CN105748358A - Aquilaria agallocha essence activating lotion and preparation method thereof - Google Patents
Aquilaria agallocha essence activating lotion and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/83—Thymelaeaceae (Mezereum family), e.g. leatherwood or false ohelo
- A61K36/835—Aquilaria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The invention relates to the field of cosmetics production and provides aquilaria agallocha essence activating lotion and a preparation method thereof.The aquilaria agallocha essence activating lotion is prepared by, by weight, 100 parts of water, 8-15 parts of 1, 3-propylene glycol, 0.6-0.8 part of phenoxyethanol, 0.5-1.5 part of aquilaria agallocha extract and 5.0-12.0 parts of sea sludge extract.The preparation method includes: adding the 1, 3-propylene glycol into the water, continuously stirring, and slowly heating to rise the temperature to obtain mixed liquid I; slowly adding the phenoxyethanol after the mixed liquid I is cooled, and evenly stirring until the mixed liquid is clear to obtain mixed liquid II; sequentially adding the aquilaria agallocha extract and the sea sludge extract into the mixed liquid II, stirring, and filtering to obtain the aquilaria agallocha essence activating lotion.The aquilaria agallocha essence activating lotion can improve the skin and fade stains.The preparation method can further guarantee the skin improving and stain fading effects of the aquilaria agallocha essence activating lotion.
Description
Technical field
The present invention relates to Cosmetic Manufacture field, compose in particular to a kind of agalloch eaglewood elite
Running water and preparation method thereof.
Background technology
At cosmetic field, composing running water, Essence etc. is the good merchantable brand in skin care item, its composition
Exquisite, effect is powerful, skin effect is notable, it is possible to nourishes rough skin, reduce pore, desalination
Obscure, skin whitening, the most anti-aging, anti-wrinkle；It is broadly divided into aqua and finish two
Class, and the battalion after the concentration that the raw material components that it uses generally extracts from plant, animal
Support material.
Agalloch eaglewood, calls, lignum aquilariae resinatum fragrant into honey, for dicotyledonous medicine Thymelaeceae magaphanerophytes, also
Refer to the timber containing resin of suspension culture of Aquilaria sinensis.Effect of agalloch eaglewood is a lot, not only to abdominal distension, stomach cold,
Suffer from a deficiency of the kidney, obvious curative effects of having panted, moreover it can be used to treatment angina pectoris and bad odor carbuncle.Additionally,
The extract of agalloch eaglewood also has sleeping anti-mood strongly fragrant, stable, anxiety of releiving, helps qi and blood to follow
The effects such as ring.In the field such as healthcare products and commodity, agalloch eaglewood is also widely used,
As: agalloch eaglewood dish, Agilawood toothpaste, perfumed soap and shampoo, agalloch eaglewood freshener, agalloch eaglewood anti-pharynx frost,
Agalloch eaglewood safety is burnt incense, agilawood essential oil atomized liquid, fragrant product etc..
Application publication number is that the application for a patent for invention document of CN105105316A discloses one
Agilawood essential oil atomized liquid, is mainly made up of following raw material: in terms of mass fraction, agilawood essential oil
1～20 part, natural botanical extraction liquid 60～90 parts, wherein, the component bag of described agilawood essential oil
Include: aromatic series compounds and sesquiterpenoids, described natural botanical extraction liquid
Component includes N-acetyl-glucosamine, aloe gel and aloe polysaccharide.This agilawood essential oil mist
The preparation method changing liquid includes: by described agilawood essential oil with described natural botanical extraction liquid successively
Add mixing and stirring, it is thus achieved that.This atomized liquid is mainly used in improving existing tobacco essence taste
Road is the sweetest, mouthfeel is poor, produce the problems such as pernicious gas.
Application publication number is that the application for a patent for invention document of CN103054777A discloses one
Agalloch eaglewood Chinese medicine shampoo and preparation method thereof, this Chinese medicine shampoo contains surfactant sodium dodecyl base
Sodium sulphate or lauryl alcohol sulfuric acid ethanolamine salt, stabilizer, smooth dose and agilawood essential oil, heavy
Essential oil content is the 1.5～8% of gross weight.This Chinese medicine shampoo can reach hair care effect,
And effect is notable.
