CN105565977A - Controlled-release fertilizer for oranges and preparation method of controlled-release fertilizer - Google Patents
Controlled-release fertilizer for oranges and preparation method of controlled-release fertilizer Download PDFInfo
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- CN105565977A CN105565977A CN201510960204.4A CN201510960204A CN105565977A CN 105565977 A CN105565977 A CN 105565977A CN 201510960204 A CN201510960204 A CN 201510960204A CN 105565977 A CN105565977 A CN 105565977A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/70—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting wettability, e.g. drying agents
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Plant Pathology (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses controlled-release fertilizer for oranges and a preparation method of the controlled-release fertilizer and belongs to the technical field of fertilizer preparation. The controlled-release fertilizer for the oranges comprises, by weight, 40-100 parts of wrapping material and 150-600 parts of fertilizer particles. The controlled-release fertilizer is prepared by steps of crushing, extracting, filtering, concentrating, fermenting, pelleting, drying, cooling, packaging and the like. The controlled-release fertilizer is moderate and stable in controlled-release speed, balanced in nutrition, capable of promoting the oranges to grow fast and healthily, capable of shortening the growth period, capable of increasing orange yield, capable of effectively preventing diseases and pests, and capable of improving soil environments. The preparation method is simple to operate and beneficial to popularization and application.
Description
Technical field
The invention belongs to fertilizer preparing technical field, be specifically related to a kind of mandarin orange orange release and release control fertilizer and preparation method thereof.
Background technology
Chemical fertilizer has been acknowledged as the volume increase of farm crop and has played very important effect.And the utilization ratio of chemical fertilizer is less than 30% at present, rest part, with soil erosion, is used chemical fertilizer and is not only caused significant wastage, also pollutes soil and groundwater resource, and therefore the slow control release type fertilizer of development is classified as the support project given priority to by country.There is slow control-release function type fertilizer at present and seldom can play applied once, fertilizer can be provided to farm crop, the object controlling worm can be played again, because slow control-release function type fertilizer saves labor, saves manpower, thus national agricultural technology center using existing fertilizer efficiency again can the medicine of preventing disease pest control weeding fertile in key popularized project.General medicine fertilizer is processed by special process by chemical fertilizer and chemical pesticide, and its fertilizer and agriculture the effective elements of the medicine do not possess slow control-release function, except not reaching crop demand in whole vegetative period, go back contaminated soil and groundwater resource.Especially the pollution of chemical pesticide is comparatively serious, by repeatedly using, often causing the pesticide residue in farm crop to exceed standard, having a strong impact on physical and mental health and the competitive power of agricultural products in China in world market of people.
Based on the situation that the ratio of above reason and current rural laborer's aging and women and children is increasing, be badly in need of one and can provide fertilizer efficiency, have again an insecticidal function; Can utilization rate of fertilizer be improved, the desinsection time can be extended again, and the Multifucntional fertilizer of non agricultural chemical residuum, therefore, develop a kind of controlled release rate moderate stable and the fertilizer with Biocidal type is development trend.
Summary of the invention
The invention provides a kind of mandarin orange orange release and release control fertilizer and preparation method thereof, cause that utilization ratio is low, the use of chemical pesticide causes Practice for Pesticide Residue in Agricultural Products large to solve current direct use chemical fertilizer, human body is produced to the problems such as larger infringement, fertilizer control release speed of the present invention is moderate and stable, balanced in nutrition, effectively can reduce the turnover rate of fertilizer, improve the utilising efficiency of fertilizer, promote that mandarin orange orange is grown up healthy and sound fast, improve mandarin orange orange output; Simultaneously also can preventing disease and pest effectively, improve edatope, keep ecological, environmental protective.
