and processing cost is higher, according to authoritative statistics, print works
One myriametre chemical fiber plus material of every processing is it is necessary to 250 tons of water consumption or so, wherein 90% is color water, waste water.And most effective measure now
Also it is only to rest in the post-processing of emission reduction and Se Shui, sewage, is not eradicated effectively.These dyeing waste waters become
Perplex the obstacle of China's textile printing, the sustainable sustainable development of printing and dyeing industry.
Pigment printing technique is simply many compared with dye printing, generally textile → stamp → drying → baking → arrangement
→ stamp finished product, stamp do not have water-washing step, drying and shrink control and cross contamination, natural or synthetic thickener in the process
Removal, alkaline agent presence, surfactant and other pollutants can be ignored, be environment protection type dye, printing technology.But
It is that the colouring component that pigment printing is selected is generally pigment, itself and fiber do not have affinity, need to adhere to by adhesive
In fiber surface, and color can not generally penetrate into fibrous inside, this has resulted in the general color permeability of pigment printing product
Poor, the disadvantages of color is not bright-coloured, and color fastness is poor, not wash resistant, and feel is partially hard, and anti-yellowing property is poor.
Dyeing, stamp are combined with pigment dyeing, stamp, take into account its advantage respectively, while doing to its defect
Be complementary to one another, can yet be regarded as it is a kind of dyeing, stamp new way, the present invention is exactly to generate in such a situa-tion.
Summary of the invention
The present invention is intended to provide a kind of dye applies integrated hydrophobic textile material dyeing, stamp paste composition and its answers
With.
A kind of dye painting integrally dyeing, stamp paste composition,
Dyeing, stamp paste composition consisting of dyeing, stamp thickened pulp 1-25%, thickener 0.5-10%,
PH adjusting agent 0.05-3% and water 62-98.45%.
It is described dyeing, stamp thickened pulp by weight percentage, by the dyeing of 20-80%, print paste and 20-80%
Dyeing, printing assistant composition.
It is described dyeing, print paste be by the way that the filter cake of disperse dyes or dry powder are made into slurry with auxiliary agent and water together,
Again by micronization processes, D90=0.1-2 μm of fineness of dyeing, print paste is prepared.
The dyeing, each ingredient of print paste by weight percentage, disperse dyes (filter cake or dry powder) 20-60%, help
Agent 5-30% and water 10-75%.
The dyeing, disperse dyes are selected from print paste: C.I. disperse yellow 3, C.I. disperse yellow 5, C.I. disperse yellow 7,
C.I. disperse yellow 11, C.I. disperse yellow 23, C.I. Disperse Yellow 42, C.I. disperse yellow 49, C.I. disperse yellow 50, C.I. disperse yellow
54, C.I. disperse yellow 56, C.I. disperse yellow 60, C.I. disperse yellow 61, C.I. dispersion yellow 64, C.I. disperse yellow 71, C.I. dispersion
Yellow 79, C.I. disperse yellow 82, C.I. disperse yellow 93, C.I. disperse yellow 97, C.I. disperse yellow 104, C.I. disperse yellow 114, C.I.
Disperse yellow 119, C.I. disperse yellow 124, C.I. disperse yellow 126, C.I. disperse yellow 134, C.I. disperse yellow 163, C.I. disperse yellow
182, C.I. disperse yellow 184, C.I. disperse yellow 201, C.I. DISPERSE Yellow 211, C.I. disperse yellow 235, C.I. disperse yellow 241,
C.I. disperse orange 3, C.I. disperse orange 5, C.I. disperse orange 13, C.I. disperse orange 20, C.I. disperse orange 25, C.I. disperse orange 25:
1, C.I. disperse orange 29, C.I. disperse orange 30, C.I. disperse orange 31, C.I. disperse orange 32, C.I. disperse orange 37, C.I. disperse orange
38:2, C.I. disperse orange 41, C.I. disperse orange 44, C.I. disperse orange 61, C.I. disperse orange 62, C.I. disperse orange 73, C.I. point
Dissipate orange 76, C.I. disperse orange 97, C.I. disperse orange 127, C.I. disperse orange 288, C.I. Red-1 200, C.I. disperse red 4, C.I.
Disperse red 5, C.I. disperse red 9, C.I. dispersion red 11, C.I. DISPERSE Red 13, C.I. disperse red 50, C.I. disperse red 53, C.I.
Disperse red 54, C.I. disperse red 54: 1, C.I. disperse red 60, C.I. disperse red 65, C.I. disperse red 72, C.I. disperse red 73,
C.I. disperse red 74, C.I. disperse red 82, C.I. disperse red 86, C.I. disperse red 91, C.I. disperse red 92, C.I. disperse red
118, C.I. DISPERSE Red 13 5, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I. Red-1 200 53, C.I. Red 167,
C.I. Red 167: 1, C.I. Red-1 200 77, C.I. Red-1 200 79, C.I. disperse red 200, C.I. disperse red 210, C.I.
Disperse red 220, C.I. disperse red 277, C.I. Disperse Red 278, C.I. Disperse Red 343, C.I. disperse red 356, C.I. disperse violet
1, C.I. disperse violet 8, C.I. disperse violet 17, C.I. disperse violet 26, C.I. disperse violet 27, C.I. disperse violet 28, C.I. disperse violet
33, C.I. disperse violet 38, C.I. disperse violet 43, C.I. disperse violet 63, C.I. disperse violet 77, C.I. disperse violet 93, C.I. dispersion
Purple 93:1, C.I. disperse blue 3, C.I. disperse blue 14, C.I. disperse blue 20, C.I. disperse blue 26, C.I. disperse blue 27, C.I. point
Dissipate indigo plant 56, C.I. Disperse Blue-56: 1, C.I. Disperse Blue-56: 2, C.I. Disperse Blue-56: 3, C.I. disperse blue 58, C.I. disperse blue
60, C.I. disperse blue 73, C.I. disperse blue 77, C.I. Disperse Blue-79, C.I. Disperse Blue-79: 1, C.I. Disperse Blue-79: 2, C.I.
Disperse blue 81, C.I. disperse blue 82, C.I. disperse blue 87, C.I. disperse blue 102, C.I. disperse blue 104, C.I. disperse blue 106,
C.I. disperse blue 118, C.I. disperse blue 143, C.I. disperse blue 148, C.I. disperse blue 165, C.I. disperse blue 165:1, C.I.
Disperse blue 165:2, C.I. disperse blue 165:3, C.I. disperse blue 183, C.I. disperse blue 183:1, C.I. disperse blue 225, C.I.
Disperse blue 257, C.I. disperse blue 270, C.I. disperse blue 281, C.I. disperse blue 291, the dispersion of C.I. disperse blue 291:1, C.I.
Indigo plant 301, C.I. disperse blue 354, C.I. disperse blue 359, C.I. disperse blue 366, C.I. disperse blue 367, C.I. disperse brown 1,
C.I. disperse brown 1:1, C.I. disperse brown 19, C.I. dispersion black one of 1 or a variety of；
Auxiliary agent is selected from polyvinyl alcohol, polyvinyl acetate, styrene and maleic anhydride multipolymer, gelatin, carboxymethyl fibre
Tie up element, carboxyethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, ethylene glycol, propylene glycol, urea, diethylene glycol (DEG), thiocarbamide, mine
One of object oils, high-carbon alcohols, polyethers or organic silicon defoaming agent or a variety of and sodium alginate, polyacrylamide, N-
Methyl-N oleoyl tarine sodium, naphthalene sulfonic acids-formaldehyde condensation products, castor oil ethylene oxide condensate, coconut oleyl alcohol epoxy
Oxide condensate, triisopropylbenzene phenol ethylene oxide condensates, sodium lignin sulfonate, castor oil oleic alcohol, dodecyl
Benzene sulfonic acid sodium salt, metacresol-formaldehyde-sodium sulfite condensation product extension agent S S, diffusion agent N, dispersing agent MF, dispersing agent CNF, methyl naphthalene
Sulfonic formaldehyde condensation compound, cresols (or phenol) sodium sulfonate formaldehyde condensation products, beta naphthal sulfonic formaldehyde condensation compound, phenolic resin sulfonation
Object, dispersing agent C S；Fatty acid salt form anionic surfactant, sulfonate type anionic surfactant, sulfate type yin from
Sub- surfactant, phosphate salt form anionic surfactant, sulfosuccinic acid ester type anionic surfactant, fatty acid
Type anionic surfactant, peptide condensation product type anionic surfactant；Ammonium salt type cationic surfactant, quaternary
Cationic surfactant, oxidation ammonium type cationic surfactant, betaine type amphoteric ionic surface active agent, imidazoline type
Zwitterionic surfactant, amino acid type amphoteric ionic surface active agent, phosphatide type zwitterionic surfactant, fatty alcohol
Ether type nonionic surfactant, alkylamine ether type nonionic surfactant, gathers alkyl phenol ether type nonionic surfactant
Ether type nonionic surfactant, fatty acid polyglycol alkoxide ester type nonionic surfactant, castor oil polyoxyethylene type are non-
Ionic surface active agent, lanolin polyoxyethylene non-ionic surfactant, sorbitol polyoxyethylene type non-ionic surface are living
Property agent, glycerol ester type nonionic surfactant, sorbierite ester type nonionic surfactant, fatty acid alkanamine type nonionic table
Face activating agent, alkylolamides type nonionic surfactant, alkyl glycosides type nonionic surfactant, alkyl pyrrolidone
Type nonionic surfactant, alcohol surfactants, acids surfactant, amine surfactants, amides surface are living
Property agent, esters surface active agent, ether surfactant, ketone surfactant, polymer types of surfactants, castor-oil plant oils
Surfactant, wool lipid surfactant, three polyglyceryl laurates, four polyglyceryl laurates, six polyglycereol laurels
One of acid esters, Tripolyglycerol monostearates, three Unigly GO 102Ss or a variety of mixing；
The wet concentration is one or more from tap water, deionized water, distilled water, high purity water, ultrapure water.
