CN105062262A - Building interior wall special-purpose antibacterial mildew-resistant emulsion paint - Google Patents
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Abstract
The invention discloses building interior wall special-purpose antibacterial mildew-resistant emulsion paint. The building interior wall special-purpose antibacterial mildew-resistant emulsion paint comprises acrylic acid emulsion, polyurethane emulsion, bisphenol A epoxy resin, diphenylsilanediol, nanometer titanium dioxide, nanometer silica sol, nanometer zinc oxide, active carbon, tourmaline nanometer powder, dodecafluoroheptyl methacrylate, a film forming assistant, sorbitan monopalmitate, lauric acid, phenolic resin, N-phenyl-N'-cyclohexyl-p-phenylenediamine, potassium citrate, propyl p-hydroxybenzoate, succinic acid, sodium alginate, imidazolidone, chitosan, water and an assistant. The building interior wall special-purpose antibacterial mildew-resistant emulsion paint can form a fine paint film, has good antibiosis and mildew resistance and excellent water resistance and workability, has a refreshing smell and has strong adhesion to a base material.
Description
Technical field
The present invention relates to emulsion paint technical field, particularly relate to the special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building.
Background technology
Emulsion paint is water-dispersible paint, and it take synthetic resin emulsion as base-material, and filler adds the coating that various auxiliary agent is refined after grinding distribution.Emulsion paint has possessed the many merits different from conventional wall coating materials, and as being easy to brushing, drying is rapid, paint film is water-fast, scrub resistance is good.
Along with the enhancing of growth in the living standard and health perception, people are to the Environmental Safety growing interest of living environment and attention, more and more stricter to the environmental requirement of indoor hardware fitting.Interiro wall latex paint is as one of the important component part of house decorative material, and it is ornamental, the feature of environmental protection and the functional common concern being subject to numerous residents.Tradition emulsion paint is relative to solvent based coating, and volatilization is slow, and in film, the residence time is long; Antibacterial and mouldproof effect is undesirable, because growing of mushroom easily putrid and deteriorated phenomenon occurs in emulsion paint storage and the process that uses; Water tolerance and weather resistance are not very desirable, long-time use easily causes cracking, peels off, shedding, variable color, non-easy cleaning, lose its decorative effect.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes the special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building, its paint film is fine and smooth, and antibacterial and mouldproof is good, and water tolerance, weather resistance and workability are excellent, and smell is pure and fresh, with the strong adhesion of ground.
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: ACRYLIC EMULSION 20-50 part, polyaminoester emulsion 10-30 part, bisphenol A epoxide resin 5-10 part, diphenyl silanodiol 2-10 part, nano titanium oxide 5-12 part, Nano silica sol 4-15 part, nano zine oxide 5-25 part, gac 1-5 part, strange ice stone nano powder 3-10 part, dodecafluoroheptyl methacrylate 3-15 part, film coalescence aid 20-30 part, sorbitol anhydride monopalmitate 1-5 part, lauric acid 3-8 part, resol 1-5 part, N-phenyl-N '-cyclohexyl Ursol D 0.5-2 part, Tripotassium Citrate 1-2 part, propylparaben 2-5 part, succsinic acid 1-3 part, sodium alginate 0.5-2 part, imidazolidone 2-6 part, chitosan 0.1-0.8 part, water 50-80 part, auxiliary agent 1-2 part.
Preferably, its raw material comprises following component by weight: ACRYLIC EMULSION 30-45 part, polyaminoester emulsion 18-25 part, bisphenol A epoxide resin 7-9 part, diphenyl silanodiol 5-8 part, nano titanium oxide 7-10 part, Nano silica sol 8-12 part, nano zine oxide 15-20 part, gac 3-4.5 part, strange ice stone nano powder 6-9 part, dodecafluoroheptyl methacrylate 9-11 part, film coalescence aid 25-28 part, sorbitol anhydride monopalmitate 2.5-4 part, lauric acid 5-7 part, resol 3-4.5 part, N-phenyl-N '-cyclohexyl Ursol D 1-1.6 part, Tripotassium Citrate 1.5-1.8 part, propylparaben 3-4.5 part, succsinic acid 1.8-2.2 part, sodium alginate 1-1.6 part, imidazolidone 3-4.6 part, chitosan 0.4-0.6 part, water 70-76 part, auxiliary agent 1.4-1.8 part.