For solving above technical problem, the present invention by the following technical solutions:
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 40-100 part, fertiliser granulates 150-600 part;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 36-90 part, ammonium phosphate 1-2.5 part, saltpetre 1-2.5 part, zinc nitrate 0.8-2 part, lime borate 0.2-0.5 part, iron(ic) chloride 0.2-0.5 part, zinc chloride 0.2-0.5 part, Manganous chloride tetrahydrate 0.2-0.5 part, cupric chloride 0.2-0.5 part, water-holding agent 0.2-0.5 part;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 15-60 part, bark of official magnolia 15-60 part, weeping willow leaf 15-60 part, trypterygine 15-60 part, leaf of tea tree 15-60 part, Herba Patriniae 15-60 part, bitter dish 15-60 part, Herba Sophorae alopecuroidis 15-60 part, waste residue 10-40 part, earthworm powder 8-32 part, yellow humic acid 6-24 part, biological bacteria 2-8 part, micro-1-4 part, amendment 1-4 part, dispersion agent 1-4 part, permeate agent 1-4 part.
Preferably, described water-holding agent comprises one or more in polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch graft acrylic acid sodium.
Preferably, described waste residue comprises one or more in marc, bagasse, edible fungi residues, sugared slag, acid-sludge, fecula, manioc waste, citric acid waste, soy sauce residues, residue of monosodium glutamate, residue from beans after making.
Preferably, described biological bacteria comprises one or more in vinelandii, brood cell liver bacterium, enzymatic microorganism, yeast, actinomycetes, root nodule bacterium, phosphorus bacteria, B. mucilaginocus, phosphate solubilizing bacteria.
Preferably, described trace element comprises one or more in iron, boron, manganese, copper, zinc, molybdenum.
Preferably, described amendment comprises one or more in wilkinite, kaolin, diatomite, gypsum.
Preferably, described dispersion agent comprises one or more in calcium lignin sulphonate, N-sodium lauroyl glutamate, sodium laurylsulfate.
Preferably, described permeate agent comprises one or more in soap powder, sodium lignosulfonate, alkyl sodium sulfonate, sodium alkyl benzene sulfonate, alkyl sulfuric ester sodium.
The present invention also provides the preparation method of a kind of mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:8-16, ultrasonic power is 140-180W, alcohol concn is 50%-80%, Extracting temperature is 50-70 DEG C, extraction time is 60-90min, gained medical filtration, mixture is obtained after being concentrated into water content≤24%, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent is at 65-80 DEG C of bottom fermentation 10-18 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 45-65 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be at 90-100 DEG C, be dried to water content≤6% after 1.5-2.5mm particle, be cooled to 25-30 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: the lapping obtained with step S2 is dried to water content≤6% after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 45-65 DEG C, obtained mandarin orange orange release and release control fertilizer.
It is as follows that instant component has effect:
China tree famous paradise tree, it contains toxin, can as sterilant, wormer and growth inhibitor.
The ether of the bark of official magnolia and methanol extract have strong anti-microbial effect to cariogenic bacteria streptococcus mutans (Streptococusmatuans), and its Antibacterial Constituents is defined as Magnolol and Honokiol.Both are 6.3 μ g/ml to the minimum inhibitory concentration (MIC) of streptococcus mutans, and its anti-microbial effect (to streptococcus mutans) is stronger than berberine.The first deduction of the bark of official magnolia divides magnocurarine and Cortex Magnoliae Officinalis volatile oil saturated aqueous solution to have certain bacteriostatic action to streptococcus aureus, sarcina and Bacillus subtilus, and the bark of official magnolia also has anti-microbial activity to pneumococcus and dysentery bacterium.
Weeping willow leaf has the effect such as clearing heat and detoxicating, expelling wind and removing dampness, antisepsis and anti-inflammation, maggot of going out, infanticide Jue.
Trypterygine can be dispeled the wind, removing toxic substances, desinsection.External application treating rheumatic arthritis, skin is itched, and kills maggot, wriggler, water-snail eradication, malicious mouse.
The extract of leaf of tea tree has potent germicidal action, and tea tree can effectively tackle for various fungal infection, can kill streptococcus aureus, diphtheria corynebacterium.
Herba Patriniae, with root stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Herba Patriniae has suppression or killing action to streptococcus aureus, dysentery bacterium, Corynebacterium diphtheriae, Pseudomonas aeruginosa.