Preferred coloring agent is selected from: C.I. disperse yellow 49, C.I. disperse yellow 50, C.I. disperse yellow 54, C.I. dispersion yellow 64,
C.I. disperse yellow 71, C.I. disperse yellow 79, C.I. disperse yellow 82, C.I. disperse yellow 93, C.I. disperse yellow 114, C.I. disperse yellow
119, C.I. disperse yellow 134, C.I. disperse yellow 163, C.I. disperse yellow 182, C.I. disperse yellow 184, C.I. disperse yellow 201,
C.I. DISPERSE Yellow 211, C.I. disperse yellow 241, C.I. disperse orange 25, C.I. disperse orange 25: 1, C.I. disperse orange 29, C.I. dispersion
Orange 30, C.I. disperse orange 31, C.I. disperse orange 44, C.I. disperse orange 73, C.I. disperse orange 76, C.I. disperse orange 97, C.I. point
Dissipate orange 288, C.I. disperse red 54, C.I. disperse red 54: 1, C.I. disperse red 60, C.I. disperse red 73, C.I. disperse red 74,
C.I. disperse red 92, C.I.C.I. DISPERSE Red 13 5, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I. Red-1 200 53, C.I.
Red 167, C.I. Red 167: 1, C.I. Red-1 200 79, C.I. disperse red 277, C.I. Disperse Red 278, C.I. dispersion
Red 343, C.I. disperse red 356, C.I. disperse violet 33, C.I. disperse violet 38, C.I. disperse violet 43, C.I. disperse violet 63, C.I.
Disperse violet 77, C.I. disperse violet 93, C.I. disperse violet 93:1, C.I. Disperse Blue-56, C.I. Disperse Blue-56: 1, C.I. disperse blue
56:2, C.I. Disperse Blue-56: 3, C.I. disperse blue 60, C.I. disperse blue 73, C.I. Disperse Blue-79, C.I. Disperse Blue-79: 1,
C.I. Disperse Blue-79: 2, C.I. disperse blue 102, C.I. disperse blue 104, C.I. disperse blue 106, C.I. disperse blue 118, C.I. point
Dissipate indigo plant 165, C.I. disperse blue 165:1, C.I. disperse blue 165:2, C.I. disperse blue 165:3, C.I. disperse blue 183, C.I. point
Dissipate indigo plant 183:1, C.I. disperse blue 291, C.I. disperse blue 291:1, C.I. disperse blue 354, C.I. disperse blue 359, C.I. dispersion
One of indigo plant 366, C.I. disperse blue 367, C.I. disperse brown 19 are a variety of；
Preferred promoter is one of mineral oils, high-carbon alcohols, polyethers or organic silicon defoaming agent or a variety of and naphthalene
Sulfonic acid-formaldehyde condensation product, castor oil ethylene oxide condensate, coconut oleyl alcohol ethylene oxide condensate, sodium lignin sulfonate, castor-oil plant
Oily oleic alcohol, neopelex, extension agent S S, diffusion agent N, dispersing agent MF, dispersing agent CNF, methyl naphthalene sulfonic acid
Formaldehyde condensation products, beta naphthal sulfonic formaldehyde condensation compound, dispersing agent C S, fatty acid salt form anionic surfactant, sulfonate type
Anionic surfactant, sulfate type anionic surfactant, phosphate salt form anionic surfactant, sulfosuccinic
Acid esters type anionic surfactant, betaine type amphoteric ionic surface active agent, imidazoline type zwitterionic surfactant,
Amino acid type amphoteric ionic surface active agent, phosphatide type zwitterionic surfactant, fatty alcohol ether type non-ionic surface active
Agent, alkyl phenol ether type nonionic surfactant, alkylamine ether type nonionic surfactant, polyether-type nonionic surface-active
Agent, fatty acid polyglycol alkoxide ester type nonionic surfactant, castor oil polyoxyethylene type nonionic surfactant, wool
Rouge polyoxyethylene non-ionic surfactant, sorbitol polyoxyethylene type nonionic surfactant, glycerol ester type nonionic
Surfactant, sorbierite ester type nonionic surfactant, fatty acid alkanamine type nonionic surfactant, alkylolamides
Type nonionic surfactant, alkyl glycosides type nonionic surfactant, alkyl pyrrolidone type nonionic surfactant,
The mixing of one or more of ethylene glycol, propylene glycol, urea, diethylene glycol (DEG).
The dyeing, printing assistant composition by weight percentage, adhesive 25-80%, softening agent 0.5-5%, are crosslinked
Agent 0.1-5%, other auxiliary agents 1-5% and water 5-73.4%.
Described adhesive is selected from pure C adhesive, phenylpropyl alcohol adhesive, butylbenzene adhesive, butyronitrile adhesive, silicone adhesive
One of agent, organosilicon modified acrylic ester binding agent, polyurethane binder are a variety of；
The softening agent is selected from: quaternary ammonium salt cationic type softening agent, fatty acid ester type cationic softener, right wax pattern
Cationic softener, polyethylene cationic softener, organic siliconresin type cationic softener, organic silicon are soft
Agent, fatty acid salt film class softening agent, high molecular polythene wax it is one or more；
The crosslinking agent is selected from: cyanate crosslinking agent (JQ-1, JQ-1E, JQ-2E, JQ-4, JQ-5, JQ-6, PAPI, can
Emulsify MDI, tetraisocyanate, blocked isocyanate etc.), polyalcohols crosslinking agent (polyethylene glycol, polypropylene glycol, trihydroxy methyl
Propane etc.), glycidol ethers crosslinking agent, inorganic matter crosslinking agent (zinc chloride, aluminium chloride, aluminum sulfate, sulphur, boric acid etc.) has
Machine monomer class crosslinking agent (styrene, α-methylstyrene, acrylonitrile, acrylic acid, methacrylic acid, glyoxal, aziridine etc.),
Organic silicon crosslinking agent (ethyl orthosilicate, methyl orthosilicate, trimethicone, amino modified siloxanes, carboxy-modified silicon oxygen
Alkane, hydroxyl modification siloxanes, vinylsiloxane etc.), benzene sulfonic acid class crosslinking agent (p-methyl benzenesulfonic acid, paratoluensulfonyl chloride etc.),
Acrylic ester cross-linking agent (diacrylate -1,4- butanediol ester, ethylene glycol dimethacrylate, TAC, butyl acrylate,
HEA, HPA, HPMA, MMA etc.), organic peroxide crosslinking agent (cumyl peroxide, peroxidating 2,4- dichloro-benzoyl
Deng), metallo-organic compound crosslinking agent (aluminium isopropoxide, zinc acetate, titanium acetylacetone etc.), multi-functional polycarbodiimide class is handed over
Join one of agent or a variety of；
Other described auxiliary agents are selected from: sodium alginate, polyacrylamide, N- methyl-N oleoyl tarine sodium, naphthalene sulphur
Acid-formaldehyde condensation products, castor oil ethylene oxide condensate, coconut oleyl alcohol ethylene oxide condensate, triisopropyl phenol epoxy second
Alkane condensation product, sodium lignin sulfonate, castor oil oleic alcohol, neopelex, metacresol-formaldehyde-sodium sulfite
Condensation product extension agent S S, diffusion agent N, dispersing agent MF, dispersing agent CNF, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, cresols (or phenol) sulphur
Sour sodium formaldehyde condensation product, beta naphthal sulfonic formaldehyde condensation compound, phenolic resin sulfonated bodies, dispersing agent C S；Fatty acid salt form, sulfonate
Type, sulfate type, phosphate salt form, sulfosuccinic acid ester type, fatty acid/peptide condensation product type anionic surfactant；Ammonium salt
Type, quaternary, oxidation ammonium type cationic surfactant；Betaine type, imidazoline type, amino acid pattern, phosphatide type both sexes from
Sub- surfactant；Fatty alcohol ether type, alkyl phenol ether type, alkylamine ether type, polyether-type, fatty acid polyglycol alkoxide ester type, castor
Sesame oil polyoxyethylene-type, lanolin polyoxyethylene-type, sorbitol polyoxyethylene type, glycerol ester type, sorbierite ester type, fatty acid alkane
Amine type, alkylolamides type, alkyl glycosides type, alkyl pyrrolidone type nonionic surfactant；Alcohols, acids, amine, acyl
The other surfaces activating agents such as amine, esters, ethers, ketone, polymerization species, castor-oil plant oils, wool lipid；Polyvinyl alcohol, poly- second
Sour ethylene, styrene and maleic anhydride multipolymer, gelatin, carboxymethyl cellulose, carboxyethyl cellulose, hydroxylmethyl cellulose
Element, hydroxyethyl cellulose, ethylene glycol, propylene glycol, urea, diethylene glycol (DEG), thiocarbamide, organic silicon defoamer, mineral oil antifoam agent, polyethers
Class defoaming agent, three polyglyceryl laurates, four polyglyceryl laurates, six polyglyceryl laurates, trimerization glycerol monostearate
One of ester, three Unigly GO 102Ss are a variety of；
The wet concentration is from one or more of tap water, deionized water, distilled water, high purity water, ultrapure water.