Although, the Related product about Lignum Aquilariae Resinatum extract, agilawood essential oil is a lot of, is played
Act on the most different；But, at cosmetic field, Lignum Aquilariae Resinatum extract is fully applied to
Essence, compose in running water, to reach to improve skin quality, desalination color spot, to alleviate and ache, calm the nerves
The document of the effect of nourishing heart but rarely has report.
In view of this, the special proposition present invention.
Summary of the invention
The first object of the present invention is to provide a kind of agalloch eaglewood elite to compose running water, described agalloch eaglewood
Elite is composed running water and can not only be kept the skin wet for skin, improve skin quality, desalination color spot, moreover it is possible to
Enough alleviations are ached, are calmed the nerves and nourish heart.
The second object of the present invention is the preparation method providing a kind of agalloch eaglewood elite to compose running water,
The agalloch eaglewood elite tax running water active ingredient that the method is simple to operate, prepare is high, skin effect is good,
And good absorbing effect.
In order to realize the above-mentioned purpose of the present invention, spy by the following technical solutions:
A kind of agalloch eaglewood elite composes running water, by weight, is mainly made up of following raw material: water
100 parts, 1,3-PD 8～15 parts, Phenoxyethanol 0.6～0.8 part, Lignum Aquilariae Resinatum extract
0.5～1.5 part, sea sludge extract 5.0～12.0 parts.
The designer of the present invention is with east health as inspiration, by long-term exploration and trial,
And experiment repeatedly and effort, constantly reform and innovate, elite determine Lignum Aquilariae Resinatum extract, sea
Sludge extract, as important source material, have devised this agalloch eaglewood elite and composes running water, make full use of
The penetration power that Lignum Aquilariae Resinatum extract is intrinsic, and combine with 1,3-PD and Phenoxyethanol, carry
Its penetration high, makes Lignum Aquilariae Resinatum extract directly arrive skin corium, keeps the skin wet, and amendment is subject to
Damage cell.
Above-mentioned agalloch eaglewood elite is composed in running water, and water uses as solvent, and 1,3-PD is as guarantor
Humectant, plays the effect making skin moisture-keeping, and Phenoxyethanol plays antisepsis, and agalloch eaglewood carries
Take thing with sea sludge extract as skin conditioning agent, play the effect of conditioning skin skin quality.
Present invention also offers the agalloch eaglewood elite described in any of the above-described scheme and compose the preparation side of running water
Method, comprises the following steps:
(1) in water, 1,3-PD is added, continuously stirred, and with the liter of 1-5 DEG C/min
Temperature speed is slowly heated intensification, it is thus achieved that mixed liquor I；
(2) after mixed liquor I being cooled to 40-55 DEG C, it is slowly added to Phenoxyethanol, uniformly
Stir clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract, stirs
Mix, after filtration, it is thus achieved that described agalloch eaglewood elite composes running water.
In step (1), need to add 1,3-PD to mix to water, otherwise hold
During easily causing subsequent heat, 1,3-PD directly contacts with reaction vessel, overheated,
There is chemical reaction；1,3-PD is added to the water, using water as solvent, can play slow
Solution effect.
Above-mentioned agalloch eaglewood elite composes the preparation technology of running water can improve Lignum Aquilariae Resinatum extract, sea mud
The dissolubility of extract, make the agalloch eaglewood elite for preparing compose active ingredient in running water be more easy to by
User absorbs.
Compared with prior art, the invention have the benefit that
(1) agalloch eaglewood elite of the present invention composes running water with Lignum Aquilariae Resinatum extract, sea sludge extract, 1,3-
Propane diols and Phenoxyethanol are that raw material is prepared, and not only fragrance is pure and fresh simple and elegant, and can
Improve skin quality, can removing acne and freckle, reduce pore, desalination melanin, skin whitening, through
Skin skin corium is that skin keeps the skin wet, solve small pox, chloasma, glossy have one's face covered with, pore
The skin problems such as thick, face is dim.