Containing the composition such as taraxasterol, choline in bitter dish, stronger germicidal action is had to staphylococcus aureus resistance bacterial strain, Hemolytic streptococcus, also there is certain lethal effect to pneumococcus, meningococcus, diphtheria corynebacterium, Pseudomonas aeruginosa, dysentery bacterium etc., therefore all have certain curative effect to icterohepatitis, pharyngolaryngitis, bacillary dysentery, cold, fever and chronic tracheitis, tonsillitis etc.
The total alkaloid of sophora alopecuroide extracted in Herba Sophorae alopecuroidis has anti-inflammatory, anticancer, anti-allergic, anti-heart disorder, antiulcer agent, leukocyte increasing, relievings asthma, antipyretic, desinsection, calmness, analgesia, the effect such as antiviral; The external application of Herba Sophorae alopecuroidis powder has suppression or killing action to staphylococcus, intestinal bacteria, suis, fungi, bacterium protein of Gardnerella vaginalis and trichomonad; The killing ability of Herba Sophorae alopecuroidis plant is between neonicotine (Anadasine) and lupin alkaloid (Lupinine), and Tocosamine is Biocidal agriculture the effective elements of the medicine.
Containing numerous nutritive ingredients in waste residue, the nutrition of demand of plant growth can be provided as fertilizer, Promoting plant growth.
Earthworm strong adaptability, growth and breeding are fast, output is high, low price, earthworm powder contains all amino acid, and content is high, and phosphorus, calcium, mineral substance, vitamin contents are also very abundant, amino acid can promote root growth, strong sprout, healthy tree, the photosynthetic function of enhancing blade and the degeneration-resistant of crop.
The use of yellow humic acid, not only can increase nutriment in a fertilizer, and effectively can improve encapsulation rate, reduces the consumption of lapping, reduces production cost.
The fertilizer that biological bacteria is made has the function of volume increase, oil recovery enhancement, also has and significantly reduces nitrate in plant materials, nitrite and heavy metal content, improves the effect such as chemical fertilizer utilization ratio and fertilizing soil.
Boron compares and concentrates in stem apex, the tip of a root, blade and floral organ in plant materials, and the content in dicotyledons is usually higher than monocotyledons.Boron can improve the nitrogenase activity of leguminous crop root nodule bacterium, and increase amount of nitrogen fixation, during boron deficiency, root stays undeveloped, affects amount of nitrogen fixation.Boron can also strengthen crop anti-adversity.
Iron is that chlorophyll formation is indispensable, and in plant body, be difficult to transfer, so blade " chlorosis " is the performance of plant iron deficiency, and first this chlorosis shows on young leaflet tablet.
Copper participates in the resistance of the photosynthesis of plant, respiration, nitrogen metabolism, enhancing plant.During scarce copper, plant strain growth is thin and weak, and young leaves turns to be yellow, and wilting withered, blade tip is curling to turn white, and has necrotic spot.
Zinc can promote that crop carries out photosynthesis, and it is the moiety of multiple enzyme, and during scarce zinc, stagnating appears in crop growth.
Containing manganese in plant chloroplast, manganese can promote seed germination and seedling growth in period, affects the accumulation in vivo of the photosynthesis of crop, respiration, nitric nitrogen during manganese deficiency.Show as chlorosis yellow between blade arteries and veins, have brown spot.
Molybdenum is nitrogen-fixing microorganism, necessary when particularly fixing air nitrogen with the root nodule bacterium of leguminous crop symbiosis.Leaf photosynthesis intensity can be promoted again simultaneously.During scarce molybdenum, plant is short and small, chlorosis between blade arteries and veins, and leaf margin is dried-up, inwardly curling, becomes wilting state.
Water-holding agent can strengthen soil water-retaining performance, improvement Soil structure, the deep percolation reducing water and loss of soil nutrient, raising efficiency of water application.
Amendment can improve soil, increases fertilizer efficiency and stimulates crop growth, is soil fertilizer conditioner and long agent is urged in soil-repairing agent, plant growth.
Dispersion agent can reduce the viscosity of fertilizer particle and high molecular polymer, and fertilizer particle can be made to be quickly dispersed in water, and high molecular polymer also can be made to play its dispersiveness simultaneously.
Permeate agent has fixing hydrophilic and oleophilic group, aligns in the surface energy of solution, and can make the material that surface tension significantly declines, and has the effect making fertilizer efficiency and drug effect synergy simultaneously.