The thickener is selected from: white carbon black, sodium bentonite, organobentonite, diatomite, attapulgite soil, molecular sieve,
The inorganic thickening agents such as Silica hydrogel, methylcellulose, ethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxy propyl cellulose
The cellulose thickeners such as element, carboxymethyl cellulose, carboxyethyl cellulose, carboxy-propyl cellulose, starch, gelatin, sodium alginate,
Casein, guar gum, chitosan, gum arabic, xanthan gum, soybean protein glue, natural rubber, lanolin, agar etc. are natural
Macromolecule and its derivative, polyacrylamide, polyvinyl alcohol, polyvinylpyrrolidone, polyoxyethylene, modified paraffin resin, card
Wave resin, polyacrylic acid, Polyacrylate Emulsion, butadiene rubber, butadiene-styrene rubber, polyurethane, modified polyurea, low molecular weight polycaprolactone
Ethylene waxes etc. synthesize macromolecule thickener, and one in the solvay-types organo-metallic compound thickener such as amino alcohol solvay-type titanate esters
Kind is a variety of；
PH adjusting agent is selected from: citric acid, adipic acid, potassium citrate, lactic acid, fumaric acid, phosphate hydrogen tri-sodium, tartaric acid, lemon
One sodium of lemon acid, malic acid, phosphoric acid, acetic acid, the acidity regulators such as hydrochloric acid, 2-amino-2-methyl-1-propanol, N- methylethanolamine,
Monoethanolamine, diethanol amine, triethanolamine, butylethanolamine, N- aminopropyl-methylethanolamine, 2- amino -2- ethyl -1,3-
Propylene glycol, butyl diethanolamine etc. have alkanolamine, ammonium hydroxide, sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, bicarbonate
One of inorganic bases regulator such as sodium, saleratus is a variety of.
A kind of dye applies the application of integrated dyeing, stamp paste composition, and the paste composition is in dyeing, stamp
Application；Wherein, dyeing, printing paste range of viscosities be selected from 500-30000 centipoise, pH range be selected from 4-10.
Color development process is selected from one of decatize or baking in the dye painting one stamp, dyeing slurry technique for applying；Hair
Color temperature is 160-210 DEG C；The color development time is 1-30 minutes；Textile after color development can be washed, soaps, be washed again, can also
Directly washing after dry, or without wash, process of soaping；Concrete technology is selected from: textile → stamp → drying → decatize →
It washes → soaping → and washes → drying → and arrange → stamp finished product, textile → stamp → drying → decatize → washing → drying →
Arrangement → stamp finished product, textile → stamp → drying → decatize → drying → arrangement → stamp finished product, textile → stamp →
Drying → baking →, which washes → soaping → and washes → drying →, arranges → stamp finished product, and textile → stamp → drying → baking →
Washing → drying → arrangement → stamp finished product, the dyeing such as textile → stamp → drying → baking → arrangement → stamp finished product, print
One of flower process.
Specific: hydrophobic textile material dyeing, printing technology method, technical process is by textile to be processed successively through printing
Flower → drying → color development → post-processing, and then obtain stamp finished product；Wherein, color development and arrangement interprocedual can be washed again and be dried
It is dry；The color development temperature is 160-210 DEG C；The color development time is 1-30 minutes；The last handling process, which can be used, to be washed → soaps
→ washing → drying → arrangement, washing → drying → arrangement individually arrange.The color development is by the way of decatize or baking；Institute
Stating washing can be used multiple washing and/or mode of soaping.
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → decatize →, which washes → soaping → and washes → drying →, to be arranged, and then obtains stamp finished product.
Wherein steam temperature is 160-210 DEG C, and steaming time is 1-30 minutes；
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → decatize → washing → drying → arrangement, and then obtain stamp finished product.
Wherein steam temperature is 160-210 DEG C, and steaming time is 1-30 minutes；
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → decatize → arrangement, and then obtain stamp finished product.Wherein steam temperature is 160-210 DEG C, and steaming time is 1-30 points
Clock；
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → baking →, which washes → soaping → and washes → drying →, to be arranged, and then obtains stamp finished product.Wherein stoving temperature is
160-210 DEG C, baking time is 1-30 minutes；
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → baking → washing → drying → arrangement, and then obtain stamp finished product.Wherein stoving temperature is 160-210 DEG C, is baked
Time is 1-30 minutes；
A kind of dyeing of hydrophobic textile material, printing technology method, the technique are textile to be processed successively through stamp
→ drying → baking → arrangement, and then obtain stamp finished product.Wherein stoving temperature is 160-210 DEG C, and baking time is 1-30 points
Clock.
Advantage for present invention:
Disperse dyeing of the present invention, stamp apply one dyeing, stamp for disperse dyes dye with paste composition.The slurry
The dyeing of shape composition, printing paste are by dyeing, stamp thickened pulp, dyeing, stamp slurry auxiliary agent, dyeing, printing paste thickener and water group
At.When carrying out stamp for hydrophobic textile material using the paste composition, process is similar to conventional dyes stamp before stamp,
Can by cylinder, flat screen printing machine by paste composition printing in textile material surface.During high temperature color development, the overwhelming majority point
Dyestuff is dissipated through molecular separating force in conjunction with hydrophobic fiber material, and the printing assistant in concentrator is in disperse dyes high temperature color development
Meanwhile crosslinking curing forms a film, and the loose colour not in conjunction with fiber is made to be adhered to fiber surface.Slurry of the present invention is used for hydrophobic textile
The advantages of dyeing of material and stamp can take into account dyeing, stamp and pigment dyeing, stamp is guaranteeing high distillation, washing
While with dry, fastness to wet rubbing, and with gay colours, soft feel, while it also can avoid traditional disperse dyes dye
The generation of color, stamp process middle and high concentration color water, is disperse dyeing, the Printing of a kind of clean and environmental protection.
And it is dyed using above-mentioned paste composition, stamp, if technique, which is selected, the processes such as washes, soaps, washes spinning
The wash water COD of fabric is between 30-2000ppm, part kind < 200ppm, part kind < 50ppm；Coloration (extension rate)
< 200, part kind coloration (extension rate) < 80, part kind coloration (extension rate) < 30；
Specific implementation method
Embodiment below can be with a person of ordinary skill in the art will more fully understand the present invention, but not with any side
The formula limitation present invention.The raw materials used specification of following embodiment is as follows: dyestuff C.I. Disperse Blue-56, C.I. disperse yellow 54, C.I. point
Dissipate red 60, C.I. Disperse Blue-79, C.I. disperse orange 30, C.I. Red 167, C.I. disperse blue 291:1, C.I. disperse orange 288,
C.I. disperse violet 93 etc. is commercial dispersants dyestuff original powder, sodium lignin sulfonate, neopelex, laruyl alcohol polyoxy second
Olefinic carboxylic acid sodium, dodecyl polyoxyethylene sodium sulphate, dispersing agent NNO, dispersing agent MF, dispersing agent CNF, surfactant B C-50,
Surfactant LS-60, surfactant LS-70, organosilicon modified acrylic ester binding agent SY-8001, ethylene glycol are city
Industrial goods are sold, water used is deionized water.Device therefor includes:Test-type dispersion machine, resistance to (Shanghai) machine of speeding
Tool Instrument Ltd., LHP-0.4 type ceramic laboratory horizontal sand mill, Shanghai De Yu mechanical & electronic equipment corporation, Ltd entirely,
Along instrument experimental facilities Co., Ltd, H-TS-III high temperature evaporates baking oven, Foshan City for APV2000 test-type high pressure homogenizer, Shanghai
Ya Nuo precision machinery Manufacturing Co., Ltd, it is public that DH6-9070 electric heating constant-temperature blowing drying box, Gongyi City give magnificent instrument Limited Liability
Department.