Preferably, its raw material comprises following component by weight: ACRYLIC EMULSION 40 parts, polyaminoester emulsion 20 parts, bisphenol A epoxide resin 8 parts, diphenyl silanodiol 6.3 parts, nano titanium oxide 8.5 parts, Nano silica sol 10 parts, nano zine oxide 17 parts, gac 4 parts, strange ice stone nano powder 8 parts, dodecafluoroheptyl methacrylate 10 parts, film coalescence aid 26 parts, sorbitol anhydride monopalmitate 3.2 parts, lauric acid 6.3 parts, 4 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 1.2 parts, Tripotassium Citrate 1.6 parts, propylparaben 4 parts, succsinic acid 2 parts, sodium alginate 1.2 parts, imidazolidone 4 parts, chitosan 0.5 part, 73 parts, water, auxiliary agent 1.6 parts.
Preferably, described ACRYLIC EMULSION is one or more the combination in pure-acrylic emulsion, benzene emulsion, organosilicon crylic acid latex, acrylate and vinyl acetate emulsion.
Preferably, the median size of described nano titanium oxide is 10-30nm; The median size of described Nano silica sol is 10-25nm; The median size of described nano zine oxide is 20-35nm.
Preferably, described film coalescence aid is one or more the combination in ethylene glycol, propylene glycol, butyl glycol ether, di-isopropyl succinate, 2,2,4-trimethylammonium-1,3-pentanediol diisobutyrates.
Preferably, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 20-30 part anhydrous methanol by the attapulgite after 5-15 part purifying by weight, stir 3-5h, then 2-4 part zinc chloride and 0.3-1.8 part iron(ic) chloride is added, after stirring, the pH value of regulation system is 9-10, stir 20-50min, centrifugal under the rotating speed of 3500-5000r/min, washing, dry, then add in 20-30 part water, stir and add 2-3.5 part cetyl trimethylammonium bromide and 5-12 part anhydrous methanol, hydro-thermal reaction 25-30h is carried out at 175-190 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 3.5-5h is reacted at 350-390 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
Preferably, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 25 parts of anhydrous methanols by the attapulgite after 10 parts of purifying by weight, stir 4h, then 3 parts of zinc chloride and 1.2 parts of iron(ic) chloride are added, after stirring, the pH value of regulation system is 9, stir 35min, centrifugal under the rotating speed of 4000r/min, washing, dry, then add in 26 parts of water, stir and add 3.2 parts of cetyl trimethylammonium bromides and 10 parts of anhydrous methanols, hydro-thermal reaction 28h is carried out at 185 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 4.3h is reacted at 380 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
The special Anti-bacterial mildew-proof latex paint of inner wall of building of the present invention can emulsion paint preparation technology conveniently be prepared from.
In the present invention, have selected ACRYLIC EMULSION, polyaminoester emulsion, bisphenol A epoxide resin and coordinate filmogen as emulsion paint according to a certain percentage, give weathering resistance, water tolerance, the erosion resistance of emulsion paint excellence, and improve the cohesive force of film, reduce the shrinking percentage of film; Diphenyl silanodiol joins in emulsion paint, can with bisphenol A epoxide resin effect, formed containing the epoxy resin of element silicon, add in system, improve flame retardant resistance and the thermotolerance of emulsion paint; Nano titanium oxide has anti-microbial property, join in emulsion paint, coordinate with Nano silica sol, nano zine oxide, gac, strange ice stone nano powder, by regulating the ratio of each filler, its performance is worked in coordination with, impart the permanent germ resistance of emulsion paint, weathering resistance, and there is the effect purified air; Dodecafluoroheptyl methacrylate joins in system, good with the consistency of raw material each in system, owing to introducing fluorine element, improves the water tolerance of emulsion paint, improves the weather resistance of emulsion paint; N-phenyl-N '-cyclohexyl Ursol D joins in emulsion paint, coordinates with resol, improves ageing resistance and the weathering resistance of emulsion paint while making emulsion paint solidify; The cooperation of propylparaben, succsinic acid, sodium alginate, imidazolidone and chitosan joins in system, improve the mildew resistance of emulsion paint, coordinate with nano titanium oxide, Nano silica sol, nano zine oxide, gac, strange ice stone nano powder the germ resistance, mildew resistance and the resistance to soiling that improve emulsion paint, improve the weathering resistance of emulsion paint.