(2) agalloch eaglewood elite of the present invention tax running water takes full advantage of the superpower penetration power of agalloch eaglewood and oozes
Power thoroughly, it is possible to dredging vascellum；Use agalloch eaglewood elite of the present invention to compose running water and be sprayed on lymph, oxter
At position, lymph can be dredged, prevent breast lobule hyperplasia.
(3), during DOMS, agalloch eaglewood elite of the present invention is used to compose running water spray muscle, permissible
Alleviate DOMS.
(4) agalloch eaglewood elite of the present invention compose running water can calm the nerves nourish heart, help enhancing brain cell live
Power, lifting memory and notice, improve resourceful degree, refresh the mind, and improves work
Efficiency.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but this
Skilled person is it will be appreciated that the following example is merely to illustrate the present invention, and should not regard
For limiting the scope of the present invention.Unreceipted actual conditions person in embodiment, according to normal condition
Or the condition of manufacturer's suggestion is carried out.Agents useful for same or instrument unreceipted production firm person, all
For the conventional products that can be obtained by commercially available purchase.
The designer of the present invention is with east health as inspiration, by long-term exploration and trial,
And experiment repeatedly and effort, constantly reform and innovate, elite determine Lignum Aquilariae Resinatum extract, sea
Sludge extract, as important source material, have devised this agalloch eaglewood elite and composes running water.This agalloch eaglewood
Elite composes running water, by weight, is mainly made up of following raw material: 100 parts of water, 1,3-
Propane diols 8～15 parts, Phenoxyethanol 0.6～0.8 part, Lignum Aquilariae Resinatum extract 0.5～1.5 parts, sea
Sludge extract 5.0～12.0 parts.
This agalloch eaglewood elite is composed running water and is taken full advantage of the penetration power that Lignum Aquilariae Resinatum extract is intrinsic, and
Combine with 1,3-PD and Phenoxyethanol, improve its penetration, make Lignum Aquilariae Resinatum extract straight
Receive and reach skin corium, keep the skin wet, revise damaged cell.
Above-mentioned agalloch eaglewood elite is composed in running water, and water uses as solvent, and 1,3-PD is as guarantor
Humectant, plays the effect making skin moisture-keeping, and Phenoxyethanol plays antisepsis, and agalloch eaglewood carries
Take thing with sea sludge extract as skin conditioning agent, play the effect of conditioning skin skin quality.
Test proves, rational amounts of components can preferably improve skin quality, desalination skin-color
Spot, as preferably, by weight, is mainly made up of following raw material: 100 parts of water, 1,3-
Propane diols 9.3～12.6 parts, Phenoxyethanol 0.70～0.76 part, Lignum Aquilariae Resinatum extract 0.6～1.3
Part, sea sludge extract 5.8～11.3 parts.
It is further preferred that by weight, mainly it is made up of following raw material: 100 parts of water, 1,3-
Propane diols 12.5 parts, Phenoxyethanol 0.75 part, Lignum Aquilariae Resinatum extract 0.6 part, sea mud carries
Take thing 11.0 parts.
Present invention also offers the agalloch eaglewood elite described in any of the above-described scheme and compose the preparation side of running water
Method, comprises the following steps:
(1) in water, 1,3-PD is added, continuously stirred, and it is slowly heated intensification, obtain
Obtain mixed liquor I；
(2) after mixed liquor I being lowered the temperature, being slowly added to Phenoxyethanol, uniform stirring is to mixing
Liquid is clear, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract, stirs
Mix, after filtration, it is thus achieved that described agalloch eaglewood elite composes running water.
In step (1), need to add 1,3-PD to mix to water, otherwise hold
During easily causing subsequent heat, 1,3-PD directly contacts with reaction vessel, overheated,
There is chemical reaction；1,3-PD is added to the water, using water as solvent, can play slow
Solution effect.
In step (1), stirring needs at the uniform velocity, and its mixing speed is unsuitable too fast, the most easily
Cause excessive thermal losses and water loss, and reduce the dissolution rate of raw material, as preferably,
The speed of described stirring is 20～30r/min.