The present invention has following beneficial effect:
(1) mandarin orange orange release and release control fertilizer controlled release rate of the present invention is moderate and stable, and fertiliser granulates is balanced in nutrition, effectively can reduce the turnover rate of fertilizer, improves the utilising efficiency of fertilizer, promotes that mandarin orange orange is grown up healthy and sound fast, improves mandarin orange orange output;
(2) in mandarin orange orange release and release control fertilizer of the present invention, lapping increases the element such as nitrogen, phosphorus, potassium, calcium, boron, zinc, iron, manganese, copper needed for the growth of mandarin orange orange, controlled release fertilizer in early stage can be avoided not enough, affect the shortcoming of mandarin orange orange growth;
(3) in mandarin orange orange release and release control fertilizer of the present invention, lapping increases water-holding agent, can strengthen soil water-retaining performance, improvement Soil structure, the deep percolation reducing water and loss of soil nutrient, raising efficiency of water application;
(4) mandarin orange orange release and release control fertilizer of the present invention uses yellow humic acid, effectively can improve encapsulation rate, reduce the consumption of lapping, reduce production cost;
(5) mandarin orange orange release and release control fertilizer of the present invention uses amendment, can improve soil, increase fertilizer efficiency and stimulate crop growth;
(6) mandarin orange orange release and release control fertilizer of the present invention uses dispersion agent, can reduce the viscosity of fertilizer particle and high molecular polymer, fertilizer particle can be made to be quickly dispersed in water, be conducive to plant absorption;
(7) mandarin orange orange release and release control fertilizer of the present invention uses permeate agent to have the effect making fertilizer efficiency and drug effect synergy;
(8) mandarin orange orange release and release control fertilizer composition of the present invention large absolutely portion degradable, can not bring environmental pollution;
(9) mandarin orange of the present invention orange release and release control fertilizer can not only preventing disease and pest effectively, shortens growth cycle, improves crop yield, and can improve edatope;
(10) mandarin orange orange release and release control fertilizer preparation method of the present invention is simple to operate, is conducive to applying.
Embodiment
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 40 parts, fertiliser granulates 600 parts;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 36 parts, 1 part, ammonium phosphate, 1 part, saltpetre, zinc nitrate 0.8 part, lime borate 0.2 part, 0.2 part, iron(ic) chloride, zinc chloride 0.2 part, Manganous chloride tetrahydrate 0.2 part, cupric chloride 0.2 part, polyacrylamide 0.2 part;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 60 parts, the bark of official magnolia 60 parts, 60 parts, weeping willow leaf, trypterygine 60 parts, leaf of tea tree 60 parts, Herba Patriniae 60 parts, bitter dish 60 parts, Herba Sophorae alopecuroidis 60 parts, marc 40 parts, earthworm powder 32 parts, yellow humic acid 24 parts, 8 parts, yeast, boron 4 parts, wilkinite 4 parts, calcium lignin sulphonate 4 parts, soap powder 4 parts.
The preparation method of described mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:8, ultrasonic power is 140W, alcohol concn is 50%, Extracting temperature is 50 DEG C, extraction time is 90min, gained medical filtration, be concentrated into water content be after 24% mixture, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent was 65 DEG C of bottom fermentations 18 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 45 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be that at 90-100 DEG C, be dried to water content after 1.5-2.5mm particle be 6%, be cooled to 25 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: it is 6% that the lapping obtained with step S2 is dried to water content after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 45-55 DEG C, obtains mandarin orange orange release and release control fertilizer.
Embodiment 2
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 100 parts, fertiliser granulates 150 parts;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 90 parts, 2.5 parts, ammonium phosphate, 2.5 parts, saltpetre, zinc nitrate 2 parts, lime borate 0.5 part, 0.5 part, iron(ic) chloride, zinc chloride 0.5 part, Manganous chloride tetrahydrate 0.5 part, cupric chloride 0.5 part, sodium polyacrylate 0.5 part;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 15 parts, the bark of official magnolia 15 parts, 15 parts, weeping willow leaf, trypterygine 15 parts, leaf of tea tree 15 parts, Herba Patriniae 15 parts, bitter dish 15 parts, Herba Sophorae alopecuroidis 15 parts, bagasse 10 parts, earthworm powder 8 parts, yellow humic acid 6 parts, enzymatic microorganism 2 parts, boron 0.5 part, manganese element 0.5 part, kaolin 1 part, N-sodium lauroyl glutamate 1 part, sodium lignosulfonate 1 part.