Every application performance detection method refers to following national standard:
The general condition regulation of GB/T 2374-2007 dyeing measurement
GB/T 4841.1-2006 dyeing standard depth colour atla 1/1
The measurement of GB/T 2394-2013 disperse dyes coloured light and intensity
The measurement of GB/T 2397-2012 disperse dyes lifting force
GB/T 3921-2008 textile color stability tests fastness to soaping
GB/T 3920-2008 textile color stability tests colour fastness to rubbing
GB/T 6152-1997 textile color stability tests color fastness to hot pressing
GB/T 8427-2008 textile color stability tests the color fastness of resistance to artificial light: xenon arc
Embodiment 1
(1) dyeing, the preparation of print paste B-1
Surfactant B C-50 45g, sodium lignin sulfonate 50g, ethylene glycol 30g and water 525g are added to dispersion tank
In, dispersion stirring make its it is complete it is molten after, C.I. Disperse Blue-56 original powder 350g is added thereto, starts dispersion machine, high speed dispersion 2 hours
Afterwards, dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained slurry will be ground after grinding
Material homogenizes 2 times by high pressure homogenizer, obtains blue dyes dyeing, print paste B-1 1000g, fineness d50≤0.5 μm,
PH=6.8.
(2) dyeing, the preparation of printing assistant
It is added to deionized water 227g in dispersion tank, opens dispersion machine, stir at low speed down, successively adds into dispersion tank
Enter surfactant FC-1 15g, bleeding agent SA-50 30g, diffusant WAX 28g, silicone softening agent 208C 55g, is crosslinked
Agent CLA-80 45g, organosilicon modified acrylic ester binding agent SY-800 600g add each raw material, dispersion stirring 30 minutes.?
To dyeing, printing assistant Z-1 1000g, pH=6.7, viscosity 1300mPa.S (NDJ-1 type rotor viscosimeter, 2# rotor, 12r/
min)。
(3) dyeing, the preparation of stamp thickened pulp B-1
Dyeing that step (1) is prepared, print paste 500g are added in dispersion machine dispersion tank, stir it is lower slowly plus
Enter dyeing, printing assistant Z1 500g, is dyed after mixing evenly, stamp thickened pulp B-1, pH=6.7, viscosity 1550mPa.S
(NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste B-1
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into dyeing, stamp thickened pulp B-1 20g, and dispersion dyed after mixing evenly, printing paste
B-1 1000g, viscosity 2520mPa.S (NDJ-1 rotational viscometer, 3# rotor, 30r/min)
Using be prepared dyeing, printing paste carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → drying →
Baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Stamp at
Every detection data of product is as follows:
Embodiment 2
(1) dyeing, the preparation of print paste Y-1
Surfactant LS-60 45g, alkaline sodium lignin sulfonate 50g, ethylene glycol 30g and water 530g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, 54 original powder 345g of C.I. disperse yellow is added thereto, starts dispersion machine, high speed dispersion 2 is small
Dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained grinding after grinding by Shi Hou
Slurry homogenizes 2 times by high pressure homogenizer, obtains weld dyeing, print paste Y-1 1000g, fineness d50≤0.7 μ
M, pH=7.2.
(2) dyeing, the preparation of printing assistant Z-1, with embodiment 1
(3) dyeing, the preparation of stamp thickened pulp Y-1
Dyeing that step (1) is prepared, print paste Y-1 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant Z-1 500g is added, it is dyed after mixing evenly, stamp thickened pulp Y-1, pH=7.0, viscosity
1500mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste Y-1
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into yellow dyeing, stamp thickened pulp Y-1 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry Y-1 1000g, viscosity 2500mPa.S (NDJ-1 rotational viscometer, 3# rotor, 30r/min)
Using be prepared dyeing, printing paste Y-1 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.
Every detection data of stamp finished product is as follows:
Embodiment 3
(1) dyeing, the preparation of print paste R-1
Surfactant LS-70 45g, alkaline sodium lignin sulfonate 50g, ethylene glycol 30g and water 530g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, C.I. disperse red 60 original powder 345g is added thereto, starts dispersion machine, high speed dispersion 2 is small
Dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained grinding after grinding by Shi Hou
Slurry homogenizes 2 times by high pressure homogenizer, obtains orchil dyeing, print paste R-1 1000g, fineness d50≤0.7 μ
M, pH=7.2.
(2) dyeing, the preparation of printing assistant Z-1, with embodiment 1
(3) dyeing, the preparation of stamp thickened pulp R-1
Dyeing that step (1) is prepared, print paste R-1 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant 500g is added, it is dyed after mixing evenly, stamp thickened pulp R-1, pH=7.0, viscosity
1450mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste R-1
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into red staining, stamp thickened pulp R-1 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry R-1 1000g, viscosity 1500mPa.S (NDJ-1 rotational viscometer, 3# rotor, 30r/min)
Using be prepared dyeing, printing paste R-1 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 4
(1) dyeing, the preparation of print paste B-2
Surfactant B C-50 45g, dispersing agent MF 50g, ethylene glycol 30g and water 525g are added in dispersion tank, point
Scattered stirring make its it is complete it is molten after, C.I. Disperse Blue-79 original powder 350g is added thereto, starts dispersion machine, will after high speed dispersion 2 hours
Dispersion pulp squeezes into horizontal sand mill and carries out circular grinding, and milling time 10 hours, the slurry for obtaining grinding after grinding passed through
It crosses high pressure homogenizer to homogenize 2 times, obtains blue dyes dyeing, print paste B-2 1000g, fineness d50≤0.5 μm, pH=
6.8。
(2) dyeing, the preparation of printing assistant
It is added to deionized water 227g in dispersion tank, opens dispersion machine, stir at low speed down, successively adds into dispersion tank
Enter surfactant EL-40 15g, bleeding agent SA-60 30g, diffusant RPG 28g, silicone softening agent RM-1 55g, is crosslinked
Agent TAC 45g, organosilicon modified acrylic ester binding agent SY-800600g add each raw material, dispersion stirring 30 minutes.It is contaminated
Color, printing assistant Z-2 1000g, pH=6.7, viscosity 1350mPa.S (NDJ-1 type rotor viscosimeter, 2# rotor, 12r/min).
(3) dyeing, the preparation of stamp thickened pulp B-2
Dyeing that step (1) is prepared, print paste 500g are added in dispersion machine dispersion tank, stir it is lower slowly plus
Enter dyeing, printing assistant Z-2 500g, is dyed after mixing evenly, stamp thickened pulp B-2, pH=6.7, viscosity
1500mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste B-2
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into dyeing, stamp thickened pulp B-2 20g, and dispersion dyed after mixing evenly, printing paste
B-2 1000g, viscosity 2500mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → drying →
Baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Stamp at
Every detection data of product is as follows:
Embodiment 5
(1) dyeing, the preparation of print paste Y-2
Surfactant LS-60 45g, dispersing agent CNF 50g, ethylene glycol 30g and water 530g are added in dispersion tank,
Dispersion stirring make its it is complete it is molten after, 30 original powder 345g of C.I. disperse orange is added thereto, starts dispersion machine, after high speed dispersion 2 hours,
Dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained slurry will be ground after grinding
It homogenizes 2 times by high pressure homogenizer, obtains weld dyeing, print paste Y-2 1000g, fineness d50≤0.7 μm, pH
=7.2.
(2) dyeing, the preparation of printing assistant Z-2, with embodiment 4
(3) dyeing, the preparation of stamp thickened pulp Y-2
Dyeing that step (1) is prepared, print paste Y-2 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant Z-2 500g is added, dye is obtained after mixing evenly applies one dyeing, stamp thickened pulp Y-2, pH=7.0,
Viscosity 1550mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste Y-2
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into yellow dyeing, stamp thickened pulp Y-2 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry Y-2 1000g, viscosity 2520mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste Y-2 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 6
(1) dyeing, the preparation of print paste R-2
Surfactant LS-60 45g, diffusion agent N 50g, ethylene glycol 30g and water 530g are added in dispersion tank, point
Scattered stirring make its it is complete it is molten after, C.I. Red 167 original powder 345g is added thereto, starts dispersion machine, after high speed dispersion 2 hours,
Dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained slurry will be ground after grinding
It homogenizes 2 times by high pressure homogenizer, obtains orchil dyeing, print paste R-2 1000g, fineness d50≤0.7 μm, pH
=7.2.
