CN104264460B - A kind of anti pilling antistatic woollen fabrics inorganic agent and preparation method thereof - Google Patents
A kind of anti pilling antistatic woollen fabrics inorganic agent and preparation method thereof Download PDFInfo
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- CN104264460B CN104264460B CN201410426463.4A CN201410426463A CN104264460B CN 104264460 B CN104264460 B CN 104264460B CN 201410426463 A CN201410426463 A CN 201410426463A CN 104264460 B CN104264460 B CN 104264460B
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- inorganic agent
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- stearmide
- ethanol
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- 239000004744 fabric Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 48
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 48
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 32
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 30
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims abstract description 16
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 16
- GTDHYNXLIKNVTJ-UHFFFAOYSA-N n-(1-hydroxy-2-methylpropan-2-yl)octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NC(C)(C)CO GTDHYNXLIKNVTJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims abstract description 16
- -1 polyoxyethylene Polymers 0.000 claims abstract description 16
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 9
- 229920002472 Starch Polymers 0.000 claims abstract description 9
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims abstract description 9
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims abstract description 9
- 235000019799 monosodium phosphate Nutrition 0.000 claims abstract description 9
- AVTYONGGKAJVTE-OLXYHTOASA-L potassium L-tartrate Chemical compound [K+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O AVTYONGGKAJVTE-OLXYHTOASA-L 0.000 claims abstract description 9
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims abstract description 9
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 9
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 9
- 239000008107 starch Substances 0.000 claims abstract description 9
- 235000019698 starch Nutrition 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims description 14
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 8
- 229910052708 sodium Inorganic materials 0.000 claims description 8
- 239000012467 final product Substances 0.000 claims description 7
- KEAYESYHFKHZAL-OUBTZVSYSA-N sodium-24 Chemical group [24Na] KEAYESYHFKHZAL-OUBTZVSYSA-N 0.000 abstract 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention provides a kind of anti pilling antistatic woollen fabrics inorganic agent, described inorganic agent is made up of each component of following mass fraction: ethyl acrylate: 18 25 parts, polyoxyethylene octylphenyl alcohol: 15 20 parts, stearmide 6 10 parts, magnesium stearate: 58 parts, sodium sulfate: 36 parts, ethylene glycol: 24 parts, Soluble tartar.: 24 parts, carboxymethyl starch sodium 24 parts, sodium dihydrogen phosphate: 13 parts, ethanol 70 80 parts, water: 350 400 parts.The present invention also provides for the preparation method of this inorganic agent.Woolen fabric anti-fluffing and anti-pilling grade is improved more than 2 grades by the anti pilling anlistatig woollen fabrics inorganic agent of the present invention, and keeps hydrophilic to be basically unchanged.Meanwhile, after using the inorganic agent of the present invention, woolen fabric is not likely to produce electrostatic, and the inorganic agent of the present invention has good anti-static effect.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, be specifically related to a kind of anti pilling antistatic woollen fabrics inorganic agent and preparation method thereof.
Background technology
Woolen fabric, during taking, due to fabric itself and by multiple external force and extraneous rubbing action, before occurring significantly to damage, is easily generated pilling phenomenon.The pilling of fabric face, typically all can occur on natural fiber and science fabric, and especially Mao Diyu hair nitrile blend fabric is made during coat more obvious and prominent.Fabric pilling impact clothing is attractive in appearance, reduces wearability.Along with growth in the living standard, people are more and more higher to the requirement of appearance of fabrics and wearability, therefore, fabric carry out anti-pilling finishing, improve wearing comfort and the quality of fabric, are increasingly subject to the attention of domestic and international dyeing and finishing worker.Meanwhile, woolen fabric there is also certain electrostatic phenomenon.
Summary of the invention
The invention provides a kind of anti pilling antistatic woollen fabrics inorganic agent, there is good anti pilling and antistatic effect.
A kind of anti pilling antistatic woollen fabrics inorganic agent of the present invention, described inorganic agent is made up of each component of following mass fraction: ethyl acrylate: 18-25 part, polyoxyethylene octylphenyl alcohol: 15-20 part, stearmide 6-10 part, magnesium stearate: 5-8 part, sodium sulfate: 3-6 part, ethylene glycol: 2-4 part, Soluble tartar.: 2-4 part, carboxymethyl starch sodium 2-4 part, sodium dihydrogen phosphate: 1-3 part, ethanol 70-80 part, water: 350-400 part.
