CN104860569A - 一种制备工业减水剂的生产*** - Google Patents
一种制备工业减水剂的生产*** Download PDFInfo
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- CN104860569A CN104860569A CN201510231386.1A CN201510231386A CN104860569A CN 104860569 A CN104860569 A CN 104860569A CN 201510231386 A CN201510231386 A CN 201510231386A CN 104860569 A CN104860569 A CN 104860569A
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- 238000006243 chemical reaction Methods 0.000 claims abstract description 87
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 77
- 238000003860 storage Methods 0.000 claims abstract description 32
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 20
- 230000007062 hydrolysis Effects 0.000 claims abstract description 19
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 18
- 238000004821 distillation Methods 0.000 claims abstract description 16
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- 239000007788 liquid Substances 0.000 claims abstract description 13
- 238000000746 purification Methods 0.000 claims abstract description 9
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 5
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract description 5
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000376 reactant Substances 0.000 claims abstract description 5
- 239000011734 sodium Substances 0.000 claims abstract description 5
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 4
- 239000000047 product Substances 0.000 claims description 31
- 239000003814 drug Substances 0.000 claims description 16
- 238000007865 diluting Methods 0.000 claims description 13
- 230000004044 response Effects 0.000 claims description 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 8
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims description 8
- 239000006227 byproduct Substances 0.000 claims description 7
- 239000013067 intermediate product Substances 0.000 claims description 6
- YZMHQCWXYHARLS-UHFFFAOYSA-N naphthalene-1,2-disulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(S(=O)(=O)O)=CC=C21 YZMHQCWXYHARLS-UHFFFAOYSA-N 0.000 claims description 4
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 claims description 4
- KCXFHTAICRTXLI-UHFFFAOYSA-N propane-1-sulfonic acid Chemical compound CCCS(O)(=O)=O KCXFHTAICRTXLI-UHFFFAOYSA-N 0.000 claims description 4
- 150000003457 sulfones Chemical class 0.000 claims description 4
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- 238000012856 packing Methods 0.000 claims description 3
- 238000010791 quenching Methods 0.000 claims description 3
- 239000002912 waste gas Substances 0.000 claims description 3
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- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 230000020477 pH reduction Effects 0.000 abstract 1
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract 1
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 239000004568 cement Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000017105 transposition Effects 0.000 description 3
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000003467 diminishing effect Effects 0.000 description 2
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- 230000008569 process Effects 0.000 description 2
- 238000006277 sulfonation reaction Methods 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 239000011398 Portland cement Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
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- 238000005265 energy consumption Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
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- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 239000003348 petrochemical agent Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
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Abstract
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CN201510231386.1A CN104860569B (zh) | 2015-05-08 | 2015-05-08 | 一种制备工业减水剂的生产*** |
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CN201510231386.1A CN104860569B (zh) | 2015-05-08 | 2015-05-08 | 一种制备工业减水剂的生产*** |
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CN104860569A true CN104860569A (zh) | 2015-08-26 |
CN104860569B CN104860569B (zh) | 2017-07-04 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104829154A (zh) * | 2015-05-20 | 2015-08-12 | 郑祖兰 | 一种制备工业减水剂的生产方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101062851A (zh) * | 2007-05-25 | 2007-10-31 | 河北久强建材有限公司 | 一种萘系减水剂的制备方法及其专用设备 |
CN201367397Y (zh) * | 2009-03-19 | 2009-12-23 | 四川吉龙化学建材有限公司 | 一种用于生产萘系减水剂或其同系分散剂的装置 |
CN201660566U (zh) * | 2010-04-13 | 2010-12-01 | 宫振鑫 | 萘系减水剂生产线设备 |
CN102515613A (zh) * | 2011-12-05 | 2012-06-27 | 马鞍山中海新材料有限公司 | 一种利用精萘副产物90萘制造萘系高效减水剂的方法 |
CN203144300U (zh) * | 2013-03-25 | 2013-08-21 | 萧县鑫固混凝土外加剂有限公司 | 一种萘系减水剂的生产*** |
CN204752545U (zh) * | 2015-05-08 | 2015-11-11 | 郑祖兰 | 一种制备工业减水剂的生产*** |
-
2015
- 2015-05-08 CN CN201510231386.1A patent/CN104860569B/zh not_active Expired - Fee Related
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101062851A (zh) * | 2007-05-25 | 2007-10-31 | 河北久强建材有限公司 | 一种萘系减水剂的制备方法及其专用设备 |
CN201367397Y (zh) * | 2009-03-19 | 2009-12-23 | 四川吉龙化学建材有限公司 | 一种用于生产萘系减水剂或其同系分散剂的装置 |
CN201660566U (zh) * | 2010-04-13 | 2010-12-01 | 宫振鑫 | 萘系减水剂生产线设备 |
CN102515613A (zh) * | 2011-12-05 | 2012-06-27 | 马鞍山中海新材料有限公司 | 一种利用精萘副产物90萘制造萘系高效减水剂的方法 |
CN203144300U (zh) * | 2013-03-25 | 2013-08-21 | 萧县鑫固混凝土外加剂有限公司 | 一种萘系减水剂的生产*** |
CN204752545U (zh) * | 2015-05-08 | 2015-11-11 | 郑祖兰 | 一种制备工业减水剂的生产*** |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104829154A (zh) * | 2015-05-20 | 2015-08-12 | 郑祖兰 | 一种制备工业减水剂的生产方法 |
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CN104860569B (zh) | 2017-07-04 |
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Inventor after: Gong Qingping Inventor before: Zheng Zulan |
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Effective date of registration: 20170607 Address after: 550003, Guiyang District, Guizhou City, Nanming Castle Peak District 10, 1 units, 8 floor, No. 1 [Tai Chi community] Applicant after: Guizhou Hengxing Kai new building materials Co Ltd Address before: Quangang District of Quanzhou city Fujian province 362801 lotus pond community No. 723 CuO wa Applicant before: Zheng Zulan |
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