(2) dyeing, the preparation of printing assistant Z-2, with embodiment 4
(3) dyeing, the preparation of stamp thickened pulp R-2
Dyeing that step (1) is prepared, print paste R-2 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant 500g is added, it is dyed after mixing evenly, stamp thickened pulp R-2, pH=7.0, viscosity
1500mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste R-2
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into red staining, stamp thickened pulp R-2 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry R-2 1000g, viscosity 2520mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste R-2 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 7
(1) dyeing, the preparation of print paste B-3
Surfactant B C-50 45g, sodium lignin sulfonate 50g, ethylene glycol 30g and water 525g are added to dispersion tank
In, dispersion stirring make its it is complete it is molten after, C.I. disperse blue 291:1 original powder 350g is added thereto, starts dispersion machine, high speed dispersion 2
After hour, dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, is obtained grinding after grinding
Slurry homogenize 2 times by high pressure homogenizer, obtain blue dyes dyeing, print paste B-3 1000g, fineness d50≤0.5
μm, pH=6.8.
(2) dyeing, the preparation of printing assistant
It is added to deionized water 227g in dispersion tank, opens dispersion machine, stir at low speed down, successively adds into dispersion tank
Enter surfactant FM 15g, bleeding agent FN-2 30g, diffusant PBE 28g, high molecular polythene wax PEC-1 55g, crosslinking
Agent CTA 45g, organosilicon modified acrylic ester binding agent SY-800 600g add each raw material, dispersion stirring 30 minutes.It obtains
Dyeing, printing assistant Z-3 1000g, pH=6.7, viscosity 1350mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/
min)。
(3) dyeing, the preparation of stamp thickened pulp B-3
Dyeing that step (1) is prepared, print paste 500g are added in dispersion machine dispersion tank, stir it is lower slowly plus
Enter dyeing, printing assistant Z-3 500g, is dyed after mixing evenly, stamp thickened pulp B-2, pH=6.7, viscosity
1550mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste B-3
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into dyeing, stamp thickened pulp B-3 20g, and dispersion dyed after mixing evenly, printing paste
B-3 1000g, viscosity 2480mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → drying →
Baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Stamp at
Every detection data of product is as follows:
Embodiment 8
(1) dyeing, the preparation of print paste Y-3
Surfactant LS-60 45g, alkaline sodium lignin sulfonate 50g, ethylene glycol 30g and water 530g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, 288 original powder 345g of C.I. disperse orange is added thereto, starts dispersion machine, high speed dispersion 2
After hour, dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, is obtained grinding after grinding
Slurry homogenize 2 times by high pressure homogenizer, obtain weld dyeing, print paste Y-3 1000g, fineness d50≤0.7
μm, pH=7.2.
(2) dyeing, the preparation of printing assistant Z-3, with embodiment 7
(3) dyeing, the preparation of stamp thickened pulp Y-3
Dyeing that step (1) is prepared, print paste Y-3 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant Z-3 500g is added, it is dyed after mixing evenly, stamp thickened pulp Y-3, pH=7.0, viscosity
1600mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste Y-3
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into yellow dyeing, stamp thickened pulp Y-3 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry Y-3 1000g, viscosity 2480mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste Y-3 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 9
(1) dyeing, the preparation of print paste R-3
Surfactant LS-60 45g, alkaline sodium lignin sulfonate 50g, ethylene glycol 30g and water 530g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, 93 original powder 345g of C.I. disperse violet is added thereto, starts dispersion machine, high speed dispersion 2 is small
Dispersion pulp is squeezed into horizontal sand mill and carries out circular grinding, milling time 10 hours, obtained grinding after grinding by Shi Hou
Slurry homogenizes 2 times by high pressure homogenizer, obtains orchil dyeing, print paste R-3 1000g, fineness d50≤0.7 μ
M, pH=7.2.
(2) dyeing, the preparation of printing assistant Z-3, with embodiment 7
(3) dyeing, the preparation of stamp thickened pulp R-3
Dyeing that step (1) is prepared, print paste R-3 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant 500g is added, it is dyed after mixing evenly, stamp thickened pulp R-3, pH=7.0, viscosity
1500mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste R-3
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into red staining, stamp thickened pulp R-3 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry R-2 1000g, viscosity 2520mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste R-3 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 10
(1) dyeing, the preparation of print paste Y-4
Surfactant LS-60 45g, alkaline sodium lignin sulfonate 50g, ethylene glycol 30g and water 530g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, 288 original powder 45g, C.I. disperse yellow of C.I. disperse orange, 54 original powder 300g is added thereto,
Start dispersion machine, after high speed dispersion 2 hours, by dispersion pulp squeeze into horizontal sand mill carry out circular grinding, milling time 10 hours,
The slurry that grinding obtains is homogenized 2 times by high pressure homogenizer after grinding, obtains weld dyeing, print paste Y-
41000g, fineness d50≤0.7 μm, pH=7.1.
(2) dyeing, the preparation of printing assistant Z-1, with embodiment 1
(3) dyeing, the preparation of stamp thickened pulp Y-4
Dyeing that step (1) is prepared, print paste Y-4 500g are added in dispersion machine dispersion tank, stirred lower slow
It is slow that dyeing, printing assistant Z-1 500g is added, it is dyed after mixing evenly, stamp thickened pulp Y-4, pH=6.9, viscosity
1750mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste Y-4
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, is stirring evenly and then adding into yellow dyeing, stamp thickened pulp Y-4 20g, and dispersion is dyed after mixing evenly, printed
Flower slurry Y-4 1000g, viscosity 2480mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste Y-4 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Embodiment 11
(1) dyeing, the preparation of print paste BL-1
Surfactant LS-60 47g, alkaline sodium lignin sulfonate 55g, ethylene glycol 30g and water 523g are added to dispersion
In tank, dispersion stirring make its it is complete it is molten after, 288 original powder 95g, C.I. Red 167 original powder 50g of C.I. disperse orange is added thereto,
C.I. Disperse Blue-79 original powder 150g, C.I. disperse blue 291:1 original powder 50g, starting dispersion machine will disperse after high speed dispersion 2 hours
Slurry squeezes into horizontal sand mill and carries out circular grinding, and milling time 10 hours, the slurry for obtaining grinding after grinding was through excessively high
Pressure homogenizer homogenizes 2 times, obtains black dyes dyeing, print paste BL-1 1000g, fineness d50≤0.7 μm, pH=6.8.
(2) dyeing, the preparation of printing assistant Z-2, with embodiment 4
(3) dyeing, the preparation of stamp thickened pulp BL-1
Dyeing that step (1) is prepared, print paste BL-1 500g are added in dispersion machine dispersion tank, under stirring
It is slowly added to dyeing, printing assistant Z-2 500g, is dyed after mixing evenly, stamp thickened pulp BL-1, pH=6.9, viscosity
1750mPa.S (NDJ-1 type rotational viscometer, 2# rotor, 12r/min).
(4) dyeing, the preparation of printing paste BL-1
By in deionized water 960g water, it is added in dispersion machine dispersion tank, starts dispersion machine, be slowly added to increase under high-speed stirred
Thick dose of PF 20g, be stirring evenly and then adding into yellow dyeing, stamp thickened pulp BL-1 20g, dispersion dyed after mixing evenly,
Printing paste Y-4 1000g, viscosity 2480mPa.S (NDJ-1 type rotational viscometer, 3# rotor, 30r/min).
Using be prepared dyeing, printing paste BL-1 carry out PLATE SCREAM PRINTING, printing technology are as follows: textile → stamp → baking
Dry → baking → arrangement → stamp finished product, in which: drying temperature is 100 DEG C, 10 minutes, and stoving temperature is 180 DEG C, 3 minutes.Print
Every detection data of flower finished product is as follows:
Claims (2)
1. a kind of dye applies one dyeing, stamp paste composition, it is characterised in that: dyeing, stamp paste composition its group
As dyeing, stamp thickened pulp 1-25%, thickener 0.5-10%, pH adjusting agent 0.05-3% and water 62-98.45%；
It is described dyeing, stamp thickened pulp by weight percentage, by the dyeing of the dyeing of 20-80%, print paste and 20-80%,
Printing assistant composition；
The dyeing, print paste then are led to by the way that the filter cake of disperse dyes or dry powder are made into slurry with auxiliary agent and water together
Micronization processes are crossed, D90=0.1-2 μm of fineness of dyeing, print paste is prepared；
Disperse dyes are selected from the dyeing, print paste: C.I. disperse yellow 3, C.I. disperse yellow 5, C.I. disperse yellow 7, C.I.