Preferably, described inorganic agent is made up of each component of following mass fraction: ethyl acrylate: 20 parts, polyoxyethylene octylphenyl alcohol: 18 parts, stearmide 8 parts, magnesium stearate: 6 parts, sodium sulfate: 4 parts, ethylene glycol: 3 parts, Soluble tartar.: 3 parts, carboxymethyl starch sodium 3 parts
Sodium dihydrogen phosphate: 2 parts, ethanol 75 parts, water: 380 parts.
The present invention also provides for the preparation method of above-mentioned inorganic agent, and step is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 80-90 DEG C, stir 30-40min；
(2) add remaining component of proportional quantity, stir 20-30min；
(3) it is cooled to room temperature and get final product.
Woolen fabric anti-fluffing and anti-pilling grade is improved more than 2 grades by the anti pilling anlistatig woollen fabrics inorganic agent of the present invention, and keeps hydrophilic to be basically unchanged.Meanwhile, after using the inorganic agent of the present invention, woolen fabric is not likely to produce electrostatic, and the inorganic agent of the present invention has good anti-static effect.
Detailed description of the invention
Below example facilitates a better understanding of the present invention, but does not limit the present invention.Experimental technique in following embodiment, if no special instructions, is conventional method.
Embodiment 1
The formula of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
Ethyl acrylate: 20g, polyoxyethylene octylphenyl alcohol: 18g, stearmide 8g, magnesium stearate: 6g, sodium sulfate: 4g, ethylene glycol: 3g, Soluble tartar.: 3g, carboxymethyl starch sodium 3g,
Sodium dihydrogen phosphate: 2g, ethanol 75g, water: 380g.
The preparation method of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 85 DEG C, stir 35min；
(2) add remaining component of proportional quantity, stir 25min；
(3) it is cooled to room temperature and get final product.
Embodiment 2
The formula of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
Ethyl acrylate: 25g, polyoxyethylene octylphenyl alcohol: 15g, stearmide 8g, magnesium stearate: 5g, sodium sulfate: 3g, ethylene glycol: 2g, Soluble tartar.: 4g, carboxymethyl starch sodium 2g,
Sodium dihydrogen phosphate: 3g, ethanol 70g, water: 350g.
The preparation method of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 80 DEG C, stir 40min；
(2) add remaining component of proportional quantity, stir 20min；
(3) it is cooled to room temperature and get final product.
Embodiment 3
The formula of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
Ethyl acrylate: 18g, polyoxyethylene octylphenyl alcohol: 20g, stearmide 5g, magnesium stearate: 8g, sodium sulfate: 6g, ethylene glycol: 4g, Soluble tartar.: 2g, carboxymethyl starch sodium 4g,
Sodium dihydrogen phosphate: 1g, ethanol 80g, water: 400g.
The preparation method of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 90 DEG C, stir 30min；
(2) add remaining component of proportional quantity, stir 30min；
(3) it is cooled to room temperature and get final product.
Embodiment 4
The formula of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
Ethyl acrylate: 22g, polyoxyethylene octylphenyl alcohol: 18g, stearmide 7g, magnesium stearate: 5g, sodium sulfate: 4g, ethylene glycol: 2g, Soluble tartar.: 3g, carboxymethyl starch sodium 4g,
Sodium dihydrogen phosphate: 1g, ethanol 75g, water: 350g.
The preparation method of the anti pilling anlistatig woollen fabrics inorganic agent of the present invention is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 80 DEG C, stir 35min；
(2) add remaining component of proportional quantity, stir 25min；
(3) it is cooled to room temperature and get final product.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention, although the present invention being described in detail with reference to previous embodiment, for a person skilled in the art, technical scheme described in foregoing embodiments still can be modified by it, or wherein portion of techniques feature is carried out equivalent.All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (3)
1. an anti pilling antistatic woollen fabrics inorganic agent, it is characterized in that: described inorganic agent is made up of each component of following mass fraction: ethyl acrylate: 18-25 part, polyoxyethylene octylphenyl alcohol: 15-20 part, stearmide 6-10 part, magnesium stearate: 5-8 part, sodium sulfate: 3-6 part, ethylene glycol: 2-4 part, Soluble tartar.: 2-4 part, carboxymethyl starch sodium 2-4 part, sodium dihydrogen phosphate: 1-3 part, ethanol 70-80 part, water: 350-400 part；The preparation method of described inorganic agent is:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 80-90 DEG C, stir 30-40min；
(2) add remaining component of proportional quantity, stir 20-30min；
(3) it is cooled to room temperature and get final product.