Carry out Performance Detection to the special Anti-bacterial mildew-proof latex paint of inner wall of building of the present invention, detected result is as follows: surface drying time is 0.6-1.8h; The time of doing solid work is 11-14h; Sticking power is 1-2 level; Snappiness is 2-3mm; Impact strength is 30-35kg.cm; 24h water tolerance, peels off without wrinkling, nothing; 48h humidity resistance, peels off without wrinkling, nothing; Resistance to combustion time 25-35min; Flame propagation ratio is 11-15; Mass loss is 1.8-3g; Char volume is 19-23cm
3; Scrub for resistance to 3000-3500 time; Artificial weathering ageing resistance 900-1000h passes through.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: ACRYLIC EMULSION 20 parts, polyaminoester emulsion 30 parts, bisphenol A epoxide resin 5 parts, diphenyl silanodiol 10 parts, nano titanium oxide 5 parts, Nano silica sol 15 parts, nano zine oxide 5 parts, gac 5 parts, strange ice stone nano powder 3 parts, dodecafluoroheptyl methacrylate 15 parts, film coalescence aid 20 parts, sorbitol anhydride monopalmitate 5 parts, lauric acid 3 parts, 5 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 0.5 part, Tripotassium Citrate 2 parts, propylparaben 2 parts, succsinic acid 3 parts, sodium alginate 0.5 part, imidazolidone 6 parts, chitosan 0.1 part, 80 parts, water, auxiliary agent 1 part.
Embodiment 2
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: ACRYLIC EMULSION 50 parts, polyaminoester emulsion 10 parts, bisphenol A epoxide resin 10 parts, diphenyl silanodiol 2 parts, nano titanium oxide 12 parts, Nano silica sol 4 parts, nano zine oxide 25 parts, gac 1 part, strange ice stone nano powder 10 parts, dodecafluoroheptyl methacrylate 3 parts, ethylene glycol 10 parts, propylene glycol 2 parts, butyl glycol ether 5 parts, di-isopropyl succinate 3 parts, 2, 2, 4-trimethylammonium-1, 3-pentanediol diisobutyrate 10 parts, sorbitol anhydride monopalmitate 1 part, lauric acid 8 parts, 1 part, resol, N-phenyl-N '-cyclohexyl Ursol D 2 parts, Tripotassium Citrate 1 part, propylparaben 5 parts, succsinic acid 1 part, sodium alginate 2 parts, imidazolidone 2 parts, chitosan 0.8 part, 50 parts, water, auxiliary agent 2 parts,
Wherein, the median size of described nano titanium oxide is 10nm; The median size of described Nano silica sol is 25nm; The median size of described nano zine oxide is 20nm.
Embodiment 3
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: pure-acrylic emulsion 20 parts, benzene emulsion 5 parts, organosilicon crylic acid latex 6 parts, acrylate and vinyl acetate emulsion 9 parts, polyaminoester emulsion 20 parts, bisphenol A epoxide resin 8 parts, diphenyl silanodiol 6.3 parts, nano titanium oxide 8.5 parts, Nano silica sol 10 parts, nano zine oxide 17 parts, gac 4 parts, strange ice stone nano powder 8 parts, dodecafluoroheptyl methacrylate 10 parts, butyl glycol ether 26 parts, sorbitol anhydride monopalmitate 3.2 parts, lauric acid 6.3 parts, 4 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 1.2 parts, Tripotassium Citrate 1.6 parts, propylparaben 4 parts, succsinic acid 2 parts, sodium alginate 1.2 parts, imidazolidone 4 parts, chitosan 0.5 part, 73 parts, water, auxiliary agent 1.6 parts,
Wherein, the median size of described nano titanium oxide is 30nm; The median size of described Nano silica sol is 10nm; The median size of described nano zine oxide is 35nm;
Described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 30 parts of anhydrous methanols by the attapulgite after 5 parts of purifying by weight, stir 3h, then 4 parts of zinc chloride and 0.3 part of iron(ic) chloride is added, after stirring, the pH value of regulation system is 10, stir 20min, centrifugal under the rotating speed of 5000r/min, washing, dry, then add in 20 parts of water, stir and add 3.5 parts of cetyl trimethylammonium bromides and 5 parts of anhydrous methanols, hydro-thermal reaction 25h is carried out at 190 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 3.5h is reacted at 350 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