Disperse yellow 11, C.I. disperse yellow 23, C.I. Disperse Yellow 42, C.I. disperse yellow 49, C.I. disperse yellow 50, C.I. disperse yellow 54,
C.I. disperse yellow 56, C.I. disperse yellow 60, C.I. disperse yellow 61, C.I. dispersion yellow 64, C.I. disperse yellow 71, C.I. disperse yellow
79, C.I. disperse yellow 82, C.I. disperse yellow 93, C.I. disperse yellow 97, C.I. disperse yellow 104, C.I. disperse yellow 114, C.I. point
Dissipate Huang 119, C.I. disperse yellow 124, C.I. disperse yellow 126, C.I. disperse yellow 134, C.I. disperse yellow 163, C.I. disperse yellow
182, C.I. disperse yellow 184, C.I. disperse yellow 201, C.I. DISPERSE Yellow 211, C.I. disperse yellow 235, C.I. disperse yellow 241,
C.I. disperse orange 3, C.I. disperse orange 5, C.I. disperse orange 13, C.I. disperse orange 20, C.I. disperse orange 25, C.I. disperse orange 25:
1, C.I. disperse orange 29, C.I. disperse orange 30, C.I. disperse orange 31, C.I. disperse orange 32, C.I. disperse orange 37, C.I. disperse orange
38:2, C.I. disperse orange 41, C.I. disperse orange 44, C.I. disperse orange 61, C.I. disperse orange 62, C.I. disperse orange 73, C.I. point
Dissipate orange 76, C.I. disperse orange 97, C.I. disperse orange 127, C.I. disperse orange 288, C.I. Red-1 200, C.I. disperse red 4, C.I.
Disperse red 5, C.I. disperse red 9, C.I. dispersion red 11, C.I. DISPERSE Red 13, C.I. disperse red 50, C.I. disperse red 53, C.I.
Disperse red 54, C.I. disperse red 54: 1, C.I. disperse red 60, C.I. disperse red 65, C.I. disperse red 72, C.I. disperse red 73,
C.I. disperse red 74, C.I. disperse red 82, C.I. disperse red 86, C.I. disperse red 91, C.I. disperse red 92, C.I. disperse red
118, C.I. DISPERSE Red 13 5, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I. Red-1 200 53, C.I. Red 167,
C.I. Red 167: 1, C.I. Red-1 200 77, C.I. Red-1 200 79, C.I. disperse red 200, C.I. disperse red 210, C.I.
Disperse red 220, C.I. disperse red 277, C.I. Disperse Red 278, C.I. Disperse Red 343, C.I. disperse red 356, C.I. disperse violet
1, C.I. disperse violet 8, C.I. disperse violet 17, C.I. disperse violet 26, C.I. disperse violet 27, C.I. disperse violet 28, C.I. disperse violet
33, C.I. disperse violet 38, C.I. disperse violet 43, C.I. disperse violet 63, C.I. disperse violet 77, C.I. disperse violet 93, C.I. dispersion
Purple 93:1, C.I. disperse blue 3, C.I. disperse blue 14, C.I. disperse blue 20, C.I. disperse blue 26, C.I. disperse blue 27, C.I. point
Dissipate indigo plant 56, C.I. Disperse Blue-56: 1, C.I. Disperse Blue-56: 2, C.I. Disperse Blue-56: 3, C.I. disperse blue 58, C.I. disperse blue
60, C.I. disperse blue 73, C.I. disperse blue 77, C.I. Disperse Blue-79, C.I. Disperse Blue-79: 1, C.I. Disperse Blue-79: 2, C.I.
Disperse blue 81, C.I. disperse blue 82, C.I. disperse blue 87, C.I. disperse blue 102, C.I. disperse blue 104, C.I. disperse blue 106,
C.I. disperse blue 118, C.I. disperse blue 143, C.I. disperse blue 148, C.I. disperse blue 165, C.I. disperse blue 165:1, C.I.
Disperse blue 165:2, C.I. disperse blue 165:3, C.I. disperse blue 183, C.I. disperse blue 183:1, C.I. disperse blue 225, C.I.
Disperse blue 257, C.I. disperse blue 270, C.I. disperse blue 281, C.I. disperse blue 291, the dispersion of C.I. disperse blue 291:1, C.I.
Indigo plant 301, C.I. disperse blue 354, C.I. disperse blue 359, C.I. disperse blue 366, C.I. disperse blue 367, C.I. disperse brown 1,
C.I. disperse brown 1:1, C.I. disperse brown 19, C.I. dispersion black one of 1 or a variety of；
Auxiliary agent is selected from polyvinyl alcohol, polyvinyl acetate, styrene and maleic anhydride and is copolymerized in the dyeing, print paste
Object, gelatin, carboxymethyl cellulose, carboxyethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, ethylene glycol, propylene glycol, urine
One of element, diethylene glycol (DEG), thiocarbamide, mineral oils, high-carbon alcohols, polyethers or organic silicon defoaming agent or a variety of and alginic acid
Sodium, polyacrylamide, N- methyl-N oleoyl tarine sodium, naphthalene sulfonic acids-formaldehyde condensation products, the contracting of coconut oleyl alcohol ethylene oxide
Close object, triisopropylbenzene phenol ethylene oxide condensates, sodium lignin sulfonate, neopelex, metacresol-formaldehyde-Asia
Sodium sulphate condensation product extension agent S S, diffusion agent N, dispersing agent MF, dispersing agent CNF, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, cresol sulfonic acid
Sodium formaldehyde condensation product, sodium phenolsulfonate formaldehyde condensation products, beta naphthal sulfonic formaldehyde condensation compound, phenolic resin sulfonated bodies, dispersing agent
CS；
Fatty acid salt form anionic surfactant, sulfonate type anionic surfactant, sulfate type anionic surface are living
Property agent, peptide condensation product type anionic surfactant；Ammonium salt type cationic surfactant, quaternary ammonium salt type cationic surface active
Agent, amine oxide type cationic surfactant, betaine type amphoteric ionic surface active agent, imidazoline type amphoteric ion surface are living
Property agent, phosphatide type zwitterionic surfactant, fatty alcohol ether type nonionic surfactant, alkyl phenol ether type non-ionic surface
Activating agent, alkylamine ether type nonionic surfactant, polyether nonionic surfactant, fatty acid polyglycol alkoxide ester type
Nonionic surfactant, castor oil polyoxyethylene type nonionic surfactant, lanolin polyoxyethylene-type non-ionic surface
Activating agent, sorbitol polyoxyethylene type nonionic surfactant, glycerol ester type nonionic surfactant, sorbierite ester type are non-
Ionic surface active agent, fatty acid alkanamine type nonionic surfactant, alkylolamides type nonionic surfactant, alkyl
One of glucoside type nonionic surfactant, alkyl pyrrolidone type nonionic surfactant or a variety of mixing；
The dyeing, printing assistant form by weight percentage, adhesive 25-80%, softening agent 0.5-5%, crosslinking agent 0.1-
5%, other auxiliary agents 1-5% and water 5-73.4%；
Described adhesive is selected from pure C adhesive, phenylpropyl alcohol adhesive, butylbenzene adhesive, butyronitrile adhesive, silicone adhesive, has
One of machine fluorine-silicon modified acrylic ester adhesive, polyurethane binder are a variety of；
The softening agent is selected from: quaternary ammonium salt cationic type softening agent, fatty acid ester type cationic softener, right wax pattern sun from
Subtype softening agent, polyethylene cationic softener, organic silicon softening agent, fatty acid salt film class softening agent, macromolecule
Polyethylene wax it is one or more；
The crosslinking agent is selected from: cyanate crosslinking agent, polyalcohols crosslinking agent, glycidol ethers crosslinking agent, and inorganic matter is handed over
Connection agent, organic silicon crosslinking agent, benzene sulfonic acid class crosslinking agent, acrylic ester cross-linking agent, organic peroxide crosslinking agent, metal have
Machine compound crosslink agent, one of multi-functional polycarbodiimide class crosslinking agent or a variety of；
Other auxiliary agents in the dyeing, printing assistant are selected from: sodium alginate, polyacrylamide, N- methyl-N oleoyl amino
Ethanesulfonic acid sodium, naphthalene sulfonic acids-formaldehyde condensation products, coconut oleyl alcohol ethylene oxide condensate, triisopropylbenzene phenol ethylene oxide condensates,
Sodium lignin sulfonate, neopelex, metacresol-formaldehyde-sodium sulfite condensation product extension agent S S, diffusion agent N, diffusion
Agent MF, dispersing agent CNF, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, cresol sulfonic acid sodium formaldehyde condensation product, sodium phenolsulfonate formaldehyde condensation
Object, beta naphthal sulfonic formaldehyde condensation compound, phenolic resin sulfonated bodies, dispersing agent C S；Fatty acid salt form, sulfonate type, sulfate type,