Inorganic agent the most according to claim 1, it is characterized in that: described inorganic agent is made up of each component of following mass fraction: ethyl acrylate: 20 parts, polyoxyethylene octylphenyl alcohol: 18 parts, stearmide 8 parts, magnesium stearate: 6 parts, sodium sulfate: 4 parts, ethylene glycol: 3 parts, Soluble tartar.: 3 parts, carboxymethyl starch sodium 3 parts, sodium dihydrogen phosphate: 2 parts, ethanol 75 parts, water: 380 parts.
3. the preparation method of the inorganic agent described in claim 1 or 2, it is characterised in that: step is as follows:
(1) ethyl acrylate of proportional quantity, polyoxyethylene octylphenyl alcohol, stearmide, magnesium stearate, ethylene glycol and ethanol are mixed, be heated to 80-90 DEG C, stir 30-40min；
(2) add remaining component of proportional quantity, stir 20-30min；
(3) it is cooled to room temperature and get final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410426463.4A CN104264460B (en) | 2014-08-27 | 2014-08-27 | A kind of anti pilling antistatic woollen fabrics inorganic agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410426463.4A CN104264460B (en) | 2014-08-27 | 2014-08-27 | A kind of anti pilling antistatic woollen fabrics inorganic agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104264460A CN104264460A (en) | 2015-01-07 |
| CN104264460B true CN104264460B (en) | 2016-11-30 |
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Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104805687A (en) * | 2015-05-12 | 2015-07-29 | 湖州厉华妤婕联合纺织有限公司 | Novel antistatic finishing agent composition for polyester fabric |
| CN105442316A (en) * | 2015-12-16 | 2016-03-30 | 常熟市中宏针织厂 | Finishing process of denim fabric |
| CN105568681A (en) * | 2015-12-16 | 2016-05-11 | 常熟市中宏针织厂 | Finishing process of knitted fabric |
| CN105442304A (en) * | 2016-01-08 | 2016-03-30 | 湖州市千金丝织厂 | Novel anti-balling-up and antistatic finishing agent and preparation method thereof |
| CN105887489A (en) * | 2016-04-29 | 2016-08-24 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting, and preparation method and application thereof |
| CN105862408A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Treating agent for preventing knitted fabric pilling and preparation method and application thereof |
| CN105780478A (en) * | 2016-04-29 | 2016-07-20 | 江苏苏扬服帽有限公司 | Finishing agent for knitting and preparation method and application of finishing agent for knitting |
| CN105926298A (en) * | 2016-04-29 | 2016-09-07 | 江苏苏扬服帽有限公司 | Efficient anti-pilling agent for knitted fabric, preparing method and application thereof |
| CN105862419A (en) * | 2016-04-29 | 2016-08-17 | 江苏苏扬服帽有限公司 | Anti-pilling agent for knitting and preparing method and application thereof |
| CN106835675A (en) * | 2016-12-23 | 2017-06-13 | 句容市申兔工艺针织厂 | A kind of antibacterial Anti-Pilling Finishes technique of modal fabric |
| CN108893984A (en) * | 2018-06-08 | 2018-11-27 | 惠州南旋毛织厂有限公司 | A kind of anti pilling sweater inorganic agent |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102978935A (en) * | 2012-12-04 | 2013-03-20 | 海泰纺织（苏州）有限公司 | Knitwear fleece material fluffing treating agent and method for preparing same |
| CN103437169A (en) * | 2013-08-02 | 2013-12-11 | 吴江市七都镇庙港雅迪针织制衣厂 | Anti-pilling and shrink-resistant woolen sweater treatment agent containing lauryl sodium sulfate |
| CN103643498A (en) * | 2013-12-02 | 2014-03-19 | 苏州市拉波尼服饰有限公司 | Process for preparing knitwear cashmere fluff treating agent |
| CN103710986A (en) * | 2013-12-02 | 2014-04-09 | 常熟市新蕾针织有限公司 | Preparation method of knitwear suede-like material pile treatment agent |
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Inventor after: Liao Yangbo Inventor before: Zhou Min |
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Effective date of registration: 20161020 Address after: 401320 Chongqing Banan District Yu Nan avenue, No. 113 6-25 Applicant after: Chongqing Wenrun Technology Co.,Ltd. Address before: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Effective date of registration: 20161020 Address after: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: 214000 Jiangsu Province, Wuxi city Xishan District Yang Jian Zhen Li an Cun Xi Hu Lu Bei Applicant before: WUXI QISHENG KNITTING GLOVES FACTORY |
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