CN104432075A - Moringa oleifera leaf oral liquid and preparation method thereof - Google Patents

Moringa oleifera leaf oral liquid and preparation method thereof Download PDF

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Publication number
CN104432075A
CN104432075A CN201410819012.7A CN201410819012A CN104432075A CN 104432075 A CN104432075 A CN 104432075A CN 201410819012 A CN201410819012 A CN 201410819012A CN 104432075 A CN104432075 A CN 104432075A
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China
Prior art keywords
extract
moringa
leaf
oral liquid
preparation
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CN201410819012.7A
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CN104432075B (en
Inventor
邱彬
黄建凡
李想
王文斌
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FUZHOU JIAYOU CHEMICAL TECHNOLOGY Co Ltd
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FUZHOU JIAYOU CHEMICAL TECHNOLOGY Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a Moringa oleifera leaf oral liquid and a preparation method thereof. Moringa oleifera leaf are taken as a main raw material; stevioside, menthol and sorbic acid are taken as auxiliary materials; according to the core, the method comprises the following steps: crushing the Moringa oleifera leaf into super-fine powder until walls are broken; heating and carrying out reflux extraction through ethanol; adding distilled water, carrying out reflux extraction, merging an extract liquid; and evaporating and concentrating at reduced pressure, so as to obtain a Moringa oleifera leaf extract, so that the nutritional ingredients in the original natural Moringa oleifera leaf and the biological activity are not destroyed by a high temperature and a chemical solvent; and the dosage form which is easy to store and transport is prepared. According to the Moringa oleifera leaf oral liquid, the bioavailability of all nutritional ingredients of the Moringa oleifera leaf is effectively improved; and a natural green health product capable of supplementing nutrients and improving the sub-health states of human bodies is provided for people.