In step (1), it should control the speed of heat temperature raising, unsuitable too fast, the most easily make
Become hot-spot；As preferably, the firing rate being slowly heated intensification is 1～3 DEG C/min.
The strict control of water temperature, is possible not only to ensure the abundant dissolving of 1,3-PD, moreover it is possible to
Enough play the sterilizing of reagent.As preferably, in step (1), it is slowly heated and is warming up to
80～85 DEG C.
In step (2), control the temperature of cooling, and in the case of keeping this temperature, add
Add Phenoxyethanol；Temperature is too high, can cause partial material volatilization or decompose.As preferably,
Described mixed liquor I is cooled to 40～45 DEG C.
After step (2) terminates, needing to carry out the inspection ageing process of 72 hours, material body exists
In ageing process, room temperature can be recovered.
As preferably, in step (2), the speed of stirring is 20～30r/min.
As preferably, in step (3), mixing time is 5～15 minutes.
Lignum Aquilariae Resinatum extract and sea sludge extract all can directly buy acquisition, it is also possible to processing
Preparation.Provide below preparation method and a kind of sea sludge extract of a kind of Lignum Aquilariae Resinatum extract
Preparation method.
Wherein, the preparation method of Lignum Aquilariae Resinatum extract is: (1) takes the agalloch eaglewood of Edgeworthia chrysantha, cuts
After becoming fritter, it is crushed to the agalloch eaglewood powder of 15 mesh；(2) in agalloch eaglewood powder, add water, be heated to
100 DEG C, and keep this temperature 12h, then carry out refrigerated separation, it is thus achieved that Lignum Aquilariae Resinatum extract (or
It is referred to as linaloe oil).Above-mentioned Lignum Aquilariae Resinatum extract includes chromone, triterpene, calacone and furans acid.
The extracting method of sea sludge extract is: take green mud and black mud, after 30 DEG C dry, cold
But to room temperature, the mixture of green mud that mass ratio is 1:1 with black mud is placed in ethanol solution (matter
Amount mark is 75%, and volume is 8 times of volume of mixture) middle extraction 24h, with 2500r/min
Centrifugation 30min, take supernatant, it is thus achieved that sea sludge extract (or be referred to as sea mud
Extract).Green mud is collected in anaerobic environment, and the deposition not experiencing excessive scale is decomposed, rich
Containing carotenoid, vitamin E, mainly antioxidant effect obtained by blue-green alge deposits,
Can be applicable to dryness and sensitive.Described black mud is in deeper lake, experiences excessive
The deposition of scale is decomposed, bigger than green mud degree of oxidation, rich in humus acid and aliphatic acid,
Can be applicable to oiliness and problem skin.
Embodiment 1
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 11.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 2
Take following raw material: water 100g, 1,3-PD 8g, Phenoxyethanol 0.6g, heavy
Fragrant extract 0.5g, sea sludge extract 5.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 3
Take following raw material: water 100g, 1,3-PD 15g, Phenoxyethanol 0.8g,
Lignum Aquilariae Resinatum extract 1.5g, sea sludge extract 12.0g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 50 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 4
Take following raw material: water 100g, 1,3-PD 9.3g, Phenoxyethanol 0.7g part,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 5.8g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 5
Take following raw material: water 100g, 1,3-PD 12.6g, Phenoxyethanol 0.76g,
Lignum Aquilariae Resinatum extract 1.3g, sea sludge extract 11.3g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 6
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 11.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 30r/min continuously stirred emulsification pot, and with 3 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Embodiment 7
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 11.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 30r/min continuously stirred emulsification pot, and with 3 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 40 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Comparative example 1
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, add Lignum Aquilariae Resinatum extract again, after stirring 10min, filter,
Take supernatant, it is thus achieved that described tax running water；
(4) detect described tax running water, qualified after, filling.
Comparative example 2
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Sea sludge extract 11.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, sea sludge extract, after stirring 10min, mistake are added again
Filter, takes supernatant, it is thus achieved that described tax running water；
(4) detect described tax running water, qualified after, filling.
Comparative example 3
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 1.0g, sea sludge extract 3.0g.