The preparation method of described mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:16, ultrasonic power is 180W, alcohol concn is 80%, Extracting temperature is 70 DEG C, extraction time is 60min, gained medical filtration, be concentrated into water content be after 20% mixture, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent was 80 DEG C of bottom fermentations 10 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 65 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be that at 90-100 DEG C, be dried to water content after 1.5-2.5mm particle be 4%, be cooled to 30 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: it is 4% that the lapping obtained with step S2 is dried to water content after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 55-65 DEG C, obtains mandarin orange orange release and release control fertilizer.
Embodiment 3
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 70 parts, fertiliser granulates 350 parts;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 63 parts, 1.8 parts, ammonium phosphate, 1.8 parts, saltpetre, zinc nitrate 1.5 parts, lime borate 0.4 part, 0.3 part, iron(ic) chloride, zinc chloride 0.3 part, Manganous chloride tetrahydrate 0.3 part, cupric chloride 0.3 part, polyacrylic acid potassium 0.1 part, ammonium polyacrylate 0.1 part, 0.1 part, starch graft acrylic acid sodium;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 35 parts, the bark of official magnolia 35 parts, 35 parts, weeping willow leaf, trypterygine 35 parts, leaf of tea tree 35 parts, Herba Patriniae 35 parts, bitter dish 35 parts, Herba Sophorae alopecuroidis 35 parts, edible fungi residues 5 parts, sugar slag 5 parts, acid-sludge 5 parts, fecula 5 parts, manioc waste 5 parts, earthworm powder 20 parts, yellow humic acid 12 parts, 1 part, vinelandii, enzymatic microorganism 1 part, phosphorus bacteria 1 part, B. mucilaginocus 1 part, phosphate solubilizing bacteria 1 part, ferro element 0.5 part, boron 0.5 part, manganese element 0.5 part, copper 0.5 part, wilkinite 0.5 part, kaolin 0.5 part, 0.5 part, diatomite, 0.5 part, gypsum, N-sodium lauroyl glutamate 1 part, sodium laurylsulfate 1 part, alkyl sodium sulfonate 1 part, sodium alkyl benzene sulfonate 1 part.
The preparation method of described mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:12, ultrasonic power is 160W, alcohol concn is 75%, Extracting temperature is 60 DEG C, extraction time is 75min, gained medical filtration, be concentrated into water content be after 22% mixture, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent was 70 DEG C of bottom fermentations 16 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 55 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be that at 90-100 DEG C, be dried to water content after 1.5-2.5mm particle be 5%, be cooled to 27 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: it is 5% that the lapping obtained with step S2 is dried to water content after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 65 DEG C, obtains mandarin orange orange release and release control fertilizer.
Embodiment 4
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 50 parts, fertiliser granulates 500 parts;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 45 parts, 1.2 parts, ammonium phosphate, 1.2 parts, saltpetre, zinc nitrate 1 part, lime borate 0.3 part, 0.3 part, iron(ic) chloride, zinc chloride 0.2 part, Manganous chloride tetrahydrate 0.2 part, cupric chloride 0.2 part, polyacrylamide 0.2 part, 0.2 part, starch graft acrylic acid sodium;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 50 parts, the bark of official magnolia 50 parts, 50 parts, weeping willow leaf, trypterygine 50 parts, leaf of tea tree 50 parts, Herba Patriniae 50 parts, bitter dish 50 parts, Herba Sophorae alopecuroidis 50 parts, citric acid waste 8 parts, soy sauce residues 8 parts, residue of monosodium glutamate 8 parts, residue from beans after making 8 parts, earthworm powder 30 parts, yellow humic acid 20 parts, brood cell liver bacterium 1 part, 1 part, yeast, 1 part, actinomycetes, root nodule bacterium 1 part, phosphorus bacteria 1 part, B. mucilaginocus 1 part, boron 1 part, zinc element 1 part, molybdenum element 1 part, 3 parts, diatomite, calcium lignin sulphonate 3 parts, sodium lignosulfonate 3 parts.