Description

A kind of leaf of Moringa oral liquid and preparation method thereof
Technical field
The present invention relates to health food processing and fabricating field, particularly a kind of leaf of Moringa oral liquid and preparation method thereof.
Background technology
Leaf of Moringa is the leaf of the perennial tropical deciduous tree Moringa tree (being also called drumstick tree) originating in India, edible.Containing profuse nutritional labeling in leaf of Moringa, calcium content is more than 4 times of milk, containing the very high trace element such as potassium, iron, zinc, also containing abundant vitamin and amino acid etc., comprising 5 kinds in eight kinds of essential amino acids, especially lysine and threonine is a kind of functional food containing fully nutrient.As long as a people is able to eat the nutritional need that about 25 grams can meet different crowd every day.In addition, find after deliberation, Moringa extract treat that ulcer, anti-inflammatory are antibacterial, hypoglycemic in addition, lipopenicillinase, step-down, the biological function such as antitumor.
Also be in the starting stage in China to the research and development application that Moringa is set at present, also not formed with Moringa is the large-scale application that health products prepared by raw material.On the other hand, nutritious due to Moringa tree, various its secondary metabolites content is high, and processing technology is more complicated, want fully to obtain nutritional labeling and be not destroyed, to be easy to preserve transport, salable leaf of Moringa health products just more difficult.The present invention, after fully analyzing the nutritional labeling of leaf of Moringa, has found for extracting a kind of new method of leaf of Moringa nutritional labeling for the preparation of oral liquid.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of leaf of Moringa oral liquid and preparation method thereof is provided.This oral liquid can supplement the nutrients, improve human body sub-health status.
In order to realize foregoing invention object, the present invention adopts following technical scheme:
A preparation method for leaf of Moringa oral liquid, comprises the following steps:
1) leaf of Moringa is crushed to broken wall;
2) then extract with alcohol heating reflux, obtain the first extract; Then in filter residue, add distilled water, heating and refluxing extraction obtains the second extract;
3) merge the first extract and the second extract, reduction vaporization is concentrated into paste, adds the allotment of 50 ~ 100 times of distilled water evenly, adds auxiliary material, mix, filling, low temperature discontinuous sterilization, obtained leaf of Moringa oral liquid.
In step 1), leaf of Moringa is ground into 500 order to 1500 order Ultramicro-powders by micronizer.
Step 2) in the preparation method of the first extract be: leaf of Moringa powder is put into refluxing extraction device, adds the ethanol of 8-10 times amount 60-70%, adjust the temperature to 60-65 DEG C, refluxing extraction 60 minutes, filters to obtain ethanol extract; Repeat extraction 3 times, merge ethanol extract, obtain the first extract.
Step 2) in the preparation method of the second extract be: the residue after alcohol extract is put into refluxing extraction device, adds 10-12 times amount distilled water, be heated to 60-70 DEG C, refluxing extraction 90 minutes, filter, obtain aqueous extract; Repeat extraction 3 times, merge aqueous extract, obtain the second extract.
Auxiliary material described in step 3) comprises stevioside, menthol, sorbic acid; In obtained leaf of Moringa oral liquid, containing 0.05-0.07 wt% stevioside, 0.8-1.2wt% menthol, 0.04-0.05 wt% sorbic acid.
Beneficial effect of the present invention is:
The present invention is fully extracted the effective nutritional labeling in leaf of Moringa, obtained leaf of Moringa oral liquid; This oral liquid can improve the efficiency that absorption of human body utilizes, and mouthfeel improves, and be easy to carry about with one use, is a kind of extra-nutrition, improves the environmental protective hygienic food of health sub-health state.
Detailed description of the invention
The present invention's the following example further illustrates the present invention, but protection scope of the present invention is not limited to the following example.
Embodiment 1
A kind of concrete preparation process of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, be crushed to broken wall with micronizer, cross 500 object Ultramicro-powders;
2) leaf of Moringa powder is put into refluxing extraction device, add the ethanol of 10 times amount 60 wt%, adjust the temperature to 60 DEG C, refluxing extraction 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merges ethanol extract, obtain the first extract;
3) reclaim residue, residue is put into refluxing extraction device, add 10 times amount distilled water, be heated to 70 DEG C, refluxing extraction 90 minutes, filter, obtain aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extract;
4) merge first and second extract, leaf of Moringa extract reduction vaporization is concentrated into paste, the distilled water allotment adding 50 times of quality is 2wt% to the concentration of leaf of Moringa, adds stevioside, menthol, sorbic acid, then filling, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.05 wt%, Determination of menthol is 1.0 wt%, Determination of sorbic is 0.04 wt%, be extracted the nutritional labeling in raw material leaf of Moringa greatly, and avoid destruction and the loss of effective nutritional labeling by effective manufacture craft; Make nutritional labeling abundant in leaf of Moringa, more easily allow human digestive organ absorb, meet the demand of people to needed by human nutrition, human body sub-health status can be improved well.
Embodiment 2
A kind of concrete preparation process of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, be crushed to broken wall with micronizer, cross 1000 object Ultramicro-powders;
2) leaf of Moringa powder is put into refluxing extraction device, add the ethanol of 8 times amount 70 wt%, adjust the temperature to 65 DEG C, refluxing extraction 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merges ethanol extract, obtain the first extract;
3) reclaim residue, residue is put into refluxing extraction device, add 12 times amount distilled water, be heated to 65 DEG C, refluxing extraction 90 minutes, filter, obtain aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extract;
4) merge first and second extract, leaf of Moringa extract reduction vaporization is concentrated into paste, the distilled water allotment adding 100 times of quality is 1wt% to the concentration of leaf of Moringa, adds stevioside, menthol, sorbic acid, then filling, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.07 wt%, Determination of menthol is 0.8 wt%, Determination of sorbic is 0.04 wt%, be extracted the nutritional labeling in raw material leaf of Moringa greatly, and avoid destruction and the loss of effective nutritional labeling by effective manufacture craft; Make nutritional labeling abundant in leaf of Moringa, more easily allow human digestive organ absorb, meet the demand of people to needed by human nutrition, human body sub-health status can be improved well.
Embodiment 3
A kind of concrete preparation process of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, be crushed to broken wall with micronizer, cross 500 object Ultramicro-powders;
2) leaf of Moringa powder is put into refluxing extraction device, add the ethanol of 9 times amount 65 wt%, adjust the temperature to 62 DEG C, refluxing extraction 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merges ethanol extract, obtain the first extract;
3) reclaim residue, residue is put into refluxing extraction device, add 11 times amount distilled water, be heated to 60 DEG C, refluxing extraction 90 minutes, filter, obtain aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extract;
4) merge first and second extract, leaf of Moringa extract reduction vaporization is concentrated into paste, the distilled water allotment adding 75 times of quality is 1.5wt% to the concentration of leaf of Moringa, adds stevioside, menthol, sorbic acid, then filling, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.06 wt%, Determination of menthol is 1.2 wt%, Determination of sorbic is 0.05 wt%, be extracted the nutritional labeling in raw material leaf of Moringa greatly, and avoid destruction and the loss of effective nutritional labeling by effective manufacture craft; Make nutritional labeling abundant in leaf of Moringa, more easily allow human digestive organ absorb, meet the demand of people to needed by human nutrition, human body sub-health status can be improved well.
The above; be only the present invention's preferably detailed description of the invention, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.