Follow the steps below preparation:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) after being sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again in mixed liquor I I,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Comparative example 4
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.3g, sea sludge extract 15.0g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 25r/min continuously stirred emulsification pot, and with 1 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) after being sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again in mixed liquor I I,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Comparative example 5
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 11.0g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 35r/min continuously stirred emulsification pot, and with 5 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) after being sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again in mixed liquor I I,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Comparative example 6
Take following raw material: water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g,
Lignum Aquilariae Resinatum extract 0.6g, sea sludge extract 11.0g.
Operate according to following steps:
(1) in the emulsification pot cleaned up, first add water, then add 1,3-in emulsification pot
Propane diols, with the mixed solution in the speed of 35r/min continuously stirred emulsification pot, and with 5 DEG C
The speed of/min is to slowly warm up to 85 DEG C, stops heating, it is thus achieved that mixed liquor I；
(2) mixed liquor I is cooled to 55 DEG C, is slowly added to Phenoxyethanol, with 25r/min
Speed continuously stirred, uniform stirring is clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) after being sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract again in mixed liquor I I,
After stirring 10min, filter, take supernatant, it is thus achieved that described agalloch eaglewood elite composes running water；
(4) detect described agalloch eaglewood elite compose running water, qualified after, filling.
Experimental example
Repeat embodiment 1～7 and comparative example 1～6, prepare agalloch eaglewood elite and compose running water or compose running water；
According to " cosmetics health specification ", above-mentioned agalloch eaglewood elite is composed running water or tax running water carries out health
Safety examination, testing result as shown in Table 1 and Table 2:
Table 1. Micro biological Tests result
Table 2. health chemical testing result
Through microorganism detection, total plate count, yeast and mold, pseudomonas aeruginosa, gold
Staphylococcus aureus, excrement colibacillus group testing result all meet the requirements；Through health chemical testing,
Lead, arsenic, mercury assay all meet the requirements.
Recruit volunteer, choose the volunteer that skin quality is coarse, dim and color spot is heavier and try
Test, with above-described embodiment 1～7 and the agalloch eaglewood elite for preparing of comparative example 1～6 compose running water or compose and live
Water is sample, and with clear water for comparison, (experimenter is divided into 14 groups, often organizes 30 to allow experimenter
People, totally 420 people) respectively use once, and assist other skin care item, experimenter every day
Other skin care item are the most identical, within 15 days, are a test period, observe experimenter's skin quality after using
Improvement situation, the number that record skin quality is improved and color spot is desalinated, result such as table 3:
Table 3. experimenter's skin quality improves condition survey table.
As shown in the above results, using the agalloch eaglewood elite of embodiment 1 preparation to compose running water can be
Effectively improve the skin quality of experimenter, desalination color spot；The agalloch eaglewood elite of embodiment 2～5 preparation
Composing running water to be slightly different with embodiment 1 in amounts of components, effect is slightly worse than embodiment 1,
But remain to be effectively improved the skin quality of experimenter, desalination color spot.
Embodiment 6～7 uses raw material components proportioning same as in Example 1, but in preparation work
In skill, condition is different from embodiment 1, and finally, effect is slightly worse than example；This is described
The preparation technology of invention agalloch eaglewood elite tax running water can affect agalloch eaglewood elite and compose effect of running water, should
This strictly controls.
Comparative example 1 lacks sea sludge extract, although can improve in the tax running water of preparation
The skin quality of part experimenter, but, for most subjects, the most to no effect.
Comparative example 2 lacks Lignum Aquilariae Resinatum extract in the tax running water of preparation, can be bright from result
Showing and find out, effect is more worse than comparative example 1, illustrates that Lignum Aquilariae Resinatum extract is as agalloch eaglewood of the present invention essence
The improvement to experimenter's skin quality of the component of running water, the desalination of color spot are composed by China, play extremely important
Effect.
In comparative example 3～4 in the tax running water of preparation, because the consumption of raw material components is not reasonable,
Significantly reduce the successful number that experimenter's skin quality is improved；Comparative example 5～6, although have employed
Raw material components same as in Example 1 and consumption, but because preparation technology there are differences, also
The successful number causing experimenter's skin quality to improve reduces.In clear water control group, the skin of experimenter
Matter and color spot do not improve.