The preparation method of described mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:10, ultrasonic power is 150W, alcohol concn is 60%, Extracting temperature is 55 DEG C, extraction time is 80min, gained medical filtration, be concentrated into water content be after 24% mixture, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent was 75 DEG C of bottom fermentations 12 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 50 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be that at 90-100 DEG C, be dried to water content after 1.5-2.5mm particle be 6%, be cooled to 29 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: it is 6% that the lapping obtained with step S2 is dried to water content after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 50 DEG C, obtains mandarin orange orange release and release control fertilizer.
Embodiment 5
A kind of mandarin orange orange release and release control fertilizer, in units of weight part, comprises following raw material: lapping 90 parts, fertiliser granulates 300 parts;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 81 parts, 2.3 parts, ammonium phosphate, 2.3 parts, saltpetre, zinc nitrate 2 parts, lime borate 0.4 part, 0.4 part, iron(ic) chloride, zinc chloride 0.4 part, Manganous chloride tetrahydrate 0.4 part, cupric chloride 0.4 part, polyacrylamide 0.4 part;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 30 parts, the bark of official magnolia 30 parts, 30 parts, weeping willow leaf, trypterygine 30 parts, leaf of tea tree 30 parts, Herba Patriniae 30 parts, bitter dish 30 parts, Herba Sophorae alopecuroidis 30 parts, edible fungi residues 20 parts, earthworm powder 16 parts, yellow humic acid 12 parts, 4 parts, yeast, boron 2 parts, 2 parts, gypsum, N-sodium lauroyl glutamate 2 parts, alkyl sodium sulfonate 2 parts.
The preparation method of described mandarin orange orange release and release control fertilizer, comprises the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:14, ultrasonic power is 170W, alcohol concn is 70%, Extracting temperature is 65 DEG C, extraction time is 70min, gained medical filtration, be concentrated into water content be after 20% mixture, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent was 80 DEG C of bottom fermentations 10 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 65 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be that at 90-100 DEG C, be dried to water content after 1.5-2.5mm particle be 6%, be cooled to 26 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: it is 5% that the lapping obtained with step S2 is dried to water content after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 65 DEG C, obtains mandarin orange orange release and release control fertilizer.
For the effect of checking mandarin orange orange of the present invention release and release control fertilizer, by following experimental verification.
(1) the result of extraction experiment of Wrapped fertilizer
Mandarin orange orange release and release control fertilizer prepared by Example 1,2,3, and Example 1 prepare without Wrapped fertilizer and with the fertilizer of polyethylene parcel in contrast, be immersed in clear water, at different time water sampling detection fertilizer solubility rate wherein, result is as shown in the table.
As seen from the above table, almost all dissolve at once without Wrapped fertilizer, show not there is slow releasing function; The fertilizer wrapped up with polyethylene, except not having the fertiliser granulates of environmental sealing (encapsulating) in initial dissolving, almost no longer disengages fertilizer thereafter; The encapsulation rate of mandarin orange orange release and release control fertilizer prepared by embodiment 1,2,3 is higher, and the fertilizer of major part encapsulating continues to disengage later.
(2) mandarin orange orange fertilizer control release effect experimental
Experiment one: the mandarin orange orange release and release control fertilizer adopting embodiment 1 to prepare carries out manurial experiment to mandarin orange orange, use once as base manure for annual, simultaneously with embodiment 1 prepare without Wrapped fertilizer particle for contrast, other planting conditions are identical, and experimental group increases production 9.9% than the mandarin orange orange mean yield of control group.
Experiment two: the mandarin orange orange release and release control fertilizer adopting embodiment 2 to prepare carries out manurial experiment to mandarin orange orange, use once as base manure for annual, simultaneously with embodiment 2 prepare without Wrapped fertilizer particle for contrast, other planting conditions are identical, and experimental group increases production 10.3% than the mandarin orange orange mean yield of control group.
Experiment three: the mandarin orange orange release and release control fertilizer adopting embodiment 3 to prepare carries out manurial experiment to mandarin orange orange, use once as base manure for annual, simultaneously with embodiment 3 prepare without Wrapped fertilizer particle for contrast, other planting conditions are identical, and experimental group increases production 10.7% than the mandarin orange orange mean yield of control group.
Comprehensive above three experiments are known, mandarin orange orange mean yield volume increase 9.9%-10.7%, visible mandarin orange orange release and release control fertilizer of the present invention, effectively can reduce the turnover rate of fertilizer, improve the utilising efficiency of fertilizer, simultaneously balanced in nutrition, can promote that mandarin orange orange is grown up healthy and sound fast, improve mandarin orange orange output.
(3) mandarin orange orange release and release control fertilizer preventing disease and pest effect experimental
Choose the mandarin orange orange ground that six block specifications are basically identical, be set to mandarin orange orange ground a, mandarin orange orange ground b, mandarin orange orange ground c, mandarin orange orange ground d, mandarin orange orange ground e, mandarin orange orange ground f, mandarin orange orange is planted on six pieces of ground, wherein mandarin orange orange ground a, mandarin orange orange ground b, mandarin orange orange ground c use same not have the common fertilizer of Biocidal, mandarin orange orange ground d, mandarin orange orange ground e, mandarin orange orange ground f use the fertilizer of embodiment 1,2,3 respectively, calculate with every mu of fertilising 120kg, observe the mandarin orange orange growing state on six pieces of mandarin orange orange ground.Result shows: mandarin orange orange ground a, mandarin orange orange ground b, the mandarin orange orange gloss difference that mandarin orange orange ground c kind is planted, plant is unhealthy, the speed of growth is slow, plant is little, yield poorly, and mandarin orange orange ground d, mandarin orange orange ground e, the mandarin orange orange good luster that mandarin orange orange ground f kind is planted, plant is healthy, leaf dark green is plump, fast growth, plant is large, output is high, with do not use the mandarin orange of product of the present invention orange compared with, every mu of volume increase 1128.5-1191.6kg, and use the disease and pest in the mandarin orange of product of the present invention orange ground substantially not have, visible mandarin orange of the present invention orange release and release control fertilizer can not only preventing disease and pest effectively, and can be balanced in nutrition, improve edatope, promote that farm crop grow up healthy and sound fast, shorten growth cycle, improve crop yield.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (9)
1. a mandarin orange orange release and release control fertilizer, is characterized in that, in units of weight part, comprise following raw material: lapping 40-100 part, fertiliser granulates 150-600 part;
Described lapping, in units of weight part, comprises following raw material: fatty acid amide 36-90 part, ammonium phosphate 1-2.5 part, saltpetre 1-2.5 part, zinc nitrate 0.8-2 part, lime borate 0.2-0.5 part, iron(ic) chloride 0.2-0.5 part, zinc chloride 0.2-0.5 part, Manganous chloride tetrahydrate 0.2-0.5 part, cupric chloride 0.2-0.5 part, water-holding agent 0.2-0.5 part;
Described fertiliser granulates, in units of weight part, comprises following raw material:
China tree 15-60 part, bark of official magnolia 15-60 part, weeping willow leaf 15-60 part, trypterygine 15-60 part, leaf of tea tree 15-60 part, Herba Patriniae 15-60 part, bitter dish 15-60 part, Herba Sophorae alopecuroidis 15-60 part, waste residue 10-40 part, earthworm powder 8-32 part, yellow humic acid 6-24 part, biological bacteria 2-8 part, micro-1-4 part, amendment 1-4 part, dispersion agent 1-4 part, permeate agent 1-4 part.
2. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described water-holding agent comprise in polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch graft acrylic acid sodium one or more.
3. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described waste residue comprise in marc, bagasse, edible fungi residues, sugared slag, acid-sludge, fecula, manioc waste, citric acid waste, soy sauce residues, residue of monosodium glutamate, residue from beans after making one or more.
4. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described biological bacteria comprise in vinelandii, brood cell liver bacterium, enzymatic microorganism, yeast, actinomycetes, root nodule bacterium, phosphorus bacteria, B. mucilaginocus, phosphate solubilizing bacteria one or more.
5. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described trace element comprise in iron, boron, manganese, copper, zinc, molybdenum one or more.
6. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described amendment comprise in wilkinite, kaolin, diatomite, gypsum one or more.
7. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described dispersion agent comprise in calcium lignin sulphonate, N-sodium lauroyl glutamate, sodium laurylsulfate one or more.
8. mandarin orange according to claim 1 orange release and release control fertilizer, is characterized in that, described permeate agent comprise in soap powder, sodium lignosulfonate, alkyl sodium sulfonate, sodium alkyl benzene sulfonate, alkyl sulfuric ester sodium one or more.
9. a preparation method for the mandarin orange orange release and release control fertilizer according to any one of claim 1-8, is characterized in that, comprise the following steps:
S1: by China tree, the bark of official magnolia, weeping willow leaf, trypterygine, leaf of tea tree, Herba Patriniae, bitter dish, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, the condition extracted is: solid-liquid ratio is 1:8-16, ultrasonic power is 140-180W, alcohol concn is 50%-80%, Extracting temperature is 50-70 DEG C, extraction time is 60-90min, gained medical filtration, mixture is obtained after being concentrated into water content≤24%, waste residue is added in mixture, earthworm powder, yellow humic acid, biological bacteria, trace element, amendment, dispersion agent, permeate agent is at 65-80 DEG C of bottom fermentation 10-18 days, fermented liquid is left standstill and abandons precipitation, and remaining ferment liquid is concentrated at 45-65 DEG C, obtain enriched material, particle diameter is caused by described enriched material to be at 90-100 DEG C, be dried to water content≤6% after 1.5-2.5mm particle, be cooled to 25-30 DEG C, obtained fertiliser granulates,
S2: after fatty acid amide, ammonium phosphate, zinc nitrate, saltpetre, lime borate, iron(ic) chloride, zinc chloride, Manganous chloride tetrahydrate, cupric chloride, water-holding agent are fully mixed, obtained lapping;
S3: the lapping obtained with step S2 is dried to water content≤6% after evenly being wrapped up by the fertiliser granulates that step S1 is obtained at temperature is 45-65 DEG C, obtained mandarin orange orange release and release control fertilizer.
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| CN106007996A (en) * | 2016-05-27 | 2016-10-12 | 广西宁明百事康生物工程有限公司 | Special ecological liquid fertilizer for navel oranges and preparation method of special ecological liquid fertilizer |
| CN106045668A (en) * | 2016-05-27 | 2016-10-26 | 邓万超 | Special fertilizer for increasing sugar-acid ratio and juice content of oranges and application method of special fertilizer |
| CN106064982A (en) * | 2016-05-27 | 2016-11-02 | 广西宁明百事康生物工程有限公司 | Improve dedicated fertilizer of Citrus sinensis Osbeck diseases and insect pests resistance and yield and preparation method thereof |
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| CN102584439A (en) * | 2012-02-08 | 2012-07-18 | 叶长东 | Tea tree slow-release fertilizer and preparation technology thereof |
| CN102584478A (en) * | 2012-03-29 | 2012-07-18 | 叶长东 | Banana controlled-release fertilizer and preparation technology |
| CN104045408A (en) * | 2013-03-11 | 2014-09-17 | 叶长东 | Cassava release-controlled fertilizer and preparation technology thereof |
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| CN106007996A (en) * | 2016-05-27 | 2016-10-12 | 广西宁明百事康生物工程有限公司 | Special ecological liquid fertilizer for navel oranges and preparation method of special ecological liquid fertilizer |
| CN106045668A (en) * | 2016-05-27 | 2016-10-26 | 邓万超 | Special fertilizer for increasing sugar-acid ratio and juice content of oranges and application method of special fertilizer |
| CN106064982A (en) * | 2016-05-27 | 2016-11-02 | 广西宁明百事康生物工程有限公司 | Improve dedicated fertilizer of Citrus sinensis Osbeck diseases and insect pests resistance and yield and preparation method thereof |
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Application publication date: 20160511 |