Claims (5)

1. a preparation method for leaf of Moringa oral liquid, is characterized in that: comprise the following steps:
1) leaf of Moringa is crushed to broken wall;
2) then extract with alcohol heating reflux, obtain the first extract; Then in filter residue, add distilled water, heating and refluxing extraction obtains the second extract;
3) merge the first extract and the second extract, reduction vaporization is concentrated into paste, adds the allotment of 50 ~ 100 times of distilled water evenly, adds auxiliary material, mix, filling, low temperature discontinuous sterilization, obtained leaf of Moringa oral liquid.
2. the preparation method of leaf of Moringa oral liquid according to claim 1, is characterized in that: in step 1), leaf of Moringa is ground into 500 order to 1500 order Ultramicro-powders by micronizer.
3. the preparation method of leaf of Moringa oral liquid according to claim 1, it is characterized in that: step 2) in the preparation method of the first extract be: leaf of Moringa powder is put into refluxing extraction device, add the ethanol of 8-10 times amount 60-70%, adjust the temperature to 60-65 DEG C, refluxing extraction 60 minutes, filters to obtain ethanol extract; Repeat extraction 3 times, merge ethanol extract, obtain the first extract.
4. the preparation method of leaf of Moringa oral liquid according to claim 1, it is characterized in that: step 2) in the preparation method of the second extract be: the residue after alcohol extract is put into refluxing extraction device, add 10-12 times amount distilled water, be heated to 60-70 DEG C, refluxing extraction 90 minutes, filter, obtain aqueous extract; Repeat extraction 3 times, merge aqueous extract, obtain the second extract.
5. the preparation method of leaf of Moringa oral liquid according to claim 1, is characterized in that: the auxiliary material described in step 3) comprises stevioside, menthol, sorbic acid; In obtained leaf of Moringa oral liquid, containing 0.05-0.07 wt% stevioside, 0.8-1.2wt% menthol, 0.04-0.05 wt% sorbic acid.
CN201410819012.7A 2014-12-25 2014-12-25 A kind of leaf of Moringa oral liquid and preparation method thereof Expired - Fee Related CN104432075B (en)

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Cited By (7)

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CN105054067A (en) * 2015-08-27 2015-11-18 大闽食品(漳州)有限公司 Preparation method of horseradish tree leaf extract good in water-solubility
CN105166912A (en) * 2015-10-22 2015-12-23 李佳忠 Compound horseradish tree and dendrobe oral solution and preparation method thereof
CN105192832A (en) * 2015-11-07 2015-12-30 三株福尔制药有限公司 Composition of probiotic fermented horseradish tree leaves as well as preparation method and application of composition
CN105685620A (en) * 2015-07-08 2016-06-22 海南木辣达生物科技有限公司 Moringa oleifera oral liquid and preparation method thereof
CN106107339A (en) * 2016-06-25 2016-11-16 韶关绿之源包装食品有限公司 Moringa method for preparing beverage
CN107348289A (en) * 2017-08-23 2017-11-17 尹飞 Moringa oleifera beverage and preparation method thereof
CN108420074A (en) * 2018-04-09 2018-08-21 江西牧威利元生物科技有限公司 A kind of tyrosinase activity inhibitor and its application

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CN103750440A (en) * 2013-12-16 2014-04-30 马鞍山市安康菌业有限公司 Horseradish tree leaf nutritious drink and preparation method thereof
CN103989174A (en) * 2014-06-10 2014-08-20 陈宗进 Moringa oleifera composite all-nutrition nutrient

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CN103750440A (en) * 2013-12-16 2014-04-30 马鞍山市安康菌业有限公司 Horseradish tree leaf nutritious drink and preparation method thereof
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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105685620A (en) * 2015-07-08 2016-06-22 海南木辣达生物科技有限公司 Moringa oleifera oral liquid and preparation method thereof
CN105054067A (en) * 2015-08-27 2015-11-18 大闽食品(漳州)有限公司 Preparation method of horseradish tree leaf extract good in water-solubility
CN105166912A (en) * 2015-10-22 2015-12-23 李佳忠 Compound horseradish tree and dendrobe oral solution and preparation method thereof
CN105166912B (en) * 2015-10-22 2018-06-22 李佳忠 A kind of compound Moringa stem of noble dendrobium oral liquid and preparation method thereof
CN105192832A (en) * 2015-11-07 2015-12-30 三株福尔制药有限公司 Composition of probiotic fermented horseradish tree leaves as well as preparation method and application of composition
CN106107339A (en) * 2016-06-25 2016-11-16 韶关绿之源包装食品有限公司 Moringa method for preparing beverage
CN107348289A (en) * 2017-08-23 2017-11-17 尹飞 Moringa oleifera beverage and preparation method thereof
CN108420074A (en) * 2018-04-09 2018-08-21 江西牧威利元生物科技有限公司 A kind of tyrosinase activity inhibitor and its application

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