Although illustrate and describing the present invention with specific embodiment, but it will be appreciated that
May be made that without departing from the spirit and scope of the present invention many other change and
Amendment.It is, therefore, intended that include in the following claims belonging in the scope of the invention
All such changes and modifications.
Claims (10)
1. an agalloch eaglewood elite composes running water, it is characterised in that by weight, mainly by with
Lower raw material is made: 100 parts of water, 1,3-PD 8～15 parts, Phenoxyethanol 0.6～0.8 part,
Lignum Aquilariae Resinatum extract 0.5～1.5 parts, sea sludge extract 5.0～12.0 parts.
Agalloch eaglewood elite the most according to claim 1 composes running water, it is characterised in that by weight
Amount part meter, is mainly made up of following raw material: 100 parts of water, 1,3-PD 9.3～12.6 parts,
Phenoxyethanol 0.70～0.76 part, Lignum Aquilariae Resinatum extract 0.6～1.3 parts, sea sludge extract
5.8～11.3 parts.
Agalloch eaglewood elite the most according to claim 1 composes running water, it is characterised in that by weight
Amount part meter, is mainly made up of following raw material: 100 parts of water, 1,3-PD 12.5 parts, benzene
Oxyethanol 0.75 part, Lignum Aquilariae Resinatum extract 0.6 part, sea sludge extract 11.0 parts.
4. the preparation method of running water is composed according to agalloch eaglewood elite described in any one of claims 1 to 3,
It is characterized in that, comprise the following steps:
(1) in water, 1,3-PD is added, continuously stirred, and with the liter of 1-5 DEG C/min
Temperature speed is slowly heated intensification, it is thus achieved that mixed liquor I；
(2) after mixed liquor I being cooled to 40-50 DEG C, it is slowly added to Phenoxyethanol, uniformly
Stir clear to mixed liquor, it is thus achieved that mixed liquor I I；
(3) in mixed liquor I I, it is sequentially added into Lignum Aquilariae Resinatum extract, sea sludge extract, stirs
Mix, after filtration, it is thus achieved that described agalloch eaglewood elite composes running water.
Preparation method the most according to claim 4, it is characterised in that step (1)
In, the speed of described stirring is 20～30r/min.
Preparation method the most according to claim 4, it is characterised in that step (1)
In, described in be slowly heated the heating rate of intensification be 1～3 DEG C/min.
Preparation method the most according to claim 4, it is characterised in that step (1)
In, it is slowly heated and is warming up to 80～85 DEG C.
Preparation method the most according to claim 4, it is characterised in that step (2)
In, mixed liquor I is cooled to 40～45 DEG C.
Preparation method the most according to claim 4, it is characterised in that step (2)
In, the speed of described stirring is 20～30r/min.
Preparation method the most according to claim 4, it is characterised in that step (3)
In, the time of described stirring is 5～15 minutes.
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| CN106176570A (en) * | 2016-08-31 | 2016-12-07 | 广东芭薇生物科技股份有限公司 | A kind of spraying for skin surface temperature drop and preparation method thereof |
| CN106361684A (en) * | 2016-08-31 | 2017-02-01 | 广东芭薇生物科技股份有限公司 | Active composition for adjusting microorganism ecological balance of skin surface |
| CN106727035A (en) * | 2017-01-23 | 2017-05-31 | 珠海市玖鑫化妆品有限公司 | The preparation technology and antiallergic of a kind of Lignum Aquilariae Resinatum extract repair facial mask |
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| CN104523520A (en) * | 2014-12-19 | 2015-04-22 | 韩嘉 | Application of Aquilaria sinensis extract used as effective constituent for whitening |
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| CN106361684A (en) * | 2016-08-31 | 2017-02-01 | 广东芭薇生物科技股份有限公司 | Active composition for adjusting microorganism ecological balance of skin surface |
| CN106727035A (en) * | 2017-01-23 | 2017-05-31 | 珠海市玖鑫化妆品有限公司 | The preparation technology and antiallergic of a kind of Lignum Aquilariae Resinatum extract repair facial mask |
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