Phosphate salt form, sulfosuccinic acid ester type, fatty acid condensates type anionic surfactant；Ammonium salt type, quaternary, oxidation
Amine-type cationic surfactant；Betaine type, imidazoline type, amino acid pattern, phosphatide type zwitterionic surfactant；Fat
Alcohol ether type, alkyl phenol ether type, alkylamine ether type, polyether-type, fatty acid polyglycol alkoxide ester type, castor oil polyoxyethylene type, sheep
Hair rouge polyoxyethylene-type, sorbitol polyoxyethylene type, glycerol ester type, sorbierite ester type, fatty acid alkanamine type, alkylolamides
Type, alkyl glycosides type, alkyl pyrrolidone type nonionic surfactant；Polyvinyl alcohol, polyvinyl acetate, styrene and suitable fourth
Enedioic acid anhydride copolymer, gelatin, carboxymethyl cellulose, carboxyethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, second two
Alcohol, propylene glycol, urea, diethylene glycol (DEG), thiocarbamide, organic silicon defoamer, mineral oil antifoam agent, polyethers defoaming agent, the three polyglycereol moons
Cinnamic acid ester, four polyglyceryl laurates, six polyglyceryl laurates, Tripolyglycerol monostearates, in three Unigly GO 102Ss
It is one or more；
The thickener is selected from: white carbon black, sodium bentonite, organobentonite, diatomite, attapulgite soil, molecular sieve, silicon are solidifying
Glue, methylcellulose, ethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose,
Carboxyethyl cellulose, carboxy-propyl cellulose, starch, gelatin, sodium alginate, casein, guar gum, chitosan, gum arabic,
Xanthan gum, natural rubber, lanolin, agar, polyacrylamide, polyvinyl alcohol, polyvinylpyrrolidone, gathers at soybean protein glue
Ethylene oxide, carbomer, polyacrylic acid, Polyacrylate Emulsion, butadiene rubber, butadiene-styrene rubber, is gathered modified paraffin resin
One of urethane, modified polyurea, low-molecular polyethylene wax, amino alcohol solvay-type titanate esters are a variety of；
PH adjusting agent is selected from: citric acid, adipic acid, potassium citrate, lactic acid, fumaric acid, phosphate hydrogen tri-sodium, tartaric acid, citric acid
One sodium, malic acid, phosphoric acid, acetic acid, hydrochloric acid, 2-amino-2-methyl-1-propanol, N- methylethanolamine, monoethanolamine, diethanol
Amine, triethanolamine, butylethanolamine, N- aminopropyl-methylethanolamine, 2- amino -2- ethyl -1,3- propylene glycol, butyl diethyl
One of hydramine, ammonium hydroxide, sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate, saleratus are a variety of；
The wet concentration is from one or more of tap water, deionized water, distilled water, high purity water, ultrapure water；
The paste composition is applied in dyeing, stamp.
2. dye according to claim 1 applies one dyeing, stamp paste composition, it is characterised in that:
The dyeing, disperse dyes are selected from print paste: C.I. disperse yellow 49, C.I. disperse yellow 50, C.I. disperse yellow 54,
C.I. dispersion yellow 64, C.I. disperse yellow 71, C.I. disperse yellow 79, C.I. disperse yellow 82, C.I. disperse yellow 93, C.I. disperse yellow
114, C.I. disperse yellow 119, C.I. disperse yellow 134, C.I. disperse yellow 163, C.I. disperse yellow 182, C.I. disperse yellow 184,
C.I. disperse yellow 201, C.I. DISPERSE Yellow 211, C.I. disperse yellow 241, C.I. disperse orange 25, C.I. disperse orange 25: 1, C.I. points
Dissipate orange 29, C.I. disperse orange 30, C.I. disperse orange 31, C.I. disperse orange 44, C.I. disperse orange 73, C.I. disperse orange 76, C.I.
Disperse orange 97, C.I. disperse orange 288, C.I. disperse red 54, C.I. disperse red 54: 1, C.I. disperse red 60, C.I. disperse red 73,
C.I. disperse red 74, C.I. disperse red 92, C.I. C.I. DISPERSE Red 13 5, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I.
Red-1 200 53, C.I. Red 167, C.I. Red 167: 1, C.I. Red-1 200 79, C.I. disperse red 277, C.I. dispersion
Red 278, C.I. Disperse Red 343, C.I. disperse red 356, C.I. disperse violet 33, C.I. disperse violet 38, C.I. disperse violet 43, C.I.
Disperse violet 63, C.I. disperse violet 77, C.I. disperse violet 93, C.I. disperse violet 93:1, C.I. Disperse Blue-56, C.I. Disperse Blue-56:
1, C.I. Disperse Blue-56: 2, C.I. Disperse Blue-56: 3, C.I. disperse blue 60, C.I. disperse blue 73, C.I. Disperse Blue-79, C.I. point
Dissipate indigo plant 79:1, C.I. Disperse Blue-79: 2, C.I. disperse blue 102, C.I. disperse blue 104, C.I. disperse blue 106, C.I. disperse blue
118, C.I. disperse blue 165, C.I. disperse blue 165:1, C.I. disperse blue 165:2, C.I. disperse blue 165:3, C.I. disperse blue
183, C.I. disperse blue 183:1, C.I. disperse blue 291, C.I. disperse blue 291:1, C.I. disperse blue 354, C.I. disperse blue
359, one of C.I. disperse blue 366, C.I. disperse blue 367, C.I. disperse brown 19 or a variety of；
Auxiliary agent is one of mineral oils, high-carbon alcohols, polyethers or organic silicon defoaming agent in the dyeing, print paste
Or a variety of and naphthalene sulfonic acids-formaldehyde condensation products, coconut oleyl alcohol ethylene oxide condensate, sodium lignin sulfonate, dodecyl benzene sulfonic acid
Sodium, extension agent S S, diffusion agent N, dispersing agent MF, dispersing agent CNF, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, the contracting of beta naphthal sulfonic acid and formaldehyde
Close object, dispersing agent C S, fatty acid salt form anionic surfactant, sulfonate type anionic surfactant, sulfate type yin
Ionic surface active agent, phosphate salt form anionic surfactant, sulfosuccinic acid ester type anionic surfactant, beet
Alkaline zwitterionic surfactant, imidazoline type zwitterionic surfactant, amino acid type amphoteric ionic surface active agent,
Phosphatide type zwitterionic surfactant, fatty alcohol ether type nonionic surfactant, alkyl phenol ether type non-ionic surface active
Agent, alkylamine ether type nonionic surfactant, polyether nonionic surfactant, fatty acid polyglycol alkoxide ester type it is non-from
Sub- surfactant, castor oil polyoxyethylene type nonionic surfactant, lanolin polyoxyethylene-type non-ionic surface active
Agent, sorbitol polyoxyethylene type nonionic surfactant, glycerol ester type nonionic surfactant, sorbierite ester type nonionic
Surfactant, fatty acid alkanamine type nonionic surfactant, alkylolamides type nonionic surfactant, alkyl glycosides
Type nonionic surfactant, alkyl pyrrolidone type nonionic surfactant, ethylene glycol, propylene glycol, urea, in diethylene glycol (DEG)
One or more of mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610580392.2A CN105970671B (en) | 2016-07-22 | 2016-07-22 | A kind of dye applies integrated dyeing, stamp paste composition and its application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610580392.2A CN105970671B (en) | 2016-07-22 | 2016-07-22 | A kind of dye applies integrated dyeing, stamp paste composition and its application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105970671A CN105970671A (en) | 2016-09-28 |
| CN105970671B true CN105970671B (en) | 2019-05-07 |
Family
ID=56951913
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610580392.2A Active CN105970671B (en) | 2016-07-22 | 2016-07-22 | A kind of dye applies integrated dyeing, stamp paste composition and its application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105970671B (en) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758322A (en) * | 2016-11-16 | 2017-05-31 | 湖北丽源科技股份有限公司 | A kind of method of terylene pad dyeing mill base and pad dyeing dacron |
| CN106752084A (en) * | 2016-12-31 | 2017-05-31 | 浙江博澳染料工业有限公司 | A kind of Novel disperse dyestuff composition and its preparation method and application |
| CN106833021A (en) * | 2017-02-17 | 2017-06-13 | 朱友富 | A kind of fastness to perspiration disperse dyes high |