Embodiment 4
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: benzene emulsion 20 parts, organosilicon crylic acid latex 10 parts, polyaminoester emulsion 25 parts, bisphenol A epoxide resin 7 parts, diphenyl silanodiol 8 parts, nano titanium oxide 7 parts, Nano silica sol 12 parts, nano zine oxide 15 parts, gac 4.5 parts, strange ice stone nano powder 6 parts, dodecafluoroheptyl methacrylate 11 parts, propylene glycol 20 parts, butyl glycol ether 5 parts, sorbitol anhydride monopalmitate 4 parts, lauric acid 5 parts, 4.5 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 1 part, Tripotassium Citrate 1.8 parts, propylparaben 3 parts, succsinic acid 2.2 parts, sodium alginate 1 part, imidazolidone 4.6 parts, chitosan 0.4 part, 76 parts, water, auxiliary agent 1.4 parts,
Wherein, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 20 parts of anhydrous methanols by the attapulgite after 15 parts of purifying by weight, stir 5h, then 2 parts of zinc chloride and 1.8 parts of iron(ic) chloride are added, after stirring, the pH value of regulation system is 9, stir 50min, centrifugal under the rotating speed of 3500r/min, washing, dry, then add in 30 parts of water, stir and add 2 parts of cetyl trimethylammonium bromides and 12 parts of anhydrous methanols, hydro-thermal reaction 30h is carried out at 175 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 5h is reacted at 350 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
Embodiment 5
The special Anti-bacterial mildew-proof latex paint of a kind of inner wall of building that the present invention proposes, its raw material comprises following component by weight: pure-acrylic emulsion 45 parts, polyaminoester emulsion 18 parts, bisphenol A epoxide resin 9 parts, diphenyl silanodiol 5 parts, nano titanium oxide 10 parts, Nano silica sol 8 parts, nano zine oxide 20 parts, gac 3 parts, strange ice stone nano powder 9 parts, dodecafluoroheptyl methacrylate 9 parts, ethylene glycol 8 parts, 2, 2, 4-trimethylammonium-1, 3-pentanediol diisobutyrate 20 parts, sorbitol anhydride monopalmitate 2.5 parts, lauric acid 7 parts, 3 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 1.6 parts, Tripotassium Citrate 1.5 parts, propylparaben 4.5 parts, succsinic acid 1.8 parts, sodium alginate 1.6 parts, imidazolidone 3 parts, chitosan 0.6 part, 70 parts, water, auxiliary agent 1.8 parts,
Wherein, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 25 parts of anhydrous methanols by the attapulgite after 10 parts of purifying by weight, stir 4h, then 3 parts of zinc chloride and 1.2 parts of iron(ic) chloride are added, after stirring, the pH value of regulation system is 9, stir 35min, centrifugal under the rotating speed of 4000r/min, washing, dry, then add in 26 parts of water, stir and add 3.2 parts of cetyl trimethylammonium bromides and 10 parts of anhydrous methanols, hydro-thermal reaction 28h is carried out at 185 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 4.3h is reacted at 380 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (8)
1. the special Anti-bacterial mildew-proof latex paint of inner wall of building, it is characterized in that, its raw material comprises following component by weight: ACRYLIC EMULSION 20-50 part, polyaminoester emulsion 10-30 part, bisphenol A epoxide resin 5-10 part, diphenyl silanodiol 2-10 part, nano titanium oxide 5-12 part, Nano silica sol 4-15 part, nano zine oxide 5-25 part, gac 1-5 part, strange ice stone nano powder 3-10 part, dodecafluoroheptyl methacrylate 3-15 part, film coalescence aid 20-30 part, sorbitol anhydride monopalmitate 1-5 part, lauric acid 3-8 part, resol 1-5 part, N-phenyl-N '-cyclohexyl Ursol D 0.5-2 part, Tripotassium Citrate 1-2 part, propylparaben 2-5 part, succsinic acid 1-3 part, sodium alginate 0.5-2 part, imidazolidone 2-6 part, chitosan 0.1-0.8 part, water 50-80 part, auxiliary agent 1-2 part.
2. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to claim 1, it is characterized in that, its raw material comprises following component by weight: ACRYLIC EMULSION 30-45 part, polyaminoester emulsion 18-25 part, bisphenol A epoxide resin 7-9 part, diphenyl silanodiol 5-8 part, nano titanium oxide 7-10 part, Nano silica sol 8-12 part, nano zine oxide 15-20 part, gac 3-4.5 part, strange ice stone nano powder 6-9 part, dodecafluoroheptyl methacrylate 9-11 part, film coalescence aid 25-28 part, sorbitol anhydride monopalmitate 2.5-4 part, lauric acid 5-7 part, resol 3-4.5 part, N-phenyl-N '-cyclohexyl Ursol D 1-1.6 part, Tripotassium Citrate 1.5-1.8 part, propylparaben 3-4.5 part, succsinic acid 1.8-2.2 part, sodium alginate 1-1.6 part, imidazolidone 3-4.6 part, chitosan 0.4-0.6 part, water 70-76 part, auxiliary agent 1.4-1.8 part.
3. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to claim 1 or 2, it is characterized in that, its raw material comprises following component by weight: ACRYLIC EMULSION 40 parts, polyaminoester emulsion 20 parts, bisphenol A epoxide resin 8 parts, diphenyl silanodiol 6.3 parts, nano titanium oxide 8.5 parts, Nano silica sol 10 parts, nano zine oxide 17 parts, gac 4 parts, strange ice stone nano powder 8 parts, dodecafluoroheptyl methacrylate 10 parts, film coalescence aid 26 parts, sorbitol anhydride monopalmitate 3.2 parts, lauric acid 6.3 parts, 4 parts, resol, N-phenyl-N '-cyclohexyl Ursol D 1.2 parts, Tripotassium Citrate 1.6 parts, propylparaben 4 parts, succsinic acid 2 parts, sodium alginate 1.2 parts, imidazolidone 4 parts, chitosan 0.5 part, 73 parts, water, auxiliary agent 1.6 parts.
4. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to any one of claim 1-3, is characterized in that, described ACRYLIC EMULSION is one or more the combination in pure-acrylic emulsion, benzene emulsion, organosilicon crylic acid latex, acrylate and vinyl acetate emulsion.
5. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to any one of claim 1-4, is characterized in that, the median size of described nano titanium oxide is 10-30nm; The median size of described Nano silica sol is 10-25nm; The median size of described nano zine oxide is 20-35nm.
6. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to any one of claim 1-5, it is characterized in that, described film coalescence aid is ethylene glycol, propylene glycol, butyl glycol ether, di-isopropyl succinate, 2,2, one or more combination in 4-trimethylammonium-1,3-pentanediol diisobutyrate.
7. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to any one of claim 1-6, is characterized in that, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 20-30 part anhydrous methanol by the attapulgite after 5-15 part purifying by weight, stir 3-5h, then 2-4 part zinc chloride and 0.3-1.8 part iron(ic) chloride is added, after stirring, the pH value of regulation system is 9-10, stir 20-50min, centrifugal under the rotating speed of 3500-5000r/min, washing, dry, then add in 20-30 part water, stir and add 2-3.5 part cetyl trimethylammonium bromide and 5-12 part anhydrous methanol, hydro-thermal reaction 25-30h is carried out at 175-190 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 3.5-5h is reacted at 350-390 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
8. the special Anti-bacterial mildew-proof latex paint of inner wall of building according to any one of claim 1-7, is characterized in that, described nano zine oxide is modified nano zinc oxide, modified nano zinc oxide is prepared according to following technique: add in 25 parts of anhydrous methanols by the attapulgite after 10 parts of purifying by weight, stir 4h, then 3 parts of zinc chloride and 1.2 parts of iron(ic) chloride are added, after stirring, the pH value of regulation system is 9, stir 35min, centrifugal under the rotating speed of 4000r/min, washing, dry, then add in 26 parts of water, stir and add 3.2 parts of cetyl trimethylammonium bromides and 10 parts of anhydrous methanols, hydro-thermal reaction 28h is carried out at 185 DEG C, reaction terminates through washing, filter, add after drying in retort furnace, 4.3h is reacted at 380 DEG C, through cooling after reaction terminates, grinding, sieve and obtain described modified nano zinc oxide.
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Application publication date: 20151118 |