| CN106893359A (en) * | 2017-02-17 | 2017-06-27 | 朱友富 | A kind of fastness to rubbing disperse dye composition high |
| CN107012696A (en) * | 2017-04-10 | 2017-08-04 | 江苏亨德利纺织印染有限公司 | Waterborne suede slurry for cotton flannelette and preparation method thereof and application method |
| CN107011701A (en) * | 2017-05-24 | 2017-08-04 | 上海贝通色彩科技有限公司 | A kind of alkali resistance disperse dye composition |
| CN107227479A (en) * | 2017-05-27 | 2017-10-03 | 北京石油化工学院 | A kind of utilization disperse dyes are the method that magnesium material differential arc oxidation film layer is coloured |
| CN107227480A (en) * | 2017-05-27 | 2017-10-03 | 北京石油化工学院 | A kind of utilization weak acid dye is the method that magnesium material differential arc oxidation film layer is coloured |
| CN107083693A (en) * | 2017-05-31 | 2017-08-22 | 浙江山川科技股份有限公司 | A kind of colouring agent and its production technology for dacron |
| CN107034694A (en) * | 2017-05-31 | 2017-08-11 | 浙江山川科技股份有限公司 | A kind of colouring agent and its production technology for dacron |
| CN107383936B (en) * | 2017-07-13 | 2019-08-13 | 浙江龙盛化工研究有限公司 | It is a kind of to disperse bright blue dye composite and dye preparations |
| CN107936616A (en) * | 2017-10-26 | 2018-04-20 | 安徽凯奇化工科技股份有限公司 | A kind of red disperse dyes composition of high color fastness |
| CN107974102A (en) * | 2017-10-30 | 2018-05-01 | 安徽凯奇化工科技股份有限公司 | A kind of composite disperse orange dye |
| CN109750526A (en) * | 2017-11-02 | 2019-05-14 | 江苏新瑞贝科技股份有限公司 | A kind of disperse dyes of liquid and preparation method thereof |
| CN108179639A (en) * | 2017-12-19 | 2018-06-19 | 江苏新瑞贝科技股份有限公司 | A kind of dyeing auxiliaries and preparation method thereof |
| CN108047760A (en) * | 2017-12-29 | 2018-05-18 | 东营安诺其纺织材料有限公司 | A kind of black dye composite of environmentally-friendly digital stamp |
| TW202008944A (en) * | 2018-08-27 | 2020-03-01 | 陳孟谷 | Environmentally cleaning cloth and method |
| CN109439056B (en) * | 2018-09-27 | 2022-03-25 | 丁贤勇 | Nonionic associative type water-based polyurethane thickener and preparation method thereof |
| CN109457505A (en) * | 2018-10-24 | 2019-03-12 | 江苏华东纺织产品检测有限公司 | A kind of square screen printing process of fleece |
| CN110330811A (en) * | 2019-07-23 | 2019-10-15 | 孚美科(绍兴)染料科技有限公司 | It is a kind of to disperse black FECT300% dye composite and its application |
| CN110358364B (en) * | 2019-08-15 | 2022-03-15 | 深圳市墨库图文技术有限公司 | High-temperature dispersion direct-injection black ink and preparation method thereof |
| CN110643200B (en) * | 2019-10-09 | 2021-04-27 | 江苏亚邦染料股份有限公司 | Red disperse dye composition for printing |
| CN110746791B (en) * | 2019-10-29 | 2021-03-02 | 维昂(山东)纺织科技有限公司 | Disperse orange dye composition, disperse orange dye, preparation method and application thereof, and colored product |
| CN111019393B (en) * | 2019-12-25 | 2022-02-11 | 沈阳化工研究院有限公司 | Yellow liquid dye composition for dyeing and printing and application thereof |
| CN111234563B (en) * | 2020-03-30 | 2022-06-21 | 南通纺织丝绸产业技术研究院 | Water-based disperse dye for water and oil resistance and application thereof |
| CN111235910B (en) * | 2020-03-31 | 2022-06-14 | 南通纺织丝绸产业技术研究院 | Water-based nano disperse dye for soft finishing and application thereof |
| WO2021196103A1 (en) * | 2020-04-01 | 2021-10-07 | 南通纺织丝绸产业技术研究院 | Water-based nano disperse dye useful for softening finishing and use thereof |
| CN112301761A (en) * | 2020-11-06 | 2021-02-02 | 安徽聚合辐化化工有限公司 | Printing method free of washing or less washing |
| CN112482046B (en) * | 2020-11-18 | 2022-06-03 | 浙江理工大学上虞工业技术研究院有限公司 | Method for processing formaldehyde-free cotton fabric with durable luster |
| CN112679989B (en) * | 2020-12-29 | 2022-09-23 | 浙江闰土股份有限公司 | Disperse dye composition, disperse dye, preparation method and application thereof |
| CN113308132B (en) * | 2021-06-10 | 2023-03-21 | 约克夏(浙江)染化有限公司 | Disperse dye composition, disperse dye, preparation method and application thereof |
| CN113529437A (en) * | 2021-07-17 | 2021-10-22 | 浙江智兴集团有限公司 | Dyeing method of elastic fabric |
| CN113755030B (en) * | 2021-08-31 | 2023-06-02 | 沈阳化工研究院有限公司 | Red light blue liquid dye composition and application thereof |
| CN113668261B (en) * | 2021-09-10 | 2023-07-07 | 拓烯科技(衢州)有限公司 | Dyeing liquid for optical resin and application method thereof |
| CN113861333B (en) * | 2021-09-17 | 2023-02-03 | 浙江工业大学 | Cross-linking type acrylic resin emulsion and synthesis method and application thereof |
| CN114479575A (en) * | 2022-01-27 | 2022-05-13 | 东方雨虹民用建材有限责任公司 | Colored concrete interface agent and preparation method thereof |
| CN114775302B (en) * | 2022-04-14 | 2023-07-07 | 邦特云纤(青岛)新材料科技有限公司 | Wide-color-gamut plant dyeing method for animal fibers and fabrics |
| CN115044229A (en) * | 2022-07-04 | 2022-09-13 | 杭州迈染新材料有限公司 | Black dye composition for dyeing diacetate fibers, disperse dye and application thereof |
| CN117430968B (en) * | 2023-09-15 | 2024-05-24 | 菲诺染料化工(无锡)有限公司 | Composite disperse blue dye composition for polylactic acid fibers |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101899784B (en) * | 2010-07-27 | 2012-08-08 | 苏州大学 | Steam-cleaning free printing process for disperse dye |
| CN105113284B (en) * | 2015-09-19 | 2017-07-07 | 苏州大学 | A kind of micro print paste and preparation method and application |
-
2016
- 2016-07-22 CN CN201610580392.2A patent/CN105970671B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN105970671A (en) | 2016-09-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105970671B (en) | A kind of dye applies integrated dyeing, stamp paste composition and its application | |
| CN106087464A (en) | A kind of dyeing, printing technology | |
| CN106049091A (en) | Dye paste composition for dye and pigment integrated dyeing and printing | |
| CN105113285B (en) | A kind of pulp-shaped dispersed dyes and preparation method and application | |
| CN100560859C (en) | Natural fabric and polyamide fibre wet method transfer printing method | |
| CN105113284B (en) | A kind of micro print paste and preparation method and application | |
| CN101289601B (en) | Cationic binder emulsion for coating coloring, preparation method and uses | |
| CN101418523B (en) | Method for producing energy-saving and environment-friendly type soft resin-bonded pigment printing nap cloth | |
| US20100273929A1 (en) | Coloring composition | |
| CN101195952A (en) | Cotton fibre and blended fabric printing and dyeing method | |
| CN103498353B (en) | Paint discharge printing technology with digital printing effect | |
| US2275991A (en) | Textile printing paste | |
| CN106758426A (en) | A kind of preprocess method of the dacron for improving the two-sided ink-jet printed effect of infiltration | |
| CN105696377A (en) | Efficient and rapid steaming printing technology adopting reactive dyes | |
| CN101768880A (en) | Pearl powder printing paste composition, preparing method thereof and application thereof | |
| CN108411651A (en) | A kind of gold stamping slurry and its preparation method and application | |
| CN105862463A (en) | Turquoise blue reserve printing method | |
| CN109972421A (en) | A kind of reactive dye ink and preparation method thereof suitable for ultrahigh speed digital printing | |
| CN102864652B (en) | Silk dye paints method | |
| US3454347A (en) | Fabric dyeing by transferring by heating or solubilizing a dye from an electrostatically deposited,heat or solvent fused water soluble dielectric carrier | |
| CN109736104B (en) | Indigo pulp dyeing process for all-cotton fabric | |
| CN107700248A (en) | A kind of digit printing coating ink and preparation method thereof | |
| CN104530755A (en) | Composite active black dye | |
| CN104878622A (en) | Processing method for improving hand feel of coat-printed textiles | |
| CN109295759A (en) | A kind of preparation method of environment-friendly type phase transformation color changing type reactive dye digit printing ink |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |